WO2018155850A1 - Rice bran wax composition comprising rice bran oil and method for preparing natural rice bran candle using same - Google Patents

Rice bran wax composition comprising rice bran oil and method for preparing natural rice bran candle using same Download PDF

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Publication number
WO2018155850A1
WO2018155850A1 PCT/KR2018/001667 KR2018001667W WO2018155850A1 WO 2018155850 A1 WO2018155850 A1 WO 2018155850A1 KR 2018001667 W KR2018001667 W KR 2018001667W WO 2018155850 A1 WO2018155850 A1 WO 2018155850A1
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Prior art keywords
rice bran
wax
oil
natural
candles
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PCT/KR2018/001667
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French (fr)
Korean (ko)
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장혜영
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장혜영
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Publication of WO2018155850A1 publication Critical patent/WO2018155850A1/en

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C5/00Candles
    • C11C5/002Ingredients
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B15/00Solidifying fatty oils, fats, or waxes by physical processes
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C5/00Candles
    • C11C5/02Apparatus for preparation thereof

Definitions

  • the present invention relates to a rice bran wax composition comprising rice bran oil and a method for producing a natural rice bran candle using the same.
  • a candle is prepared by melting a flammable solid, such as paraffin, at a predetermined temperature, burying the wick, and molding a predetermined shape.
  • the manufactured candle is used to generate a fire by heating the flammable solid by burning the wick. It is used as a fuel for lighting.
  • the candle is used for various purposes such as lighting for blackout in general homes and businesses, or for decorating the atmosphere at various banquets and event venues, and the shape of the candle is also manufactured in various shapes such as cylindrical, square, polygonal, etc. It is becoming.
  • Korean Patent Publication No. 10-2013-0034159 in Document 1 discloses a technical content of a method for preparing soybean scented candles using soy wax.
  • Korean Patent Publication No. 10-2010-0098019 of Document 2 discloses a technique for producing an environmentally friendly candle using natural edible crude oil obtained from coconut, palm, cotton, corn, soybean or palm. have.
  • rice bran oil contains a large amount of fatty acids and can be used as a combustible raw material, and although it is an available resource that can be produced in Korea, most of them depend on imports. As a result, it is believed that the production of natural candles using rice bran oil as a basic raw material will enable the utilization of rice bran and the development and dissemination of healing and aroma culture.
  • the present invention has been made to solve the problems of the prior art as described above, by using the rice bran oil, which is an environmentally friendly natural material, can be stably burned for a long time, soot does not occur, easy to mold in various shapes
  • the purpose of the present invention is to provide a waxy wax composition capable of producing natural rice bran candles and a method of manufacturing natural rice bran candles using the same.
  • the present invention provides a rice bran composition comprising 50 to 150 parts by weight of rice bran oil and 10 to 50 parts by weight of stearic acid.
  • the rice bran wax composition is characterized in that it further comprises one or more selected from the group consisting of emulsifiers and essential oils (essential oil).
  • the rice bran wax composition is characterized in that it comprises 30 to 70 parts by weight of rice bran oil, 10 to 20 parts by weight of stearic acid, 10 to 20 parts by weight of propylene glycol and 1 to 15 parts by weight of essential oils.
  • the present invention is a method for producing a natural rice bran candle using the rice bran wax composition described above, (a) after mixing the rice bran oil and stearic acid, and then heated to a temperature of 50 to 90 °C to prepare a raw material mixture Making; (b) stirring the raw material mixture to prepare a rice bran wax having a bubble layer therein; And (c) supplying the rice bran wax to a mold having a wick fixed thereto.
  • the present invention is a method for producing a natural rice bran candle using the rice bran wax composition described above, (a) after mixing the rice bran oil and stearic acid, and then heated to a temperature of 50 to 90 °C to prepare a raw material mixture Making; (b) stirring the raw material mixture to prepare a rice bran wax having a bubble layer therein; (c) oxidizing the rice bran wax; And (d) heating the rice bran wax oxidized in the above step to prepare a wax solution, and supplying the prepared wax solution to a container having a wick fixed thereto.
  • the rice bran wax composition according to the present invention is a natural rice bran candle which can be uniformly burned during combustion using rice bran oil, does not generate soot and does not contain chemical additives, and is harmless to the human body. It can be manufactured by DIY (Do it yourself) by consumers.
  • the manufacturing method of the natural rice bran candles according to the present invention it is possible to prepare a cream or solid type of rice bran wax using the rice bran wax composition, and by molding the rice bran candle using the prepared rice bran, various to suit the taste.
  • Natural rice bran candles can be shaped to maximize consumer satisfaction.
  • the natural rice bran candles produced are excellent in combustion efficiency and stable for a long time, and do not generate soot. It can be easily used in various environments.
  • the present invention provides a rice bran wax composition
  • a rice bran wax composition comprising rice bran oil and stearic acid.
  • the rice bran oil is a high quality oil extracted from rice bran or rice bran, which contains a large amount of fatty acids such as triacylglycerol, and has excellent combustion efficiency, and has an iodine value of 100 to 130, and is biodegradable.
  • a dry natural vegetable oil it is also called brown rice oil in Korea.
  • the stearic acid is an oily raw material containing a saturated fatty acid, it is preferable to use a purity of 70 to 90% obtained from pure vegetable raw materials such as palm oil, the hardness and burning efficiency of the candle prepared from rice bran wax composition It acts to strengthen the oil and to minimize the amount of residues produced.
  • the rice bran wax composition does not generate soot during combustion, including rice bran oil and stearic acid, and allows flat combustion while maintaining an even flame, and may form a natural rice bran candle that emits a scent of rice bran.
  • the natural wax composition may include 50 to 150 parts by weight of rice bran oil and 10 to 50 parts by weight of stearic acid, when the stearic acid is contained less than 50 parts by weight of the small flame is formed to reduce the combustion efficiency, There is a problem that the strength of the candle formed by the wax composition is lowered, and when it contains more than 150 parts by weight, a large flame is formed, which makes it difficult to achieve uniform planar combustion, and the strength is increased so that the candle molded into the wax composition is easily broken. There is a problem such as losing. More preferably, the natural wax composition may include rice bran oil and stearic acid in a weight ratio of 10: 3.
  • the natural wax composition may be configured to additionally include a hydrogenated fatty acid or natural wax component, such as to form a specific pattern or texture in the rice bran candles to be prepared or to enhance the hardness, beeswax (beewax) and the like Representative examples.
  • a hydrogenated fatty acid or natural wax component such as to form a specific pattern or texture in the rice bran candles to be prepared or to enhance the hardness, beeswax (beewax) and the like Representative examples.
  • the rice bran wax composition may further comprise an emulsifier, an essential oil or a mixture thereof.
  • the emulsifier evenly dissolves the rice bran oil and stearic acid to prevent agglomeration and thus have a homogeneous mixing rate, and serves to adjust the viscosity together with stearic acid, thereby uniform burning of the candle molded into the wax composition. It is possible to play a role in improving the preservation, and the emulsifiers are exemplified as propylene glycol, ethylene glycol, lecithin and the like which are environmentally friendly materials.
  • the rice bran wax composition may be configured to include the emulsifier in a ratio of 10 to 50 parts by weight to form a candle having excellent combustion efficiency, more preferably, the natural wax composition is based on the total weight of the composition In the range of 25 to 35 parts by weight may include an emulsifier.
  • the essential oil is a natural vegetable essential oil extracted from plants with the essential oils, when the candle formed by molding a wax composition is burned by a flame, emits a subtle fragrance component to create an aroma atmosphere, Can be used without restriction.
  • the essential oil is lavender oil having a calming and calming effect of mind and body, chamomile oil, marjoram oil or Melissa oil to help calm and induce sleep, rosemary oil to help improve concentration, and eucalyptus oil having a neuropathic relief effect , Basil oil or bergamot oil having an uplifting effect, citronella oil having an insect repellent effect of repelling insects or mosquitoes, phytoncide oil or botanica oil having an odor removing effect, etc.
  • One blended oil is also available, as well as a variety of vegetable essential oils.
  • the rice bran wax composition may comprise the essential oil in a ratio of 1 to 30 parts by weight to form a candle having excellent combustion efficiency and aromaticity, more preferably, the natural wax composition is the total weight of the composition Based on 1 to 10 parts by weight of the essential oil may be included.
  • the wax composition may be configured to further include a pigment that is harmless to the human body, through which, it is possible to form a natural rice bran candle having a variety of colors.
  • the wax composition may further include an antiseptic such as dehydroacetic acid and an antioxidant such as butylated hydroxy anisol in a range that does not impair the physical properties of the composition. It can be further improved.
  • an antiseptic such as dehydroacetic acid
  • an antioxidant such as butylated hydroxy anisol
  • the wax composition according to the present invention as described above is for the purpose of adjusting the combustion intensity, strength or hardness, the odor intensity, etc. according to the area of the candle for manufacturing, etc., or according to the area of the candle for producing, etc.
  • the content of emulsifiers and essential oils can be controlled.
  • the rice bran wax composition may include 100 parts by weight of rice bran oil, 30 parts by weight of stearic acid, or 50 parts by weight of rice bran oil, 15 parts by weight of stearic acid, 15 parts by weight of propylene glycol and 5 to 10 parts by weight of essential oils. It may include.
  • 100 parts by weight of rice bran oil, 30 parts by weight of stearic acid, propylene glycol and lecithin-containing mixture may include 30 parts by weight and essential oils 5 to 20 parts by weight, formed by molding the composition as described above
  • the natural rice bran candles form a stable structure for a long time, and even after burning for a certain period of time, the entire surface of the candle does not bleed and is capable of uniform planar combustion.
  • the rice bran wax composition may be mixed by applying the same weight ratio.
  • the wax composition according to the present invention is capable of uniform flat combustion during combustion using rice bran oil, does not generate soot, and does not contain chemical additives, so it is harmless to the human body and can produce various indoor atmospheres.
  • Rice bran candles can be formed.
  • the wax composition it is possible to form a candle of the cream or cured solid type can be molded in a variety of candles directly desired by the user, the description of such a candle to be described in more detail in the manufacturing method to be described later do.
  • the present invention is a method for producing a natural rice bran candle using the rice bran wax composition described above, (a) mixing the rice bran oil and stearic acid, and then heating to a temperature of 50 to 90 °C to prepare a raw material mixture ; (b) stirring the raw material mixture to prepare a rice bran wax having a bubble layer therein; And (c) supplying the rice bran wax to a mold having a wick fixed thereto.
  • the step (a) is a step of mixing the rice bran oil and stearic acid, and then heated to a temperature of 50 to 90 °C to prepare a raw material mixture, in this step, to homogeneously mix the rice bran oil and stearic acid, 50 Continuous stirring while heating to a temperature of ⁇ 90 °C can be prepared a homogeneous raw material mixture.
  • Step (b) is a step of preparing a rice bran wax having a bubble layer therein by stirring the raw material mixture, in this step, the raw material mixture is continuously mixed (stirring) or whipping (whhipping) to the rice bran oil And stearic acid can be sufficiently mixed to form a plurality of bubbles therein and to form a rice bran wax that is thick and creamy.
  • a method of continuously whipping or stirring the rice bran wax containing the raw material mixture and the emulsifier may be used, and after sufficiently stirring or whipping for a predetermined time in one direction, stirring or whipping again for a predetermined time in the reverse direction.
  • bubbles are formed in the inside to prepare a mild creamy rice bran wax, and the creamy rice bran wax prepared in this way does not release even when stored indoors for a long time and maintains a stable form. It shows the characteristic to make.
  • the step of mixing the raw material mixture and the step of mixing the emulsifier to the raw material mixture before the step of stirring or whipping further comprising a step to be described later by whipping or stirring the mixture containing the raw material mixture and the emulsifier It can be configured to control the physical properties of the rice bran candles produced in.
  • this step after mixing the raw material mixture and the emulsifier, in the step before stirring or whipping, further comprising the step of mixing the essential oils can produce a natural rice bran candle that emits aroma upon combustion, 40 to 50 Adding essential oil to the mixture having a temperature of °C to minimize the loss of the fragrance components contained in the essential oil, it is possible to produce rice bran candles that maximize the divergence of the fragrance components during combustion.
  • the step (c) is a step of supplying the rice bran wax to the mold, the wick is fixed, in this step, the cream type rice bran wax in the form of a plurality of bubbles formed therein as described above in a container having a fixed wick cream type Natural rice bran candles can be produced.
  • the cream-type candle as described above is a pack of rice bran wax is formed in a cream state, soaked in a spray-type airtight container that can support the foam or cream and spray it in a spray form, or block external exposure ( Packed in a pack, tube or airtight container can be stored in the form of creamy rice wax containing a large amount of pores, it can be provided to consumers by mass distribution of the rice bran wax produced in this way.
  • Cream-type rice bran wax stored in the above airtight container is fixed to wicks in various containers desired by the consumer, and then, through the method of supplying the rice bran wax to the container, the natural rice bran candles having various shapes according to consumer's preferences are provided. Can be formed.
  • a tool such as a spatula to scoop up the cream type wax composition stored in the closed container, or squeezing the cream type rice bran wax stored in the pack or tube type closed container.
  • the present invention is a method for producing a natural rice bran candle using the rice bran wax composition described above, (a) after mixing the rice bran oil and stearic acid, and then heated to a temperature of 50 to 90 °C to prepare a raw material mixture Making; (b) mixing the raw material mixture and an emulsifier and then stirring to prepare a rice bran wax having a bubble layer formed therein; (c) oxidizing the rice bran wax; And (d) heating the rice bran wax oxidized in the above step to prepare a wax solution, and supplying the prepared wax solution to a container having a wick fixed thereto.
  • the step (a) is a step of mixing the rice bran oil and stearic acid, and then heated to a temperature of 50 to 90 °C to prepare a raw material mixture, in this step, to homogeneously mix the rice bran oil and stearic acid, 50 Continuous stirring while heating to a temperature of ⁇ 90 °C can be prepared a homogeneous raw material mixture.
  • the step (b) is a step of preparing a wax composition having a bubble layer formed therein by stirring the raw material mixture, in this step, the raw material mixture is continuously mixed (stirring) or whipping (whhipping) to the rice bran oil And stearic acid can be sufficiently mixed to form a plurality of bubbles therein and to form a rice bran wax that is thick and creamy.
  • the step of stirring the raw material mixture is further configured to include the step of mixing the emulsifier to the raw material mixture, whip the mixture containing the raw material mixture and the emulsifier to be prepared to the rice bran to be described later It can be configured to adjust the physical properties of the rice bran candles prepared in the step.
  • the step (c) is a step of oxidizing the rice bran wax, in this step, as oxidized by reacting the oxidized rice bran wax in the form of a plurality of bubbles therein with air, candles prepared in the step to be described later It is possible to enhance the hardness of, thereby producing a rice bran wax is enhanced hardness.
  • the hardness of the strengthened rice bran wax can be stored in a pack (pack) or sealed container that can block the external exposure, and can be stored in large quantities using this method can supply the rice bran wax to consumers.
  • the step (d) is a step of preparing a wax solution by heating the rice bran wax oxidized in the step, and supplying the prepared wax solution to the container fixed to the wick, in this step, the hardness of the wax solution strengthened as described above Melting and liquefying, and supplying the prepared wax solution to the container of various shapes fixed to the wick can be produced natural rice bran candles in the shape according to the shape of the container.
  • the rice bran candles as described above can be manufactured by the consumer by DIY (Do it yourself) molding using rice bran wax, so that various kinds of natural rice bran candles can be produced at various event sites.
  • the step may further comprise the step of mixing the essential oil in the wax solution, by adding the essential oil to the mixture having a temperature of 40 to 50 °C fragrance components contained in the essential oil to minimize the loss of, can be produced natural rice bran candles that maximize the emission of fragrance during combustion.
  • the container may be made of a predetermined shape using a flame retardant material such as non-flammable or flame retardant plastic, such as glass, thin film aluminum, stainless steel alloy, etc., and observe the natural rice bran candles to be supported therein from the outside of the container It may be preferably used to be made in a transparent or translucent form so that it can.
  • a flame retardant material such as non-flammable or flame retardant plastic, such as glass, thin film aluminum, stainless steel alloy, etc.
  • the container may be made of a polygonal shape, such as a triangle, a square, a star, etc., a streamlined shape such as a heart shape, a circular shape, an animal, and the like, and the natural rice bran candles formed using such a container may be formed through combustion.
  • a polygonal shape such as a triangle, a square, a star, etc.
  • a streamlined shape such as a heart shape, a circular shape, an animal, and the like
  • the natural rice bran candles formed using such a container may be formed through combustion.
  • it can also be expected to serve as an ornament.
  • the wick formed on the container may use a wood wick processed into a flat shape of a material such as birch, paper mulberry, bamboo, etc.
  • the wood wick may be made of one plane, but attached two or more It is also possible to use a multi-layer wood wick that can induce a strong capillary phenomenon.
  • natural wicks made of a combination of natural fibers such as hemp and cotton can also be used without limitation, and candles can be burned at the same time by fixing one or more wicks at the same time according to the cross-sectional area of the candle to be molded. It may be prepared.
  • Natural rice bran candles with various shapes can be manufactured to maximize consumer satisfaction, and the natural rice bran candles produced have excellent combustion efficiency, long-term stable structure, and no soot. It can be easily used in various environments such as shops, businesses, and event sites.
  • the rice bran wax was heated to 60 ° C. to prepare molten wax, and the prepared molten wax was supplied to a circular container in which a wick was fixed, thereby preparing rice bran candles.
  • effectin is a commercial preparation of herbal components, including deer antler, cheonhwabun, Angelica, yulpi, rhubarb and forget-me-not extract prepared by dissolving the extract in propylene glycol, rice bran oil and stearic acid as an emulsifier While uniformly dissolving it plays a role of adjusting the viscosity, it may also play a role of essential oil (essential oil) to impart the aroma of herbal ingredients.
  • essential oil essential oil
  • a wooden wick was fixedly formed at the center bottom of a 50 mL round container, and the prepared rice bran was removed with a spatula and supplied to the container to prepare a creamy rice bran candle.
  • a rice bran wax was prepared in the same manner as in Example 2 except that a raw material mixture containing rice bran oil and beeswax wax (3 tablets) was used, and the prepared rice bran was spread on a thin plate to react with oxygen, and dried. After drying, the lid was covered with a thin plate and kept closed.
  • the stored rice bran wax was heated to a temperature of 60 ° C. and melted, and 15 drops (approximately 5 mL) of natural lavender oil were mixed with the molten rice bran wax, followed by whipping using a whip to obtain a clean liquid molten rice bran wax.
  • the obtained rice bran wax was repeatedly whisked in one direction and in the opposite direction so as to have a thick liquid state of soup level, thereby preparing a solid type rice bran wax having a soft whipped cream shape.
  • Solid type rice bran wax containing fragrance was supplied to a 10 mL container fixed with a wick, and then slowly cured to prepare a solid rice bran candle.
  • Rice bran candles were prepared in the same manner as in Example 2, except that 15 g of a mixture of lecithin and effectin (5 g of lecithin and 10 g of effectin) was added to the same raw material mixture as in Example 1 to prepare a raw material mixture. .
  • Rice bran wax was prepared in the same manner as in Example 1 except that 55 g of rice bran oil and 45 g of stearic acid were dissolved to prepare a raw material mixture. Candles were prepared.
  • Rice bran candles were prepared in the same manner as in Example 4, except that 15 g of lecithin was added to the same raw material mixture as in Example 4 to prepare rice bran.
  • the wick of the cream-type rice bran candles according to Example 2 and the solid-type rice bran candles according to Example 3 were lit, and the characteristics such as burning time, soot and residue formation were investigated. Analyzed.
  • the rice bran candles produced by the method according to Example 2 were continuously burned for more than 6 hours, and it was confirmed that they produced a savory flavor peculiar to rice bran oil, soot was not formed, and the residue remained after burning. It can be confirmed that it does not produce a good combustion efficiency.
  • the rice bran candles prepared by the method according to Example 3 was confirmed that after solidified, it is excellent in durability and can be stored stably without change in shape even during transportation, and 3 without generating soot and residues. It was confirmed that the combustion was continuously and stably over time.
  • the combustion characteristics were analyzed by lighting the wicks of rice bran candles according to Example 4 and Comparative Example 2, and in the case of the natural candles of Comparative Example 2, more solid characteristics While the texture was formed during fabrication, the size of the flame formed during combustion was weak, and the flame was extinguished due to the continuous combustion. In the case of the natural candle manufactured by the method of Example 4, it was confirmed that the combustion was excellent and the planar combustion was continuously induced stably.
  • the rice bran wax composition according to the present invention is not released for a long time to maintain a stable state, it can be effectively utilized in the production of natural candles, and with conventional waxes such as soy wax Alternatively, it could be seen that there is no scattering of fine wax grains having stickiness, and that natural candles of the same size can be easily produced without using a tool such as a scale.
  • the rice bran wax composition it was confirmed that the cream-type rice bran and solid-type rice bran candle can be stably formed, the prepared rice bran can be burned flat, soot and residues are generated. It was confirmed that it has excellent characteristics capable of stable combustion for a long time.

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
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Abstract

The present invention provides a rice bran wax composition comprising 50 to 150 parts by weight of a rice bran oil and 10 to 50 parts by weight of stearic acid. Employing a rice bran oil, a rice bran wax composition according to the present invention shows uniform and flat combustion and does not generate soot upon burning. The composition is harmless to the human body thanks to no chemical additives therein and can be molded by a consumer in a do-it-yourself (DIY) manner into natural rice bran candles which allows various indoor expressions. According to a method for preparing a natural rice bran candle of the present invention, a rice bran wax composition can be prepared into a rice bran wax in a cream or solid type and the prepared rice bran wax can be molded into a rice bran candle. Hence, natural rice bran candles of various shapes can be produced to suit the preferences of consumers, thereby maximizing the satisfaction of the consumers. The prepared natural rice bran candles has outstanding combustion efficiency, is stable for a long period of time, and does not produce soot, thereby finding easy applications in various circumstances such as use in homes, business places, event spots, etc.

Description

미강 오일을 포함하는 미강 왁스 조성물 및 이를 이용한 천연 미강 양초의 제조방법Rice bran wax composition comprising rice bran oil and method for producing natural rice bran candle using same
본 발명은 미강 오일을 포함하는 미강 왁스 조성물과 이를 이용하여 천연 미강 양초를 제조하는 방법에 관한 것이다.The present invention relates to a rice bran wax composition comprising rice bran oil and a method for producing a natural rice bran candle using the same.
일반적으로 양초는 파라핀(paraffin) 등과 같은 가연성 고체를 일정 온도에서 녹여 심지를 매립하고, 소정의 형상으로 성형하여 제조하고 있으며, 제조한 양초는 심지에 불을 붙여 가연성 고체를 가열해 불을 생성하는 등화용 연료로 활용되고 있다.Generally, a candle is prepared by melting a flammable solid, such as paraffin, at a predetermined temperature, burying the wick, and molding a predetermined shape.The manufactured candle is used to generate a fire by heating the flammable solid by burning the wick. It is used as a fuel for lighting.
상기한 양초는 일반가정, 업소 등에서 정전시 조명용으로 사용하거나, 각종 연회 및 이벤트 행사장에서 분위기를 연출하기 위한 장식용 등 다양한 용도로 사용되고 있으며, 양초의 형상 또한 원통형, 사각형, 다각형 등과 같이 다양한 형상으로 제조되고 있다. The candle is used for various purposes such as lighting for blackout in general homes and businesses, or for decorating the atmosphere at various banquets and event venues, and the shape of the candle is also manufactured in various shapes such as cylindrical, square, polygonal, etc. It is becoming.
최근 소득 수준이 향상되고 삶에 질이 개선됨에 따라, 콩 기름, 코코넛 오일 등과 같은 천연 물질을 활용한 다양한 형태의 양초가 제조되고 있으며, 특히, 연소시 불꽃의 생성 및 향기 발산이 동시에 이루어져 분위기 연출이 가능한 향초가 제조되어 시판되고 있어 이에 대한 소비자의 관심이 증가함에 따라 관련분야에서 다양한 연구가 진행되고 있다.Recently, as income levels improve and quality of life is improved, various types of candles using natural materials such as soybean oil and coconut oil are being manufactured. This possible herb has been manufactured and marketed, and as the consumer's interest in this increases, various researches are being conducted in related fields.
일례로, 문헌 1의 한국공개특허 제10-2013-0034159호에는 소이왁스를 활용한 콩향초의 제조방법에 관한 기술 내용이 개시된 바 있다.For example, Korean Patent Publication No. 10-2013-0034159 in Document 1 discloses a technical content of a method for preparing soybean scented candles using soy wax.
또 다른 예로 문헌 2의 한국공개특허 제10-2010-0098019호에는 코코넛, 팜, 면, 옥수수, 콩 또는 야자 등으로부터 수득한 천연식용 원유를 이용하여 친환경 양초를 하는 방법에 관한 기술 내용이 개시된 바 있다.As another example, Korean Patent Publication No. 10-2010-0098019 of Document 2 discloses a technique for producing an environmentally friendly candle using natural edible crude oil obtained from coconut, palm, cotton, corn, soybean or palm. have.
한편, 미강 오일은 다량의 지방산을 포함하여 가연성 원료로 활용이 가능하고 국내에서 생산가능한 가용 자원임에도 불구하고 대부분 수입에 의존하고 있는 실정으로 국내실정에 대한 안타까움과 함께 국내 쌀겨 또는 미강의 활용 활성화 방안의 모색하던바, 미강 오일을 기본 원재료로 이용해 천연 양초를 제조하면 미강의 활용 활성화와 힐링 및 아로마 문화의 발전 및 보급을 동시에 달성할 수 있을 것으로 판단된다.On the other hand, rice bran oil contains a large amount of fatty acids and can be used as a combustible raw material, and although it is an available resource that can be produced in Korea, most of them depend on imports. As a result, it is believed that the production of natural candles using rice bran oil as a basic raw material will enable the utilization of rice bran and the development and dissemination of healing and aroma culture.
하지만, 종래에는 미강 오일을 이용하여 우수한 연소효율을 가지면서도, 소비자의 기호에 맞는 다양한 형상의 구현이 가능한 천연 양초를 제조할 수 있는 방법에 관한 기술 내용은 개시된 바 없어, 이에 대한 연구가 필요하다.However, in the related art, there is no disclosure about a method of manufacturing a natural candle having excellent combustion efficiency using the rice bran oil and capable of realizing various shapes according to a consumer's preference. .
본 발명이 속하는 기술분야의 선행기술문헌으로는, 한국공개특허 제10-2013-0034159호, 한국공개특허 제10-2010-0098019호, 한국공개특허 제10-2016-0122500호, 공개실용신안 제20-2013-0000547호 등이 있다.Prior art documents in the technical field to which the present invention belongs, Korean Patent Publication No. 10-2013-0034159, Korean Patent Publication No. 10-2010-0098019, Korean Patent Publication No. 10-2016-0122500, Utility Model No. 20-2013-0000547.
본 발명은 상기한 바와 같은 종래기술의 문제점을 해결하기 위해 안출된 것으로, 친환경 천연 물질인 미강 오일을 활용하여 장시간 안정하게 연소가 가능하고, 그을음이 발생되지 않으며, 다양한 모양으로 손쉽게 성형이 용이한 천연 미강 양초를 제조할 수 있는 미강 왁스 조성물과 이를 이용하여 천연 미강 양초를 제조하는 방법에 관한 기술 내용을 제공하고자 하는 것이다.The present invention has been made to solve the problems of the prior art as described above, by using the rice bran oil, which is an environmentally friendly natural material, can be stably burned for a long time, soot does not occur, easy to mold in various shapes The purpose of the present invention is to provide a waxy wax composition capable of producing natural rice bran candles and a method of manufacturing natural rice bran candles using the same.
상기한 바와 같은 기술적 과제를 달성하기 위해서 본 발명은, 미강 오일 50 내지 150 중량부 및 스테아르산 10 내지 50 중량부를 포함하는 미강 왁스 조성물을 제공한다.In order to achieve the above technical problem, the present invention provides a rice bran composition comprising 50 to 150 parts by weight of rice bran oil and 10 to 50 parts by weight of stearic acid.
또한, 상기 미강 왁스 조성물은 유화제 및 정유(essential oil)로 이루어진 군으로부터 선택되는 1종 이상을 추가로 포함하는 것을 특징으로 한다.In addition, the rice bran wax composition is characterized in that it further comprises one or more selected from the group consisting of emulsifiers and essential oils (essential oil).
또한, 상기 미강 왁스 조성물은 미강 오일 30 내지 70 중량부, 스테아르산 10 내지 20 중량부, 프로필렌글리콜 10 내지 20 중량부 및 정유 1 내지 15 중량부를 포함하는 것을 특징으로 한다.In addition, the rice bran wax composition is characterized in that it comprises 30 to 70 parts by weight of rice bran oil, 10 to 20 parts by weight of stearic acid, 10 to 20 parts by weight of propylene glycol and 1 to 15 parts by weight of essential oils.
또한, 본 발명은 상기에 기재된 미강 왁스 조성물을 이용하여 천연 미강 양초를 제조하는 방법에 있어서, (a) 미강 오일 및 스테아르산을 혼합한 후, 50 내지 90 ℃의 온도로 가열하여 원재료 혼합물을 제조하는 단계; (b) 상기 원재료 혼합물을 교반하여 내부에 기포층이 형성된 미강 왁스를 제조하는 단계; 및 (c) 심지가 고정된 몰드에 상기 미강 왁스를 공급하는 단계;를 포함하는 크림타입 천연 미강 양초의 제조방법을 제공한다.In addition, the present invention is a method for producing a natural rice bran candle using the rice bran wax composition described above, (a) after mixing the rice bran oil and stearic acid, and then heated to a temperature of 50 to 90 ℃ to prepare a raw material mixture Making; (b) stirring the raw material mixture to prepare a rice bran wax having a bubble layer therein; And (c) supplying the rice bran wax to a mold having a wick fixed thereto.
또한, 본 발명은 상기에 기재된 미강 왁스 조성물을 이용하여 천연 미강 양초를 제조하는 방법에 있어서, (a) 미강 오일 및 스테아르산을 혼합한 후, 50 내지 90 ℃의 온도로 가열하여 원재료 혼합물을 제조하는 단계; (b) 상기 원재료 혼합물을 교반하여 내부에 기포층이 형성된 미강 왁스를 제조하는 단계; (c) 상기 미강 왁스를 산화시키는 단계; 및 (d) 상기 단계에서 산화시킨 미강 왁스를 가열하여 왁스 용액을 제조하고, 제조한 왁스 용액을 심지가 고정된 용기에 공급하는 단계;를 포함하는 고체타입 천연 미강 양초의 제조방법을 제공한다.In addition, the present invention is a method for producing a natural rice bran candle using the rice bran wax composition described above, (a) after mixing the rice bran oil and stearic acid, and then heated to a temperature of 50 to 90 ℃ to prepare a raw material mixture Making; (b) stirring the raw material mixture to prepare a rice bran wax having a bubble layer therein; (c) oxidizing the rice bran wax; And (d) heating the rice bran wax oxidized in the above step to prepare a wax solution, and supplying the prepared wax solution to a container having a wick fixed thereto.
본 발명에 따른 미강 왁스 조성물은 미강 오일을 이용하여 연소시 균일한 평면 연소가 가능하고, 그을음이 발생되지 않으며 화학첨가물이 들어 있지 않아 인체에 무해하고, 다양한 실내 분위기의 연출이 가능한 천연 미강 양초를 소비자 스스로 DIY(Do it yourself) 성형하여 제조할 수 있다.The rice bran wax composition according to the present invention is a natural rice bran candle which can be uniformly burned during combustion using rice bran oil, does not generate soot and does not contain chemical additives, and is harmless to the human body. It can be manufactured by DIY (Do it yourself) by consumers.
본 발명에 따른 천연 미강 양초의 제조방법에 따르면, 미강 왁스 조성물을 이용해 크림타입 또는 고체타입의 미강 왁스의 제조가 가능하고, 제조한 미강 왁스를 이용하여 미강 양초를 성형함에 따라, 기호에 맞는 다양한 형상을 갖는 천연 미강 양초를 제조할 수 있어 소비자의 만족도를 극대화시킬 수 있으며, 제조한 천연 미강 양초는 연소 효율이 우수하며 장기간 안정할 뿐만 아니라 그을음 등이 발생되지 않아 일반가정, 업소, 이벤트 현장 등의 다양한 환경에서 손쉽게 활용이 가능하다.According to the manufacturing method of the natural rice bran candles according to the present invention, it is possible to prepare a cream or solid type of rice bran wax using the rice bran wax composition, and by molding the rice bran candle using the prepared rice bran, various to suit the taste. Natural rice bran candles can be shaped to maximize consumer satisfaction. The natural rice bran candles produced are excellent in combustion efficiency and stable for a long time, and do not generate soot. It can be easily used in various environments.
이하, 본 발명을 상세히 설명하도록 한다. Hereinafter, the present invention will be described in detail.
본 발명은, 미강 오일 및 스테아르산을 포함하는 미강 왁스 조성물을 제공한다.The present invention provides a rice bran wax composition comprising rice bran oil and stearic acid.
상기 미강 오일(rice bran oil)은 쌀겨 또는 미강에서 추출한 고급오일로서, 트리아실글리세롤(triacylglycerol) 등의 지방산을 다량 포함하여 연소 효율이 우수하고, 요오드가가 100 내지 130이며, 생분해성을 가지는 반건성 천연 식물성 오일로서, 국내에서는 현미 오일이라고도 불리운다. The rice bran oil is a high quality oil extracted from rice bran or rice bran, which contains a large amount of fatty acids such as triacylglycerol, and has excellent combustion efficiency, and has an iodine value of 100 to 130, and is biodegradable. As a dry natural vegetable oil, it is also called brown rice oil in Korea.
상기 스테아르산(stearic acid)은 포화 지방산을 포함하는 오일성 원료로서, 팜유 등의 순수 식물성 원료로부터 수득한 순도 70 내지 90%인 것을 사용하는 바람직하며, 미강 왁스 조성물로 제조한 양초의 경도 및 연소 효율을 강화시키는 역할을 하며, 잔류물의 생성량을 최소화시키는 역할을 한다.The stearic acid (stearic acid) is an oily raw material containing a saturated fatty acid, it is preferable to use a purity of 70 to 90% obtained from pure vegetable raw materials such as palm oil, the hardness and burning efficiency of the candle prepared from rice bran wax composition It acts to strengthen the oil and to minimize the amount of residues produced.
따라서, 상기 미강 왁스 조성물은 미강 오일 및 스테아르산을 포함하여 연소시 그을음이 발생되지 않고, 고른 불꽃을 유지하면서도 평면 연소가 가능하며, 고소한 미강의 향기를 발산하는 천연 미강 양초를 형성할 수 있다.Accordingly, the rice bran wax composition does not generate soot during combustion, including rice bran oil and stearic acid, and allows flat combustion while maintaining an even flame, and may form a natural rice bran candle that emits a scent of rice bran.
이를 위해, 상기 천연 왁스 조성물은 50 내지 150 중량부의 미강 오일 및 10 내지 50 중량부의 스테아르산을 포함할 수 있으며, 상기 스테아르산이 50 중량부 미만으로 포함할 경우 작은 불꽃이 형성되어 연소 효율이 떨어지고, 왁스 조성물이 형성하는 양초의 강도가 낮아지는 문제가 있으며, 150 중량부를 초과하도록 포함할 경우에는 큰 불꽃이 형성되어 균일한 평면 연소가 이루어지기 힘들고, 강도가 높아져 왁스 조성물로 성형한 양초가 쉽게 부스러지는 등의 문제가 있다. 보다 바람직하게는, 상기 천연 왁스 조성물은 미강 오일 및 스테아르산을 10 : 3의 중량비로 포함할 수 있다.To this end, the natural wax composition may include 50 to 150 parts by weight of rice bran oil and 10 to 50 parts by weight of stearic acid, when the stearic acid is contained less than 50 parts by weight of the small flame is formed to reduce the combustion efficiency, There is a problem that the strength of the candle formed by the wax composition is lowered, and when it contains more than 150 parts by weight, a large flame is formed, which makes it difficult to achieve uniform planar combustion, and the strength is increased so that the candle molded into the wax composition is easily broken. There is a problem such as losing. More preferably, the natural wax composition may include rice bran oil and stearic acid in a weight ratio of 10: 3.
또한, 상기 천연 왁스 조성물은 제조될 미강 양초에 특정한 무늬 또는 결을 형성시키거나 경도를 강화하기 위해서, 수소 첨가된 지방산 또는 천연 왁스성분 등을 추가적으로 포함하도록 구성할 수 있으며, 밀랍(beewax) 등을 대표적인 예로 들 수 있다.In addition, the natural wax composition may be configured to additionally include a hydrogenated fatty acid or natural wax component, such as to form a specific pattern or texture in the rice bran candles to be prepared or to enhance the hardness, beeswax (beewax) and the like Representative examples.
상기 미강 왁스 조성물은 유화제, 정유(essential oil) 또는 이들의 혼합물을 추가로 포함할 수 있다.The rice bran wax composition may further comprise an emulsifier, an essential oil or a mixture thereof.
상기 유화제는 미강 오일 및 스테아르산을 고르게 용해시켜 뭉침이 발생되지 않아 균질한 혼합도를 갖게 하고, 스테아르산과 함께 점도를 조절하는 역할을 하며, 이를 통해 상기 왁스 조성물로 성형한 양초의 균일한 연소를 가능케하고, 보존성을 향상시키는 역할을 하며, 상기 유화제는 친환경적인 소재인 프로필렌글리콜, 에틸렌글리콜, 레시틴 등을 대표적인 예로 들 수 있다.The emulsifier evenly dissolves the rice bran oil and stearic acid to prevent agglomeration and thus have a homogeneous mixing rate, and serves to adjust the viscosity together with stearic acid, thereby uniform burning of the candle molded into the wax composition. It is possible to play a role in improving the preservation, and the emulsifiers are exemplified as propylene glycol, ethylene glycol, lecithin and the like which are environmentally friendly materials.
바람직하게는, 상기 미강 왁스 조성물은 10 내지 50 중량부의 비율로 상기 유화제를 포함하도록 구성하여 우수한 연소 효율을 갖는 양초를 형성시킬 수 있으며, 보다 바람직하게는, 상기 천연 왁스 조성물은 조성물의 총중량을 기준으로 25 내지 35 중량부의 범위로 유화제를 포함할 수 있다.Preferably, the rice bran wax composition may be configured to include the emulsifier in a ratio of 10 to 50 parts by weight to form a candle having excellent combustion efficiency, more preferably, the natural wax composition is based on the total weight of the composition In the range of 25 to 35 parts by weight may include an emulsifier.
상기 정유(essetial oil)는 왁스 조성물을 성형하여 형성시킨 양초가 불꽃에 의해 연소될 시, 은은한 향기성분을 방출하여 아로마 분위기를 연출하는 역할을 하며, 상기와 같은 정유로 식물로부터 추출한 천연 식물성 정유라면 제한받지 않고 사용할 수 있다. The essential oil (essetial oil) is a natural vegetable essential oil extracted from plants with the essential oils, when the candle formed by molding a wax composition is burned by a flame, emits a subtle fragrance component to create an aroma atmosphere, Can be used without restriction.
특히, 상기 정유는 심신 안정 및 진정 효과를 갖는 라벤더 오일, 진정 효과 및 숙면 유도에 도움을 주는 카모마일 오일, 마조람 오일 또는 멜리사 오일, 집중력 향상에 도움을 주는 로즈마리 오일, 신경통증 완화 효과를 갖는 유칼립투스 오일, 정신 고양효과를 갖는 바질 오일 또는 버가못 오일, 벌레 또는 모기를 쫓아내는 방충효과를 갖는 시트로넬라 오일, 냄새 제거 효과를 갖는 피톤치드 오일 또는 보타니카 오일 등을 대표적인 예로 들 수 있으며, 상기 오일들을 혼합한 혼합 오일 또한 활용이 가능하며, 이밖에도 다양한 식물성 정유를 사용할 수 있다.In particular, the essential oil is lavender oil having a calming and calming effect of mind and body, chamomile oil, marjoram oil or Melissa oil to help calm and induce sleep, rosemary oil to help improve concentration, and eucalyptus oil having a neuropathic relief effect , Basil oil or bergamot oil having an uplifting effect, citronella oil having an insect repellent effect of repelling insects or mosquitoes, phytoncide oil or botanica oil having an odor removing effect, etc. One blended oil is also available, as well as a variety of vegetable essential oils.
바람직하게는, 상기 미강 왁스 조성물은 상기 정유를 1 내지 30 중량부의 비율로 포함하도록 구성하여 우수한 연소 효율 및 방향성을 갖는 양초를 형성시킬 수 있으며, 보다 바람직하게는, 상기 천연 왁스 조성물은 조성물의 총중량을 기준으로 1 내지 10 중량부의 범위로 정유를 포함할 수 있다.Preferably, the rice bran wax composition may comprise the essential oil in a ratio of 1 to 30 parts by weight to form a candle having excellent combustion efficiency and aromaticity, more preferably, the natural wax composition is the total weight of the composition Based on 1 to 10 parts by weight of the essential oil may be included.
또한, 상기 왁스 조성물은 인체에 무해한 색소를 추가로 포함하도록 구성할 수 있으며, 이를 통해, 다양한 색상을 갖는 천연 미강 양초를 형성할 수 있게 된다.In addition, the wax composition may be configured to further include a pigment that is harmless to the human body, through which, it is possible to form a natural rice bran candle having a variety of colors.
나아가, 상기 왁스 조성물은 조성물의 물성을 해치지 않는 범위에서 디히드로아세트산(dehydroacetic acid) 등과 같은 방부제와 부틸하이드록시 아니솔(butylated hydroxy anisol) 등과 같은 산화방지제 등을 추가로 포함하도록 구성하여 장기 안정성을 더욱 향상시킬 수 있다.Furthermore, the wax composition may further include an antiseptic such as dehydroacetic acid and an antioxidant such as butylated hydroxy anisol in a range that does not impair the physical properties of the composition. It can be further improved.
상기한 바와 같은 본 발명에 따른 왁스 조성물은, 제조하기 위한 양초의 면적 등에 따른 연소 강도, 강도 또는 경도, 발향 세기의 조절 등을 위한 목적이나, 제조하기 위한 양초의 면적 등에 따라 미강 오일, 스테아르산, 유화제 및 정유의 포함함량을 조절할 수 있다.The wax composition according to the present invention as described above is for the purpose of adjusting the combustion intensity, strength or hardness, the odor intensity, etc. according to the area of the candle for manufacturing, etc., or according to the area of the candle for producing, etc. The content of emulsifiers and essential oils can be controlled.
일례로, 상기 미강 왁스 조성물은 미강 오일 100 중량부, 스테아르산 30 중량부를 포함할 수 있으며, 또는, 미강 오일 50 중량부, 스테아르산 15 중량부, 프로필렌글리콜 15 중량부 및 정유 5 내지 10 중량부를 포함할 수 있다. 또는, 미강 오일 100 중량부, 스테아르산 30 중량부, 프로필렌글리콜 및 레시틴 포함 혼합물(2:1의 중량비) 30 중량부 및 정유 5 내지 20 중량부를 포함할 수 있으며, 상기와 같은 조성물을 성형하여 형성시킨 천연 미강 양초는 장기간 안정한 구조를 형성하고, 일정 시간 연소된 후에도 양초 표면전체에 불이 번지지 않으며 균일한 평면 연소가 가능할 뿐만 아니라, 장시간 연소시에도 점화된 불꽃이 꺼지지 않아 우수한 특성을 나타낼 수 있다. 또한, 상기 미강 왁스 조성물은 동일한 중량비를 적용하여 혼합할 수 있다.For example, the rice bran wax composition may include 100 parts by weight of rice bran oil, 30 parts by weight of stearic acid, or 50 parts by weight of rice bran oil, 15 parts by weight of stearic acid, 15 parts by weight of propylene glycol and 5 to 10 parts by weight of essential oils. It may include. Alternatively, 100 parts by weight of rice bran oil, 30 parts by weight of stearic acid, propylene glycol and lecithin-containing mixture (weight ratio of 2: 1) may include 30 parts by weight and essential oils 5 to 20 parts by weight, formed by molding the composition as described above The natural rice bran candles form a stable structure for a long time, and even after burning for a certain period of time, the entire surface of the candle does not bleed and is capable of uniform planar combustion. . In addition, the rice bran wax composition may be mixed by applying the same weight ratio.
상기한 바와 같은 본 발명에 따른 왁스 조성물은 미강 오일을 이용하여 연소시 균일한 평면 연소가 가능하고, 그을음이 발생되지 않으며 화학첨가물이 들어 있지 않아 인체에 무해하고, 다양한 실내 분위기의 연출이 가능한 천연 미강 양초를 형성할 수 있다.As described above, the wax composition according to the present invention is capable of uniform flat combustion during combustion using rice bran oil, does not generate soot, and does not contain chemical additives, so it is harmless to the human body and can produce various indoor atmospheres. Rice bran candles can be formed.
특히, 상기 왁스 조성물은, 크림타입 또는 경화 고체타입의 양초를 형성할 수 있어 사용자가 직접 원하는 형태의 다양한 양초의 성형이 가능하며, 이와 같은 양초에 대한 설명은 후술할 제조방법에서 보다 상세히 설명하도록 한다.In particular, the wax composition, it is possible to form a candle of the cream or cured solid type can be molded in a variety of candles directly desired by the user, the description of such a candle to be described in more detail in the manufacturing method to be described later do.
이하, 본 발명에 따른 천연 미강 양초의 제조방법을 상세히 설명하도록 한다.Hereinafter, a method of manufacturing natural rice bran candles according to the present invention will be described in detail.
본 발명은 상기에 기재된 미강 왁스 조성물을 이용하여 천연 미강 양초를 제조하는 방법에 있어서, (a) 미강 오일 및 스테아르산을 혼합한 후, 50 내지 90 ℃의 온도로 가열하여 원재료 혼합물을 제조하는 단계; (b) 상기 원재료 혼합물을 교반하여 내부에 기포층이 형성된 미강 왁스를 제조하는 단계; 및 (c) 심지가 고정된 몰드에 상기 미강 왁스를 공급하는 단계;를 포함하는 크림타입 천연 미강 양초의 제조방법을 제공한다.The present invention is a method for producing a natural rice bran candle using the rice bran wax composition described above, (a) mixing the rice bran oil and stearic acid, and then heating to a temperature of 50 to 90 ℃ to prepare a raw material mixture ; (b) stirring the raw material mixture to prepare a rice bran wax having a bubble layer therein; And (c) supplying the rice bran wax to a mold having a wick fixed thereto.
상기 단계 (a)는 미강 오일 및 스테아르산을 혼합한 후, 50 내지 90 ℃의 온도로 가열하여 원재료 혼합물을 제조하는 단계로서, 본 단계에서는 상기 미강 오일 및 스테아르산을 균질하게 혼합하기 위해서, 50 내지 90 ℃의 온도로 가열하면서 지속적으로 교반하여 균질한 원재료 혼합물을 제조할 수 있다. The step (a) is a step of mixing the rice bran oil and stearic acid, and then heated to a temperature of 50 to 90 ℃ to prepare a raw material mixture, in this step, to homogeneously mix the rice bran oil and stearic acid, 50 Continuous stirring while heating to a temperature of ~ 90 ℃ can be prepared a homogeneous raw material mixture.
상기 단계 (b)는 상기 원재료 혼합물을 교반하여 내부에 기포층이 형성된 미강 왁스를 제조하는 단계로서, 본 단계에서는 상기 원재료 혼합물을 지속적으로 교반(stirring) 또는 휘핑(whipping)을 통해 혼합하여 미강 오일 및 스테아르산을 충분히 혼합시켜, 내부에 다수의 기포가 형성되고 걸쭉한 크림상태를 이루는 미강 왁스를 형성시킬 수 있다.Step (b) is a step of preparing a rice bran wax having a bubble layer therein by stirring the raw material mixture, in this step, the raw material mixture is continuously mixed (stirring) or whipping (whhipping) to the rice bran oil And stearic acid can be sufficiently mixed to form a plurality of bubbles therein and to form a rice bran wax that is thick and creamy.
이를 위해, 본 단계에서는 상기 원재료 혼합물 및 유화제를 포함하는 미강 왁스를 지속적으로 휘핑하거나 교반하는 방법을 사용할 수 있으며, 일방향으로 일정시간 동안 충분히 교반 또는 휘핑한 후, 다시 역방향으로 일정시간 동안 교반 또는 휘핑하는 방법을 수회 반복수행하여 내부에 기포가 형성되어 부드러운 크림형태의 미강 왁스를 제조할 수 있으며, 이와 같은 방법으로 제조한 크림형태의 미강 왁스는 장시간 실내에서 보관시에도 풀어지지 않고 안정적인 형태를 유지하는 특성을 나타낸다.To this end, in this step, a method of continuously whipping or stirring the rice bran wax containing the raw material mixture and the emulsifier may be used, and after sufficiently stirring or whipping for a predetermined time in one direction, stirring or whipping again for a predetermined time in the reverse direction. By repeating the method several times, bubbles are formed in the inside to prepare a mild creamy rice bran wax, and the creamy rice bran wax prepared in this way does not release even when stored indoors for a long time and maintains a stable form. It shows the characteristic to make.
또한, 본 단계에서는 상기 원재료 혼합물을 교반 또는 휘핑하기 전단계에 상기 원재료 혼합물에 유화제를 혼합하는 단계를 추가로 포함하도록 구성하고, 원재료 혼합물 및 유화제를 포함하는 혼합물을 휘핑 또는 교반하도록 구성하여 후술할 단계에서 제조되는 미강 양초의 물성을 조절하도록 구성할 수 있다.In addition, in this step, the step of mixing the raw material mixture and the step of mixing the emulsifier to the raw material mixture before the step of stirring or whipping, further comprising a step to be described later by whipping or stirring the mixture containing the raw material mixture and the emulsifier It can be configured to control the physical properties of the rice bran candles produced in.
나아가, 본 단계에서는 상기 원재료 혼합물 및 유화제를 혼합한 후, 교반 또는 휘핑하기 전단계에서, 정유를 혼합하는 단계를 추가로 포함하여 연소시 향기를 발산하는 천연 미강 양초를 제조할 수 있으며, 40 내지 50 ℃의 온도를 갖는 혼합물에 정유를 첨가하여 정유에 포함된 향기성분의 손실을 최소화하고, 연소시 향기 성분의 발산을 최대화한 미강 양초를 제조할 수 있다.Further, in this step, after mixing the raw material mixture and the emulsifier, in the step before stirring or whipping, further comprising the step of mixing the essential oils can produce a natural rice bran candle that emits aroma upon combustion, 40 to 50 Adding essential oil to the mixture having a temperature of ℃ to minimize the loss of the fragrance components contained in the essential oil, it is possible to produce rice bran candles that maximize the divergence of the fragrance components during combustion.
상기 단계 (c)는 심지가 고정된 몰드에 상기 미강 왁스를 공급하는 단계로서, 본 단계에서는 상기와 같이 내부에 다수의 기포가 형성된 크림상태의 미강 왁스를 심지가 고정형성된 용기에 공급하여 크림타입의 천연 미강 양초를 제조할 수 있다.The step (c) is a step of supplying the rice bran wax to the mold, the wick is fixed, in this step, the cream type rice bran wax in the form of a plurality of bubbles formed therein as described above in a container having a fixed wick cream type Natural rice bran candles can be produced.
구체적으로, 상기와 같은 크림타입의 양초는 미강 왁스가 크림상태로 형성되어, 거품 또는 크림을 담지하고 이를 스프레이 형식으로 분사할 수 있는 스프레이형 밀폐용기 등에 담지하거나, 외부 노출을 차단할 수 있는 팩(pack), 튜브(tube) 또는 밀폐용기에 담지시켜 기공을 다량 포함하는 크림형태의 미강 왁스를 보관할 수 있으며, 이와 같은 방식을 이용해 제조된 미강 왁스를 대량유통하여 소비자에게 제공할 수 있다.Specifically, the cream-type candle as described above is a pack of rice bran wax is formed in a cream state, soaked in a spray-type airtight container that can support the foam or cream and spray it in a spray form, or block external exposure ( Packed in a pack, tube or airtight container can be stored in the form of creamy rice wax containing a large amount of pores, it can be provided to consumers by mass distribution of the rice bran wax produced in this way.
상기와 같은 스프레이형 밀폐용기에 보관된 크림타입의 미강 왁스는 소비자가 원하는 다양한 용기에 심지를 고정한 후, 미강 왁스를 용기에 공급하는 방법을 통해 소비자의 기호에 맞는 다양한 형상을 갖는 천연 미강 양초를 형성시킬 수 있다. Cream-type rice bran wax stored in the above airtight container is fixed to wicks in various containers desired by the consumer, and then, through the method of supplying the rice bran wax to the container, the natural rice bran candles having various shapes according to consumer's preferences are provided. Can be formed.
또는, 주걱 등의 도구를 이용해 밀폐형 용기에 보관된 크림타입 왁스 조성물을 퍼담는 방법(scoop up), 팩 또는 튜브타입 밀폐형 용기에 보관된 크림타입 미강 왁스를 짜내는 방법(squeezing) 등을 이용해 용기에 미강 왁스를 주입하고, 공작도구 등을 이용해 성형하여 소비자의 기호에 맞는 다양한 형상을 갖는 크림타입의 천연 미강 양초를 제조할 수 있으며, 상기와 같은 크림타입 미강 왁스는 종래의 양초제조를 위한 왁스와는 달리, 끈적한 점성을 갖는 미세 왁스입자의 비산이 없으면서도, 소비자가 스스로 DIY(Do it yourself) 성형이 가능하여 각종 이벤트 현장에서 다양한 용도의 천연 미강 양초의 제작을 위한 용도로 손쉽게 활용이 가능하다.Alternatively, use a tool such as a spatula to scoop up the cream type wax composition stored in the closed container, or squeezing the cream type rice bran wax stored in the pack or tube type closed container. Injected rice bran wax and molded using a machine tool or the like to produce a cream-type natural rice bran candles having a variety of shapes according to the consumer's preference, the cream-type rice bran wax as described above for wax production of conventional candles Unlike the waxy sticky viscous particles, the consumer can do DIY (Do it yourself) molding on their own, making it easy to use for the production of natural rice bran candles at various events. Do.
또는, 본 발명은 상기에 기재된 미강 왁스 조성물을 이용하여 천연 미강 양초를 제조하는 방법에 있어서, (a) 미강 오일 및 스테아르산을 혼합한 후, 50 내지 90 ℃의 온도로 가열하여 원재료 혼합물을 제조하는 단계; (b) 상기 원재료 혼합물 및 유화제를 혼합한 후, 교반하여 내부에 기포층이 형성된 미강 왁스를 제조하는 단계; (c) 상기 미강 왁스를 산화시키는 단계; 및 (d) 상기 단계에서 산화시킨 미강 왁스를 가열하여 왁스 용액을 제조하고, 제조한 왁스 용액을 심지가 고정된 용기에 공급하는 단계;를 포함하는 고체타입 천연 미강 양초의 제조방법을 제공한다.Alternatively, the present invention is a method for producing a natural rice bran candle using the rice bran wax composition described above, (a) after mixing the rice bran oil and stearic acid, and then heated to a temperature of 50 to 90 ℃ to prepare a raw material mixture Making; (b) mixing the raw material mixture and an emulsifier and then stirring to prepare a rice bran wax having a bubble layer formed therein; (c) oxidizing the rice bran wax; And (d) heating the rice bran wax oxidized in the above step to prepare a wax solution, and supplying the prepared wax solution to a container having a wick fixed thereto.
상기 단계 (a)는 미강 오일 및 스테아르산을 혼합한 후, 50 내지 90 ℃의 온도로 가열하여 원재료 혼합물을 제조하는 단계로서, 본 단계에서는 상기 미강 오일 및 스테아르산을 균질하게 혼합하기 위해서, 50 내지 90 ℃의 온도로 가열하면서 지속적으로 교반하여 균질한 원재료 혼합물을 제조할 수 있다. The step (a) is a step of mixing the rice bran oil and stearic acid, and then heated to a temperature of 50 to 90 ℃ to prepare a raw material mixture, in this step, to homogeneously mix the rice bran oil and stearic acid, 50 Continuous stirring while heating to a temperature of ~ 90 ℃ can be prepared a homogeneous raw material mixture.
상기 단계 (b)는 상기 원재료 혼합물을 교반하여 내부에 기포층이 형성된 왁스 조성물을 제조하는 단계로서, 본 단계에서는 상기 원재료 혼합물을 지속적으로 교반(stirring) 또는 휘핑(whipping)을 통해 혼합하여 미강 오일 및 스테아르산을 충분히 혼합시켜, 내부에 다수의 기포가 형성되고 걸쭉한 크림상태를 이루는 미강 왁스를 형성시킬 수 있다.The step (b) is a step of preparing a wax composition having a bubble layer formed therein by stirring the raw material mixture, in this step, the raw material mixture is continuously mixed (stirring) or whipping (whhipping) to the rice bran oil And stearic acid can be sufficiently mixed to form a plurality of bubbles therein and to form a rice bran wax that is thick and creamy.
또한, 본 단계에서는 상기 원재료 혼합물을 교반하기 전단계에 상기 원재료 혼합물에 유화제를 혼합하는 단계를 추가로 포함하도록 구성하고, 원재료 혼합물 및 유화제를 포함하는 혼합물을 휘핑하여 미강 왁스를 제조하도록 구성하여 후술할 단계에서 제조되는 미강 양초의 물성을 조절하도록 구성할 수 있다.In addition, in this step, the step of stirring the raw material mixture is further configured to include the step of mixing the emulsifier to the raw material mixture, whip the mixture containing the raw material mixture and the emulsifier to be prepared to the rice bran to be described later It can be configured to adjust the physical properties of the rice bran candles prepared in the step.
상기 단계 (c)는 상기 미강 왁스를 산화시키는 단계로서, 본 단계에서는 상기와 같이 내부에 다수의 기포가 형성된 크림상태의 미강 왁스를 공기와 반응시켜 산화시킴에 따라, 후술할 단계에서 제조되는 양초의 경도를 강화시킬 수 있으며, 이에 의해 경도가 강화된 미강 왁스를 제조할 수 있다. 이와 같이 경도가 강화된 미강 왁스는 외부 노출을 차단할 수 있는 팩(pack) 또는 밀폐용기 등에 담지시켜 보관할 수 있으며, 이와 같은 방법을 이용해 대량유통이 가능해 소비자에게 미강 왁스를 공급할 수 있다.The step (c) is a step of oxidizing the rice bran wax, in this step, as oxidized by reacting the oxidized rice bran wax in the form of a plurality of bubbles therein with air, candles prepared in the step to be described later It is possible to enhance the hardness of, thereby producing a rice bran wax is enhanced hardness. Thus, the hardness of the strengthened rice bran wax can be stored in a pack (pack) or sealed container that can block the external exposure, and can be stored in large quantities using this method can supply the rice bran wax to consumers.
상기 단계 (d)는 상기 단계에서 산화시킨 미강 왁스를 가열하여 왁스 용액을 제조하고, 제조한 왁스 용액을 심지가 고정된 용기에 공급하는 단계로서, 본 단계에서는 상기와 같이 경도가 강화된 왁스 용액을 용융시켜 액화시키고, 제조한 왁스 용액을 심지가 고정된 다양한 형상의 용기에 공급하여 용기의 형상에 따라 성형된 상태의 천연 미강 양초를 제조할 수 있다.The step (d) is a step of preparing a wax solution by heating the rice bran wax oxidized in the step, and supplying the prepared wax solution to the container fixed to the wick, in this step, the hardness of the wax solution strengthened as described above Melting and liquefying, and supplying the prepared wax solution to the container of various shapes fixed to the wick can be produced natural rice bran candles in the shape according to the shape of the container.
상기와 같은 미강 양초는 미강 왁스를 이용해 소비자가 스스로 DIY(Do it yourself) 성형을 통해 제조가 가능하여 각종 이벤트 현장에서 다양한 용도의 천연 미강 양초를 제작할 수 있다.The rice bran candles as described above can be manufactured by the consumer by DIY (Do it yourself) molding using rice bran wax, so that various kinds of natural rice bran candles can be produced at various event sites.
또한, 본 단계에서는 상기 왁스 용액을 제조한 후, 상기 왁스 용액에 정유를 혼합하는 단계를 추가로 포함할 수 있으며, 40 내지 50 ℃의 온도를 갖는 혼합물에 정유를 첨가하여 정유에 포함된 향기성분의 손실을 최소화하고, 연소시 향기를 발산을 극대화한 천연 미강 양초를 제조할 수 있다.In addition, in this step, after preparing the wax solution, the step may further comprise the step of mixing the essential oil in the wax solution, by adding the essential oil to the mixture having a temperature of 40 to 50 ℃ fragrance components contained in the essential oil To minimize the loss of, can be produced natural rice bran candles that maximize the emission of fragrance during combustion.
한편, 상기 용기는 유리, 박막 알루미늄, 스테인레스 스틸 합금 등과 같은 불연성 또는 난연성 플라스틱 등과 같은 난연성 소재를 이용하여 소정의 형상으로 제작된 것을 사용할 수 있으며, 내부에 담지될 천연 미강 양초를 용기의 외부에서도 관찰할 수 있도록 투명하거나 반투명한 형태로 제조된 것을 바람직하게 사용할 수 있다.On the other hand, the container may be made of a predetermined shape using a flame retardant material such as non-flammable or flame retardant plastic, such as glass, thin film aluminum, stainless steel alloy, etc., and observe the natural rice bran candles to be supported therein from the outside of the container It may be preferably used to be made in a transparent or translucent form so that it can.
상기 용기는 삼각형, 사각형, 별형 등과 같은 다각형의 형상, 하트형, 원형 등과 같은 유선형의 형상, 동물 등의 다양한 형상으로 제작된 것일 수 있으며, 이와 같은 용기를 이용해 성형한 천연 미강 양초는 연소를 통한 조명공급 및 향기 공급 역할 이외에도 장식품으로서의 역할 또한 기대할 수 있게 된다.The container may be made of a polygonal shape, such as a triangle, a square, a star, etc., a streamlined shape such as a heart shape, a circular shape, an animal, and the like, and the natural rice bran candles formed using such a container may be formed through combustion. In addition to the lighting and fragrance supply, it can also be expected to serve as an ornament.
또한, 상기 용기에 형성되는 심지는 자작나무, 닥나무, 대나무 등과 같은 소재를 평면 형상으로 가공한 나무 심지를 사용할 수도 있으며, 상기 나무 심지는 1개의 평면으로 이루어진 것을 사용할 수도 있으나, 2장 이상을 부착하여 강한 모세관 현상을 유도할 수 있는 복수층 형태의 나무 심지를 사용할 수도 있다.In addition, the wick formed on the container may use a wood wick processed into a flat shape of a material such as birch, paper mulberry, bamboo, etc. The wood wick may be made of one plane, but attached two or more It is also possible to use a multi-layer wood wick that can induce a strong capillary phenomenon.
또는, 대마, 목면 등의 천연 섬유를 합사하여 제조한 천연 면심지 또한 제한없이 이용이 가능하며, 성형하는 양초의 단면적에 따라, 1개 이상의 심지를 고정형성시켜, 동시에 여러개의 불꽃을 연소시키는 양초를 제조할 수도 있다.Alternatively, natural wicks made of a combination of natural fibers such as hemp and cotton can also be used without limitation, and candles can be burned at the same time by fixing one or more wicks at the same time according to the cross-sectional area of the candle to be molded. It may be prepared.
상기한 바와 같은 본 발명에 따른 천연 미강 양초의 제조방법에 따르면, 상기 미강 왁스 조성물을 이용해 크림타입 또는 고체타입의 미강 왁스를 제조하고, 제조한 미강 왁스를 이용하여 양초를 성형함에 따라, 기호에 맞는 다양한 형상을 갖는 천연 미강 양초를 제조할 수 있어 소비자의 만족도를 극대화시킬 수 있을 뿐만 아니라, 제조한 천연 미강 양초는 연소 효율이 우수하고, 장기간 안정한 구조를 가지며, 그을음 등이 발생되지 않아 일반가정, 업소, 이벤트 현장 등의 다양한 환경에서 손쉽게 활용이 가능하다.According to the manufacturing method of natural rice bran candles according to the present invention as described above, by preparing the rice bran wax of the cream or solid type using the rice bran wax composition, by molding the candle using the prepared rice bran, Natural rice bran candles with various shapes can be manufactured to maximize consumer satisfaction, and the natural rice bran candles produced have excellent combustion efficiency, long-term stable structure, and no soot. It can be easily used in various environments such as shops, businesses, and event sites.
이하, 본 발명을 실시예를 들어 더욱 상세히 설명하도록 한다.Hereinafter, the present invention will be described in more detail with reference to Examples.
제시된 실시예는 본 발명의 구체적인 예시일 뿐이며, 본 발명의 범위를 제한하기 위한 것은 아니다.The examples presented are merely illustrative of the invention and are not intended to limit the scope of the invention.
<실시예 1> 미강 양초의 제조Example 1 Preparation of Rice Bran Candle
비이커(beaker)에 미강 오일 100 g을 공급하여 60 ℃로 예열한 후, 스테아르산 30 g을 용해시켜 원재료 혼합물을 제조하고, 제조한 원재료 혼합물을 휘핑기(whipper)를 이용해 한쪽 방향으로 휘핑하여 스프정도의 걸쭉한 액상상태가 되도록 휘핑한 후, 휘핑한 원재료 혼합물을 다시 반대 방향으로 휘핑하고, 이와 같은 방향을 전환하는 휘핑과정을 반복하여 연노랑색의 색상을 띄는 미강 왁스를 제조하였으며, 제조한 미강 왁스를 25 ℃ 상온의 밀폐용기에 보관하였다.After supplying 100 g of rice bran oil to a beaker and preheating it to 60 ° C., 30 g of stearic acid was dissolved to prepare a raw material mixture, and the prepared raw material mixture was whipped in one direction using a whipper to make a soup. After whipping to a thick liquid state of the mixture, whip the whipped raw material mixture in the opposite direction again and repeat the whipping process to switch the direction, to prepare a pale yellow wax of pale yellow color, the prepared rice bran wax It was stored in a sealed container at 25 ℃ room temperature.
상기 미강 왁스를 60 ℃로 가열하여 용융 왁스를 제조하고, 제조한 용융 왁스를 면심지가 고정형성된 원형 용기에 공급하여 미강 양초를 제조하였다.The rice bran wax was heated to 60 ° C. to prepare molten wax, and the prepared molten wax was supplied to a circular container in which a wick was fixed, thereby preparing rice bran candles.
<실시예 2> 크림타입 미강 양초의 제조Example 2 Preparation of Cream-Type Rice Bran Candle
비이커(beaker)에 미강 오일 50 g을 공급하여 60 ℃까지 예열한 후, 스테아르산 15 g을 용해시켜 원재료 혼합물을 제조하였다. 제조한 원재료 혼합물에 이펙틴 15 g을 첨가하여 원재료 혼합물을 제조하고, 제조한 원재료 혼합물을 휘핑기(whipper)를 이용해 한쪽 방향으로 휘핑하여 스프정도의 걸쭉한 액상상태가 되도록 휘핑한 후, 휘핑한 원재료 혼합물을 다시 반대 방향으로 휘핑하고, 이를 다시 원래의 방향으로 휘핑하여 내부에 다량의 기포층이 형성된 부드러운 생크림 형상을 갖는 크림타입의 미강 왁스를 제조하였다. After supplying 50 g of rice bran oil to a beaker and preheating it to 60 ° C., 15 g of stearic acid was dissolved to prepare a raw material mixture. 15 g of effectin was added to the prepared raw material mixture to prepare a raw material mixture.The raw material mixture was whipped in one direction using a whipper to whip to a thick liquid state of soup, and then whipped raw material mixture Was whipped in the opposite direction again, and whipped in the original direction again to prepare a creamy rice bran wax having a soft fresh cream shape in which a large amount of bubble layers were formed therein.
상기 이펙틴(effectin, 유로코스텍사)은 추출물을 프로필렌글리콜에 용해시켜 제조한 녹용, 천화분 ,당귀 ,율피 ,대황, 망초 추출물 포함 한방성분의 상용제제로서, 유화제의 역할을 하여 미강 오일 및 스테아르산을 균일하게 용해시키면서 점도를 조절하는 역할을 하면서도, 한방성분의 향기를 부여하는 정유(essential oil)의 역할 또한 할 수 있다.The effectin (effectin, Eurocostec Co., Ltd.) is a commercial preparation of herbal components, including deer antler, cheonhwabun, Angelica, yulpi, rhubarb and forget-me-not extract prepared by dissolving the extract in propylene glycol, rice bran oil and stearic acid as an emulsifier While uniformly dissolving it plays a role of adjusting the viscosity, it may also play a role of essential oil (essential oil) to impart the aroma of herbal ingredients.
50 mL 용량의 원형 용기의 중앙 바닥부분에 나무 심지를 고정형성하고, 제조한 미강 왁스를 주걱으로 덜어내어 용기에 공급하여 크림타입의 미강 양초를 제조하였다.A wooden wick was fixedly formed at the center bottom of a 50 mL round container, and the prepared rice bran was removed with a spatula and supplied to the container to prepare a creamy rice bran candle.
<< 실시예Example 3> 고체타입  3> solid type 미강Rice bran 양초의 제조 Manufacture of candles
미강 오일 및 밀랍 왁스(3 알)를 포함하는 원재료 혼합물을 사용하는 것을 제외하고는 실시예 2과 동일한 방법으로 미강 왁스를 제조하고, 제조한 미강 왁스 를 산소와 반응하도록 얇은 판에 펴서 건조하였으며, 건조한 후에는 얇은 판에 뚜껑을 덮어 밀폐보관하였다.A rice bran wax was prepared in the same manner as in Example 2 except that a raw material mixture containing rice bran oil and beeswax wax (3 tablets) was used, and the prepared rice bran was spread on a thin plate to react with oxygen, and dried. After drying, the lid was covered with a thin plate and kept closed.
보관한 미강 왁스를 60 ℃의 온도로 가열하여 용융시키고, 용융시킨 미강 왁스에 천연 라벤더 오일 15 방울(대략 5mL)을 혼합한 후, 휘핑기(whipper)를 이용해 휘핑하여 깨끗한 액상의 용융 미강 왁스를 수득하였으며, 수득한 미강 왁스를 스프정도의 걸쭉한 액상상태가 되도록 일방향 휘핑 및 반대 방향으로 휘핑을 반복 수행하여 부드러운 생크림 형상을 갖는 향료 포함 고체타입 미강 왁스를 제조하였다. The stored rice bran wax was heated to a temperature of 60 ° C. and melted, and 15 drops (approximately 5 mL) of natural lavender oil were mixed with the molten rice bran wax, followed by whipping using a whip to obtain a clean liquid molten rice bran wax. In addition, the obtained rice bran wax was repeatedly whisked in one direction and in the opposite direction so as to have a thick liquid state of soup level, thereby preparing a solid type rice bran wax having a soft whipped cream shape.
향료 포함 고체타입 미강 왁스를 면심지가 고정된 10 mL 용량의 용기에 공급한 후, 서서히 경화시켜 고체타입 미강 양초를 제조하였다.Solid type rice bran wax containing fragrance was supplied to a 10 mL container fixed with a wick, and then slowly cured to prepare a solid rice bran candle.
<< 실시예Example 4> 고체타입  4> solid type 미강Rice bran 양초의 제조 Manufacture of candles
실시예 1과 동일한 원재료 혼합물에 레시틴 및 이펙틴의 혼합물 15 g(레시틴 5 g 및 이펙틴 10 g)을 첨가하여 원재료 혼합물을 제조하는 것을 제외하고는 실시예 2와 동일한 방법으로 미강 양초를 제조하였다.Rice bran candles were prepared in the same manner as in Example 2, except that 15 g of a mixture of lecithin and effectin (5 g of lecithin and 10 g of effectin) was added to the same raw material mixture as in Example 1 to prepare a raw material mixture. .
<< 비교예Comparative example 1> 고체타입  1> solid type 미강Rice bran 양초의 제조 Manufacture of candles
미강 오일 55 g 및 스테아르산 45 g을 용해시켜 원재료 혼합물을 제조하는 것을 제외하고는 실시예 1과 동일한 방법으로 미강 왁스를 제조하였으며, 제조한 미강 왁스를 면심지가 고정형성된 원형 용기에 공급하여 미강 양초를 제조하였다.Rice bran wax was prepared in the same manner as in Example 1 except that 55 g of rice bran oil and 45 g of stearic acid were dissolved to prepare a raw material mixture. Candles were prepared.
<< 비교예Comparative example 2> 고체타입 천연 양초의 제조 2> Preparation of Solid Type Natural Candles
실시예 4와 동일한 원재료 혼합물에 레시틴 15 g을 첨가하여 미강 왁스를 제조하는 것을 제외하고는 실시예 4와 동일한 방법으로 미강 양초를 제조하였다.Rice bran candles were prepared in the same manner as in Example 4, except that 15 g of lecithin was added to the same raw material mixture as in Example 4 to prepare rice bran.
<< 실험예Experimental Example > 제조한 > Manufactured 미강Rice bran 왁스 및  Wax and 미강Rice bran 양초의 특성 평가 Characterization of the candle
제조한 미강 왁스 및 천연 양초가 갖는 특성을 평가하기 위해서, 실시예 1 내지 4, 비교예 1 및 비교예 2에 따른 방법으로 제조한 천연 양초의 특성을 분석하였다.In order to evaluate the properties of the prepared rice bran wax and natural candles, the properties of the natural candles prepared by the method according to Examples 1 to 4, Comparative Example 1 and Comparative Example 2 were analyzed.
(1) 실시예 1 및 비교예 1(1) Example 1 and Comparative Example 1
실시예 1에 따른 방법으로 제조한 미강 왁스의 특성을 분석한 결과, 3일 이상 25 ℃의 상온에서 변형이 없이 안정한 형태를 유지하였으며, 이를 통해, 제조한 미강 왁스의 장기 안정성이 우수함을 확인할 수 있었다.As a result of analyzing the characteristics of the rice bran wax prepared by the method according to Example 1, it maintained a stable form without deformation at room temperature of 25 ℃ for more than three days, through which, it can be confirmed that the long-term stability of the prepared rice bran wax is excellent. there was.
또한, 실시예 1에 따른 방법으로 제조한 천연 양초의 강도를 분석한 결과, 크림형상의 무른 양초를 형성한다는 사실을 확인할 수 있었고, 제조한 천연 양초의 심지에 불을 붙여 연소시킨 결과 균일한 평면 연소가 가능한 것을 확인할 수 있었다.In addition, as a result of analyzing the strength of the natural candles prepared by the method according to Example 1, it was confirmed that the cream-shaped soft candles were formed, and the fire of the wick of the natural candles produced by burning the uniform flat surface It was confirmed that combustion was possible.
반면에, 비교예 1에 따른 방법으로 제조한 왁스 조성물의 경우에는 우수한 외관을 형성할 수 있음을 확인할 수 있었으나, 천연 양초를 연소시키는 경우에는 일정시간이 경과한 후, 양초의 표면 전체에 불이 옮겨붙어 퍼지는 현상이 나타난다는 사실을 확인할 수 있어, 스테아르산의 포함함량이 높은 경우에는 연소 효율이 급증해 바람직하지 못한 결과를 야기할 수 있음을 확인할 수 있었다.On the other hand, in the case of the wax composition prepared by the method according to Comparative Example 1, it was confirmed that it can form an excellent appearance, but when burning a natural candle, after a certain time has elapsed, the entire surface of the candle is lit It can be confirmed that the phenomenon of sticking and spreading is observed. When the content of stearic acid is high, the combustion efficiency increases rapidly, which may cause undesirable results.
(2) 실시예 2 및 실시예 3(2) Example 2 and Example 3
제조한 천연 양초의 연소의 특성을 분석하기 위해서, 실시예 2에 따른 크림형 미강 양초 및 실시예 3에 따른 고체타입 미강 양초의 심지에 불을 붙여 연소시간, 그을음 및 잔류물 형성 등의 특성을 분석하였다. In order to analyze the characteristics of the burning of the natural candles produced, the wick of the cream-type rice bran candles according to Example 2 and the solid-type rice bran candles according to Example 3 were lit, and the characteristics such as burning time, soot and residue formation were investigated. Analyzed.
그 결과, 실시예 2에 따른 방법으로 제조한 미강 양초는 6시간 이상 연속적으로 연소하며, 미강 오일 특유의 고소한 향을 생성하는 것을 확인할 수 있었고, 그을음이 형성되지 않았으며, 연소된 후에도 잔류물이 생성되지 않아 우수한 연소효율을 갖는다는 사실을 확인할 수 있었다.As a result, the rice bran candles produced by the method according to Example 2 were continuously burned for more than 6 hours, and it was confirmed that they produced a savory flavor peculiar to rice bran oil, soot was not formed, and the residue remained after burning. It can be confirmed that it does not produce a good combustion efficiency.
또한, 실시예 3에 따른 방법으로 제조한 미강 양초는 굳은 후, 견고함이 우수하여 수송시에도 형상의 변화가 없이 안정하게 보관이 가능하다는 사실을 확인할 수 있었고, 그을음 및 잔류물의 생성이 없이 3시간 동안 연속적으로 안정하게 연소된다는 사실을 확인할 수 있었다.In addition, the rice bran candles prepared by the method according to Example 3 was confirmed that after solidified, it is excellent in durability and can be stored stably without change in shape even during transportation, and 3 without generating soot and residues. It was confirmed that the combustion was continuously and stably over time.
(3) 실시예 4 및 비교예 2(3) Example 4 and Comparative Example 2
제조한 천연 양초의 연소의 특성을 분석하기 위해서, 실시예 4 및 비교예 2에 따른 미강 양초의 심지에 불을 붙여 연소 특성을 분석한 결과, 비교예 2의 천연 양초의 경우에는, 좀더 단단한 특성을 유지하고, 제작시 결 무늬가 형성되었으나, 연소시 형성되는 불꽃의 크기가 약하고, 지속적으로 연소가 진행되지 못해 불꽃이 꺼지는 특성을 나타내어 추가적인 유화제를 첨가할 필요성이 있다는 사실을 확인할 수 있었던 반면에, 실시예 4의 방법으로 제조한 천연 양초의 경우에는 평면 연소가 우수하고, 지속적으로 안정하게 연소가 유도된다는 사실을 확인할 수 있었다.In order to analyze the characteristics of the burning of the manufactured natural candles, the combustion characteristics were analyzed by lighting the wicks of rice bran candles according to Example 4 and Comparative Example 2, and in the case of the natural candles of Comparative Example 2, more solid characteristics While the texture was formed during fabrication, the size of the flame formed during combustion was weak, and the flame was extinguished due to the continuous combustion. In the case of the natural candle manufactured by the method of Example 4, it was confirmed that the combustion was excellent and the planar combustion was continuously induced stably.
상기한 바와 같은 결과를 통해, 본 발명에 따른 미강 왁스 조성물은 장시간 동안 풀어지지 않고 안정한 상태를 유지하여, 천연 양초 제조에 효과적으로 활용이 가능하다는 사실을 확인할 수 있었고, 소이 왁스 등과 같은 종래의 왁스와 달리, 끈적임을 갖는 미세 왁스 알갱이의 비산이 없고, 저울 등과 같은 도구를 사용할 필요 없이 손쉽게 동일 크기의 천연 양초를 제조할 수 있음을 확인할 수 있었다. 또한, 상기 미강 왁스 조성물을 이용할 경우, 크림타입의 미강 양초 및 고체타입의 미강 양초를 안정하게 형성시킬 수 있음을 확인할 수 있었고, 제조한 미강 양초는 평면 연소가 가능하고, 그을음 및 잔류물이 발생되지 않으며, 장시간 안정한 연소가 가능한 우수한 특성을 갖는다는 사실을 확인할 수 있었다.Through the results as described above, it was confirmed that the rice bran wax composition according to the present invention is not released for a long time to maintain a stable state, it can be effectively utilized in the production of natural candles, and with conventional waxes such as soy wax Alternatively, it could be seen that there is no scattering of fine wax grains having stickiness, and that natural candles of the same size can be easily produced without using a tool such as a scale. In addition, when using the rice bran wax composition, it was confirmed that the cream-type rice bran and solid-type rice bran candle can be stably formed, the prepared rice bran can be burned flat, soot and residues are generated. It was confirmed that it has excellent characteristics capable of stable combustion for a long time.

Claims (5)

  1. 미강 오일 50 내지 150 중량부 및 스테아르산 10 내지 50 중량부를 포함하는 미강 왁스 조성물.Rice bran composition comprising 50 to 150 parts by weight of rice bran oil and 10 to 50 parts by weight of stearic acid.
  2. 제1항에 있어서, The method of claim 1,
    유화제 및 정유(essential oil)로 이루어진 군으로부터 선택되는 1종 이상을 추가로 포함하는 것을 특징으로 하는 미강 왁스 조성물.Rice bran wax composition, characterized in that it further comprises one or more selected from the group consisting of emulsifiers and essential oils.
  3. 제2항에 있어서,The method of claim 2,
    미강 오일 30 내지 70 중량부, 스테아르산 10 내지 20 중량부, 프로필렌글리콜 10 내지 20 중량부 및 정유 1 내지 15 중량부를 포함하는 것을 특징으로 하는 미강 왁스 조성물.Rice bran wax composition comprising 30 to 70 parts by weight of rice bran oil, 10 to 20 parts by weight of stearic acid, 10 to 20 parts by weight of propylene glycol and 1 to 15 parts by weight of essential oils.
  4. 제1항 내지 제3항 중 어느 한 항에 기재된 미강 왁스 조성물을 이용하여 천연 양초를 제조하는 방법에 있어서,In the method for producing a natural candle using the rice bran wax composition according to any one of claims 1 to 3,
    (a) 미강 오일 및 스테아르산을 혼합한 후, 50 내지 90 ℃의 온도로 가열하여 원재료 혼합물을 제조하는 단계;(a) mixing rice bran oil and stearic acid, and then heating to a temperature of 50 to 90 ° C. to prepare a raw material mixture;
    (b) 상기 원재료 혼합물을 교반하여 내부에 기포층이 형성된 미강 왁스를 제조하는 단계; 및(b) stirring the raw material mixture to prepare a rice bran wax having a bubble layer therein; And
    (c) 심지가 고정된 몰드에 상기 미강 왁스를 공급하는 단계;를 포함하는 크림타입 천연 양초의 제조방법.(c) supplying the rice bran wax to a mold having a wick fixed thereto.
  5. 제1항 내지 제3항 중 어느 한 항에 기재된 미강 왁스 조성물을 이용하여 천연 양초를 제조하는 방법에 있어서,In the method for producing a natural candle using the rice bran wax composition according to any one of claims 1 to 3,
    (a) 미강 오일 및 스테아르산을 혼합한 후, 50 내지 90 ℃의 온도로 가열하여 원재료 혼합물을 제조하는 단계;(a) mixing rice bran oil and stearic acid, and then heating to a temperature of 50 to 90 ° C. to prepare a raw material mixture;
    (b) 상기 원재료 혼합물을 교반하여 내부에 기포층이 형성된 미강 왁스를 제조하는 단계;(b) stirring the raw material mixture to prepare a rice bran wax having a bubble layer therein;
    (c) 상기 미강 왁스를 산화시키는 단계; 및(c) oxidizing the rice bran wax; And
    (d) 상기 단계에서 산화시킨 미강 왁스를 가열하여 왁스 용액을 제조하고, 제조한 왁스 용액을 심지가 고정된 용기에 공급하는 단계;를 포함하는 고체타입 천연 양초의 제조방법.(d) heating the rice bran wax oxidized in the above step to produce a wax solution, and supplying the prepared wax solution to a container having a wick fixed thereto.
PCT/KR2018/001667 2017-02-22 2018-02-07 Rice bran wax composition comprising rice bran oil and method for preparing natural rice bran candle using same WO2018155850A1 (en)

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