WO2018049548A1 - Antirust paint and preparation method therefor - Google Patents

Antirust paint and preparation method therefor Download PDF

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Publication number
WO2018049548A1
WO2018049548A1 PCT/CN2016/098783 CN2016098783W WO2018049548A1 WO 2018049548 A1 WO2018049548 A1 WO 2018049548A1 CN 2016098783 W CN2016098783 W CN 2016098783W WO 2018049548 A1 WO2018049548 A1 WO 2018049548A1
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parts
rosin
calcium carbonate
iron oxide
cellulose acetate
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PCT/CN2016/098783
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French (fr)
Chinese (zh)
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张勇健
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张勇健
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Priority to PCT/CN2016/098783 priority Critical patent/WO2018049548A1/en
Publication of WO2018049548A1 publication Critical patent/WO2018049548A1/en

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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/08—Anti-corrosive paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • C09D133/04—Homopolymers or copolymers of esters
    • C09D133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
    • C09D133/08—Homopolymers or copolymers of acrylic acid esters

Definitions

  • the invention relates to the field of coatings, in particular to an anti-rust coating and a preparation method thereof.
  • the invention provides an anti-rust paint and a preparation method thereof, and the invention has the characteristics of simple composition, reasonable ratio and relatively low production cost.
  • the present invention provides the following technical solutions:
  • An anti-rust coating consisting of the following mass fraction of ingredients: 10-20 parts of acrylic resin, 6-8 parts of tetrachloroisophthalonitrile, 5-7 parts of calcium carbonate, 6-8 parts of coal tar pitch, sulfonated oil 2-4 parts, 3-5 parts of iron oxide, 4-6 parts of ammonium metaborate, 8-12 parts of cellulose acetate, 4-6 parts of rosin, and 1-3 parts of preservative.
  • a method for preparing an anti-rust coating has the following steps:
  • Step 1 Transfer acrylic resin, tetrachloroisophthalonitrile, calcium carbonate, coal tar pitch, sulfonated oil, iron oxide, ammonium metaborate, cellulose acetate and rosin into the reaction kettle, and raise the temperature to 50 ° C ⁇ 60 ° C , heat stirring for 40 minutes to 50 minutes;
  • Step 2 adding a preservative, controlling the temperature in the reaction vessel to room temperature, and stirring for 20 minutes to 30 minutes to obtain an anti-rust paint.
  • the invention has the advantages that the composition of the invention is simple, the ratio is reasonable, the coating has corrosion resistance and wear resistance, is suitable for use in a harsh environment, is convenient to produce, and has relatively low production cost.
  • Embodiment 1 is a diagrammatic representation of Embodiment 1:
  • the rustproof coating is composed of the following mass fraction formula components: 10-20 parts of acrylic resin, 6-8 parts of tetrachloroisophthalonitrile, 5-7 parts of calcium carbonate, 6-8 parts of coal tar pitch, sulfonated oil 2 - 4 parts, 3-5 parts of iron oxide, 4-6 parts of ammonium metaborate, 8-12 parts of cellulose acetate, 4-6 parts of rosin, and 1-3 parts of preservative.
  • Embodiment 2 is a diagrammatic representation of Embodiment 1:
  • An anti-rust coating consists of the following mass fraction of ingredients: 10 parts of acrylic resin, 6 parts of tetrachloroisophthalonitrile, 5 parts of calcium carbonate, 6 parts of coal tar pitch, 2 parts of sulfonated oil, 3 parts of iron oxide, partial 4 parts of ammonium borate, 8 parts of cellulose acetate, 4 parts of rosin, and 1 part of preservative.
  • Embodiment 3 is a diagrammatic representation of Embodiment 3
  • An anti-rust coating consists of the following mass fraction formula: 15 parts of acrylic resin, 7 parts of tetrachloroisophthalonitrile, 6 parts of calcium carbonate, 7 parts of coal tar pitch, 3 parts of sulfonated oil, 4 parts of iron oxide, partial 5 parts of ammonium borate, 10 parts of cellulose acetate, 5 parts of rosin, and 2 parts of preservative.
  • Embodiment 4 is a diagrammatic representation of Embodiment 4:
  • An anti-rust coating consists of the following mass fraction of ingredients: 20 parts of acrylic resin, 8 parts of tetrachloroisophthalonitrile, 7 parts of calcium carbonate, 8 parts of coal tar pitch, 4 parts of sulfonated oil, 5 parts of iron oxide, partial 6 parts of ammonium borate, 12 parts of cellulose acetate, 6 parts of rosin, and 3 parts of preservative.
  • Embodiment 5 is a diagrammatic representation of Embodiment 5:
  • a method for preparing an anti-rust coating has the following steps:
  • Step 1 Transfer acrylic resin, tetrachloroisophthalonitrile, calcium carbonate, coal tar pitch, sulfonated oil, iron oxide, ammonium metaborate, cellulose acetate and rosin into the reaction kettle, and raise the temperature to 50 ° C ⁇ 60 ° C , heat stirring for 40 minutes to 50 minutes;
  • Step 2 adding a preservative, controlling the temperature in the reaction vessel to room temperature, and stirring for 20 minutes to 30 minutes to obtain an anti-rust paint.

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Paints Or Removers (AREA)

Abstract

Provided are an antirust paint and a preparation method therefor. The antirust paint consists of the following ingredients in parts by mass: 10-20 parts of acrylic acid resins, 6-8 parts of chlorothalonil, 5-7 parts of calcium carbonate, 6-8 parts of coal bitumen, 2-4 parts of sulfonated oil, 3-5 parts of iron oxide, 4-6 parts of ammonium metaborate, 8-12 parts of cellulose acetate, 4-6 parts of rosin, and 1-3 parts of antiseptics. The paint has simple ingredients, is appropriate in proportion, and is low in production cost.

Description

一种防锈涂料及其制备方法Anti-rust paint and preparation method thereof 技术领域Technical field
本发明涉及涂料领域，具体而言涉及一种防锈涂料及其制备方法。The invention relates to the field of coatings, in particular to an anti-rust coating and a preparation method thereof.
背景技术Background technique
在现代工业和日常生活中，各种腐蚀随处可见，尤其是工程装备处于潮湿、高盐、多风、强气流环境中，为极端恶劣环境，裸露在外的部件容易受到严重的腐蚀，使其使用寿命降低，成分增加。现有的防锈涂料其组分复杂，配比不合理，制备工艺复杂，无法满足使用者的需求故此，现有的防锈涂料有待于进一步完善。In modern industry and daily life, various kinds of corrosion can be seen everywhere, especially in the environment of humid, high-salt, windy and strong airflow. For extremely harsh environments, exposed parts are prone to severe corrosion and use. Life is reduced and ingredients are increased. The existing anti-rust paints have complex components, unreasonable ratios, complicated preparation processes, and cannot meet the needs of users. Therefore, the existing anti-rust paints need to be further improved.
发明内容Summary of the invention
本发明提供了一种防锈涂料及其制备方法，本发明具有组分简单，配比合理，生产成本相对较低的特点。The invention provides an anti-rust paint and a preparation method thereof, and the invention has the characteristics of simple composition, reasonable ratio and relatively low production cost.
为实现上述目的，本发明提供如下技术方案：To achieve the above object, the present invention provides the following technical solutions:
一种防锈涂料，由以下质量分数配方成分组成：丙烯酸树脂10-20份、四氯间苯二腈6-8份、碳酸钙5-7份、煤焦沥青6-8份、磺化油2-4份、氧化铁3-5份、偏硼酸铵4-6份、醋酸纤维素8-12份、松香4-6份、防腐剂1-3份。An anti-rust coating consisting of the following mass fraction of ingredients: 10-20 parts of acrylic resin, 6-8 parts of tetrachloroisophthalonitrile, 5-7 parts of calcium carbonate, 6-8 parts of coal tar pitch, sulfonated oil 2-4 parts, 3-5 parts of iron oxide, 4-6 parts of ammonium metaborate, 8-12 parts of cellulose acetate, 4-6 parts of rosin, and 1-3 parts of preservative.
进一步：由以下质量分数配方成分组成：丙烯酸树脂10份、四氯间苯二腈6份、碳酸钙5份、煤焦沥青6份、磺化油2份、氧化铁3份、偏硼酸铵4 份、醋酸纤维素8份、松香4份、防腐剂1份。Further: composed of the following mass fraction formula ingredients: 10 parts of acrylic resin, 6 parts of tetrachloroisophthalonitrile, 5 parts of calcium carbonate, 6 parts of coal tar pitch, 2 parts of sulfonated oil, 3 parts of iron oxide, ammonium metaborate 4 Parts, 8 parts of cellulose acetate, 4 parts of rosin, 1 part of preservative.
进一步：由以下质量分数配方成分组成：丙烯酸树脂15份、四氯间苯二腈7份、碳酸钙6份、煤焦沥青7份、磺化油3份、氧化铁4份、偏硼酸铵5份、醋酸纤维素10份、松香5份、防腐剂2份。Further: composed of the following mass fraction formula ingredients: 15 parts of acrylic resin, 7 parts of tetrachloroisophthalonitrile, 6 parts of calcium carbonate, 7 parts of coal tar pitch, 3 parts of sulfonated oil, 4 parts of iron oxide, ammonium metaborate 5 Parts, 10 parts of cellulose acetate, 5 parts of rosin, 2 parts of preservative.
进一步：由以下质量分数配方成分组成：丙烯酸树脂20份、四氯间苯二腈8份、碳酸钙7份、煤焦沥青8份、磺化油4份、氧化铁5份、偏硼酸铵6份、醋酸纤维素12份、松香6份、防腐剂3份。Further: consisting of the following mass fraction formula ingredients: 20 parts of acrylic resin, 8 parts of tetrachloroisophthalonitrile, 7 parts of calcium carbonate, 8 parts of coal tar pitch, 4 parts of sulfonated oil, 5 parts of iron oxide, and ammonium metaborate 6 A portion, 12 parts of cellulose acetate, 6 parts of rosin, and 3 parts of preservative.
进一步：一种防锈涂料的制备方法具有以下几个步骤：Further: a method for preparing an anti-rust coating has the following steps:
步骤一：将丙烯酸树脂、四氯间苯二腈、碳酸钙、煤焦沥青、磺化油、氧化铁、偏硼酸铵、醋酸纤维素和松香转入反应釜中，升温至50℃～60℃，保温搅拌40分钟～50分钟；Step 1: Transfer acrylic resin, tetrachloroisophthalonitrile, calcium carbonate, coal tar pitch, sulfonated oil, iron oxide, ammonium metaborate, cellulose acetate and rosin into the reaction kettle, and raise the temperature to 50 ° C ~ 60 ° C , heat stirring for 40 minutes to 50 minutes;
步骤二：加入防腐剂，控制反应釜内温度为室温，保温搅拌20分钟～30分钟后既得一种防锈涂料。Step 2: adding a preservative, controlling the temperature in the reaction vessel to room temperature, and stirring for 20 minutes to 30 minutes to obtain an anti-rust paint.
本发明的有益效果是：本发明组分简单，配比合理，涂层具有耐腐蚀、耐磨性，适合于恶劣的环境使用，生产方便，生产成本相对较低。The invention has the advantages that the composition of the invention is simple, the ratio is reasonable, the coating has corrosion resistance and wear resistance, is suitable for use in a harsh environment, is convenient to produce, and has relatively low production cost.
具体实施方式detailed description
下面将结合本发明实施例，对本发明实施例中的技术方案进行清楚、完整地描述，显然，所描述的实施例仅仅是本发明一部分实施例，而不是全部 的实施例。基于本发明中的实施例，本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例，都属于本发明保护的范围。The technical solutions in the embodiments of the present invention are clearly and completely described in the following with reference to the embodiments of the present invention. It is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all An embodiment. All other embodiments obtained by those skilled in the art based on the embodiments of the present invention without creative efforts are within the scope of the present invention.
实施例一：Embodiment 1:
一种防锈涂料由以下质量分数配方成分组成：丙烯酸树脂10-20份、四氯间苯二腈6-8份、碳酸钙5-7份、煤焦沥青6-8份、磺化油2-4份、氧化铁3-5份、偏硼酸铵4-6份、醋酸纤维素8-12份、松香4-6份、防腐剂1-3份。The rustproof coating is composed of the following mass fraction formula components: 10-20 parts of acrylic resin, 6-8 parts of tetrachloroisophthalonitrile, 5-7 parts of calcium carbonate, 6-8 parts of coal tar pitch, sulfonated oil 2 - 4 parts, 3-5 parts of iron oxide, 4-6 parts of ammonium metaborate, 8-12 parts of cellulose acetate, 4-6 parts of rosin, and 1-3 parts of preservative.
实施例二：Embodiment 2:
一种防锈涂料由以下质量分数配方成分组成：丙烯酸树脂10份、四氯间苯二腈6份、碳酸钙5份、煤焦沥青6份、磺化油2份、氧化铁3份、偏硼酸铵4份、醋酸纤维素8份、松香4份、防腐剂1份。An anti-rust coating consists of the following mass fraction of ingredients: 10 parts of acrylic resin, 6 parts of tetrachloroisophthalonitrile, 5 parts of calcium carbonate, 6 parts of coal tar pitch, 2 parts of sulfonated oil, 3 parts of iron oxide, partial 4 parts of ammonium borate, 8 parts of cellulose acetate, 4 parts of rosin, and 1 part of preservative.
实施例三：Embodiment 3:
一种防锈涂料由以下质量分数配方成分组成：丙烯酸树脂15份、四氯间苯二腈7份、碳酸钙6份、煤焦沥青7份、磺化油3份、氧化铁4份、偏硼酸铵5份、醋酸纤维素10份、松香5份、防腐剂2份。An anti-rust coating consists of the following mass fraction formula: 15 parts of acrylic resin, 7 parts of tetrachloroisophthalonitrile, 6 parts of calcium carbonate, 7 parts of coal tar pitch, 3 parts of sulfonated oil, 4 parts of iron oxide, partial 5 parts of ammonium borate, 10 parts of cellulose acetate, 5 parts of rosin, and 2 parts of preservative.
实施例四：Embodiment 4:
一种防锈涂料由以下质量分数配方成分组成：丙烯酸树脂20份、四氯间苯二腈8份、碳酸钙7份、煤焦沥青8份、磺化油4份、氧化铁5份、偏硼酸铵6份、醋酸纤维素12份、松香6份、防腐剂3份。 An anti-rust coating consists of the following mass fraction of ingredients: 20 parts of acrylic resin, 8 parts of tetrachloroisophthalonitrile, 7 parts of calcium carbonate, 8 parts of coal tar pitch, 4 parts of sulfonated oil, 5 parts of iron oxide, partial 6 parts of ammonium borate, 12 parts of cellulose acetate, 6 parts of rosin, and 3 parts of preservative.
实施例五：Embodiment 5:
一种防锈涂料的制备方法具有以下几个步骤：A method for preparing an anti-rust coating has the following steps:
步骤一：将丙烯酸树脂、四氯间苯二腈、碳酸钙、煤焦沥青、磺化油、氧化铁、偏硼酸铵、醋酸纤维素和松香转入反应釜中，升温至50℃～60℃，保温搅拌40分钟～50分钟；Step 1: Transfer acrylic resin, tetrachloroisophthalonitrile, calcium carbonate, coal tar pitch, sulfonated oil, iron oxide, ammonium metaborate, cellulose acetate and rosin into the reaction kettle, and raise the temperature to 50 ° C ~ 60 ° C , heat stirring for 40 minutes to 50 minutes;
步骤二：加入防腐剂，控制反应釜内温度为室温，保温搅拌20分钟～30分钟后既得一种防锈涂料。Step 2: adding a preservative, controlling the temperature in the reaction vessel to room temperature, and stirring for 20 minutes to 30 minutes to obtain an anti-rust paint.
此外，应当理解，虽然本说明书按照实施方式加以描述，但并非每个实施方式仅包含一个独立的技术方案，说明书的这种叙述方式仅仅是为清楚起见，本领域技术人员应当将说明书作为一个整体，各实施例中的技术方案也可以经适当组合，形成本领域技术人员可以理解的其他实施方式。 In addition, it should be understood that although the description is described in terms of embodiments, not every embodiment includes only one independent technical solution. The description of the specification is merely for the sake of clarity, and those skilled in the art should regard the specification as a whole. The technical solutions in the respective embodiments may also be combined as appropriate to form other embodiments that can be understood by those skilled in the art.

Claims (5)

  1. 一种防锈涂料，其特征在于：由以下质量分数配方成分组成：An anti-rust paint characterized by: consisting of the following mass fraction formula ingredients:
    丙烯酸树脂10-20份、四氯间苯二腈6-8份、碳酸钙5-7份、煤焦沥青6-8份、磺化油2-4份、氧化铁3-5份、偏硼酸铵4-6份、醋酸纤维素8-12份、松香4-6份、防腐剂1-3份。10-20 parts of acrylic resin, 6-8 parts of tetrachloroisophthalonitrile, 5-7 parts of calcium carbonate, 6-8 parts of coal tar pitch, 2-4 parts of sulfonated oil, 3-5 parts of iron oxide, metaboric acid 4-6 parts of ammonium, 8-12 parts of cellulose acetate, 4-6 parts of rosin, and 1-3 parts of preservative.
  2. 根据权利要求1所述的一种防锈涂料，其特征在于：由以下质量分数配方成分组成：The rust preventive paint according to claim 1, which is composed of the following mass fraction formula ingredients:
    丙烯酸树脂10份、四氯间苯二腈6份、碳酸钙5份、煤焦沥青6份、磺化油2份、氧化铁3份、偏硼酸铵4份、醋酸纤维素8份、松香4份、防腐剂1份。10 parts of acrylic resin, 6 parts of tetrachloroisophthalonitrile, 5 parts of calcium carbonate, 6 parts of coal tar pitch, 2 parts of sulfonated oil, 3 parts of iron oxide, 4 parts of ammonium metaborate, 8 parts of cellulose acetate, rosin 4 1 part of preservative.
  3. 根据权利要求1所述的一种防锈涂料，其特征在于：由以下质量分数配方成分组成：The rust preventive paint according to claim 1, which is composed of the following mass fraction formula ingredients:
    丙烯酸树脂15份、四氯间苯二腈7份、碳酸钙6份、煤焦沥青7份、磺化油3份、氧化铁4份、偏硼酸铵5份、醋酸纤维素10份、松香5份、防腐剂2份。15 parts of acrylic resin, 7 parts of tetrachloroisophthalonitrile, 6 parts of calcium carbonate, 7 parts of coal tar pitch, 3 parts of sulfonated oil, 4 parts of iron oxide, 5 parts of ammonium metaborate, 10 parts of cellulose acetate, rosin 5 2 parts of preservatives.
  4. 根据权利要求1所述的一种防锈涂料，其特征在于：由以下质量分数配方成分组成：The rust preventive paint according to claim 1, which is composed of the following mass fraction formula ingredients:
    丙烯酸树脂20份、四氯间苯二腈8份、碳酸钙7份、煤焦沥青8份、磺化油4份、氧化铁5份、偏硼酸铵6份、醋酸纤维素12份、松香6份、防腐 剂3份。20 parts of acrylic resin, 8 parts of tetrachloroisophthalonitrile, 7 parts of calcium carbonate, 8 parts of coal tar pitch, 4 parts of sulfonated oil, 5 parts of iron oxide, 6 parts of ammonium metaborate, 12 parts of cellulose acetate, rosin 6 Separation 3 parts.
  5. 根据权利要求1所述的一种防锈涂料及其制备方法，其特征在于：具有以下几个步骤：A rust preventive coating according to claim 1 and a preparation method thereof, comprising the following steps:
    步骤一：将丙烯酸树脂、四氯间苯二腈、碳酸钙、煤焦沥青、磺化油、氧化铁、偏硼酸铵、醋酸纤维素和松香转入反应釜中，升温至50℃～60℃，保温搅拌40分钟～50分钟；Step 1: Transfer acrylic resin, tetrachloroisophthalonitrile, calcium carbonate, coal tar pitch, sulfonated oil, iron oxide, ammonium metaborate, cellulose acetate and rosin into the reaction kettle, and raise the temperature to 50 ° C ~ 60 ° C , heat stirring for 40 minutes to 50 minutes;
    步骤二：加入防腐剂，控制反应釜内温度为室温，保温搅拌20分钟～30分钟后既得一种防锈涂料。 Step 2: adding a preservative, controlling the temperature in the reaction vessel to room temperature, and stirring for 20 minutes to 30 minutes to obtain an anti-rust paint.
PCT/CN2016/098783 2016-09-13 2016-09-13 Antirust paint and preparation method therefor WO2018049548A1 (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4943885A (en) * 1972-09-01 1974-04-25
CN102079890A (en) * 2009-12-01 2011-06-01 周林 Tetrachloroisophthalonitrile antirust paint
CN105602391A (en) * 2016-02-25 2016-05-25 中山诺顿科研技术服务有限公司 Antirust coating

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4943885A (en) * 1972-09-01 1974-04-25
CN102079890A (en) * 2009-12-01 2011-06-01 周林 Tetrachloroisophthalonitrile antirust paint
CN105602391A (en) * 2016-02-25 2016-05-25 中山诺顿科研技术服务有限公司 Antirust coating

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
ZHANG, GUANGHUA: "Technology of Coating Formula", TECHNOLOGY OF FINE CHEMICALS FORMULA, 30 November 1999 (1999-11-30), pages 125, 129, 135 - 136 *

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