WO2017022920A1 - High-viscosity fluid dispersion/emulsification device - Google Patents

High-viscosity fluid dispersion/emulsification device Download PDF

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Publication number
WO2017022920A1
WO2017022920A1 PCT/KR2016/002671 KR2016002671W WO2017022920A1 WO 2017022920 A1 WO2017022920 A1 WO 2017022920A1 KR 2016002671 W KR2016002671 W KR 2016002671W WO 2017022920 A1 WO2017022920 A1 WO 2017022920A1
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WO
WIPO (PCT)
Prior art keywords
rotor
stator
dispersion
housing
dispersion medium
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PCT/KR2016/002671
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French (fr)
Korean (ko)
Inventor
이범섭
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주식회사 케이엔에스컴퍼니
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Publication of WO2017022920A1 publication Critical patent/WO2017022920A1/en

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/50Mixing liquids with solids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/60Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application

Definitions

  • the present invention relates to a high-viscosity fluid dispersion emulsifying apparatus, and in particular, the powder of particle size pre-crushed to a predetermined size is charged into the apparatus without suction by the suction force by the impeller rotation, and the particles are improved by the improved rotor and stator structure.
  • the present invention relates to a high viscosity fluid dispersion emulsifier with an improved structure to be more uniformly dispersed in a liquid to improve work efficiency and quality.
  • Dispersion is a dispersion in which a solid is dispersed in a liquid or a liquid is spread evenly in a liquid and is present in a stable state.
  • an dispersion is an emulsion that causes a liquid to mix with a liquid having an interface. Can be divided.
  • the mixture comprising the liquid or solid dispersion and the liquid dispersion medium was stirred at high speed using a rotary stirring device, and the dispersion was dispersed into the dispersion medium by shear force, so as to generate a dispersion system such as an emulsion (emulsion) or a suspension (suspension).
  • a dispersion system such as an emulsion (emulsion) or a suspension (suspension).
  • emulsion emulsion
  • suspension uspension
  • a surfactant is usually added to promote dispersion of the dispersoid in the dispersion medium or to stabilize the dispersion system.
  • the degree of dispersion of the dispersion in the dispersion medium improves as the amount of surfactant added increases, and the stronger the shearing force applied to the dispersion-based raw material mixture from the stirring apparatus, the better. Therefore, when it is going to realize predetermined
  • the content of the surfactant is small in view of the quality, and the reason is that when the surfactant is used in the production process of the dispersion system, the surfactant is inevitably included in the waste water discharged in the production process.
  • the wastewater containing the surfactant is difficult to be purified, for example, by a conventional wastewater treatment method such as an activated sludge method. Therefore, it is desirable to reduce the amount of surfactant added as much as possible in the production process of the dispersion system.
  • WO 2003/103819 discloses a stirring device having a rotary impeller and a multistage screen member for preventing the generation of vortices, and using the stirring device.
  • a dispersing apparatus such as a homogenizer is disclosed in which the dispersoid is dispersed into a dispersing medium to generate a dispersing system.
  • An object of the present invention was devised to solve the problems of the conventional dispersion emulsifying apparatus, it is possible to inject the fine dispersion of the solid dispersion powder in the liquid dispersion medium by the suction force by the rotational force of the impeller, the reduced surfactant It is to provide a high viscosity dispersion emulsifying apparatus having an improved rotor / stator structure to use and more efficiently to obtain a uniform high viscosity dispersion.
  • the dispersion emulsifying apparatus having a rotor which rotates by a motor, comprising: a first stator fixed inside the housing, a first rotor rotatably disposed inside the first stator, and a housing at the front of the first rotor / stator; And a second rotor rotatably disposed inside the second stator fixed inside, wherein the first rotor and the second rotor discharge the internal fluid by rotation, so that the pressure in the housing is reduced and the dispersoid is generated by the suction force. And a dispersion medium are introduced into the housing directly from each container.
  • the first rotor has a plurality of spokes which are formed at the same height as the rim between the hub and the rim, and the first stator has a plurality of annular bosses and rims connected to the outer circumferential surface of the drive shaft connected to the output shaft of the motor. Spokes, wherein the spokes of the first rotor are inclined to deliver fluid rearward and are configured to break up agglomerates of dispersoid between the spokes and the spokes of the first stator during rotation of the first rotor.
  • the spokes of the first rotor are preferably formed to be inclined 5 to 20 degrees clockwise between the rim and the hub, respectively.
  • the second rotor is integrally provided with a plurality of dispersing wings spaced apart at regular intervals, projecting forward on a disc that extends radially outward from the outer circumferential surface of the boss so as to disperse the dispersoid in the dispersion medium.
  • the dispersing wings are preferably formed to be inclined in the range of 25 ° to 40 ° with respect to the diameter of the boss.
  • the second rotor / stator is disposed in an induction part in which the solid dispersion inlet and the liquid dispersion inlet of the housing are formed, and a first rotor / stator is disposed in a body detachably coupled to the induction part, and the first and second rotors are disposed. They are preferably driven together by a drive shaft connected to the output shaft of the motor.
  • the induction part is provided with a suction rotor disposed in front of the second rotor / stator to increase the suction force to the solid dispersion and the liquid dispersion medium, the suction rotor is connected to the output shaft of the motor is an extension portion formed by extending the rear
  • the drive shaft is adapted to rotate with the first and second rotors.
  • a plurality of dispersing wings integrally spaced apart at regular intervals, protruded forward on a radially outwardly-circuited disk disposed adjacent to the outlet side at the rear of the first rotor / stator and inclined with respect to the diameter are integrally provided.
  • a discharge rotor may be further provided to facilitate discharge of the high viscosity emulsion by centrifugal force.
  • the solid dispersion powder and the liquid dispersion medium which are pulverized by the suction force by the rotational force of the suction rotor and the first rotor are introduced together to prevent the occurrence of the surrounding contamination problem caused by the scattering of the conventional solid dispersion powder, and the solid
  • dispersing the dispersant and the liquid dispersion medium into the chamber at the same time and rotating and dispersing the rotor disposed inside the stator a mechanically homogeneous high viscosity emulsion can be obtained, thereby eliminating the use of surfactants or at least reducing the use of surfactants. It is possible to reduce the occurrence of contamination problems and to improve the quality of the emulsifier, and to perform the dispersing and emulsifying operations more quickly and efficiently.
  • FIG. 1 is a schematic perspective view of a dispersion emulsifying apparatus according to a first embodiment of the present invention.
  • Figure 2 is a schematic exploded perspective view showing the rotor / stator structure installed in the housing of the dispersion emulsification apparatus of Figure 1;
  • FIG. 3 is a perspective view of the assembled state of the first rotor / stator and the second rotor / stator of FIG.
  • FIG. 4 is an exploded perspective view of the first rotor / stator and the second rotor / stator of FIG. 4;
  • FIG. 5 is a schematic cross-sectional view of a state in which a hose is attached to the nipple of the dispersion emulsifying apparatus of FIG.
  • FIG. 6 is a schematic perspective view of the dispersion emulsifying apparatus of the second embodiment of the present invention.
  • FIG. 7 is a schematic exploded perspective view showing a suction rotor and a rotor / stator structure installed in a housing of the dispersion emulsifying apparatus of FIG. 6;
  • FIG. 7 is a schematic exploded perspective view showing a suction rotor and a rotor / stator structure installed in a housing of the dispersion emulsifying apparatus of FIG. 6;
  • FIG. 8 is a perspective view of the suction rotor, the first rotor / stator and the second rotor / stator assembled state.
  • FIG. 9 is an exploded perspective view of the suction rotor, first rotor / stator and second rotor / stator of FIG. 9; FIG.
  • FIG. 10 is a cross-sectional view of the dispersion emulsification apparatus of FIG.
  • FIG. 11 is a perspective view showing a rotor / stator arrangement in which an emulsion discharge rotor is added to the outlet side at the rear of the first rotor / stator of the dispersion emulsifying apparatus of still another embodiment of FIG. 1;
  • FIG. 11 is a perspective view showing a rotor / stator arrangement in which an emulsion discharge rotor is added to the outlet side at the rear of the first rotor / stator of the dispersion emulsifying apparatus of still another embodiment of FIG. 1;
  • the dispersion emulsification apparatus 100 of the present invention is a housing 101, the solid dispersion inlet 103 and the liquid dispersion medium inlet 104 is formed on one side and the mixed fluid outlet 105 is formed on the other side ),
  • the first rotor 120 / stator 130 installed in the housing, the second rotor 220 / stator 230 and the motor 160 for driving the first and second rotor / stators together Include.
  • the housing 101 is a base portion 106 for receiving the drive shaft 162 connected to the output shaft 161 of the motor 160, a mixed fluid that is flange-coupled at the front side of the body and mixed with a solid dispersion and a dispersion medium, that is,
  • the body 107 is formed with a discharge port 105 for discharging the emulsion into the receiving tank, the solid dispersion and the liquid dispersion medium is flanged in front of the body and the solid dispersion inlet 103 and the liquid dispersion medium inlet 104 is formed And an induction part 108 leading to the stator.
  • the second rotor 220 / stator 230 is disposed in the guide portion 108 of the housing, the first rotor 120 / stator 130 is disposed inside the front end of the main body 107 of the housing,
  • the flanges of the induction part 108 and the main body 107 of the housing can be separated so that the first and second rotors / stators can be disassembled and easily cleaned.
  • the first rotor 120 is formed of a plurality of, six spokes 121 in the illustrated embodiment is formed is connected to the hub 122 and the rim 123 is formed at the same height as the rim, the first rotor (
  • the spokes 121 of 120 are inclined at 5 to 20 degrees in the clockwise direction between the rim and the hub, respectively, preferably at 10 degrees.
  • the inclination of the spoke is smaller than 5 °, the load by the dispersoid and dispersion medium during rotation becomes too large, and when it is larger than 20 °, the suction force is reduced.
  • the first stator 130 includes an annular boss 131 and a rim 132 fixed to an outer circumferential surface of the drive shaft connected to the output shaft of the motor, and a plurality of spokes 133 integrally connecting the boss and the rim,
  • the upper and lower heights of the rim 132 are formed to have a height at which the first rotor 120 is disposed inside and the spoke 133 is formed on the lower side thereof.
  • the first rotor 120 is installed such that the spokes 121 are maintained at a distance of 0.1 to 0.3 mm from the spokes 133 of the first stator 130, whereby the first rotor 120 is stator 130. As it rotates inward, the spokes 121 of the first rotor pass through the spokes 133 of the first stator 130 and pulverize the solid dispersion particle mass therebetween so that the solid dispersion is uniformly dispersed in the dispersion medium. do.
  • the shear force is increased, so that the agglomerates of the solid dispersion can be pulverized and uniformly dispersed. This increases and the fluidity of the emulsion is lowered, when the gap is greater than 0.3mm the fluidity of the emulsion is increased, but agglomeration of the solid dispersion can occur.
  • the second rotor 220 / stator 230 is disposed adjacent to the front of the first rotor 120 / stator 130 installed inside the main body 107 so that the solid dispersion is better dispersed in the dispersion medium. It is provided inside the body guide portion 108 of.
  • the second stator 230 is adjacent to the front side of the first stator 130 in the second rotor 220 / stator 230 installed adjacent to the front of the first rotor 120 / stator 130.
  • the second rotor 220 is fixed to the inner wall of the housing, and the second rotor 220 is disposed in the inner space of the second stator 230 so that the boss 225 is fitted into and fixed to the outer circumferential surface of the motor output shaft, thereby fixing the first rotor 120 by the motor 160.
  • the second rotor 220 are rotated inside the respective stators 130 and 230.
  • the second rotor 220 protrudes forward on the disk 223 extended radially outward from the outer circumferential surface of the boss so as to disperse the dispersoid in the dispersion medium and spaced at regular intervals inclined with respect to the diameter.
  • a plurality of dispersing blades 224 are integrally provided, and the second stator 230 has a rim 232 protruding rearward from an outer end of an annular bottom portion 231 having an inner side opening, and the bottom portion ( A plurality of protrusions 233 formed rearwardly from the rear surface of the rear surface 231, that is, adjacent to the outer side of the dispersing blade 224 of the rotor 220, are spaced apart from each other at a predetermined distance from the inner surface of the rim 232. have.
  • the dispersion medium and the dispersoid are dispersed in the eddy state by the second rotor while the dispersoid is uniformly dispersed and emulsified.
  • the dispersing blades 224 are preferably formed to be inclined in the range of 25 ° to 40 ° with respect to the diameter of the boss, when the inclination at an angle smaller than the 25 ° is better dispersibility but the rotational resistance is increased, than 40 ° Larger angles reduce rolling resistance but result in poor dispersion.
  • a suction force is generated to push the fluid backward so that the dispersoid and the dispersion medium flow into the housing.
  • the dispersion emulsifying apparatus of the present invention is suitable for emulsion dispersion and emulsification having a high viscosity, for example, a viscosity of 1,000 ⁇ 5,000cps, for this purpose, the motor 160 is the first rotor 120 and the second rotor 220 ) Rotate at 500rpm ⁇ 3,000rpm to disperse the dispersoid between the first and second rotors and stators with the suction of dispersant and dispersant, and at the same time pulverize the agglomerate of dispersant To be distributed.
  • a high viscosity for example, a viscosity of 1,000 ⁇ 5,000cps
  • the motor 160 is the first rotor 120 and the second rotor 220 ) Rotate at 500rpm ⁇ 3,000rpm to disperse the dispersoid between the first and second rotors and stators with the suction of dispersant and dispersant, and at the same time
  • the rotation speed less than 500rpm is difficult to obtain the required dispersion degree of the solid dispersion in the dispersion medium, and the rotation speed greater than 3,000rpm is too large a burden of the motor load for the rotors to rotate in the high viscosity emulsion
  • the motor rotation speed in the above range is suitable because it is generated.
  • a solid dispersoid inlet 103 formed in the induction part of the housing is provided with a nipple 112 to which a flexible hose 113, which is briefly illustrated in a line, is connected to the liquid dispersion medium inlet.
  • 104 is connected to a dispersion medium reservoir, such as water, via a pipe.
  • Reference numeral 109 which is not described in the drawings, is an inlet for the case of using a plurality of liquid dispersion media, for example.
  • the fluid flow in the housing is moved backward so that the pressure in the housing is lowered, whereby the dispersoid and the dispersion medium which are pulverized in nano units are stored in the respective storage containers. Flows into the housing 101 from.
  • the solid dispersion is introduced into the housing by the pressure difference between the pressure in the housing and the atmospheric pressure in the reservoir by entering the dispersal reservoir through a hose connected to the solid dispersion inlet 103, thereby a solid dispersion in nano units. It flows into the housing 101 quickly without being scattered in this workshop.
  • the solid dispersion introduced into the housing 101 through the solid dispersion inlet 103 is formed by dispersing medium introduced into the housing from the liquid dispersion medium inlet 104 through a pipe connected to the dispersion medium storage container 170.
  • the rotors 120 and 220 are mixed and dispersed by the stators 130 and 230, and in particular, agglomerates in which solid dispersions of fine particles in nano units are agglomerated by a shear action between the first rotor 120 and the stator 130. To break.
  • the dispersion medium storage container 170 contains a dispersion medium such as water or a liquid emulsifier for emulsification by being mixed with a solid dispersion, mixed with a solid dispersion in a dispersion emulsifier to be uniformly dispersed, and then a dispersion medium storage container from the dispersion emulsion device. Is discharged. This dispersion emulsification process can be repeated several times as necessary.
  • a dispersion medium such as water or a liquid emulsifier for emulsification by being mixed with a solid dispersion, mixed with a solid dispersion in a dispersion emulsifier to be uniformly dispersed, and then a dispersion medium storage container from the dispersion emulsion device. Is discharged. This dispersion emulsification process can be repeated several times as necessary.
  • the solid dispersion inlet 103 of the housing is provided with a nipple and a flexible hose is connected, and the liquid dispersion medium inlet 104 is connected to a dispersion medium reservoir 170 such as water through a pipe.
  • the air flow in the housing is moved backwards so that the pressure in the housing is lowered, whereby the dispersoid and the dispersion medium, which are pulverized in nano units, are separated from each reservoir. It is introduced into and dispersed and emulsified, and the emulsion is discharged into the dispersion medium storage container and then flowed back into the emulsifying apparatus, whereby dispersion and emulsification are performed to the required extent by repeatedly performing the dispersion and emulsification process.
  • the solid dispersion is introduced directly into the housing by a pressure difference between the pressure in the housing and the atmospheric pressure in the storage container through a hose connected to the solid dispersion inlet 103, thereby providing a solid dispersion in nano units. It enters the housing quickly without being scattered in the workshop.
  • the spokes 121 of the first rotor pass through the spokes 133 of the first stator 130 by the rotation of the first rotor 120 disposed at the rear, and the solid dispersion particles therebetween are collected. Further grinding results in an emulsion in which the solid dispersion is more uniformly dispersed in the dispersion medium.
  • the emulsion dispersed in this way is discharged into the dispersion medium storage container 170 and then introduced into the emulsifying apparatus again through the inlet, for example, to undergo a dispersion emulsification process several times repeatedly, so that the emulsion having the required degree of dispersibility is Obtained.
  • FIG. 6 to 10 show an emulsifying apparatus according to another embodiment of the present invention, wherein the suction rotor 110 is provided in the induction part 108 of the housing 101 to promote the inflow of the solid dispersion and the liquid dispersion medium.
  • the suction rotor 110 is fastened by bolts to the drive shaft 162 connected to the output shaft 161 of the motor 160 is the extension portion 115 extending rearward hub.
  • the second stator 230 is fixed inside the rear end of the induction part 108 of the housing, and the second rotor 220 is rotatably disposed inside the second stator 230.
  • the first stator 130 is fixed inside the front end of the housing body 106 flanged to the induction part 108 and the first rotor 120 is rotatably disposed inside the first stator 130.
  • suction rotor 110 and the first and second rotors 120 and 220 are fitted into and fixed to the outer circumferential surface of the end of the drive shaft 162 connected to the output shaft of the motor, thereby being driven by the motor 160 and the first and second rotors. 120 and 130 are rotated together.
  • the suction rotor 110 has a plurality of hubs 111, in the illustrated embodiment, four spokes 114 are formed at the same height as the overall height of the rim 116, and the first rotor 120 is also connected. In the illustrated embodiment, six spokes 121 are formed at the same height as the rim between the hub 122 and the rim 123.
  • the first and second rotor and stator structures are the same as in the first embodiment described above.
  • the spokes 112 and 121 of the suction rotor 110 and the first rotor 120 are formed to be inclined at 5 to 20 degrees in the clockwise direction between the rim and the hub, and are preferably formed to be inclined at 10 degrees. If the inclination of the spoke is less than 5 °, the load at the time of rotation becomes too large, and if it is larger than 20 °, the suction force is reduced.
  • the suction rotor 110 by arranging the suction rotor 110 in front of the second rotor 220, the first and second rotors 120 and 220 and the suction rotor 110 cooperate with each other to increase the emulsion of high viscosity with the increased suction force.
  • the fluidity in the process of dispersion emulsification by the suction force by the first and second rotors is improved to enable a smooth flow of the high viscosity emulsion, so that a high quality high viscosity emulsion can be obtained quickly.
  • FIG. 11 illustrates a structure in which a discharging rotor 220 'is further disposed adjacent to the outlet side at the rear of the first stator 130 for the dispersion emulsifying apparatus of still another embodiment of FIG.
  • the discharge rotor 220 ′ may have a structure in which a plurality of dispersing wings are provided on a disc, similarly to the second rotor 220 having a plurality of dispersing wings 224 on a disc 223. And spaced rearward from the first rotor / stator (120/130) and adjacent the outlet.
  • the discharge rotor 220 is easily discharged by applying a centrifugal force to the high viscosity emulsion dispersed and emulsified through the first and second rotors / stators, and the dispersibility is improved. This, in turn, increases the flow rate of the emulsion and thus the rate of introduction of the dispersion and the dispersion medium can also be increased.
  • the present invention can be used to obtain a high viscosity emulsion by uniformly dispersing and emulsifying the solid dispersion and the liquid dispersion medium.
  • induction unit 110 suction rotor
  • Rim 120 First rotor
  • Boss 132 Rim
  • spoke 220 second rotor

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Abstract

The present invention relates to a high-viscosity fluid dispersion/emulsification device comprising a housing, which has a solid dispersoid inlet and a liquid dispersion medium inlet formed on one side thereof and a mixed fluid outlet formed on the other side thereof, a stator, which is installed inside the housing, and a rotor, which is arranged therein and rotated by a motor, the high-viscosity fluid dispersion/emulsification device comprising: a first stator (130) fixed inside the housing; a first rotor (120) arranged to be able to rotate inside the first stator; and a second rotor (220) arranged to be able to rotate inside a second stator (230), which is fixed inside the housing in front of the first rotor (120)/stator (130), wherein the first rotor (120) and the second rotor (220) are configured such that the inner fluid is discharged by rotation, and the resulting pressure drop inside the housing generates a suction force, which introduces the dispersoid and the dispersion medium directly into the housing from respective containers. The present invention is advantageous in that the suction force, which results from rotational forces of the suction rotor and the first rotor, introduces unpulverized solid dispersoid powder and a liquid dispersion medium together, thereby preventing the problem of contamination of surroundings resulting from scattering of solid dispersoid powder. Furthermore, the solid dispersoid and the liquid dispersion medium are simultaneously suctioned into the chamber and, by rotating the rotor that is arranged inside the stator, are dispersed and discharged, making it possible to obtain a high-viscosity emulsion, which is mechanically homogeneous, quickly and efficiently. In addition, a reduced amount of surfactant is used, thereby lowering occurrences of environment contamination problems and improving the quality of the emulsifier.

Description

고점도 유체 분산유화장치High Viscosity Fluid Dispersing Emulsifier
본 발명은 고점도 유체 분산유화장치에 관한 것으로, 특히 소정 크기로 미리 분쇄된 입자 크기의 분말을 임펠러 회전에 의한 흡인력으로 주변을 오염시키지 않고 장치에 장입하고, 개선된 로터와 스테이터 구조로 입자를 보다 더 미분화하면서 액체 속에 균일하게 분산하여 작업효율과 품질을 향상시키도록 개선된 구조의 고점도 유체 분산유화장치에 관한 것이다.The present invention relates to a high-viscosity fluid dispersion emulsifying apparatus, and in particular, the powder of particle size pre-crushed to a predetermined size is charged into the apparatus without suction by the suction force by the impeller rotation, and the particles are improved by the improved rotor and stator structure. The present invention relates to a high viscosity fluid dispersion emulsifier with an improved structure to be more uniformly dispersed in a liquid to improve work efficiency and quality.
최근 기초 소재산업은 있어서 식품, 화장품, 잉크, 페인트, 접착제, 코팅제, 정밀화학 및 나노 신소재와 첨단 전자재료에 이르기까지 입자의 분산과 유화 등 세밀성과 균일성이 완제품의 품질에 영향을 미치는 중요한 공정으로 이를 위해 다양한 방식의 분산과 유화장치가 개발되어 사용되고 있다.In recent years, the basic material industry is an important process in which fineness and uniformity, such as dispersion and emulsification of particles, from food, cosmetics, ink, paint, adhesives, coatings, fine chemicals, and nano-materials to advanced electronic materials, affect the quality of finished products. To this end, various methods of dispersing and emulsifying devices have been developed and used.
분산은 고체가 액체에 또는 액체가 액체에 균일하게 퍼져 안정된 상태로 존재하는 것으로, 대상에 따라 고체를 액체에 분산시키는 분산 (suspension)과 계면이 존재하는 액체와 액체를 섞이게 만드는 유화(emulsion)로 나눌 수 있다.Dispersion is a dispersion in which a solid is dispersed in a liquid or a liquid is spread evenly in a liquid and is present in a stable state. According to an object, an dispersion is an emulsion that causes a liquid to mix with a liquid having an interface. Can be divided.
액체 또는 고체 분산질과 액체 분산매를 포함하는 혼합물을 회전식 교반장치를 사용하여 고속회전 교반하고, 전단력에 의해 분산질을 분산매 안으로 분산시켜, 에멀젼(유화액)이나 서스펜션(현탁액) 등의 분산계를 생성하도록 한 분산유화장치가 널리 알려져 있다. The mixture comprising the liquid or solid dispersion and the liquid dispersion medium was stirred at high speed using a rotary stirring device, and the dispersion was dispersed into the dispersion medium by shear force, so as to generate a dispersion system such as an emulsion (emulsion) or a suspension (suspension). One dispersion emulsifier is widely known.
그리고, 이러한 분산계의 생성 프로세스에 있어서는, 보통 분산매 안에서 분산질의 분산을 촉진시키거나, 분산계를 안정시키기 위하여 계면활성제가 첨가된다.또한, 이러한 분산계의 생성 프로세스에 있어서, 분산질의 분산매 안에서의 분산도(분산성)는, 계면활성제의 첨가량이 많을수록 좋아지며, 교반장치로부터 분산계 원료혼합물에 가해지는 전단력이 강할수록 좋아진다. 따라서, 소정의 분산도를 실현하려고 하는 경우, 계면활성제의 첨가량이 많을수록 전단력이 약해도 되지만, 계면활성제의 첨가량이 적을수록 강한 전단력이 필요하게 된다. 그런데, 일반적으로 분산계에서는, 그 품질의 관점에서 계면활성제의 함유량은 적은 것이 바람직하며, 그 이유는 분산계의 생성 프로세스에서 계면활성제를 사용한 경우, 상기 생성 프로세스에서 배출되는 폐수 등에는 필연적으로 계면활성제가 포함되게 되는데, 계면활성제를 포함하는 폐수는 예를 들어, 활성오니법 등의 보통의 폐수처리 방법으로는 정화하기 어렵다. 따라서, 분산계의 생성 프로세스에서는 계면활성제의 첨가량을 가능한 한 줄이는 것이 바람직하다.In the production process of such a dispersion system, a surfactant is usually added to promote dispersion of the dispersoid in the dispersion medium or to stabilize the dispersion system. In addition, in the production process of the dispersion system, the degree of dispersion of the dispersion in the dispersion medium ( Dispersibility) improves as the amount of surfactant added increases, and the stronger the shearing force applied to the dispersion-based raw material mixture from the stirring apparatus, the better. Therefore, when it is going to realize predetermined | prescribed dispersion degree, although the shearing force may become weak, so that the addition amount of surfactant is large, the strong shear force is needed, so that the addition amount of surfactant is small. By the way, in general, in the dispersion system, it is preferable that the content of the surfactant is small in view of the quality, and the reason is that when the surfactant is used in the production process of the dispersion system, the surfactant is inevitably included in the waste water discharged in the production process. The wastewater containing the surfactant is difficult to be purified, for example, by a conventional wastewater treatment method such as an activated sludge method. Therefore, it is desirable to reduce the amount of surfactant added as much as possible in the production process of the dispersion system.
이를 위한 분산유화장치의 예로서, 국제공개공보 WO 2003/103819 (2003.12.18. 국제공개)에는 회전식 임펠러 및 와류의 발생을 방지하는 다단식 스크린 부재를 구비한 교반장치와, 상기 교반장치를 사용하여 분산질을 분산매 안으로 분산시켜 분산계(分散系)를 생성하도록 한 호모게나이저 등의 분산장치가 개시되어 있다.As an example of a dispersing emulsion apparatus for this purpose, WO 2003/103819 (December 18, 2003) discloses a stirring device having a rotary impeller and a multistage screen member for preventing the generation of vortices, and using the stirring device. A dispersing apparatus such as a homogenizer is disclosed in which the dispersoid is dispersed into a dispersing medium to generate a dispersing system.
그러나, 이러한 종래 분산유화장치에서는 미분쇄된 분말상의 고체 분산질을 액체 분산매가 수용된 용기에 장입할 때 분말이 비산하여 주변을 오염시키는 문제가 있었고, 분산매에 고체 분산질을 투입한 다음 교반하는 경우에는 고체 분산질의 응집에 의해 균일한 분산액을 얻기까지 작업 시간이 많이 소요되어 보다 효율적이고 균질한 분산상을 얻을 수 있는 분산유화장치가 필요하였다.However, in such a conventional dispersion emulsifier, when the powdered solid dispersion is pulverized into a container containing a liquid dispersion medium, the powder is scattered to contaminate the surroundings, and when the solid dispersion is added to the dispersion medium and then stirred. In order to obtain a uniform dispersion by agglomeration of a solid dispersion, it takes a long time to obtain a dispersion emulsification apparatus that can obtain a more efficient and homogeneous dispersed phase.
또한, 에멀젼이 고점도인 경우에는 로터의 회전 속도가 크게 저하되고 분산질의 분산 및 유화가 원활하지 못하여 작업 시간이 많이 소요되고, 고품질의 에멀젼을 얻기 어려운 점이 있었다.In addition, when the emulsion has a high viscosity, the rotational speed of the rotor is greatly reduced, dispersion and emulsification of dispersoids are not smooth, and a lot of work time is required, and it is difficult to obtain a high quality emulsion.
[선행기술문헌][Preceding technical literature]
[특허문헌][Patent Documents]
국제공개공보 WO 2003/103819 (2003.12.18. 국제공개)International publication WO 2003/103819 (2003.12.18. International publication)
본 발명의 목적은 종래의 분산유화장치에 대한 문제점을 해결하기 위하여 창안된 것으로, 임펠러의 회전력에 의한 흡인력으로 미분쇄된 고체 분산질 분말을 액체 분산매에 투입할 수 있으며, 감소된 계면활정제를 사용하고 보다 효율적으로 균일한 고점도의 분산액을 얻을 수 있도록 개선된 회전자/고정자 구조를 갖는 고점도용 분산유화장치를 제공하는 것이다.An object of the present invention was devised to solve the problems of the conventional dispersion emulsifying apparatus, it is possible to inject the fine dispersion of the solid dispersion powder in the liquid dispersion medium by the suction force by the rotational force of the impeller, the reduced surfactant It is to provide a high viscosity dispersion emulsifying apparatus having an improved rotor / stator structure to use and more efficiently to obtain a uniform high viscosity dispersion.
상기한 목적을 달성하기 위하여, 본 발명에 따른 분산유화장치는, 고체 분산질 유입구와 액체 분산매 유입구가 일측에 형성되고 타측에는 혼합 유체 배출구가 형성된 하우징과, 그 하우징 속에 설치된 스테이터와 그 내측에 배치되어 모터로 회전하는 로터를 구비한 고점도 유체 분산유화장치에 있어서, 하우징 내측에 고정된 제 1 스테이터와, 제 1 스테이터 내측에서 회전가능하게 배치된 제 1 로터, 상기 제 1로터/스테이터 전측에서 하우징 내측에 고정된 제 2 스테이터 내측에서 회전가능하게 배치된 제 2 로터를 포함하며, 상기 제 1 로터와 제 2 로터는 회전에 의해 내부 유체를 배출시켜 하우징 내의 압력이 저하되어 발생되는 흡인력으로 분산질과 분산매를 각각의 용기로 부터 직접 하우징내로 유입시키도록 된 것을 특징으로 하여 구성된다.In order to achieve the above object, the dispersion emulsifying apparatus according to the present invention, the solid dispersion inlet and the liquid dispersion medium inlet is formed on one side and the mixed fluid outlet is formed on the other side, the stator installed in the housing and disposed inside A high viscosity fluid dispersion emulsifying apparatus having a rotor which rotates by a motor, comprising: a first stator fixed inside the housing, a first rotor rotatably disposed inside the first stator, and a housing at the front of the first rotor / stator; And a second rotor rotatably disposed inside the second stator fixed inside, wherein the first rotor and the second rotor discharge the internal fluid by rotation, so that the pressure in the housing is reduced and the dispersoid is generated by the suction force. And a dispersion medium are introduced into the housing directly from each container.
상기 제 1 로터는 허브와 림 사이에서 림과 같은 높이로 형성되어 연결된 복수개의 스포크를 구비하고, 상기 제 1 스테이터는 모터의 출력축과 연결된 구동축 외주면에 고정되는 환형으로 된 보스와 림을 연결하는 복수개의 스포크를 포함하며, 상기 제 1 로터의 스포크는 유체를 후방으로 송출하도록 경사져 있으며, 상기 제 1 로터 회전시 그 스포크와 제 1 스테이터의 스포크 사이에서 분산질의 뭉침을 분쇄하도록 구성된다.The first rotor has a plurality of spokes which are formed at the same height as the rim between the hub and the rim, and the first stator has a plurality of annular bosses and rims connected to the outer circumferential surface of the drive shaft connected to the output shaft of the motor. Spokes, wherein the spokes of the first rotor are inclined to deliver fluid rearward and are configured to break up agglomerates of dispersoid between the spokes and the spokes of the first stator during rotation of the first rotor.
상기 제 1 로터의 스포크들은 각각 림과 허브 사이에서 시계방향으로 5~20°로 경사지게 형성되는 것이 바람직하다.The spokes of the first rotor are preferably formed to be inclined 5 to 20 degrees clockwise between the rim and the hub, respectively.
상기 제 2 로터는 분산질을 분산매에서 분산시키도록 보스의 외주면에서 반경방향 외측으로 확장된 원판상에서 전방으로 돌출되고 직경에 대하여 경사지게 일정 간격으로 이격된 다수의 분산날개들을 일체로 구비한다.The second rotor is integrally provided with a plurality of dispersing wings spaced apart at regular intervals, projecting forward on a disc that extends radially outward from the outer circumferential surface of the boss so as to disperse the dispersoid in the dispersion medium.
상기 분산날개들은 보스의 직경에 대하여 25°~40°범위에서 경사지게 형성되는 것이 바람직하다.The dispersing wings are preferably formed to be inclined in the range of 25 ° to 40 ° with respect to the diameter of the boss.
상기 하우징의 고체 분산질 유입구와 액체 분산매 유입구가 형성된 유도부에 상기 제 2 로터/스테이터가 배치되고, 상기 유도부와 분리가능하게 결합된 본체에 제 1 로터/스테이터가 배치되며, 상기 제 1 및 2 로터들은 모터의 출력축에 연결된 구동축에 의해 함께 구동되는 것이 바람직하다.The second rotor / stator is disposed in an induction part in which the solid dispersion inlet and the liquid dispersion inlet of the housing are formed, and a first rotor / stator is disposed in a body detachably coupled to the induction part, and the first and second rotors are disposed. They are preferably driven together by a drive shaft connected to the output shaft of the motor.
상기 유도부에는 고체 분산질과 액체 분산매에 대한 흡인력을 증가시키도록 제 2로터/스테이터 앞쪽에 배치되는 흡입로터가 제공되며, 상기 흡입로터는 허브가 후방으로 연장되어 형성되는 연장부가 모터의 출력축에 연결된 구동축에 의해 제 1 및 2 로터들과 함께 회전하도록 되는 것이 바람직하다.The induction part is provided with a suction rotor disposed in front of the second rotor / stator to increase the suction force to the solid dispersion and the liquid dispersion medium, the suction rotor is connected to the output shaft of the motor is an extension portion formed by extending the rear Preferably, the drive shaft is adapted to rotate with the first and second rotors.
또 다른 실시예로서, 제 1 로터/스테이터 후방에서 배출구측에 인접하여 배치되고 반경방향 외측으로 확장된 원판상에서 전방으로 돌출되고 직경에 대하여 경사지게 일정 간격으로 이격된 다수의 분산날개들을 일체로 구비한 배출용 로터를 추가로 구비하여 원심력에 의해 고점도 에멀젼이 용이하게 배출되도록 할 수도 있다.In another embodiment, a plurality of dispersing wings integrally spaced apart at regular intervals, protruded forward on a radially outwardly-circuited disk disposed adjacent to the outlet side at the rear of the first rotor / stator and inclined with respect to the diameter are integrally provided. A discharge rotor may be further provided to facilitate discharge of the high viscosity emulsion by centrifugal force.
본 발명에 따라 흡입 로터와 제 1 로터의 회전력에 의한 흡인력으로 미분쇄된 고체 분산질 분말과 액체 분산매를 함께 유입시켜 종래 고체 분산질 분말의 비산에 따른 주변 오염 문제 발생을 방지하는 효과와, 고체 분산질과 액체 분산매를 동시에 챔버내로 흡입하여 고정자 내측에 배치된 로터를 회전시켜 분산시켜 토출함으로써 기계적으로 균질한 고점도의 에멀젼을 얻을 수 있어 계면활성제를 사용하지 않거나 적어도 계면활성제의 사용을 감소하여 환경오염의 문제 발생을 낮추고 유화제의 품질 향상을 꾀할 수 있고, 분산 및 유화 작업을 보다 신속하고 효율적으로 수행할 수 있는 효과가 있다.In accordance with the present invention, the solid dispersion powder and the liquid dispersion medium which are pulverized by the suction force by the rotational force of the suction rotor and the first rotor are introduced together to prevent the occurrence of the surrounding contamination problem caused by the scattering of the conventional solid dispersion powder, and the solid By dispersing the dispersant and the liquid dispersion medium into the chamber at the same time and rotating and dispersing the rotor disposed inside the stator, a mechanically homogeneous high viscosity emulsion can be obtained, thereby eliminating the use of surfactants or at least reducing the use of surfactants. It is possible to reduce the occurrence of contamination problems and to improve the quality of the emulsifier, and to perform the dispersing and emulsifying operations more quickly and efficiently.
도 1은 본 발명의 제 1 실시예에 의한 분산유화장치의 개략적인 사시도.1 is a schematic perspective view of a dispersion emulsifying apparatus according to a first embodiment of the present invention.
도 2는 도 1의 분산유화장치의 하우징내에 설치된 로터/스테이터 구조를 보여주는 개략적인 분해사시도.Figure 2 is a schematic exploded perspective view showing the rotor / stator structure installed in the housing of the dispersion emulsification apparatus of Figure 1;
도 3은 도 2의 제 1 로터/스테이터와 제 2 로터/스테이터의 조립상태의 사시도.3 is a perspective view of the assembled state of the first rotor / stator and the second rotor / stator of FIG.
도 4는 도 4의 제 1 로터/스테이터와 제 2 로터/스테이터의 분해사시도.4 is an exploded perspective view of the first rotor / stator and the second rotor / stator of FIG. 4;
도 5는 도 1의 분산유화장치의 니플에 호스가 부착된 상태의 개략적인 단면도.5 is a schematic cross-sectional view of a state in which a hose is attached to the nipple of the dispersion emulsifying apparatus of FIG.
도 6은 본 발명의 제 2 실시예의 분산유화장치의 개략적인 사시도.6 is a schematic perspective view of the dispersion emulsifying apparatus of the second embodiment of the present invention.
도 7은 도 6의 분산유화장치의 하우징내에 설치된 흡입로터와 로터/스테이터 구조를 보여주는 개략적인 분해사시도.FIG. 7 is a schematic exploded perspective view showing a suction rotor and a rotor / stator structure installed in a housing of the dispersion emulsifying apparatus of FIG. 6; FIG.
도 8은 흡입로터와 제 1 로터/스테이터와 제 2 로터/스테이터들이 조립된 상태의 사시도.8 is a perspective view of the suction rotor, the first rotor / stator and the second rotor / stator assembled state.
도 9는 도 9의 흡입로터와 제 1 로터/스테이터와 제 2 로터/스테이터의 분해사시도.FIG. 9 is an exploded perspective view of the suction rotor, first rotor / stator and second rotor / stator of FIG. 9; FIG.
도 10은 도 6의 분산유화장치의 단면도.10 is a cross-sectional view of the dispersion emulsification apparatus of FIG.
도 11은 도 1의 또 다른 실시예의 분산유화장치의 제 1 로터/스테이터 후방에서 배출구측에 에멀젼의 배출용 로터를 추가한 로터/스테이터 배열 구조를 보여주는 사시도. FIG. 11 is a perspective view showing a rotor / stator arrangement in which an emulsion discharge rotor is added to the outlet side at the rear of the first rotor / stator of the dispersion emulsifying apparatus of still another embodiment of FIG. 1; FIG.
이하에서는 본 발명에 의한 분산유화장치의 일 실시예를 도시한 첨부 도면을 참조하여 본 발명을 보다 상세히 설명하기로 한다.Hereinafter, with reference to the accompanying drawings showing an embodiment of the dispersion emulsifying apparatus according to the present invention will be described in detail the present invention.
도 1 내지 4에 있어서, 본 발명의 분산유화장치(100)는 고체 분산질 유입구(103)와 액체 분산매 유입구(104)가 일측에 각각 형성되고 타측에는 혼합 유체 배출구(105)가 형성된 하우징(101)과, 그 하우징 속에 설치된 제 1 로터(120)/스테이터(130)와, 제 2 로터(220)/스테이터(230) 및 상기 제 1 및 제 2 로터/스테이터 들을 함께 구동하는 모터(160)를 포함한다. 1 to 4, the dispersion emulsification apparatus 100 of the present invention is a housing 101, the solid dispersion inlet 103 and the liquid dispersion medium inlet 104 is formed on one side and the mixed fluid outlet 105 is formed on the other side ), The first rotor 120 / stator 130 installed in the housing, the second rotor 220 / stator 230 and the motor 160 for driving the first and second rotor / stators together Include.
상기 하우징(101)은 모터(160)의 출력축(161)과 연결된 구동축(162)을 수용하는 베이스부(106), 그 바디의 전측에서 플랜지 결합되며 고체 분산질과 분산매가 혼합된 혼합 유체, 즉 에멀젼을 수용탱크로 배출하기 위한 배출구(105)가 형성된 본체(107), 상기 본체 앞쪽에서 플랜지 결합되며 고체 분산질 유입구(103)와 액체 분산매 유입구(104)가 형성된 고체 분산질과 액체 분산매들을 로터/스테이터로 유도하는 유도부(108)를 포함하여 구성된다.The housing 101 is a base portion 106 for receiving the drive shaft 162 connected to the output shaft 161 of the motor 160, a mixed fluid that is flange-coupled at the front side of the body and mixed with a solid dispersion and a dispersion medium, that is, The body 107 is formed with a discharge port 105 for discharging the emulsion into the receiving tank, the solid dispersion and the liquid dispersion medium is flanged in front of the body and the solid dispersion inlet 103 and the liquid dispersion medium inlet 104 is formed And an induction part 108 leading to the stator.
상기 제 2 로터(220)/스테이터(230)는 상기 하우징의 유도부(108)에 배치되고, 제 1 로터(120)/스테이터(130)는 하우징의 본체(107)의 전단부 내측에 배치됨으로써, 상기 하우징의 유도부(108)와 본체(107)의 플랜지를 분리시켜 제 1 및 2 로터/스테이터들을 분해하여 쉽게 세척할 수 있게 된다.The second rotor 220 / stator 230 is disposed in the guide portion 108 of the housing, the first rotor 120 / stator 130 is disposed inside the front end of the main body 107 of the housing, The flanges of the induction part 108 and the main body 107 of the housing can be separated so that the first and second rotors / stators can be disassembled and easily cleaned.
상기 제 1 로터(120)는 복수개, 도시된 실시예에서 6개의 스포크(121)가 허브(122)와 림(123) 사이에서 림과 같은 높이로 형성되어 연결되어 구성되며, 상기 제 1 로터(120)의 스포크(121)들은 각각 림과 허브 사이에서 시계방향으로 5~20°로 경사지게 형성되며, 바람직하게는 10°로 경사지게 형성된다. 상기 스포크의 경사가 5°보다 작으면 회전시의 분산질과 분산매에 의한 부하가 지나치게 커지고, 20°보다 크면 흡인력이 감소된다.The first rotor 120 is formed of a plurality of, six spokes 121 in the illustrated embodiment is formed is connected to the hub 122 and the rim 123 is formed at the same height as the rim, the first rotor ( The spokes 121 of 120 are inclined at 5 to 20 degrees in the clockwise direction between the rim and the hub, respectively, preferably at 10 degrees. When the inclination of the spoke is smaller than 5 °, the load by the dispersoid and dispersion medium during rotation becomes too large, and when it is larger than 20 °, the suction force is reduced.
상기 제 1 스테이터(130)는 모터의 출력축과 연결된 구동축 외주면에 고정되는 환형으로 된 보스(131)와 림(132) 및 상기 보스와 림을 일체로 연결하는 복수개의 스포크(133)를 포함하며, 상기 림(132)의 상하 높이는 그 내측에 제 1 로터(120)가 배치되고, 그 하측에 상기 스포크(133)가 형성되는 높이를 갖게 형성된다.The first stator 130 includes an annular boss 131 and a rim 132 fixed to an outer circumferential surface of the drive shaft connected to the output shaft of the motor, and a plurality of spokes 133 integrally connecting the boss and the rim, The upper and lower heights of the rim 132 are formed to have a height at which the first rotor 120 is disposed inside and the spoke 133 is formed on the lower side thereof.
상기 제 1 로터(120)는 그 스포크(121)가 제 1 스테이터(130)의 스포크(133)와 0.1~0.3mm의 간격이 유지되도록 설치되며, 이로써 제 1 로터(120)가 스테이터(130) 내측에서 회전함에 따라 제 1 로터의 스포크(121)가 제 1 스테이터(130)의 스포크(133)를 스쳐 지나면서 그 사이의 고체 분산질 입자 덩어리들을 분쇄하여 고체분산질이 분산매에 균일하게 분산되게 한다.The first rotor 120 is installed such that the spokes 121 are maintained at a distance of 0.1 to 0.3 mm from the spokes 133 of the first stator 130, whereby the first rotor 120 is stator 130. As it rotates inward, the spokes 121 of the first rotor pass through the spokes 133 of the first stator 130 and pulverize the solid dispersion particle mass therebetween so that the solid dispersion is uniformly dispersed in the dispersion medium. do.
상기 제 1 로터의 스포크(121)와 제 1 스테이터(130)의 스포크(133) 사이의 간격이 작을수록 전단력이 커져 고체 분산질의 뭉침을 분쇄하여 균일하게 분산시킬 수 있으나, 0.1mm 보다 작으면 저항이 커지고 에멀젼의 유동성이 저하되고, 간격이 0.3mm 보다 크면 에멀젼의 유동성은 증가되지만 고체 분산질의 뭉침 현상이 발생될 수 있게 된다.As the spacing between the spokes 121 of the first rotor and the spokes 133 of the first stator 130 is smaller, the shear force is increased, so that the agglomerates of the solid dispersion can be pulverized and uniformly dispersed. This increases and the fluidity of the emulsion is lowered, when the gap is greater than 0.3mm the fluidity of the emulsion is increased, but agglomeration of the solid dispersion can occur.
고체 분산질이 분산매에 보다 더 잘 분산되도록 하기 위하여 상기 본체(107) 내부에 설치된 제 1 로터(120)/스테이터(130)의 앞쪽에 인접하여 제 2 로터(220)/스테이터(230)가 하우징의 본체 유도부(108) 내측에 제공된다.The second rotor 220 / stator 230 is disposed adjacent to the front of the first rotor 120 / stator 130 installed inside the main body 107 so that the solid dispersion is better dispersed in the dispersion medium. It is provided inside the body guide portion 108 of.
상기 제 1 로터(120)/스테이터(130) 앞쪽에 인접하여 설치되는 제 2 로터(220)/스테이터(230)에서 상기 제 2 스테이터(230)는 상기 제 1 스테이터(130)의 전측에 인접하여 하우징 내벽에 고정되고, 상기 제 2 스테이터(230) 내측 공간에 제 2 로터(220)가 배치되어 모터 출력축 외주면에 보스(225)가 끼워져 고정됨으로써 모터(160)에 의해 상기 제 1 로터(120)와 제 2 로터(220)가 각각의 스테이터(130)(230)들 내측에서 회전된다. The second stator 230 is adjacent to the front side of the first stator 130 in the second rotor 220 / stator 230 installed adjacent to the front of the first rotor 120 / stator 130. The second rotor 220 is fixed to the inner wall of the housing, and the second rotor 220 is disposed in the inner space of the second stator 230 so that the boss 225 is fitted into and fixed to the outer circumferential surface of the motor output shaft, thereby fixing the first rotor 120 by the motor 160. And the second rotor 220 are rotated inside the respective stators 130 and 230.
상기 제 2 로터(220)는 제 2 로터(220)는 분산질을 분산매에서 분산시키도록 보스의 외주면에서 반경방향 외측으로 확장된 원판(223)상에서 전방으로 돌출되고 직경에 대하여 경사지게 일정 간격으로 이격된 다수의 분산날개(224)들을 일체로 구비하며, 상기 제 2 스테이터(230)는 내측이 개구된 환형의 바닥부(231) 외측단부에 림(232)이 후방으로 돌출되고, 그 바닥부(231)의 후방측 표면에서 후방으로, 즉 로터(220)의 분산날개(224)의 외측에 인접하여 서로 일정 간격 이격되어 형성된 다수의 돌출부(233)이 림(232) 내측면에서 이격되어 형성되어 있다. 이로써, 제 2로터에 의해 분산매와 분산질은 와류 상태로 후방으로 유동하면서 분산질이 균일하게 분산되어 유화된다.The second rotor 220 protrudes forward on the disk 223 extended radially outward from the outer circumferential surface of the boss so as to disperse the dispersoid in the dispersion medium and spaced at regular intervals inclined with respect to the diameter. A plurality of dispersing blades 224 are integrally provided, and the second stator 230 has a rim 232 protruding rearward from an outer end of an annular bottom portion 231 having an inner side opening, and the bottom portion ( A plurality of protrusions 233 formed rearwardly from the rear surface of the rear surface 231, that is, adjacent to the outer side of the dispersing blade 224 of the rotor 220, are spaced apart from each other at a predetermined distance from the inner surface of the rim 232. have. As a result, the dispersion medium and the dispersoid are dispersed in the eddy state by the second rotor while the dispersoid is uniformly dispersed and emulsified.
상기 분산날개(224)들은 보스의 직경에 대하여 25°~40°범위에서 경사지게 형성되는 것이 바람직하며, 상기 25°보다 작은 각도로 경사지는 경우 분산성은 더 좋게 되지만 회전 저항이 증가되고, 40° 보다 큰 각도는 회전 저항이 감소되지만 분산성이 좋지 않게 된다. 또한, 제 2로터(220)의 회전에 의해서도 유체를 후방으로 밀어 분산질과 분산매가 하우징내로 유입되게 하는 흡인력이 발생된다.The dispersing blades 224 are preferably formed to be inclined in the range of 25 ° to 40 ° with respect to the diameter of the boss, when the inclination at an angle smaller than the 25 ° is better dispersibility but the rotational resistance is increased, than 40 ° Larger angles reduce rolling resistance but result in poor dispersion. In addition, by the rotation of the second rotor 220, a suction force is generated to push the fluid backward so that the dispersoid and the dispersion medium flow into the housing.
상기한 본 발명의 분산유화장치는 고점도 예를들어 1,000~5,000cps의 점도를 갖는 에멀젼 분산 및 유화에 적합하며, 이를 위해 상기 모터(160)는 상기 제 1 로터(120)와 제 2 로터(220)를 500rpm ~ 3,000rpm으로 회전시켜 분산질과 분산매의 흡입과 함께 제 1 및 2 로터들과 스테이터들 사이에서 분산질이 분산매에 분산되게 함과 동시에 분산질의 뭉침을 분쇄하여 분산질이 분산매에 균일하게 분산되게 한다.The dispersion emulsifying apparatus of the present invention is suitable for emulsion dispersion and emulsification having a high viscosity, for example, a viscosity of 1,000 ~ 5,000cps, for this purpose, the motor 160 is the first rotor 120 and the second rotor 220 ) Rotate at 500rpm ~ 3,000rpm to disperse the dispersoid between the first and second rotors and stators with the suction of dispersant and dispersant, and at the same time pulverize the agglomerate of dispersant To be distributed.
상기 회전속도 범위에서 500rpm 보다 작은 회전속도는 분산매에서의 고체 분산질의 요구되는 분산 정도를 얻기 어렵고, 3,000rpm 보다 큰 회전속도는 고점도의 에멀젼에서 로터들이 회전하기 위한 모터 부하의 부담이 지나치게 큰 문제점이 발생되므로 상기한 범위의 모터 회전속도가 적당하다.In the rotation speed range, the rotation speed less than 500rpm is difficult to obtain the required dispersion degree of the solid dispersion in the dispersion medium, and the rotation speed greater than 3,000rpm is too large a burden of the motor load for the rotors to rotate in the high viscosity emulsion The motor rotation speed in the above range is suitable because it is generated.
도 5에 도시된 바와 같이 상기 하우징의 유도부에 형성된 고체 분산질 유입구(103)에는 니플(112)이 제공되어 도면에서 간략하게 선으로 도시된 가요성있는 호스(113)가 연결되고, 액체 분산매 유입구(104)는 파이프를 통해 물과 같은 분산매 저장용기에 연결된다. 도면에서 미설명된 부호 (109)는 예를들어 복수의 액체 분산매를 사용하는 경우를 대비한 유입구이다.As shown in FIG. 5, a solid dispersoid inlet 103 formed in the induction part of the housing is provided with a nipple 112 to which a flexible hose 113, which is briefly illustrated in a line, is connected to the liquid dispersion medium inlet. 104 is connected to a dispersion medium reservoir, such as water, via a pipe. Reference numeral 109, which is not described in the drawings, is an inlet for the case of using a plurality of liquid dispersion media, for example.
상기 제 1 로터(120)와 제 2 로터(220)의 회전시 하우징내의 유체 흐름을 후방으로 이동시켜 하우징내의 압력이 강하되며, 이에 의해 나노 단위로 미분쇄된 분산질과 분산매가 각각의 저장용기로 부터 하우징(101)내로 유입된다.When the first rotor 120 and the second rotor 220 are rotated, the fluid flow in the housing is moved backward so that the pressure in the housing is lowered, whereby the dispersoid and the dispersion medium which are pulverized in nano units are stored in the respective storage containers. Flows into the housing 101 from.
특히, 고체 분산질 유입구(103)에 연결된 호스를 통해 분산질 저장용기에 넣음으로써 고체 분산질은 하우징내의 압력과 저장용기내의 대기압의 압력차에 의해 하우징내로 유입되며, 이로써 나노 단위의 고체 분산질이 작업장에서 비산되지 않고 신속하게 하우징(101)에 유입된다. In particular, the solid dispersion is introduced into the housing by the pressure difference between the pressure in the housing and the atmospheric pressure in the reservoir by entering the dispersal reservoir through a hose connected to the solid dispersion inlet 103, thereby a solid dispersion in nano units. It flows into the housing 101 quickly without being scattered in this workshop.
상기 고체 분산질 유입구(103)를 통해 하우징(101)내로 유입된 고체 분산질은 분산매 저장용기(170)에 연결된 파이프를 통해 액체 분산매 유입구(104)로 부터 하우징내로 유입된 분산매와 제 1 및 2 로터(120,220)/스테이터(130,230)들에 의해 혼합 및 분산되며, 특히, 나노 단위의 미세 입자로 된 고체 분산질이 뭉쳐진 덩어리가 제 1 로터(120)와 스테이터(130) 사이의 전단작용에 의해 부서지게 된다.The solid dispersion introduced into the housing 101 through the solid dispersion inlet 103 is formed by dispersing medium introduced into the housing from the liquid dispersion medium inlet 104 through a pipe connected to the dispersion medium storage container 170. The rotors 120 and 220 are mixed and dispersed by the stators 130 and 230, and in particular, agglomerates in which solid dispersions of fine particles in nano units are agglomerated by a shear action between the first rotor 120 and the stator 130. To break.
상기 분산매 저장용기(170)에는 고체 분산질과 혼합되어 유화시키기 위한 물이나 액상 유화제와 같은 분산매가 수용되어 분산유화장치에서 고체 분산질과 혼합되어 균일하게 분산된 다음 분산유화장치로 부터 분산매 저장용기로 토출된다. 이러한 분산 유화과정은 필요에 따라 수회 반복될 수 있다. The dispersion medium storage container 170 contains a dispersion medium such as water or a liquid emulsifier for emulsification by being mixed with a solid dispersion, mixed with a solid dispersion in a dispersion emulsifier to be uniformly dispersed, and then a dispersion medium storage container from the dispersion emulsion device. Is discharged. This dispersion emulsification process can be repeated several times as necessary.
상기 하우징의 고체 분산질 유입구(103)에는 니플이 제공되어 가요성있는 호스가 연결되고, 액체 분산매 유입구(104)는 파이프를 통해 물과 같은 분산매 저장용기(170)에 연결된다. The solid dispersion inlet 103 of the housing is provided with a nipple and a flexible hose is connected, and the liquid dispersion medium inlet 104 is connected to a dispersion medium reservoir 170 such as water through a pipe.
상기 제 1 로터(120)와 제 2 로터의 회전시 하우징내의 공기 흐름을 후방으로 이동시켜 하우징내의 압력이 강하되며, 이에 의해 나노 단위로 미분쇄된 분산질과 분산매가 각각의 저장용기로 부터 하우징내로 유입되어 분산 및 유화되며, 그에 의한 에멀젼은 분산매 저장용기로 배출된 다음 다시 유화장치로 유입되어 분산 및 유화 과정이 반복하여 수행됨으로써 요구되는 정도로 분산 및 유화가 이루어진다.When the first rotor 120 and the second rotor rotates, the air flow in the housing is moved backwards so that the pressure in the housing is lowered, whereby the dispersoid and the dispersion medium, which are pulverized in nano units, are separated from each reservoir. It is introduced into and dispersed and emulsified, and the emulsion is discharged into the dispersion medium storage container and then flowed back into the emulsifying apparatus, whereby dispersion and emulsification are performed to the required extent by repeatedly performing the dispersion and emulsification process.
특히, 고체 분산질 유입구(103)에 연결된 호스를 통해 분산질 저장용기에 넣고 하우징내의 압력과 저장용기내의 대기압의 압력차에 의해 고체 분산질이 하우징내로 바로 유입되며, 이로써 나노 단위의 고체 분산질이 작업장에서 비산되지 않고 신속하게 하우징에 유입된다. In particular, the solid dispersion is introduced directly into the housing by a pressure difference between the pressure in the housing and the atmospheric pressure in the storage container through a hose connected to the solid dispersion inlet 103, thereby providing a solid dispersion in nano units. It enters the housing quickly without being scattered in the workshop.
그런 다음, 하우징 앞쪽의 유도부(108)에 배치된 제 2 로터(220)가 회전하면서 분산날개(224)에 의해 반경방향 외측으로 분산매와 분산질을 와류 상태로 유동시켜서 그 외측의 제 2 스테이터(230)의 다수의 이격된 돌출부(233)들에 부딪히게 하여 분산질의 뭉침을 분쇄함과 함께 분산질이 분산매에 분산되게 한다.Then, as the second rotor 220 disposed in the induction part 108 in front of the housing rotates, the dispersion medium and the dispersoid are vortexed outward in the radial direction by the dispersal wing 224, and the second stator (outside thereof) A plurality of spaced apart protrusions 233 of 230 are struck to break up the agglomerates of the dispersoid and disperse the dispersoid in the dispersion medium.
그런 다음 뒤쪽에 배치된 상기 제1 로터(120)의 회전에 의해 제 1 로터의 스포크(121)가 제 1 스테이터(130)의 스포크(133)를 스쳐 지나면서 그 사이의 고체 분산질 입자 덩어리들을 더욱 분쇄하여 고체 분산질이 분산매에 보다 균일하게 분산된 에멀젼이 얻어진다.Then, the spokes 121 of the first rotor pass through the spokes 133 of the first stator 130 by the rotation of the first rotor 120 disposed at the rear, and the solid dispersion particles therebetween are collected. Further grinding results in an emulsion in which the solid dispersion is more uniformly dispersed in the dispersion medium.
이와 같이 분산된 에멀젼은 상기 분산매 저장용기(170)로 배출된 다음 유입구를 통해 다시 유화장치내로 유입되어 예를들어 수회 반복적으로 분산유화과정을 거치도록 함으로써, 요구되는 정도의 분산성을 갖는 에멀젼이 얻어진다.The emulsion dispersed in this way is discharged into the dispersion medium storage container 170 and then introduced into the emulsifying apparatus again through the inlet, for example, to undergo a dispersion emulsification process several times repeatedly, so that the emulsion having the required degree of dispersibility is Obtained.
도 6 내지 10은 본 발명의 다른 실시예에 의한 유화장치를 보여주며, 흡입로터(110)가 고체 분산질과 액체 분산매의 유입을 촉진시키도록 하우징(101)의 유도부(108)에 제공된다. 6 to 10 show an emulsifying apparatus according to another embodiment of the present invention, wherein the suction rotor 110 is provided in the induction part 108 of the housing 101 to promote the inflow of the solid dispersion and the liquid dispersion medium.
상기 흡입로터(110)는 허브(111)가 후방으로 연장된 연장부(115)가 모터(160)의 출력축(161)에 연결된 구동축(162)에 볼트에 의해 체결고정된다. 제 2 스테이터(230)가 상기 하우징의 유도부(108)의 후단부 내측에 고정되고, 제 2 로터(220)가 상기 제 2 스테이터(230) 내측에서 회전가능하게 배치된다.The suction rotor 110 is fastened by bolts to the drive shaft 162 connected to the output shaft 161 of the motor 160 is the extension portion 115 extending rearward hub. The second stator 230 is fixed inside the rear end of the induction part 108 of the housing, and the second rotor 220 is rotatably disposed inside the second stator 230.
제 1 스테이터(130)는 상기 유도부(108)와 플랜지 결합되는 하우징 본체(106)의 전단부 내측에 고정되고 제 1 로터(120)는 상기 제 1 스테이터(130) 내측에서 회전가능하게 배치된다. The first stator 130 is fixed inside the front end of the housing body 106 flanged to the induction part 108 and the first rotor 120 is rotatably disposed inside the first stator 130.
상기 흡입로터(110)와 제 1 및 제 2 로터(120,220)들은 모터의 출력축에 연결된 구동축(162) 단부 외주면에 끼워져 고정됨으로써 모터(160)에 의해 상기 흡입로터(110)와 제 1 및 2 로터(120,130)들이 함께 회전된다. The suction rotor 110 and the first and second rotors 120 and 220 are fitted into and fixed to the outer circumferential surface of the end of the drive shaft 162 connected to the output shaft of the motor, thereby being driven by the motor 160 and the first and second rotors. 120 and 130 are rotated together.
상기 흡입 로터(110)는 허브(111)에서 복수개, 도시된 실시예에서는 4개의 스포크(114)가 림(116)의 전체 높이와 같은 높이로 형성되어 연결되며, 상기 제 1 로터(120)도 복수개, 도시된 실시예에서 6개의 스포크(121)가 허브(122)와 림(123) 사이에서 림과 같은 높이로 형성되어 연결되어 있다. 상기 제 1 및 제 2 로터와 스테이터 구조는 전술한 제 1 실시예에서와 같다.The suction rotor 110 has a plurality of hubs 111, in the illustrated embodiment, four spokes 114 are formed at the same height as the overall height of the rim 116, and the first rotor 120 is also connected. In the illustrated embodiment, six spokes 121 are formed at the same height as the rim between the hub 122 and the rim 123. The first and second rotor and stator structures are the same as in the first embodiment described above.
상기 흡입로터(110)와 제 1 로터(120)의 스포크(112, 121)들은 각각 림과 허브 사이에서 시계방향으로 5~20°로 경사지게 형성되며, 바람직하게는 10°로 경사지게 형성된다. 상기 스포크의 경사가 5°보다 작으면 회전시의 부하가 지나치게 커지고, 20°보다 크면 흡인력이 감소된다.The spokes 112 and 121 of the suction rotor 110 and the first rotor 120 are formed to be inclined at 5 to 20 degrees in the clockwise direction between the rim and the hub, and are preferably formed to be inclined at 10 degrees. If the inclination of the spoke is less than 5 °, the load at the time of rotation becomes too large, and if it is larger than 20 °, the suction force is reduced.
본 발명에 따라 제 2 로터(220) 전측에 흡입로터(110)를 배치함으로써 제 1 및 2 로터(120,220)와 흡입로터(110)가 협동하여 증가된 흡인력으로 고점도의 에멀젼을 앞서 설명한 제 1 실시예에서 제 1 및 제 2 로터들에 의한 흡입력으로 분산 유화하는 과정에서 유동성이 떨어지는 것을 개선하여 고점도 에멀젼의 원활한 유동을 가능하게 하여 고품질의 고점도 에멀젼을 신속하게 얻을 수 있게 한다.According to the present invention, by arranging the suction rotor 110 in front of the second rotor 220, the first and second rotors 120 and 220 and the suction rotor 110 cooperate with each other to increase the emulsion of high viscosity with the increased suction force. In the example, the fluidity in the process of dispersion emulsification by the suction force by the first and second rotors is improved to enable a smooth flow of the high viscosity emulsion, so that a high quality high viscosity emulsion can be obtained quickly.
도 11에는 도 1의 또 다른 실시예의 분산유화장치용으로 제 1 스테이터(130) 후방에서 배출구측에 인접하여 배출용 로터(220')를 추가로 배치한 구조가 도시되어 있다. 상기한 배출용 로터(220')는 원판(223) 상에 다수의 분산날개(224)를 구비한 제 2 로터(220)와 동일하게 원판상에 다수의 분산날개를 구비한 구조로 구성될 수 있으며, 제 1로터/스테이터 (120/130)에서 후방으로 이격되어 배출구에 인접하여 후방에 배치된다. FIG. 11 illustrates a structure in which a discharging rotor 220 'is further disposed adjacent to the outlet side at the rear of the first stator 130 for the dispersion emulsifying apparatus of still another embodiment of FIG. The discharge rotor 220 ′ may have a structure in which a plurality of dispersing wings are provided on a disc, similarly to the second rotor 220 having a plurality of dispersing wings 224 on a disc 223. And spaced rearward from the first rotor / stator (120/130) and adjacent the outlet.
상기한 배출용 로터(220')는 제 1 및 제 2 로터/스테이터를 통하여 분산 및 유화된 고점도의 에멀젼에 원심력을 작용하여 용이하게 배출되게 하고, 또한 분산성이 향상된다. 이로써, 결국 에멀젼의 유속을 증가시키고 따라서 분산질과 분산매의 유입 속도 또한 증가될 수 있다. The discharge rotor 220 'is easily discharged by applying a centrifugal force to the high viscosity emulsion dispersed and emulsified through the first and second rotors / stators, and the dispersibility is improved. This, in turn, increases the flow rate of the emulsion and thus the rate of introduction of the dispersion and the dispersion medium can also be increased.
본 발명은 고체 분산질과 액상의 분산매를 균일하게 분산 및 유화시켜 고점도 에멀젼을 얻는데 이용될 수 있다.The present invention can be used to obtain a high viscosity emulsion by uniformly dispersing and emulsifying the solid dispersion and the liquid dispersion medium.
[부호의 설명][Description of the code]
100 : 분산유화장치 101 : 하우징100: dispersion emulsion 101: housing
103 : 분산질 유입구 104 : 분산매 유입구103: dispersoid inlet 104: dispersion medium inlet
105 : 혼합 유체 배출구 107 : 본체105: mixed fluid outlet 107: the main body
108 : 유도부 110 : 흡입 로터108: induction unit 110: suction rotor
111 : 허브 114 : 스포크111: hub 114: spoke
116 : 림 120 : 제 1 로터 116: Rim 120: First rotor
121 : 스포크 122 : 허브121: spoke 122: hub
123 : 림 130 : 제 1 스테이터123: Rim 130: First stator
131 : 보스 132 : 림131: Boss 132: Rim
133 : 스포크 220 : 제 2 로터133: spoke 220: second rotor
224 : 분산날개 225 : 보스224: Scatter Wing 225: Boss
230 : 제 2 스테이터 223 : 원판230: second stator 223: disc
231 : 바닥부 232 : 림231: bottom 232: rim
160 : 모터 162 : 구동축 160: motor 162: drive shaft

Claims (8)

  1. 고체 분산질 유입구와 액체 분산매 유입구가 일측에 형성되고 타측에는 혼합 유체 배출구가 형성된 하우징과, 그 하우징 속에 설치된 스테이터와 그 내측에 배치되어 모터로 회전하는 로터를 구비한 고점도 유체 분산유화장치에 있어서,In the high viscosity fluid dispersion emulsifying apparatus having a solid dispersion inlet and a liquid dispersion medium inlet is formed on one side and a mixed fluid outlet on the other side, a stator installed in the housing and a rotor disposed therein and rotated by a motor,
    하우징 내측에 고정된 제 1 스테이터(130)와, 제 1 스테이터 내측에서 회전가능하게 배치된 제 1 로터(120), 상기 제 1로터(120)/스테이터(130) 전측에서 하우징 내측에 고정된 제 2 스테이터(230) 내측에서 회전가능하게 배치된 제 2 로터(220)를 포함하며, A first stator 130 fixed inside the housing, a first rotor 120 rotatably disposed inside the first stator, and a first fixed inside the housing at the front of the first rotor 120 / stator 130 A second rotor 220 rotatably disposed inside the second stator 230,
    상기 제 1 로터(120)와 제 2 로터(220)는 회전에 의해 내부 유체를 배출시켜 하우징 내의 압력이 저하되어 발생되는 흡인력으로 분산질과 분산매를 각각의 용기로 부터 직접 하우징내로 유입시키도록 된 것을 특징으로 하는 고점도 유체 분산유화장치.The first rotor 120 and the second rotor 220 discharge the internal fluid by the rotation, so that the dispersoid and the dispersion medium are introduced into the housing directly from the respective containers by the suction force generated by the pressure in the housing being lowered. High viscosity fluid dispersion emulsifying apparatus, characterized in that.
  2. 제 1항에 있어서, 상기 제 1 로터(120)는 허브(122)와 림(123) 사이에서 림과 같은 높이로 형성되어 연결된 복수개의 스포크(121)를 구비하고, 상기 제 1 스테이터(130)는 모터의 출력축과 연결된 구동축 외주면에 고정되는 환형으로 된 보스(131)와 림(132)을 연결하는 복수개의 스포크(133)를 포함하며, 상기 제 1 로터(120)의 스포크(121)는 유체를 후방으로 송출하도록 경사져 있으며, 상기 제 1 로터(120) 회전시 그 스포크(121)와 제 1 스테이터(130)의 스포크(133) 사이에서 분산질의 뭉침을 분쇄하도록 된 것을 특징으로 하는 고점도 분산유화장치.According to claim 1, wherein the first rotor 120 has a plurality of spokes 121 formed and connected to the same height as the rim between the hub 122 and the rim 123, the first stator 130 It includes a plurality of spokes 133 connecting the rim 132 and the annular boss 131 is fixed to the outer peripheral surface of the drive shaft connected to the output shaft of the motor, the spoke 121 of the first rotor 120 is a fluid Is inclined so as to be discharged to the rear, and the high viscosity dispersed oil, characterized in that to crush the aggregates of the dispersoid between the spoke 121 and the spoke 133 of the first stator 130 when the first rotor 120 is rotated Device.
  3. 제2항에 있어서, 상기 제 1 로터(120)의 스포크(121)들은 각각 림과 허브 사이에서 시계방향으로 5~20°로 경사지게 형성된 것을 특징으로 하는 고점도 분산유화장치.The high viscosity dispersed emulsion of claim 2, wherein the spokes 121 of the first rotor 120 are formed to be inclined at 5 to 20 degrees in a clockwise direction between the rim and the hub, respectively.
  4. 제 1항에 있어서, 상기 제 2 로터(220)는 분산질을 분산매에서 분산시키도록 보스의 외주면에서 반경방향 외측으로 확장된 원판(223)상에서 전방으로 돌출되고 직경에 대하여 경사지게 일정 간격으로 이격된 다수의 분산날개(224)들을 일체로 구비한 것을 특징으로 하는 고점도 분산유화장치.2. The second rotor (220) of claim 1, wherein the second rotor (220) projects forward on a disc (223) that extends radially outward from the outer circumferential surface of the boss to disperse the dispersoid in the dispersion medium and is spaced at regular intervals inclined to the diameter. High viscosity dispersion emulsifying apparatus, characterized in that provided with a plurality of dispersing wings (224) integrally.
  5. 제 4항에 있어서, 상기 분산날개(224)들은 보스의 직경에 대하여 25°~40°범위에서 경사지게 형성된 것을 특징으로 하는 고점도 분산유화장치.5. The high viscosity dispersion emulsifying apparatus according to claim 4, wherein the dispersing blades 224 are formed to be inclined at a range of 25 to 40 degrees with respect to the diameter of the boss.
  6. 전기한 항들중 어느 한 항에 있어서, 상기 하우징(101)의 고체 분산질 유입구(103)와 액체 분산매 유입구(104)가 형성된 유도부(108)에 상기 제 2 로터(220)/스테이터(230)가 배치되고, 분리세척 가능하게 상기 유도부와 분리가능하게 결합된 본체(107)에 제 1 로터(120)/스테이터(130)가 배치되며, 상기 제 1 및 2 로터(120,220)들은 모터의 출력축에 연결된 구동축(162)에 의해 함게 구동되는 것을 특징으로 하는 고점도 분산유화장치.According to any one of the preceding, wherein the second rotor 220 / stator 230 is formed in the induction portion 108 formed with the solid dispersion inlet 103 and the liquid dispersion inlet 104 of the housing 101 The first rotor 120 / stator 130 is disposed in the main body 107 is disposed, detachably coupled to the induction portion, the first and second rotors 120, 220 are connected to the output shaft of the motor High viscosity dispersed emulsion, characterized in that driven together by the drive shaft (162).
  7. 제 6 항에 있어서, 상기 유도부에는 고체 분산질과 액체 분산매에 대한 흡인력을 증가시키도록 제 2로터(220)/스테이터(230) 앞쪽에 배치된 흡입로터(110)가 제공되며, 상기 흡입로터(110)는 허브(111)가 후방으로 연장된 연장부(115)가 모터(160)의 출력축(161)에 연결된 구동축(162)에 의해 제 1 및 2 로터들과 함께 회전하도록 된 것을 특징으로 하는 고점도 분산유화장치.According to claim 6, The induction part is provided with a suction rotor 110 disposed in front of the second rotor 220 / stator 230 to increase the suction force for the solid dispersion and the liquid dispersion medium, the suction rotor ( 110 is characterized in that the extension portion 115 from which the hub 111 extends rearward is rotated together with the first and second rotors by the drive shaft 162 connected to the output shaft 161 of the motor 160. High viscosity dispersion emulsifier.
  8. 제 1 항에 있어서, 제 1 로터(120)/스테이터(130) 후방에서 배출구측에 인접하여 배치되고 반경방향 외측으로 확장된 원판상에서 전방으로 돌출되고 직경에 대하여 경사지게 일정 간격으로 이격된 다수의 분산날개들을 일체로 구비한 배출용 로터(220')를 추가로 구비하여 원심력에 의해 고점도 에멀젼이 용이하게 배출되도록 한 것을 특징으로 하는 고점도 분산유화장치.2. A plurality of dispersions as set forth in claim 1, characterized by a plurality of dispersions spaced at regular intervals, protruded forward on a disc that is disposed radially outwardly and disposed adjacent to the outlet side at the rear of the first rotor (120) / stator (130). High-viscosity dispersion emulsifying apparatus, characterized in that the discharge rotor (220 ') having a wing integrally provided to facilitate the discharge of high viscosity emulsion by centrifugal force.
PCT/KR2016/002671 2015-07-31 2016-03-16 High-viscosity fluid dispersion/emulsification device WO2017022920A1 (en)

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