WO2018058283A1 - Insecticide and preparation method therefor - Google Patents

Insecticide and preparation method therefor Download PDF

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Publication number
WO2018058283A1
WO2018058283A1 PCT/CN2016/100281 CN2016100281W WO2018058283A1 WO 2018058283 A1 WO2018058283 A1 WO 2018058283A1 CN 2016100281 W CN2016100281 W CN 2016100281W WO 2018058283 A1 WO2018058283 A1 WO 2018058283A1
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parts
juice
insecticide
wormwood
methamidophos
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French (fr)
Chinese (zh)
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王建明
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王建明
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/26Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-nitrogen bonds
    • A01N57/28Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-nitrogen bonds containing acyclic or cycloaliphatic radicals

Definitions

  • An insecticide consists of the following ingredients in a mass fraction: 15 parts of wormwood juice, arsenic trioxide 7 6 parts of methamidophos, 6 parts of methamidophos, 11 parts of saffron, 7 parts of chlorfluazuron, 5 parts of allicin, 15 parts of chili juice, 10 parts of wormwood juice, 11 parts of geranium, 10 parts of arboreal bark, Averm. 2 copies.
  • a method for preparing an insecticide has the following steps:

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  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

Provided are an insecticide and a preparation method therefor. The insecticide is composed of the following formulation components in parts by mass: 10-20 parts of wormwood juice, 6-8 parts of arsenic trioxide, 5-7 parts of methamidophos, 10-12 parts of Crocus sativus, 6-8 parts of chlorfluazuron, 4-6 parts of allicin, 10-20 parts of chilli juice, 5-15 parts of Artemisia argyi juice, 10-12 parts of Geranium wilfordii, 5-15 parts of Artemisia tridentata bark, and 1-3 parts of avermectin. The preparation method is simple. The effect of killing scale insects is significant. The insecticide has no toxic side effects for humans and livestock, does not pollute the ecological environment and is a low-toxicity, safe and environmentally friendly green insecticide.

Description

一种杀虫剂及其制备方法Insecticide and preparation method thereof 技术领域Technical field
本发明涉及高分子材料领域,具体而言涉及一种杀虫剂及其制备方法。The invention relates to the field of polymer materials, in particular to an insecticide and a preparation method thereof.
背景技术Background technique
介壳虫是半翅目,蚧总科昆虫的总称,介壳虫是花卉和果树上最常见的害虫,常见的有吹绵蚧、樟蚌圆盾蚧、糠片蚧、朝鲜球坚蚧、桑白蚧、康氏粉蚧、扶桑绵粉蚧等,介壳虫常群集于枝、叶、果上,吸取植物汁液为生,严重时会造成枝条凋萎或全株死亡,此外,介壳虫的分泌物还能诱发煤污病,危害极大。Scale insects are the general name of the Hemiptera, the genus Insects. The scale insects are the most common pests on flowers and fruit trees. Commonly, there are blown mites, 樟蚌 蚧 蚧, 糠 蚧, Korean 蚧 蚧, 桑白蚧, Kang's whitefly, Fusang powder, etc., scale insects often cluster on branches, leaves, and fruits, sucking plant juice for a living, in severe cases, the branches will wither or the whole plant will die, in addition, the secretion of scale insects It can also induce coal pollution, which is extremely harmful.
目前,杀灭介壳虫效果较好的杀虫成分为速扑杀,其杀虫效果较好,但是速扑杀属高毒农药,毒性大,对人畜毒副作用以及对生态环境影响较大。因此,需要研究一种杀灭介壳虫效果显著,并且对人畜无毒副作用的杀虫剂。At present, the insecticidal component with better effect on killing scale insects is quick-killing, and its insecticidal effect is better, but the speed-killing is a highly toxic pesticide, which is highly toxic, has a great impact on human and animal toxic side effects and on the ecological environment. Therefore, it is necessary to study an insecticide which has a remarkable effect of killing scale insects and has no toxic side effects on humans and animals.
发明内容Summary of the invention
本发明提供了一种杀虫剂及其制备方法,本发明对人畜有毒副作用以及污染生态环境的问题。The invention provides an insecticide and a preparation method thereof, and the invention has the problems of toxic side effects on humans and animals and pollution of the ecological environment.
为实现上述目的,本发明提供如下技术方案:To achieve the above object, the present invention provides the following technical solutions:
一种杀虫剂,由以下质量分数配方成分组成:蒿草汁10-20份、三氧化二砷6-8份、甲胺磷5-7份、藏红花10-12份、氟啶脲6-8份、大蒜素4-6份、辣椒汁 10-20份、艾草汁5-15份、老鹳草10-12份、山艾树皮5-15份、阿维菌素1-3份。An insecticide consisting of the following ingredients in a mass fraction: 10-20 parts of wormwood juice, 6-8 parts of arsenic trioxide, 5-7 parts of methamidophos, 10-12 parts of saffron, 6-8 parts of fluridazine, Allicin 4-6 parts, chili juice 10-20 parts, 5-15 parts of wormwood juice, 10-12 parts of geranium, 5-15 parts of sage bark, and 1-3 parts of avermectin.
进一步:由以下质量分数配方成分组成:蒿草汁10份、三氧化二砷6份、甲胺磷5份、藏红花10份、氟啶脲6份、大蒜素4份、辣椒汁10份、艾草汁5份、老鹳草10份、山艾树皮5份、阿维菌素1份。Further: consisting of the following mass fraction formula ingredients: 10 parts of wormwood juice, 6 parts of arsenic trioxide, 5 parts of methamidophos, 10 parts of saffron, 6 parts of fluazironil, 4 parts of allicin, 10 parts of chili juice, wormwood juice 5 10 parts of geranium, 5 parts of sage bark, and 1 part of avermectin.
进一步:由以下质量分数配方成分组成:蒿草汁15份、三氧化二砷7份、甲胺磷6份、藏红花11份、氟啶脲7份、大蒜素5份、辣椒汁15份、艾草汁10份、老鹳草11份、山艾树皮10份、阿维菌素2份。Further: consisting of the following mass fraction formula ingredients: 15 parts of wormwood juice, 7 parts of arsenic trioxide, 6 parts of methamidophos, 11 parts of saffron, 7 parts of fluazironil, 5 parts of allicin, 15 parts of chili juice, wormwood juice 10 11 parts of geranium, 10 parts of sage bark, and 2 parts of avermectin.
进一步:由以下质量分数配方成分组成:蒿草汁20份、三氧化二砷8份、甲胺磷7份、藏红花12份、氟啶脲8份、大蒜素6份、辣椒汁20份、艾草汁15份、老鹳草12份、山艾树皮15份、阿维菌素3份。Further: consisting of the following mass fraction formula ingredients: 20 parts of wormwood juice, 8 parts of arsenic trioxide, 7 parts of methamidophos, 12 parts of saffron, 8 parts of fluridazine, 6 parts of allicin, 20 parts of chili juice, wormwood juice 15 12 parts of geranium, 15 parts of sage bark, and 3 parts of avermectin.
进一步:一种杀虫剂的制备方法具有以下几个步骤:Further: a method for preparing an insecticide has the following steps:
步骤一:将蒿草汁、藏红花、大蒜素、辣椒汁、艾草汁、老鹳草、山艾树皮,加热至50-70℃煎煮2-4h;Step 1: wormwood juice, saffron, allicin, chili juice, wormwood juice, geranium, sage bark, heated to 50-70 ° C for 2-4 h;
步骤二:将步骤一过滤,合并滤液;Step 2: Filter step one and combine the filtrates;
步骤三:将步骤二加入三氧化二砷、甲胺磷、氟啶脲和阿维菌素,后混合加热至100℃后放置室温后既得一种杀虫剂。Step 3: Add the arsenic trioxide, methamidophos, fluridazine and avermectin to the second step, and then mix and heat to 100 ° C and then leave the room temperature to obtain an insecticide.
本发明的有益效果是:The beneficial effects of the invention are:
1、本发明无污染在使用后对环境不造成任何危害; 1. The invention has no pollution and does not cause any harm to the environment after use;
2、本发明,制备方法简单,杀灭介壳虫效果显著;2. The invention has simple preparation method and remarkable effect on killing scale insects;
3、本发明是一种低毒、安全、环保的绿色杀虫剂。3. The invention is a low toxicity, safe and environmentally friendly green insecticide.
具体实施方式detailed description
下面将结合本发明实施例,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。The technical solutions in the embodiments of the present invention are clearly and completely described in the following with reference to the embodiments of the present invention. It is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments obtained by those skilled in the art based on the embodiments of the present invention without creative efforts are within the scope of the present invention.
实施例一:Embodiment 1:
一种杀虫剂由以下质量分数配方成分组成:蒿草汁10-20份、三氧化二砷6-8份、甲胺磷5-7份、藏红花10-12份、氟啶脲6-8份、大蒜素4-6份、辣椒汁10-20份、艾草汁5-15份、老鹳草10-12份、山艾树皮5-15份、阿维菌素1-3份。An insecticide consists of the following ingredients in a mass fraction: 10-20 parts of wormwood juice, 6-8 parts of arsenic trioxide, 5-7 parts of methamidophos, 10-12 parts of saffron, 6-8 parts of fluridazine, garlic 4-6 parts, 10-20 parts of chili juice, 5-15 parts of wormwood juice, 10-12 parts of geranium, 5-15 parts of sage bark, and 1-3 parts of avermectin.
实施例二:Embodiment 2:
一种杀虫剂由以下质量分数配方成分组成:蒿草汁10份、三氧化二砷6份、甲胺磷5份、藏红花10份、氟啶脲6份、大蒜素4份、辣椒汁10份、艾草汁5份、老鹳草10份、山艾树皮5份、阿维菌素1份。An insecticide consists of the following ingredients in a mass fraction: 10 parts of wormwood juice, 6 parts of arsenic trioxide, 5 parts of methamidophos, 10 parts of saffron, 6 parts of fluazironil, 4 parts of allicin, 10 parts of chili juice, and 5 parts of grass juice, 10 parts of geranium, 5 parts of sage bark, and 1 part of avermectin.
实施例三:Embodiment 3:
一种杀虫剂由以下质量分数配方成分组成:蒿草汁15份、三氧化二砷7 份、甲胺磷6份、藏红花11份、氟啶脲7份、大蒜素5份、辣椒汁15份、艾草汁10份、老鹳草11份、山艾树皮10份、阿维菌素2份。An insecticide consists of the following ingredients in a mass fraction: 15 parts of wormwood juice, arsenic trioxide 7 6 parts of methamidophos, 6 parts of methamidophos, 11 parts of saffron, 7 parts of chlorfluazuron, 5 parts of allicin, 15 parts of chili juice, 10 parts of wormwood juice, 11 parts of geranium, 10 parts of arboreal bark, Averm. 2 copies.
实施例四:Embodiment 4:
一种杀虫剂由以下质量分数配方成分组成:蒿草汁20份、三氧化二砷8份、甲胺磷7份、藏红花12份、氟啶脲8份、大蒜素6份、辣椒汁20份、艾草汁15份、老鹳草12份、山艾树皮15份、阿维菌素3份。An insecticide consists of the following ingredients in a mass fraction: 20 parts of wormwood juice, 8 parts of arsenic trioxide, 7 parts of methamidophos, 12 parts of saffron, 8 parts of chlorfluazuron, 6 parts of allicin, 20 parts of chili juice, and 15 parts of grass juice, 12 parts of geranium, 15 parts of sage bark, and 3 parts of avermectin.
实施例五:Embodiment 5:
一种杀虫剂的制备方法具有以下几个步骤:A method for preparing an insecticide has the following steps:
步骤一:将蒿草汁、藏红花、大蒜素、辣椒汁、艾草汁、老鹳草、山艾树皮,加热至50-70℃煎煮2-4h;Step 1: wormwood juice, saffron, allicin, chili juice, wormwood juice, geranium, sage bark, heated to 50-70 ° C for 2-4 h;
步骤二:将步骤一过滤,合并滤液;Step 2: Filter step one and combine the filtrates;
步骤三:将步骤二加入三氧化二砷、甲胺磷、氟啶脲和阿维菌素,后混合加热至100℃后放置室温后既得一种杀虫剂。Step 3: Add the arsenic trioxide, methamidophos, fluridazine and avermectin to the second step, and then mix and heat to 100 ° C and then leave the room temperature to obtain an insecticide.
此外,应当理解,虽然本说明书按照实施方式加以描述,但并非每个实施方式仅包含一个独立的技术方案,说明书的这种叙述方式仅仅是为清楚起见,本领域技术人员应当将说明书作为一个整体,各实施例中的技术方案也可以经适当组合,形成本领域技术人员可以理解的其他实施方式。 In addition, it should be understood that although the description is described in terms of embodiments, not every embodiment includes only one independent technical solution. The description of the specification is merely for the sake of clarity, and those skilled in the art should regard the specification as a whole. The technical solutions in the respective embodiments may also be combined as appropriate to form other embodiments that can be understood by those skilled in the art.

Claims (5)

  1. 一种杀虫剂,其特征在于:由以下质量分数配方成分组成:An insecticide characterized by consisting of the following mass fraction formula ingredients:
    蒿草汁10-20份、三氧化二砷6-8份、甲胺磷5-7份、藏红花10-12份、氟啶脲6-8份、大蒜素4-6份、辣椒汁10-20份、艾草汁5-15份、老鹳草10-12份、山艾树皮5-15份、阿维菌素1-3份。10-20 parts of wormwood juice, 6-8 parts of arsenic trioxide, 5-7 parts of methamidophos, 10-12 parts of saffron, 6-8 parts of fluridazine, 4-6 parts of allicin, 10-20 parts of chili juice, 5-15 parts of wormwood juice, 10-12 parts of geranium, 5-15 parts of sage bark, and 1-3 parts of avermectin.
  2. 根据权利要求1所述的一种杀虫剂,其特征在于:由以下质量分数配方成分组成:An insecticide according to claim 1, which is composed of the following mass fraction formula ingredients:
    蒿草汁10份、三氧化二砷6份、甲胺磷5份、藏红花10份、氟啶脲6份、大蒜素4份、辣椒汁10份、艾草汁5份、老鹳草10份、山艾树皮5份、阿维菌素1份。10 parts of wormwood juice, 6 parts of arsenic trioxide, 5 parts of methamidophos, 10 parts of saffron, 6 parts of chlorfluazuron, 4 parts of allicin, 10 parts of chili juice, 5 parts of wormwood juice, 10 parts of geranium, mountain AI 5 parts of bark and 1 part of avermectin.
  3. 根据权利要求1所述的一种杀虫剂,其特征在于:由以下质量分数配方成分组成:An insecticide according to claim 1, which is composed of the following mass fraction formula ingredients:
    蒿草汁15份、三氧化二砷7份、甲胺磷6份、藏红花11份、氟啶脲7份、大蒜素5份、辣椒汁15份、艾草汁10份、老鹳草11份、山艾树皮10份、阿维菌素2份。15 parts of wormwood juice, 7 parts of arsenic trioxide, 6 parts of methamidophos, 11 parts of saffron, 7 parts of chlorfluazuron, 5 parts of allicin, 15 parts of chili juice, 10 parts of wormwood juice, 11 parts of geranium, Shanai 10 parts of bark and 2 parts of avermectin.
  4. 根据权利要求1所述的一种杀虫剂,其特征在于:由以下质量分数配方成分组成:An insecticide according to claim 1, which is composed of the following mass fraction formula ingredients:
    蒿草汁20份、三氧化二砷8份、甲胺磷7份、藏红花12份、氟啶脲8份、大蒜素6份、辣椒汁20份、艾草汁15份、老鹳草12份、山艾树皮15份、 阿维菌素3份。20 parts of wormwood juice, 8 parts of arsenic trioxide, 7 parts of methamidophos, 12 parts of saffron, 8 parts of chlorfluazuron, 6 parts of allicin, 20 parts of chili juice, 15 parts of wormwood juice, 12 parts of geranium, Shanai 15 bark, 3 parts of avermectin.
  5. 一种根据权利要求1所述的一种杀虫剂的制备方法,其特征在于:具有以下几个步骤:A method for preparing an insecticide according to claim 1, characterized by the following steps:
    步骤一:将蒿草汁、藏红花、大蒜素、辣椒汁、艾草汁、老鹳草、山艾树皮,加热至50-70℃煎煮2-4h;Step 1: wormwood juice, saffron, allicin, chili juice, wormwood juice, geranium, sage bark, heated to 50-70 ° C for 2-4 h;
    步骤二:将步骤一过滤,合并滤液;Step 2: Filter step one and combine the filtrates;
    步骤三:将步骤二加入三氧化二砷、甲胺磷、氟啶脲和阿维菌素,后混合加热至100℃后放置室温后既得一种杀虫剂。 Step 3: Add the arsenic trioxide, methamidophos, fluridazine and avermectin to the second step, and then mix and heat to 100 ° C and then leave the room temperature to obtain an insecticide.
PCT/CN2016/100281 2016-09-27 2016-09-27 Insecticide and preparation method therefor WO2018058283A1 (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110754484A (en) * 2019-09-27 2020-02-07 贵州省果树科学研究所 Mulberry scale control method for reducing pesticide residues in dragon orchard
CN116369086A (en) * 2023-05-25 2023-07-04 浙江石原金牛化工有限公司 Method for preventing and controlling waxberry wilting disease

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102633745A (en) * 2012-04-05 2012-08-15 南开大学 Alpha-methoxy imino group-4-methyl-1, 2, 3-thiadiazole-5-methyl carboxylic ester derivatives and preparation method and application thereof
CN103518778A (en) * 2013-10-25 2014-01-22 卢逸凡 Insecticide
CN105028469A (en) * 2015-07-31 2015-11-11 南通惠然生物科技有限公司 Efficient and environment-friendly pestcide

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102633745A (en) * 2012-04-05 2012-08-15 南开大学 Alpha-methoxy imino group-4-methyl-1, 2, 3-thiadiazole-5-methyl carboxylic ester derivatives and preparation method and application thereof
CN103518778A (en) * 2013-10-25 2014-01-22 卢逸凡 Insecticide
CN105028469A (en) * 2015-07-31 2015-11-11 南通惠然生物科技有限公司 Efficient and environment-friendly pestcide

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110754484A (en) * 2019-09-27 2020-02-07 贵州省果树科学研究所 Mulberry scale control method for reducing pesticide residues in dragon orchard
CN116369086A (en) * 2023-05-25 2023-07-04 浙江石原金牛化工有限公司 Method for preventing and controlling waxberry wilting disease
CN116369086B (en) * 2023-05-25 2024-01-19 浙江石原金牛化工有限公司 Method for preventing and controlling waxberry wilting disease

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