WO2016076575A1 - Hydrogel mask pack composition, hydrogel mask pack prepared therefrom, and preparation method therefor - Google Patents

Hydrogel mask pack composition, hydrogel mask pack prepared therefrom, and preparation method therefor Download PDF

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Publication number
WO2016076575A1
WO2016076575A1 PCT/KR2015/011890 KR2015011890W WO2016076575A1 WO 2016076575 A1 WO2016076575 A1 WO 2016076575A1 KR 2015011890 W KR2015011890 W KR 2015011890W WO 2016076575 A1 WO2016076575 A1 WO 2016076575A1
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Prior art keywords
extract
polypeptide
mask pack
hydrogel mask
weight
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PCT/KR2015/011890
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French (fr)
Korean (ko)
Inventor
최영권
호환기
심보미
나승연
Original Assignee
코스맥스아이큐어주식회사
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Publication of WO2016076575A1 publication Critical patent/WO2016076575A1/en

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706Algae
    • A61K8/9717Rhodophycota or Rhodophyta [red algae], e.g. Porphyra
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9771Ginkgophyta, e.g. Ginkgoaceae [Ginkgo family]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin

Definitions

  • the present invention relates to a hydrogel mask pack composition, a hydrogel mask pack prepared through the same, and a method for manufacturing the same, and more particularly, to a hydrogel composition having improved strength of the hydrogel mask pack and a hydrogel mask pack prepared through the same. It is about.
  • Skin care mask is a product that attaches a substance to the skin to make it clean and beautiful, and then removes or rinses it after a certain time. It can be used for the whole body as well as the face.
  • the mask pack is for nourishing the skin of the face by attaching it to the face while containing active substances or cosmetics containing various ingredients useful for the skin, such as moisturizers, whitening agents, etc. It is used as a method of attaching a mask pack made of nonwoven fabric to the face for a certain time to absorb.
  • Skincare masks may be non-woven, dry, or hydrogel type masks, depending on the formulation. Hydrogel masks may be classified into water-soluble hydrogel masks and insoluble hydrogel masks.
  • the skin care hydrogel mask is a product combining medicinal technology with a simple cosmetic mask. By storing an effective cosmetic ingredient inside the water-soluble polymer in the hydrogel, it can be seen as a skin care delivery system designed to continuously and effectively deliver the efficacy and effect of the active ingredient.
  • hydrogels are well known as materials suitable for use as matrix for controlled release of drugs (NA Pappas ed., "Hydrogels in Medicine and Pharmacy, Vol. 11; Polymers", CRC Press, Inc., 1987). This is used as a drug carrier that uses a hydrogel as a matrix to contain hormones such as progesterone, thereby releasing hormones slowly and controlling the amount of hormone delivered to the body.
  • US Patent No. 5,344,655 to Sakai et al. Discloses a technique for delivering drugs through the skin using a hydrogel base containing a water-soluble polymer such as a cellulose derivative.
  • U.S. Patent No. 4,593,053 to Zevner et al discloses the use of skin-friendly, pressure-sensitive hydrogels. Transdemal delivery of drugs delivers hormones such as progesterone, progestin, estrogen, and testosterone into the body through the skin, released only in a controlled amount from the hydrogel attached to the skin and delivered to the body through the percutaneous body. It is a high dosage technique.
  • US Patent No. 6,214,374 to Schiller et al. Discloses a composition, method and apparatus for hydrogels for effective transdermal delivery of drugs without blocking the skin.
  • Hydrogel masks are required to quickly deliver the active ingredients contained within a short time within 20 to 30 minutes after attaching the hydrogel to the skin, but for this purpose, active ingredients in the hydrogel are quickly and evenly delivered into the skin. Should have However, as long as it maintains the hydrogel state, the effective cosmetic ingredients in the gel have a limit to having a satisfactory amount and speed to be transferred from the hydrogel to the skin, and as time passes, water and active ingredients in the hydrogel evaporate. It will dry up, leaving you unable to benefit. Therefore, even if the hydrogel has good adhesion and wettability, the limit of the content of the active ingredient contained in the hydrogel and the speed of delivery of the active cosmetic ingredient to the skin are also limited to the skin penetration efficiency of the hydrogel mask pack. Will be forced to have.
  • the current hydrogel mask pack is generally prepared by adding a water and polyalcohol to carrageenan and gum and stirring by heating to 60 ⁇ 85 to form a cross-linked form according to the temperature change to make a gel form.
  • the hydrogel mask pack is inconvenient to use when the area is large and the elasticity is inconvenient, and the elasticity is increased by increasing the content, but there is an inconvenience in that the viscosity is high during manufacturing. Therefore, when the hydrogel mask pack is prepared at 60 or more after stirring, there is a problem in that it is difficult to use peptides or various active ingredients that are weak at high temperatures.
  • the object of the present invention is purified water in a molded article made of a hydrogel mask pack composition containing purified water, polyhydric alcohol, carrageenan, locust bean gum, xanthan gum and tamarind seed gum Hydrogel mask which can add various active ingredients which are enhanced in strength by adding a essence containing at least one selected from the group consisting of polyhydric alcohols, natural extracts and functional additives to produce a hydrogel mask pack. To provide a pack.
  • the present invention provides a hydrogel composition containing purified water, carrageenan, locust bean gum, xanthan gum and tamarind seed gum.
  • the hydrogel mask pack composition may further contain a polyhydric alcohol.
  • the polyhydric alcohol may include one or more selected from the group consisting of butylene glycol, polyethylene glycol, glycerin, ethanol, sorbitol and trehalose.
  • the hydrogel mask pack composition is purified water 90 to 99% by weight, carrageenan 0.1 to 2% by weight, locust bean gum 0.1 to 2% by weight, xanthan gum 0.1 to 1% by weight and tamarind Sea gum may contain 0.005 to 7% by weight.
  • the hydrogel mask pack composition may further contain 0.1 to 10% by weight of polyhydric alcohol.
  • Another aspect of the present invention provides a hydrogel mask pack comprising a molded body of the hydrogel mask pack composition.
  • the molded product means a molded product in the form of a mask prepared by heating and cooling the hydrogel mask pack composition containing the purified water, carrageenan, locust bean gum, xanthan gum and tamarind seed gum.
  • it may include 30 to 70 parts by weight of the essence containing one or more selected from the group consisting of purified water, polyhydric alcohol and natural extracts based on 100 parts by weight of the molded body.
  • the essence may contain 40 to 300 parts by weight of polyhydric alcohol with respect to 100 parts by weight of purified water.
  • the polyhydric alcohol may include glycerin and butylene glycol in a weight ratio of 1: 0.1 to 2.5.
  • the tamarind seed gum and the polyhydric alcohol contained in the essence may be included in the weight ratio of 1: 20 to 80.
  • the essence may contain 0.01 to 20 parts by weight of natural extract, based on 100 parts by weight of purified water.
  • the essence may contain 0.001 to 20 parts by weight of the functional additive, based on 100 parts by weight of purified water.
  • the natural extract is green tea extract, licorice extract, medicinal extract of green tea, extract of baekryeok, golden extract, pueraria extract, red ginseng extract, apricot extract, oil extract, orange extract, lemon extract, bamboo Extract, Guava Extract, Rosemary Extract, Cornus Extract, Ganoderma Lucidum Extract, Ginkgo Extract, Seosiokyuksan Extract, Consonant Extract, Chinese Quince Extract, White Lotus Extract, Paprika Extract, Aloe Extract, Scrubber Extract, Seaweed Extract, Grapefruit Extract, Carrot Extract Seed Extract, Grape Seed Extract, March Extract, Caviar Extract, Pomegranate Extract, Ginseng Extract, Peach Extract, Cheongung Extract, Centella asiatica Extract, Chamomile Extract, Licorice Root Extract, High Ginseng Extract, Angelica Extract, Peppermint Extract, Sambaekcho Extract, Crop Extract , Vinegar extract, dandelion extract, calendula extract, yellow white skin extract, tang It
  • the functional additive is glycerin, panthenol, hyaluronic acid, ceramide, beta glucan, arbutin, vitamin C, whitens, retinol, elastin, collagen, coenzyme Q10, effectin, EGF, propolis, It may include one or more selected from the group consisting of allantoin, phytostane, infraacid and antioxidant vitamin E (natural tocopherol).
  • the functional additive further contains a peptide
  • the peptide is rh-Polypeptide-64, rh-Oligopeptide-33, sh-oligopeptide-1, sh-Polypeptide-11, sh-Polypeptide -1, rh-Polypeptide-7, rh-Polypeptide-62, rh-Oligopeptide-2, sh-Polypeptide-31, rh-Polypeptide-3, rh-Polypeptide-14, sh-Polypeptide-13, rh-Polypeptide-8 , sh-Polypeptide-59, sh-Polypeptide-16, rh-Polypeptide-4, rh-Polypeptide-66, rh-Polypeptide-67, rh-Polypeptide-60, rh-Polypeptide-51, rh-Polypeptide-58, sh At least one member selected from the group consisting of -Polypeptide-19,
  • the thermal shortening of the hydrogel mask pack may be 3 ⁇ 4 m.
  • the non-rupture strength of the hydrogel mask pack is 6 ⁇ 7 kg / cm 2 Can be.
  • Another aspect of the present invention is a step of preparing a mixture by mixing the hydrogel mask pack composition; Heating the mixture prepared in step 1 to 60 to 90 ° C. and then applying the same on a thin film; Step 3 of producing a molded body by cooling and drying the mixture applied on the thin film in the step 2; 4 steps of cutting the molded body in the form of a mask; And a step 5 of filling the molded article in the mask form with an essence containing at least one selected from the group consisting of purified water, polyhydric alcohol, natural extracts and functional additives; It provides a method of manufacturing a hydrogel mask pack comprising a.
  • the mixture in the second step may be applied to the thin film 500 ⁇ 2000 ⁇ m thickness by a wrap coating method.
  • the mixture applied on the thin film in the third step may be cooled to 0 ⁇ 30 °C.
  • the mixture applied on the thin film in the third step may be dried at 70 ⁇ 110 °C.
  • the molded article prepared in step 3 may have a thickness of 100 ⁇ 1000 ⁇ m.
  • hydrogel mask pack due to the dehydration action of tamarind seed gum and polyhydric alcohol, hydrogen bonds are formed by agglomeration of molecules of tamarind seed gum, which may result in gelation, thereby improving the strength of the hydrogel.
  • Hydrogel mask pack can be prepared. When gelling in the same manner as described above can be added to the active ingredient sensitive to temperature in the essence can be prepared a functional hydrogel mask pack.
  • the present invention relates to a hydrogel composition comprising tamarind seed gum, a hydrogel mask pack prepared through the same, and a method for preparing the same, and more particularly, a mask including tamarind seed gum and an essence as a composition of a hydrogel mask pack.
  • the present invention relates to a hydrogel mask pack composition and a method of manufacturing a hydrogel mask pack using the same, in which the strength of the pack can be improved.
  • the present invention provides a hydrogel composition containing purified water, carrageenan, locust bean gum, xanthan gum and tamarind seed gum.
  • the present invention will be described in more detail for each component.
  • the hydrogel composition according to the present invention can be prepared in a gel state by mixing, heating and cooling by containing purified water, carrageenan, locust bean gum, xanthan gum and tamarind seed gum.
  • the hydrogel composition according to the present invention may further contain a polyhydric alcohol, and the tamarind seed gum is mixed with the polyhydric alcohol to cause dehydration, and the thickening and gelation of the tamarind seed gum are carried out, so that the hydrolysis is performed.
  • a molded article of the hydrogel mask pack detachable to the skin can be prepared from the gel composition.
  • the polyhydric alcohol may include at least one selected from the group consisting of butylene glycol, polyethylene glycol, glycerin, ethanol, sorbitol and trehalose, preferably selected from the group consisting of butylene glycol, polyethylene glycol and glycerin It is good that it is 1 or more types.
  • the purified water is included to dissolve the carrageenan, locust bean gum, xanthan gum and tamarind seed gum and supply water, preferably 90 to 99% by weight, more preferably 95 to 99 It is preferably included in weight percent.
  • the polyhydric alcohol may be selectively added, and when mixed with gums such as carrageenan, locust bean gum, xanthan gum, and tamarind seed gum, dehydration reactions serve to help gel the compositions, and 0.1 to 10 It is preferably included in the weight%, more preferably 0.1 to 5% by weight.
  • gums such as carrageenan, locust bean gum, xanthan gum, and tamarind seed gum
  • hydrogel mask pack comprising a molded body of the hydrogel composition.
  • the hydrogel composition may be gelled in the process of mixing the hydrogel composition and then heating and cooling, and may further include an essence containing the at least one selected from the group consisting of purified water, polyhydric alcohol, and natural extract. Can be.
  • an essence containing one or more selected from the group consisting of purified water, polyhydric alcohol, natural extracts and functional additives based on 100 parts by weight of the molded body.
  • the essence preferably contains 40 to 300 parts by weight of polyhydric alcohol with respect to 100 parts by weight of purified water.
  • the purified water is included to supply water in the hydrogel mask pack
  • the polyhydric alcohol is mixed with the molecules of tamarind seed gum contained in the molded body prepared from the hydrogel composition may cause dehydration and thickening and gelation Since it is additionally carried out, it may serve to improve the strength of the hydrogel mask pack in a new crosslinking method.
  • the polyhydric alcohol is included to be out of the range, there is a problem that the strength of the mask pack is not sufficiently improved.
  • the polyhydric alcohol may include glycerin and butylene glycol, preferably contained in a weight ratio of 1: 0.1 to 2.5, and more preferably included in a weight ratio of 1: 0.5 to 2 good.
  • the hydrogel mask pack according to the present invention preferably comprises tamarind seed gum and polyhydric alcohols contained in the essence in a weight part of 1: 20 ⁇ 80, more preferably 1: 30 ⁇ It is preferably included in 60 parts by weight.
  • the essence may contain 0.01 to 20 parts by weight of the natural extract with respect to 100 parts by weight of purified water.
  • the natural extract can provide an active ingredient that is supplied to the skin.
  • the natural extract can be used as long as it is included as an active ingredient that can be supplied to the skin, preferably green tea extract, licorice extract, gingko extract, lettuce extract, golden extract, pueraria extract, red ginseng extract, Apricot Extract, Oil Extract, Orange Extract, Lemon Extract, bamboo Extract, Guava Extract, Rosemary Extract, Cornus Extract, Ganoderma lucidum Extract, Ginkgo Extract, Seogyok Oksan Acid Extract, Consonant Extract, Chinese Quince Extract, White Lotus Extract, Paprika Extract, Aloe Water Extract, Aloe Sea Extract Extract, Seaweed Extract, Carrot Extract, Soybean Extract, Grapefruit Seed Extract, Grape Seed Extract, March Extract, Caviar Extract, Pomegranate Extract, Ginseng Extract, Peach Extract, Cheongung Extract, Centella Extract, Chamomile Extract, Herbal Root Extract, Ginseng Extract , Peppermint extract, triticale extract, fish extract, peony extract , Wood vinegar, dandelion extract, calendula extract, yellowish
  • the essence may contain 0.001 to 20 parts by weight of functional additives, preferably 0.01 to 10 parts by weight with respect to 100 parts by weight of purified water.
  • the functional additive may provide an active ingredient to be supplied to the skin, and when the functional additive is included in less than 0.001 part by weight, there is a problem in that the functional ingredient is lowered due to less active ingredient to be supplied to the skin, and more than 20 parts by weight. In this case, there is a problem that the unit price is increased because it is included in excess.
  • the functional additives are glycerin, panthenol, hyaluronic acid, ceramide, beta glucan, arbutin, vitamin C, whitetene, retinol, elastin, collagen, coenzyme Q10, effectin, EGF, propolis, allantoin, phytostane, infraacid and antioxidant It may include one or more selected from the group consisting of vitamin E (natural tocopherol).
  • the gelation is performed through dehydration between gums such as tamarind seed gum and polyhydric alcohol, it does not need to be heated to a high temperature, and thus there is no limitation in adding a weak active ingredient to temperature, thereby Sensitive peptides can be added.
  • the peptide is rh-Polypeptide-64, rh-Oligopeptide-33, sh-oligopeptide-1, sh-Polypeptide-11, sh-Polypeptide-1, rh-Polypeptide-7, rh-Polypeptide-62, rh-Oligopeptide-2 , sh-Polypeptide-31, rh-Polypeptide-3, rh-Polypeptide-14, sh-Polypeptide-13, rh-Polypeptide-8, sh-Polypeptide-59, sh-Polypeptide-16, rh-Polypeptide-4, rh -Polypeptide-66, rh-Polypeptide-67, rh-Polypeptide-60, rh-Polypeptide-51, rh-Polypeptide-58, sh-Polypeptide-19, sh-Polypeptide-22, sh-Polypeptide-5, rh-Polypeptide It may include one or more selected from
  • the thermal shortening of the hydrogel mask pack according to the present invention is preferably 3-4 m, more preferably 3.2-4.
  • the non-rupture strength of the hydrogel mask pack is preferably 6 ⁇ 7 kg / cm 2 , more preferably 6.2 ⁇ 7 kg / cm 2 It is good.
  • the present invention is a step of preparing a mixture by mixing the hydrogel mask pack composition; Heating the mixture prepared in step 1 to 60 to 90 ° C. and then applying the same on a thin film; Step 3 of producing a molded body by cooling and drying the mixture applied on the thin film in the step 2; 4 steps of cutting the molded body in the form of a mask; And a step 5 of filling the molded article in the mask form with an essence containing at least one selected from the group consisting of purified water, polyhydric alcohol, natural extracts and functional additives; It provides a method of manufacturing a hydrogel mask pack comprising a.
  • the present invention will be described in more detail step by step.
  • purified water, carrageenan, locust bean gum, xanthan gum and tamarind seed gum may be mixed and stirred to prepare a mixture.
  • carrageenan 0.1 ⁇ 2% by weight
  • locust bean gum 0.1 ⁇ 2% by weight
  • xanthan gum 0.1 ⁇ 1% by weight
  • tamarind seed gum 0.005 ⁇ 7% by weight
  • the polyhydric alcohol may be selectively added, and when mixed with gums such as carrageenan, locust bean gum, xanthan gum, and tamarind seed gum, dehydration reactions serve to help gel the compositions, and 0.1 to 10 It is preferably included in the weight%, more preferably 0.1 to 5% by weight.
  • gums such as carrageenan, locust bean gum, xanthan gum, and tamarind seed gum
  • the mixture prepared in the first step may be applied to a thin film after heating to 60 ⁇ 90 °C.
  • the mixture prepared in step 1 shows fluidity in a sol state and is heated to 60 to 90 ° C., then coated on a thin film, and then gelled in the course of cooling to form a molded article of the hydrogel composition in a film form.
  • the molded product in the third step, may be manufactured by cooling and drying the mixture applied on the thin film in the second step.
  • the mixture applied on the thin film is fluidized in a sol state and heated to 60 ⁇ 90 °C and then gelled in the process of coating on the thin film to cool the molded article of the hydrogel mask pack composition is 500 ⁇ m ⁇ 2000 ⁇ m thick film form It may be prepared as, and then compressed into a film having a thickness of 100 ⁇ 1000 ⁇ m through cooling and drying.
  • step 3 it is preferable to cool the mixture applied on the thin film in step 3 at 0 ⁇ 3 °C 0, and more preferably at 10 ⁇ 25 °C, but if the mixture can be cooled to prepare a molded article It is not specifically limited.
  • the mixture applied on the thin film in the step 3 it is preferable to dry the mixture applied on the thin film in the step 3 at 70 ⁇ 110 °C, more preferably at 80 ⁇ 100 °C. If the drying time is less than 70 °C has a problem that the drying time is long, there is a problem that the molded body may be damaged by being excessively heated when drying over 110 °C.
  • the fourth step in the fourth step it can be manufactured in a form that can be tried by cutting the molded body in the form of a mask.
  • the molded article cut in the form of the mask can be produced hydrogel mask pack by applying the essence in a later step.
  • step 5 an essence containing at least one selected from the group consisting of purified water, polyhydric alcohol, natural extracts and functional additives may be applied to the molded article in the form of a mask. have.
  • a hydrogel mask pack was prepared in the same manner as in Example 1, except that the hydrogel mask pack composition and the essence were prepared in the same composition as in Table 1 and Table 2.
  • a hydrogel mask pack was prepared in the same manner as in Example 1, except that the hydrogel composition and the essence were mixed with the composition shown in Table 3 below.

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Abstract

The present invention relates to a hydrogel mask pack composition, a hydrogel mask pack prepared therefrom, and a preparation method therefor and, more specifically, to: a hydrogel mask pack composition containing tamarind seed gum and essence as a composition for a hydrogel mask pack, thereby improving the strength of a mask pack; and a method for preparing a hydrogel mask pack by using the same.

Description

하이드로겔 마스크팩 조성물, 이를 통해 제조된 하이드로겔 마스크팩 및 이의 제조방법Hydrogel mask pack composition, hydrogel mask pack prepared by the same and a method of manufacturing the same
본 발명은 하이드로겔 마스크팩 조성물, 이를 통해 제조된 하이드로겔 마스크팩 및 이의 제조방법에 관한 것으로, 보다 상세하게는 하이드로겔 마스크팩의 강도가 향상되는 하이드로겔 조성물 및 이를 통해 제조된 하이드로겔 마스크팩에 관한 것이다.The present invention relates to a hydrogel mask pack composition, a hydrogel mask pack prepared through the same, and a method for manufacturing the same, and more particularly, to a hydrogel composition having improved strength of the hydrogel mask pack and a hydrogel mask pack prepared through the same. It is about.
스킨케어 마스크(skin care mask)란 피부를 깨끗하고 아름답게 하기 위해 미용에 도움이 되는 물질을 피부 표면에 붙였다가 일정 시간이 지난 후 떼어내거나 헹궈내는 제품이다. 이는 얼굴뿐 아니라 전신에 사용될 수도 있다. 일반적으로, 마스크팩은 보습제, 미백제 등과 같은, 피부에 유용한 여러 성분이 함유한 활성물질이나 화장품 등을 함유한 상태에서 얼굴에 부착하여 얼굴의 피부에 영양을 공급하기 위한 것으로서, 많은 양을 피부 깊이 흡수시키기 위해 부직포 등으로 제작된 마스크팩을 일정시간 얼굴에 부착하는 방법으로 사용된다.Skin care mask is a product that attaches a substance to the skin to make it clean and beautiful, and then removes or rinses it after a certain time. It can be used for the whole body as well as the face. In general, the mask pack is for nourishing the skin of the face by attaching it to the face while containing active substances or cosmetics containing various ingredients useful for the skin, such as moisturizers, whitening agents, etc. It is used as a method of attaching a mask pack made of nonwoven fabric to the face for a certain time to absorb.
손쉽게 얼굴 마사지를 하기 위하여 최근에는 부직포, 미용필름 등을 일정한 형태로 압축시켜서 마사지할 얼굴부위에 덮어씌울 수 있도록 원형이나 얼굴 모양의 여러 가지 종류의 마스크팩이 출시되고 있다.Recently, various types of mask packs of round or face shape have been released to compress a nonwoven fabric, a beauty film, etc. in a certain form so as to cover the face to be massaged.
스킨케어 마스크는 제형에 따라 부직포, 건조, 하이드로젤 타입 마스크가 있으며, 하이드로젤 마스크는 수용성 하이드로젤 마스크와 불용성 하이드로젤 마스크로 분류될 수 있다. 상기 스킨케어 하이드로젤 마스크는 단순한 화장용 마스크에 의약용 기술을 접목한 제품이다. 유효한 화장성분을 하이드로젤 내의 수용성 고분자 내부에 저장함으로써 유효성분의 효능 및 효과를 지속적, 효과적으로 전달되도록 고안된 스킨케어 전달 시스템으로 볼 수 있다.Skincare masks may be non-woven, dry, or hydrogel type masks, depending on the formulation. Hydrogel masks may be classified into water-soluble hydrogel masks and insoluble hydrogel masks. The skin care hydrogel mask is a product combining medicinal technology with a simple cosmetic mask. By storing an effective cosmetic ingredient inside the water-soluble polymer in the hydrogel, it can be seen as a skin care delivery system designed to continuously and effectively deliver the efficacy and effect of the active ingredient.
보다 구체적으로, 하이드로겔은 약품조절방출(controlled release of drugs)을 위한 기지체로서 사용되기에 적합한 물질로 잘 알려져 있다(N. A. Pappas ed., "Hydrogels in Medicine and Pharmacy, Vol. 11; Polymers", CRC Press, Inc.,1987). 이는 하이드로겔을 기지체로 사용하여 그 속에 프로게스테론과 같은 호르몬을 함유시켜서 호르몬이 서서히 방출되어 몸 안으로 전달되는 호르몬의 양을 조절하는 약물전달체로서 이용되는 것이다. 사카이 등의 미국특허번호 제5,344,655호에 의하면 셀룰로즈 유도체 같은 수용성 고분자를 함유한 하이드로겔 기지를 사용하여 피부를 통하여 약물을 전달하는 기술이 공개되어 있다. 폭스 등의 미국특허번호 제5,405,366호에 의하면 광가교가 가능한 수용성 고분자를 함유하는 접착성 하이드로겔을 만들어 경피 약물전달시스템(transdermal drug delivery system)에 사용하는 기술이 알려져 있다. 제브너 등의 미국특허번호 제4,593,053호에 의하면 피부에 친화적이고 압력감응 하이드로겔을 만들어 사용하는 것을 공개하고 있다. 약물의 경피전달(transdemal delivery of drugs)은 프로게스테론, 프로게스틴, 에스트로겐, 테스토스테론 등 호르몬을 피부를 통하여 체내로 전달하는 것으로 피부에 부착된 하이드로겔에서부터 서서히 조절된 양만큼만 방출되어 경피를 통하여 체내로 전달되는 고도의 투약 기술이다. 슈밀러 등의 미국특허번호 제6,214,374에 의하면 피부에 차단되지 않고 효과적인 약물의 경피전달을 위한 하이드로겔의 조성, 방법 및 그 장치를 공개하고 있다. 베르너 등의 미국특허번호 제5,064,654호에 의하면 약물의 경피전달을 위한 접착성 하이드로겔의 조성을 공개하고 있다. 사포타 등의 미국특허번호 제4,942,158호에 의하면 약물의 경피전달을 증진시키기 위하여 침투증진제가 첨가된 하이드로겔의 조성을 공개하고 있다. 또한, 롤프 등의 미국특허번호 제6,361,790호 및 제 6,406,712호에 의하면 하이드로겔을 이용한 드레싱, 패치 등의 피부적용 방법을 공개하고 있다.More specifically, hydrogels are well known as materials suitable for use as matrix for controlled release of drugs (NA Pappas ed., "Hydrogels in Medicine and Pharmacy, Vol. 11; Polymers", CRC Press, Inc., 1987). This is used as a drug carrier that uses a hydrogel as a matrix to contain hormones such as progesterone, thereby releasing hormones slowly and controlling the amount of hormone delivered to the body. US Patent No. 5,344,655 to Sakai et al. Discloses a technique for delivering drugs through the skin using a hydrogel base containing a water-soluble polymer such as a cellulose derivative. US Pat. No. 5,405,366 to Fox et al. Discloses a technique for making an adhesive hydrogel containing water-crosslinkable water-soluble polymers for use in transdermal drug delivery systems. U.S. Patent No. 4,593,053 to Zevner et al discloses the use of skin-friendly, pressure-sensitive hydrogels. Transdemal delivery of drugs delivers hormones such as progesterone, progestin, estrogen, and testosterone into the body through the skin, released only in a controlled amount from the hydrogel attached to the skin and delivered to the body through the percutaneous body. It is a high dosage technique. US Patent No. 6,214,374 to Schiller et al. Discloses a composition, method and apparatus for hydrogels for effective transdermal delivery of drugs without blocking the skin. U.S. Patent No. 5,064,654 to Werner et al discloses the composition of an adhesive hydrogel for transdermal delivery of drugs. US Pat. No. 4,942,158 to Sapota et al. Discloses the composition of hydrogels with penetration enhancers added to enhance transdermal delivery of drugs. In addition, US Pat. Nos. 6,361,790 and 6,406,712 to Rolf et al. Disclose a skin application method such as a dressing and a patch using a hydrogel.
위와 같은 종래의 기술은 모두 하이드로겔을 피부에 적용하고 있으나 겔상태 그대로 유지하면서 기지체인 하이드로겔 속에 함유되어 있는 약물이 피부쪽으로 서서히 방출되도록 조절하는 기능만을 갖고 있는 것에 불과하다.All of the above conventional techniques apply hydrogel to the skin but only have the function of controlling the drug contained in the matrix hydrogel to be released slowly toward the skin while maintaining the gel state.
하이드로젤 마스크는 하이드로젤을 피부에 붙인 후 20 ~ 30분 내의 단시간 이내에 함유된 유효성분이 신속히 피부 속으로 전달될 필요성이 크게 요구되나 이를 위해서는 하이드로젤 내의 유효 성분이 피부 속으로 신속하고 고르게 전달되는 특징을 가져야 한다. 그러나 하이드로젤 상태를 그대로 유지하고 있는 한 젤 속의 유효한 화장 성분이 하이드로젤로부터 피부로 전달되는데 만족할 만한 양과 속도를 가지는 데에 한계를 가지게 됨에 따라 시간이 지나면서 오히려 하이드로젤 내의 수분 및 유효성분이 증발되어 말라버려 효과를 누릴 수 없게 된다. 따라서 하이드로젤이 특유의 부착성과 습윤성이 좋다하여도 하이드로젤 내에 함유되어 있는 유효성분의 함유량의 한계와 더불어 이러한 유효 화장 성분의 피부로의 전달 속도의 한계는 하이드로젤 마스크팩의 피부 침투 효율성에도 한계를 가질 수밖에 없게 되는 것이다.Hydrogel masks are required to quickly deliver the active ingredients contained within a short time within 20 to 30 minutes after attaching the hydrogel to the skin, but for this purpose, active ingredients in the hydrogel are quickly and evenly delivered into the skin. Should have However, as long as it maintains the hydrogel state, the effective cosmetic ingredients in the gel have a limit to having a satisfactory amount and speed to be transferred from the hydrogel to the skin, and as time passes, water and active ingredients in the hydrogel evaporate. It will dry up, leaving you unable to benefit. Therefore, even if the hydrogel has good adhesion and wettability, the limit of the content of the active ingredient contained in the hydrogel and the speed of delivery of the active cosmetic ingredient to the skin are also limited to the skin penetration efficiency of the hydrogel mask pack. Will be forced to have.
또한, 현재 일반적으로 하이드로겔 마스크팩은 카라기난 및 검류에 물과 다가알코올을 첨가 후 60 ~ 85로 가열 교반하여 온도의 변화에 따른 가교 형태를 이루어 겔 형태를 만드는 방법을 사용하여 제조한다. 특히, 하이드로겔 마스크 팩의 경우 면적이 커서 탄력성이 떨어지면 사용하는데 불편하며, 함량을 늘리면 탄력성이 증가하지만 제조시 점도가 높아 불편한 점이 있다. 따라서, 하이드로겔 마스크팩의 제조시 60 이상에서 교반시킨 후 도포해야 하여 고온에 약한 펩타이드류 또는 각종 유효 성분을 사용하는데 제한이 있는 문제점이 있다.In addition, the current hydrogel mask pack is generally prepared by adding a water and polyalcohol to carrageenan and gum and stirring by heating to 60 ~ 85 to form a cross-linked form according to the temperature change to make a gel form. In particular, the hydrogel mask pack is inconvenient to use when the area is large and the elasticity is inconvenient, and the elasticity is increased by increasing the content, but there is an inconvenience in that the viscosity is high during manufacturing. Therefore, when the hydrogel mask pack is prepared at 60 or more after stirring, there is a problem in that it is difficult to use peptides or various active ingredients that are weak at high temperatures.
본 발명은 이와 같은 문제점을 해결하기 위하여 안출된 것으로, 본 발명의 목적은 정제수, 다가알코올, 카라기난, 로커스트빈 검, 잔탄검 및 타마린드씨 검을 함유하는 하이드로겔 마스크팩 조성물로 제조된 성형체에 정제수, 다가 알코올, 천연추출물 및 기능성 첨가제로 이루어진 군으로부터 선택되는 1종 이상을 함유하는 에센스를 첨가하여 하이드로겔 마스크팩을 제조함으로써 강도가 향상되고 온도에 민감한 각종 유효성분들을 첨가할 수 있는 하이드로겔 마스크팩을 제공하는데 있다.The present invention has been made to solve the above problems, the object of the present invention is purified water in a molded article made of a hydrogel mask pack composition containing purified water, polyhydric alcohol, carrageenan, locust bean gum, xanthan gum and tamarind seed gum Hydrogel mask which can add various active ingredients which are enhanced in strength by adding a essence containing at least one selected from the group consisting of polyhydric alcohols, natural extracts and functional additives to produce a hydrogel mask pack. To provide a pack.
이를 위하여 본 발명은 정제수, 카라기난, 로커스트빈 검, 잔탄검 및 타마린드씨검을 함유하는 하이드로겔 조성물을 제공한다.To this end, the present invention provides a hydrogel composition containing purified water, carrageenan, locust bean gum, xanthan gum and tamarind seed gum.
본 발명의 바람직한 일실시예에 있어서, 상기 하이드로겔 마스크팩 조성물은 다가알코올을 더 함유할 수 있다.In a preferred embodiment of the present invention, the hydrogel mask pack composition may further contain a polyhydric alcohol.
본 발명의 바람직한 일실시예에 있어서, 상기 다가알코올은 부틸렌글리콜, 폴리에틸렌 글리콜, 글리세린, 에탄올, 솔비톨 및 트레할로스로 이루어진 군으로부터 선택되는 1종 이상을 포함할 수 있다.In a preferred embodiment of the present invention, the polyhydric alcohol may include one or more selected from the group consisting of butylene glycol, polyethylene glycol, glycerin, ethanol, sorbitol and trehalose.
본 발명의 바람직한 일실시예에 있어서, 상기 하이드로겔 마스크팩 조성물은 정제수 90 ~ 99 중량%, 카라기난 0.1 ~ 2 중량%, 로커스트빈 검 0.1 ~ 2 중량%, 잔탄검 0.1 ~ 1 중량% 및 타마린드씨검 0.005 ~ 7 중량%를 함유할 수 있다.In a preferred embodiment of the present invention, the hydrogel mask pack composition is purified water 90 to 99% by weight, carrageenan 0.1 to 2% by weight, locust bean gum 0.1 to 2% by weight, xanthan gum 0.1 to 1% by weight and tamarind Sea gum may contain 0.005 to 7% by weight.
본 발명의 바람직한 일실시예에 있어서, 상기 하이드로겔 마스크팩 조성물은 다가알코올 0.1 ~ 10 중량%을 더 함유할 수 있다.In a preferred embodiment of the present invention, the hydrogel mask pack composition may further contain 0.1 to 10% by weight of polyhydric alcohol.
본 발명의 다른 태양은 상기 하이드로겔 마스크팩 조성물의 성형체를 포함하는 것을 특징으로 하는 하이드로겔 마스크팩을 제공한다.Another aspect of the present invention provides a hydrogel mask pack comprising a molded body of the hydrogel mask pack composition.
본 발명에 있어서, 상기 성형체란, 상기 정제수, 카라기난, 로커스트빈 검, 잔탄검 및 타마린드씨검을 함유하는 하이드로겔 마스크팩 조성물을 가열 및 냉각하여 제조된 마스크 형태의 성형물을 의미한다. In the present invention, the molded product means a molded product in the form of a mask prepared by heating and cooling the hydrogel mask pack composition containing the purified water, carrageenan, locust bean gum, xanthan gum and tamarind seed gum.
본 발명의 바람직한 일실시예에 있어서, 상기 성형체 100 중량부에 대하여 정제수, 다가 알코올 및 천연추출물로 이루어진 군으로부터 선택되는 1종 이상을 함유하는 에센스 30 ~ 70 중량부를 포함할 수 있다.In a preferred embodiment of the present invention, it may include 30 to 70 parts by weight of the essence containing one or more selected from the group consisting of purified water, polyhydric alcohol and natural extracts based on 100 parts by weight of the molded body.
본 발명의 바람직한 일실시예에 있어서, 상기 에센스는 정제수 100 중량부에 대해서, 다가알코올 40 ~ 300 중량부를 함유할 수 있다.In one preferred embodiment of the present invention, the essence may contain 40 to 300 parts by weight of polyhydric alcohol with respect to 100 parts by weight of purified water.
본 발명의 바람직한 일실시예에 있어서, 상기 다가 알코올은 글리세린 및 부틸렌 글라이콜을 1:0.1 ~ 2.5의 중량비로 포함할 수 있다.In a preferred embodiment of the present invention, the polyhydric alcohol may include glycerin and butylene glycol in a weight ratio of 1: 0.1 to 2.5.
본 발명의 바람직한 일실시예에 있어서, 상기 성형체에 포함된 타마린드씨 검과 에센스에 포함된 다가알코올을 1: 20 ~ 80의 중량비로 포함할 수 있다.In a preferred embodiment of the present invention, the tamarind seed gum and the polyhydric alcohol contained in the essence may be included in the weight ratio of 1: 20 to 80.
본 발명의 바람직한 일실시예에 있어서, 상기 에센스는 정제수 100 중량부에 대해서, 천연추출물 0.01 ~ 20 중량부를 함유할 수 있다.In one preferred embodiment of the present invention, the essence may contain 0.01 to 20 parts by weight of natural extract, based on 100 parts by weight of purified water.
본 발명의 바람직한 일실시예에 있어서, 상기 에센스는 정제수 100 중량부에 대해서, 기능성 첨가제 0.001 ~ 20 중량부를 함유할 수 있다.In a preferred embodiment of the present invention, the essence may contain 0.001 to 20 parts by weight of the functional additive, based on 100 parts by weight of purified water.
본 발명의 바람직한 일실시예에 있어서, 상기 천연추출물은 녹차추출물, 감초추출물, 닥나무추출물, 상백피추출물, 황금추출물, 푸에리라리아추출물, 홍삼추출물, 살구추출물, 오일추출물, 오렌지추출물, 레몬추출물, 대나무추출물, 구아바추출물, 로즈마리추출물, 산수유추출물, 영지추출물, 은행추출물, 서시옥욕산추출물, 자음단추출물, 모과추출물, 백련초추출물, 파프리카추출물, 알로에추출물, 수세미추출물, 해초추출물, 당근추출물, 대두추출물, 자몽씨추출물, 포도씨추출물, 마치현추출물, 캐비어추출물, 석류추출물, 인삼추출물, 복숭아추출물, 천궁추출물, 병풀추출물, 캐모마일추출물, 자초근추출물, 고삼추출물, 당귀추출물, 박하추출물, 삼백초추출물, 어성초추출물, 작약추출물, 목초액, 민들레추출물, 카렌듈라추출물, 황백피추출물, 탱자추출물, 황금추출물, 회향추출물, 컴푸리추출물, 율피추출물, ROE(로즈마리오일추출물) 및 자몽씨추출물로 이루어진 군으로부터 선택되는 1종 이상을 포함할 수 있다.In a preferred embodiment of the present invention, the natural extract is green tea extract, licorice extract, medicinal extract of green tea, extract of baekryeok, golden extract, pueraria extract, red ginseng extract, apricot extract, oil extract, orange extract, lemon extract, Bamboo Extract, Guava Extract, Rosemary Extract, Cornus Extract, Ganoderma Lucidum Extract, Ginkgo Extract, Seosiokyuksan Extract, Consonant Extract, Chinese Quince Extract, White Lotus Extract, Paprika Extract, Aloe Extract, Scrubber Extract, Seaweed Extract, Grapefruit Extract, Carrot Extract Seed Extract, Grape Seed Extract, March Extract, Caviar Extract, Pomegranate Extract, Ginseng Extract, Peach Extract, Cheongung Extract, Centella asiatica Extract, Chamomile Extract, Licorice Root Extract, High Ginseng Extract, Angelica Extract, Peppermint Extract, Sambaekcho Extract, Crop Extract , Vinegar extract, dandelion extract, calendula extract, yellow white skin extract, tang It may include extract, Gold extract, fennel extract, com Puri extract, yulpi extract, ROE (rosemary oil extract) and at least one member selected from the group consisting of grapefruit seed extract.
본 발명의 바람직한 일실시예에 있어서, 상기 기능성 첨가제는 글리세린, 판테놀, 히아루론산, 세라마이드, 베타글루칸, 알부틴, 비타민C, 화이텐스, 레티놀, 엘라스틴, 콜라겐, 코엔자임Q10, 이펙틴, EGF, 프로폴리스, 알란토인, 피토스탄, 인프라산 및 항산화제 비타민E(천연토코페롤)으로 이루어진 군으로부터 선택되는 1종 이상을 포함할 수 있다.In a preferred embodiment of the present invention, the functional additive is glycerin, panthenol, hyaluronic acid, ceramide, beta glucan, arbutin, vitamin C, whitens, retinol, elastin, collagen, coenzyme Q10, effectin, EGF, propolis, It may include one or more selected from the group consisting of allantoin, phytostane, infraacid and antioxidant vitamin E (natural tocopherol).
본 발명의 바람직한 일실시예에 있어서, 상기 기능성 첨가제는 펩타이드를 더 함유하고, 상기 펩타이드는 rh-Polypeptide-64, rh-Oligopeptide-33, sh-oligopeptide-1, sh-Polypeptide-11, sh-Polypeptide-1, rh-Polypeptide-7, rh-Polypeptide-62, rh-Oligopeptide-2, sh-Polypeptide-31, rh-Polypeptide-3, rh-Polypeptide-14, sh-Polypeptide-13, rh-Polypeptide-8, sh-Polypeptide-59, sh-Polypeptide-16, rh-Polypeptide-4, rh-Polypeptide-66, rh-Polypeptide-67, rh-Polypeptide-60, rh-Polypeptide-51, rh-Polypeptide-58, sh-Polypeptide-19, sh-Polypeptide-22, sh-Polypeptide-5, rh-Polypeptide-33, rh-Oligopeptide-4, 및 rh-Polypeptide-9으로 이루어진 군으로부터 선택되는 1종 이상일 수 있다.In a preferred embodiment of the present invention, the functional additive further contains a peptide, the peptide is rh-Polypeptide-64, rh-Oligopeptide-33, sh-oligopeptide-1, sh-Polypeptide-11, sh-Polypeptide -1, rh-Polypeptide-7, rh-Polypeptide-62, rh-Oligopeptide-2, sh-Polypeptide-31, rh-Polypeptide-3, rh-Polypeptide-14, sh-Polypeptide-13, rh-Polypeptide-8 , sh-Polypeptide-59, sh-Polypeptide-16, rh-Polypeptide-4, rh-Polypeptide-66, rh-Polypeptide-67, rh-Polypeptide-60, rh-Polypeptide-51, rh-Polypeptide-58, sh At least one member selected from the group consisting of -Polypeptide-19, sh-Polypeptide-22, sh-Polypeptide-5, rh-Polypeptide-33, rh-Oligopeptide-4, and rh-Polypeptide-9.
본 발명의 바람직한 일실시예에 있어서, 상기 하이드로겔 마스크팩의 열단장은 3 ~ 4 m일 수 있다.In a preferred embodiment of the present invention, the thermal shortening of the hydrogel mask pack may be 3 ~ 4 m.
본 발명의 바람직한 일실시예에 있어서, 상기 하이드로겔 마스크팩의 비파열강도는 6 ~ 7 kg/cm2 일 수 있다.In one preferred embodiment of the present invention, the non-rupture strength of the hydrogel mask pack is 6 ~ 7 kg / cm 2 Can be.
본 발명의 또 다른 태양은 상기 하이드로겔 마스크팩 조성물을 혼합하여 혼합물을 제조하는 1단계; 상기 1단계에서 제조된 혼합물을 60 ~ 90℃로 가열한 후 박막 위에 도포하는 2단계; 상기 2단계에서 박막 위에 도포된 혼합물을 냉각 및 건조하여 성형체를 제조하는 3단계; 상기 성형체를 마스크 형태로 재단하는 4단계; 및 상기 마스크 형태의 성형체에 정제수, 다가 알코올, 천연추출물 및 기능성 첨가제로 이루어진 군으로부터 선택되는 1종 이상을 함유하는 에센스를 충진하는 5단계; 를 포함하는 하이드로겔 마스크팩의 제조방법을 제공한다.Another aspect of the present invention is a step of preparing a mixture by mixing the hydrogel mask pack composition; Heating the mixture prepared in step 1 to 60 to 90 ° C. and then applying the same on a thin film; Step 3 of producing a molded body by cooling and drying the mixture applied on the thin film in the step 2; 4 steps of cutting the molded body in the form of a mask; And a step 5 of filling the molded article in the mask form with an essence containing at least one selected from the group consisting of purified water, polyhydric alcohol, natural extracts and functional additives; It provides a method of manufacturing a hydrogel mask pack comprising a.
본 발명의 바람직한 일실시예에 있어서, 상기 2단계에서 혼합물을 랩코팅 방법으로 박막 위에 500 ~ 2000 ㎛ 두께로 도포할 수 있다.In a preferred embodiment of the present invention, the mixture in the second step may be applied to the thin film 500 ~ 2000 ㎛ thickness by a wrap coating method.
본 발명의 바람직한 일실시예에 있어서, 상기 3단계에서 박막 위에 도포된 혼합물을 0 ~ 30℃로 냉각할 수 있다.In a preferred embodiment of the present invention, the mixture applied on the thin film in the third step may be cooled to 0 ~ 30 ℃.
본 발명의 바람직한 일실시예에 있어서, 상기 3단계에서 박막 위에 도포된 혼합물을 70 ~ 110℃에서 건조할 수 있다.In a preferred embodiment of the present invention, the mixture applied on the thin film in the third step may be dried at 70 ~ 110 ℃.
본 발명의 바람직한 일실시예에 있어서, 상기 3단계에서 제조된 성형체는 두께가 100 ~ 1000 ㎛일 수 있다.In one preferred embodiment of the present invention, the molded article prepared in step 3 may have a thickness of 100 ~ 1000 ㎛.
본 발명에 따른 하이드로겔 마스크팩은 타마린드씨 검과 다가알코올이 가지는 탈수작용에 의해 타마린드씨 검의 분자가 응집함으로써 수소결합이 형성되어 겔화가 나타날 수 있으므로 이를 통해 하이드로겔의 강도를 향상시킨 하이드로겔 마스크팩을 제조할 수 있다. 상기와 같은 방법으로 겔화하는 경우 에센스에 온도에 민감한 유효성분을 추가할 수 있어 기능성 하이드로겔 마스크팩을 제조할 수 있다.In the hydrogel mask pack according to the present invention, due to the dehydration action of tamarind seed gum and polyhydric alcohol, hydrogen bonds are formed by agglomeration of molecules of tamarind seed gum, which may result in gelation, thereby improving the strength of the hydrogel. Hydrogel mask pack can be prepared. When gelling in the same manner as described above can be added to the active ingredient sensitive to temperature in the essence can be prepared a functional hydrogel mask pack.
본 발명은 타마린드씨 검을 포함하는 하이드로겔 조성물, 이를 통해 제조된 하이드로겔 마스크팩 및 이의 제조방법에 관한 것으로, 보다 상세하게는 하이드로겔 마스크팩의 조성물로서 타마린드씨검 및 에센스를 포함하여 마스크팩의 강도가 향상될 수 있는 하이드로겔 마스크팩 조성물 및 이를 이용한 하이드로겔 마스크팩의 제조방법에 관한 것이다.The present invention relates to a hydrogel composition comprising tamarind seed gum, a hydrogel mask pack prepared through the same, and a method for preparing the same, and more particularly, a mask including tamarind seed gum and an essence as a composition of a hydrogel mask pack. The present invention relates to a hydrogel mask pack composition and a method of manufacturing a hydrogel mask pack using the same, in which the strength of the pack can be improved.
이에, 본 발명은 정제수, 카라기난, 로커스트빈 검, 잔탄검 및 타마린드씨 검을 함유하는 하이드로겔 조성물을 제공한다. 이하, 본 발명을 구성 성분 별로 보다 상세하게 설명한다.Accordingly, the present invention provides a hydrogel composition containing purified water, carrageenan, locust bean gum, xanthan gum and tamarind seed gum. Hereinafter, the present invention will be described in more detail for each component.
본 발명에 따른 하이드로겔 조성물은 정제수, 카라기난, 로커스트빈검, 잔탄검 및 타마린드씨 검을 함유함으로써, 혼합되어 가열된 후 냉각되면서 겔 상태로 제조될 수 있다.The hydrogel composition according to the present invention can be prepared in a gel state by mixing, heating and cooling by containing purified water, carrageenan, locust bean gum, xanthan gum and tamarind seed gum.
본 발명에 따른 하이드로겔 조성물은 다가알코올을 더 함유할 수 있고, 상기 타마린드씨 검이 다가알코올과 혼합되어 탈수 작용이 일어나고 타마린드씨검의 분자가 응집함으로써 증점 및 겔화가 수행되므로, 상기 하이드로겔 조성물로부터 피부에 탈착가능한 하이드로겔 마스크팩의 성형체를 제조할 수 있다.The hydrogel composition according to the present invention may further contain a polyhydric alcohol, and the tamarind seed gum is mixed with the polyhydric alcohol to cause dehydration, and the thickening and gelation of the tamarind seed gum are carried out, so that the hydrolysis is performed. A molded article of the hydrogel mask pack detachable to the skin can be prepared from the gel composition.
이때 상기 다가알코올은 부틸렌 글리콜, 폴리에틸렌 글리콜, 글리세린, 에탄올, 솔비톨 및 트레할로스로 이루어진 군으로부터 선택되는 1종 이상을 포함할 수 있고, 바람직하게는 부틸렌 글리콜, 폴리에틸렌 글리콜 및 글리세린으로 이루어진 군으로부터 선택되는 1종 이상인 것이 좋다.At this time, the polyhydric alcohol may include at least one selected from the group consisting of butylene glycol, polyethylene glycol, glycerin, ethanol, sorbitol and trehalose, preferably selected from the group consisting of butylene glycol, polyethylene glycol and glycerin It is good that it is 1 or more types.
이때, 상기 정제수는 상기 카라기난, 로커스트빈 검, 잔탄검 및 타마린드씨 검 등을 용해하고 수분을 공급하기 위하여 포함되는 것으로 90 ~ 99 중량%로 포함되는 것이 바람직하며, 더욱 바람직하게는 95 ~ 99 중량%로 포함되는 것이 좋다. 상기 카라기난, 로커스트빈 검, 잔탄검 및 타마린드씨 검은 겔화되어 상온에서 하이드로겔 마스크팩의 형태를 유지할 수 있도록 포함되며, 카라기난 0.1 ~ 2중량%, 로커스트빈 검 0.1 ~ 2 중량%, 잔탄검 0.1 ~ 1 중량% 및 타마린드씨검 0.005 ~ 7 중량%로 포함되는 것이 바람직하고, 더욱 바람직하게는 카라기난 0.5 ~1.5 중량%, 로커스트빈 검 0.5 ~ 1.5 중량%, 잔탄검 0.3 ~ 0.8 중량% 및 타마린드씨검 0.01 ~ 3 중량%인 것이 좋다. 상기 하이드로겔 조성물이 상기 범위를 벗어나는 경우 상기 조성물을 통해 제조되는 성형체의 강도가 저하되는 문제점이 있다.At this time, the purified water is included to dissolve the carrageenan, locust bean gum, xanthan gum and tamarind seed gum and supply water, preferably 90 to 99% by weight, more preferably 95 to 99 It is preferably included in weight percent. The carrageenan, locust bean gum, xanthan gum and tamarind seed black gelled to maintain the form of the hydrogel mask pack at room temperature, carrageenan 0.1 ~ 2% by weight, locust bean gum 0.1 ~ 2% by weight, xanthan gum 0.1 It is preferable to include from 1% by weight to 0.005 to 7% by weight of tamarind seed gum, more preferably 0.5 to 1.5% by weight of carrageenan, 0.5 to 1.5% by weight of locust bean gum, 0.3 to 0.8% by weight of xanthan gum and tama Lind Seagum is preferably 0.01 to 3% by weight. If the hydrogel composition is out of the range, there is a problem that the strength of the molded body produced through the composition is lowered.
또한, 상기 다가알코올은 선택적으로 첨가 가능하고, 상기 카라기난, 로커스트빈 검, 잔탄검 및 타마린드씨 검 등의 검류와 혼합되는 경우 탈수반응을 일으켜 상기 조성물들의 겔화를 돕는 역할을 하며, 0.1 ~ 10 중량%로 포함되는 것이 바람직하고, 더욱 바람직하게는 0.1 ~ 5 중량%로 포함되는 것이 좋다.In addition, the polyhydric alcohol may be selectively added, and when mixed with gums such as carrageenan, locust bean gum, xanthan gum, and tamarind seed gum, dehydration reactions serve to help gel the compositions, and 0.1 to 10 It is preferably included in the weight%, more preferably 0.1 to 5% by weight.
상기 하이드로겔 조성물의 성형체를 포함하는 하이드로겔 마스크팩을 제공한다. 상기 하이드로겔 조성물을 혼합한 후 가열하고 냉각하는 과정에서 겔화됨으로써 성형체를 제조할 수 있고, 상기 성형체에 정제수, 다가 알코올 및 천연추출물로 이루어진 군으로부터 선택되는 1종 이상을 함유하는 에센스를 더 포함할 수 있다.It provides a hydrogel mask pack comprising a molded body of the hydrogel composition. The hydrogel composition may be gelled in the process of mixing the hydrogel composition and then heating and cooling, and may further include an essence containing the at least one selected from the group consisting of purified water, polyhydric alcohol, and natural extract. Can be.
이때, 상기 성형체 100 중량부에 대하여 정제수, 다가 알코올, 천연추출물 및 기능성 첨가제로 이루어진 군으로부터 선택되는 1종 이상을 함유하는 에센스 20 ~ 80 중량부를 포함하는 것이 바람직하다. 상기 에센스가 하이드로겔 조성물의 성형체 100 중량부에 대하여 20 중량부 미만으로 포함되는 경우 타마린드의 다가알코올에 의한 가교가 약하여 강도가 낮아지는 문제점이 있고, 80 중량부를 초과하는 경우 끈적이고 사용감이 떨어지는 문제점이 있다.At this time, it is preferable to include 20 to 80 parts by weight of an essence containing one or more selected from the group consisting of purified water, polyhydric alcohol, natural extracts and functional additives based on 100 parts by weight of the molded body. When the essence is included in less than 20 parts by weight with respect to 100 parts by weight of the molded article of the hydrogel composition, there is a problem that the strength is lowered due to weak crosslinking by polyhydric alcohol of tamarind. There is a problem.
본 발명에 따른 하이드로겔 마스크팩 조성물에 있어서, 상기 에센스는 정제수 100 중량부에 대해서, 다가알코올 40 ~ 300 중량부를 함유하는 것이 바람직하다. 이때, 상기 정제수는 하이드로겔 마스크팩에서 수분을 공급하기 위하여 포함되는 것이고, 다가알코올은 하이드로겔 조성물로부터 제조된 성형체에 포함되는 타마린드씨 검의 분자와 혼합되어 탈수 작용이 일어날 수 있어 증점 및 겔화가 추가적으로 수행되므로, 새로운 가교방식으로 하이드로겔 마스크팩의 강도를 향상시키는 역할을 할 수 있다. 상기 다가 알코올이 상기 범위를 벗어나도록 포함되는 경우에는 마스크팩의 강도가 충분히 향상되기 어려운 문제점이 있다.In the hydrogel mask pack composition according to the present invention, the essence preferably contains 40 to 300 parts by weight of polyhydric alcohol with respect to 100 parts by weight of purified water. At this time, the purified water is included to supply water in the hydrogel mask pack, the polyhydric alcohol is mixed with the molecules of tamarind seed gum contained in the molded body prepared from the hydrogel composition may cause dehydration and thickening and gelation Since it is additionally carried out, it may serve to improve the strength of the hydrogel mask pack in a new crosslinking method. When the polyhydric alcohol is included to be out of the range, there is a problem that the strength of the mask pack is not sufficiently improved.
이때, 상기 다가알코올은 글리세린 및 부틸렌 글라이콜을 포함할 수 있고, 바람직하게는 1: 0.1 ~ 2.5의 중량비로 포함되는 것이 좋고, 더욱 바람직하게는 1:0.5 ~ 2의 중량비로 포함되는 것이 좋다.In this case, the polyhydric alcohol may include glycerin and butylene glycol, preferably contained in a weight ratio of 1: 0.1 to 2.5, and more preferably included in a weight ratio of 1: 0.5 to 2 good.
또한, 본 발명에 따른 하이드로겔 마스크팩은 상기 성형체에 포함된 타마린드씨검과 에센스에 포함된 다가알코올을 1: 20 ~ 80의 중량부로 포함하는 것이 바람직하고, 더욱 바람직하게는 1 : 30 ~ 60 의 중량부로 포함하는 것이 좋다.In addition, the hydrogel mask pack according to the present invention preferably comprises tamarind seed gum and polyhydric alcohols contained in the essence in a weight part of 1: 20 ~ 80, more preferably 1: 30 ~ It is preferably included in 60 parts by weight.
본 발명에 따른 하이드로겔 마스크팩 조성물에 있어서, 상기 에센스는 정제수 100 중량부에 대해서, 천연추출물 0.01 ~ 20 중량부를 함유할 수 있다.In the hydrogel mask pack composition according to the present invention, the essence may contain 0.01 to 20 parts by weight of the natural extract with respect to 100 parts by weight of purified water.
상기 천연 추출물은 피부에 공급되는 유효성분을 제공할 수 있다.The natural extract can provide an active ingredient that is supplied to the skin.
상기 천연추출물은 피부에 공급될 수 있는 유효성분으로서 포함되는 것이라면 어느 것이든 사용가능하고, 바람직하게는 녹차추출물, 감초추출물, 닥나무추출물, 상백피추출물, 황금추출물, 푸에리라리아추출물, 홍삼추출물, 살구추출물, 오일추출물, 오렌지추출물, 레몬추출물, 대나무추출물, 구아바추출물, 로즈마리추출물, 산수유추출물, 영지추출물, 은행추출물, 서시옥욕산추출물, 자음단추출물, 모과추출물, 백련초추출물, 파프리카추출물, 알로에추출물, 수세미추출물, 해초추출물, 당근추출물, 대두추출물, 자몽씨추출물, 포도씨추출물, 마치현추출물, 캐비어추출물, 석류추출물, 인삼추출물, 복숭아추출물, 천궁추출물, 병풀추출물, 캐모마일추출물, 자초근추출물, 고삼추출물, 당귀추출물, 박하추출물, 삼백초추출물, 어성초추출물, 작약추출물, 목초액, 민들레추출물, 카렌듈라추출물, 황백피추출물, 탱자추출물, 황금추출물, 회향추출물, 컴푸리추출물, 율피추출물, ROE(로즈마리오일추출물) 및 자몽씨추출물로 이루어진 군으로부터 선택되는 1종 이상을 포함할 수 있다.The natural extract can be used as long as it is included as an active ingredient that can be supplied to the skin, preferably green tea extract, licorice extract, gingko extract, lettuce extract, golden extract, pueraria extract, red ginseng extract, Apricot Extract, Oil Extract, Orange Extract, Lemon Extract, Bamboo Extract, Guava Extract, Rosemary Extract, Cornus Extract, Ganoderma lucidum Extract, Ginkgo Extract, Seogyok Oksan Acid Extract, Consonant Extract, Chinese Quince Extract, White Lotus Extract, Paprika Extract, Aloe Water Extract, Aloe Sea Extract Extract, Seaweed Extract, Carrot Extract, Soybean Extract, Grapefruit Seed Extract, Grape Seed Extract, March Extract, Caviar Extract, Pomegranate Extract, Ginseng Extract, Peach Extract, Cheongung Extract, Centella Extract, Chamomile Extract, Herbal Root Extract, Ginseng Extract , Peppermint extract, triticale extract, fish extract, peony extract , Wood vinegar, dandelion extract, calendula extract, yellowish white extract, tanza extract, golden extract, fennel extract, extract extract, yulpi extract, ROE (rosemary oil extract) and grapefruit seed extract Can be.
본 발명에 따른 하이드로겔 마스크팩 조성물에 있어서, 상기 에센스는 정제수 100 중량부에 대해서, 기능성 첨가제 0.001 ~ 20 중량부를 함유할 수 있고, 바람직하게는 0.01 ~ 10 중량부를 함유할 수 있다. 상기 기능성 첨가제는 피부에 공급되는 유효성분을 제공할 수 있고, 상기 기능성 첨가제가 0.001 중량부 미만으로 포함되는 경우에는 피부에 공급될 수 있는 유효성분이 적어 기능성이 저하되는 문제점이 있고, 20 중량부를 초과하는 경우에는 필요 이상으로 과량 포함되어 단가가 상승하는 문제점이 있다.In the hydrogel mask pack composition according to the present invention, the essence may contain 0.001 to 20 parts by weight of functional additives, preferably 0.01 to 10 parts by weight with respect to 100 parts by weight of purified water. The functional additive may provide an active ingredient to be supplied to the skin, and when the functional additive is included in less than 0.001 part by weight, there is a problem in that the functional ingredient is lowered due to less active ingredient to be supplied to the skin, and more than 20 parts by weight. In this case, there is a problem that the unit price is increased because it is included in excess.
상기 기능성 첨가제는 글리세린, 판테놀, 히아루론산, 세라마이드, 베타글루칸, 알부틴, 비타민C, 화이텐스, 레티놀, 엘라스틴, 콜라겐, 코엔자임Q10, 이펙틴, EGF, 프로폴리스, 알란토인, 피토스탄, 인프라산 및 항산화제 비타민E(천연토코페롤)으로 이루어진 군으로부터 선택되는 1종 이상을 포함할 수 있다.The functional additives are glycerin, panthenol, hyaluronic acid, ceramide, beta glucan, arbutin, vitamin C, whitetene, retinol, elastin, collagen, coenzyme Q10, effectin, EGF, propolis, allantoin, phytostane, infraacid and antioxidant It may include one or more selected from the group consisting of vitamin E (natural tocopherol).
이때, 본 발명에 따르면 타마린드씨 검 등의 검류와 다가 알코올 사이의 탈수작용을 통한 겔화가 이루어지므로 고온으로 가온하지 않아도 되므로, 온도에 약한 유효성분을 추가하는 데 제한이 없고, 이로 인해 온도에 민감한 펩타이드 류를 첨가할 수 있다. 상기 펩타이드는 rh-Polypeptide-64, rh-Oligopeptide-33, sh-oligopeptide-1, sh-Polypeptide-11, sh-Polypeptide-1, rh-Polypeptide-7, rh-Polypeptide-62, rh-Oligopeptide-2, sh-Polypeptide-31, rh-Polypeptide-3, rh-Polypeptide-14, sh-Polypeptide-13, rh-Polypeptide-8, sh-Polypeptide-59, sh-Polypeptide-16, rh-Polypeptide-4, rh-Polypeptide-66, rh-Polypeptide-67, rh-Polypeptide-60, rh-Polypeptide-51, rh-Polypeptide-58, sh-Polypeptide-19, sh-Polypeptide-22, sh-Polypeptide-5, rh-Polypeptide-33, rh-Oligopeptide-4, rh-Polypeptide-9 등으로 이루어진 군으로부터 선택되는 1종 이상을 포함할 수 있다.At this time, according to the present invention, since the gelation is performed through dehydration between gums such as tamarind seed gum and polyhydric alcohol, it does not need to be heated to a high temperature, and thus there is no limitation in adding a weak active ingredient to temperature, thereby Sensitive peptides can be added. The peptide is rh-Polypeptide-64, rh-Oligopeptide-33, sh-oligopeptide-1, sh-Polypeptide-11, sh-Polypeptide-1, rh-Polypeptide-7, rh-Polypeptide-62, rh-Oligopeptide-2 , sh-Polypeptide-31, rh-Polypeptide-3, rh-Polypeptide-14, sh-Polypeptide-13, rh-Polypeptide-8, sh-Polypeptide-59, sh-Polypeptide-16, rh-Polypeptide-4, rh -Polypeptide-66, rh-Polypeptide-67, rh-Polypeptide-60, rh-Polypeptide-51, rh-Polypeptide-58, sh-Polypeptide-19, sh-Polypeptide-22, sh-Polypeptide-5, rh-Polypeptide It may include one or more selected from the group consisting of -33, rh-Oligopeptide-4, rh-Polypeptide-9 and the like.
본 발명에 따른 하이드로겔 마스크팩의 열단장은 3 ~ 4 m인 것이 바람직하고, 더욱 바람직하게는 3.2 ~ 4인 것이 좋다. 또한, 상기 하이드로겔 마스크팩의 비파열강도는 6 ~ 7 kg/cm2인 것이 바람직하고, 더욱 바람직하게는 6.2~ 7 kg/cm2 인 것이 좋다.The thermal shortening of the hydrogel mask pack according to the present invention is preferably 3-4 m, more preferably 3.2-4. In addition, the non-rupture strength of the hydrogel mask pack is preferably 6 ~ 7 kg / cm 2 , more preferably 6.2 ~ 7 kg / cm 2 It is good.
본 발명은 상기 하이드로겔 마스크팩 조성물을 혼합하여 혼합물을 제조하는 1단계; 상기 1단계에서 제조된 혼합물을 60 ~ 90℃로 가열한 후 박막 위에 도포하는 2단계; 상기 2단계에서 박막 위에 도포된 혼합물을 냉각 및 건조하여 성형체를 제조하는 3단계; 상기 성형체를 마스크 형태로 재단하는 4단계; 및 상기 마스크 형태의 성형체에 정제수, 다가 알코올, 천연추출물 및 기능성 첨가제로 이루어진 군으로부터 선택되는 1종 이상을 함유하는 에센스를 충진하는 5단계; 를 포함하는 하이드로겔 마스크팩의 제조방법을 제공한다. 이하, 본 발명을 단계별로 보다 상세하게 설명한다.The present invention is a step of preparing a mixture by mixing the hydrogel mask pack composition; Heating the mixture prepared in step 1 to 60 to 90 ° C. and then applying the same on a thin film; Step 3 of producing a molded body by cooling and drying the mixture applied on the thin film in the step 2; 4 steps of cutting the molded body in the form of a mask; And a step 5 of filling the molded article in the mask form with an essence containing at least one selected from the group consisting of purified water, polyhydric alcohol, natural extracts and functional additives; It provides a method of manufacturing a hydrogel mask pack comprising a. Hereinafter, the present invention will be described in more detail step by step.
본 발명에 따른 하이드로겔 마스크팩의 제조방법에 있어서, 상기 1단계에서는 정제수, 카라기난, 로커스트빈 검, 잔탄검 및 타마린드씨 검을 혼합한 후 교반하여 혼합물을 제조할 수 있다.In the method of manufacturing a hydrogel mask pack according to the present invention, in the first step, purified water, carrageenan, locust bean gum, xanthan gum and tamarind seed gum may be mixed and stirred to prepare a mixture.
이때, 상기 1단계에서 정제수 90 ~ 99 중량%, 카라기난 0.1 ~ 2 중량%, 로커스트빈 검 0.1 ~ 2 중량%, 잔탄검 0.1 ~ 1 중량% 및 타마린드씨 검 0.005 ~ 7 중량%를 혼합하는 것이 바람직하며, 더욱 바람직하게는 카라기난 0.5 ~ 1.5 중량%, 로커스트빈 검 0.5 ~ 1.5 중량%, 잔탄검 0.3 ~ 0.8 중량% 및 타마린드씨 검 0.01 ~ 3 중량%인 것이 좋다. 상기 하이드로겔 조성물이 상기 범위를 벗어나는 경우 상기 조성물을 통해 제조되는 성형체의 강도가 저하되는 문제점이 있다.At this time, in the step 1 to mix the purified water 90 ~ 99% by weight, carrageenan 0.1 ~ 2% by weight, locust bean gum 0.1 ~ 2% by weight, xanthan gum 0.1 ~ 1% by weight and tamarind seed gum 0.005 ~ 7% by weight Preferably, more preferably, 0.5 to 1.5% by weight of carrageenan, 0.5 to 1.5% by weight of locust bean gum, 0.3 to 0.8% by weight of xanthan gum, and 0.01 to 3% by weight of tamarind seed gum. If the hydrogel composition is out of the range, there is a problem that the strength of the molded body produced through the composition is lowered.
또한, 상기 다가알코올은 선택적으로 첨가 가능하고, 상기 카라기난, 로커스트빈 검, 잔탄검 및 타마린드씨 검 등의 검류와 혼합되는 경우 탈수반응을 일으켜 상기 조성물들의 겔화를 돕는 역할을 하며, 0.1 ~ 10 중량%로 포함되는 것이 바람직하고, 더욱 바람직하게는 0.1 ~ 5 중량%로 포함되는 것이 좋다.In addition, the polyhydric alcohol may be selectively added, and when mixed with gums such as carrageenan, locust bean gum, xanthan gum, and tamarind seed gum, dehydration reactions serve to help gel the compositions, and 0.1 to 10 It is preferably included in the weight%, more preferably 0.1 to 5% by weight.
본 발명에 따른 하이드로겔 마스크팩의 제조방법에 있어서, 상기 2단계에서는 상기 1단계에서 제조된 혼합물을 60 ~ 90℃로 가열한 후 박막 위에 도포할 수 있다. 상기 1단계에서 제조된 혼합물은 졸 상태로 유동성을 나타내며 60 ~ 90℃로 가열한 후 박막 위에 도포한 후 냉각시키는 과정에서 겔화되어 하이드로겔 조성물의 성형체가 필름형태로 제조될 수 있다.In the method of manufacturing a hydrogel mask pack according to the present invention, in the second step, the mixture prepared in the first step may be applied to a thin film after heating to 60 ~ 90 ℃. The mixture prepared in step 1 shows fluidity in a sol state and is heated to 60 to 90 ° C., then coated on a thin film, and then gelled in the course of cooling to form a molded article of the hydrogel composition in a film form.
본 발명에 따른 하이드로겔 마스크팩의 제조방법에 있어서, 상기 3단계에서는 상기 2단계에서 박막 위에 도포된 혼합물을 냉각 및 건조하여 성형체를 제조할 수 있다. 이때, 상기 박막 위에 도포된 혼합물은 졸 상태로 유동성을 나타내며 60 ~ 90℃로 가열한 후 박막 위에 도포하여 냉각시키는 과정에서 겔화되어 하이드로겔 마스크팩 조성물의 성형체가 500 ㎛ ~ 2000 ㎛ 두께의 필름형태로 제조될 수 있고, 이후 냉각 및 건조를 거치면서 100 ~ 1000 ㎛ 두께의 필름형태로 압축될 수 있다.In the method of manufacturing a hydrogel mask pack according to the present invention, in the third step, the molded product may be manufactured by cooling and drying the mixture applied on the thin film in the second step. At this time, the mixture applied on the thin film is fluidized in a sol state and heated to 60 ~ 90 ℃ and then gelled in the process of coating on the thin film to cool the molded article of the hydrogel mask pack composition is 500 ㎛ ~ 2000 ㎛ thick film form It may be prepared as, and then compressed into a film having a thickness of 100 ~ 1000 ㎛ through cooling and drying.
이때, 상기 3단계에서 박막 위에 도포된 혼합물을 0 ~ 3℃0에서 냉각하는 것이 바람직하고, 더욱 바람직하게는 10 ~ 25℃에서 냉각하는 것이 좋으나, 상기 혼합물을 냉각시켜 성형체를 제조할 수 있다면 이에 특별히 한정되는 것은 아니다.At this time, it is preferable to cool the mixture applied on the thin film in step 3 at 0 ~ 3 ℃ 0, and more preferably at 10 ~ 25 ℃, but if the mixture can be cooled to prepare a molded article It is not specifically limited.
또한, 상기 3단계에서 박막 위에 도포된 혼합물을 70 ~ 110℃에서 건조하는 것이 바람직하고, 더욱 바람직하게는 80 ~ 100℃에서 건조하는 것이 좋다. 70℃ 미만으로 건조하는 경우 건조시간이 길어지는 문제점이 있고, 110℃를 초과하여 건조하는 경우 과도하게 가온되어 성형체가 손상될 수 있는 문제점이 있다.In addition, it is preferable to dry the mixture applied on the thin film in the step 3 at 70 ~ 110 ℃, more preferably at 80 ~ 100 ℃. If the drying time is less than 70 ℃ has a problem that the drying time is long, there is a problem that the molded body may be damaged by being excessively heated when drying over 110 ℃.
본 발명에 따른 하이드로겔 마스크팩 조성물에 있어서, 상기 4단계에서는 상기 성형체를 마스크 형태로 재단하여 시착가능한 형태로 제조할 수 있다.In the hydrogel mask pack composition according to the invention, in the fourth step it can be manufactured in a form that can be tried by cutting the molded body in the form of a mask.
상기 마스크 형태로 재단된 성형체는 이후의 단계에서 에센스를 도포함으로써 하이드로겔 마스크팩을 제조할 수 있다.The molded article cut in the form of the mask can be produced hydrogel mask pack by applying the essence in a later step.
본 발명에 따른 하이드로겔 마스크팩의 제조방법에 있어서, 상기 5단계에서는 마스크 형태의 성형체에 정제수, 다가 알코올, 천연추출물 및 기능성 첨가제로 이루어진 군으로부터 선택되는 1종 이상을 함유하는 에센스를 도포할 수 있다.In the method of manufacturing a hydrogel mask pack according to the present invention, in step 5, an essence containing at least one selected from the group consisting of purified water, polyhydric alcohol, natural extracts and functional additives may be applied to the molded article in the form of a mask. have.
종래의 하이드로겔 마스크팩의 제조방법에 따르면, 하이드로겔 마스크팩을 만들기 위하여 고온으로 가온하는 과정이 필요하며 60 ~ 90℃로 가열하므로, 온도에 약한 유효성분을 추가하는 데 제한이 있었다. 그러나, 본 발명에 따르면 가열된 후 냉각되어 제조된 겔 형태의 성형체에 다가알코올을 함유하는 에센스를 충진함으로써, 강도가 향상되고, 동시에 온도에 민감한 펩타이드 류를 첨가할 수 있는 장점이 있다. 보다 상세하게는, 상기 에센스가 하이드로겔 마스크팩 조성물의 성형체 상에 충진됨으로써 하이드로겔 마스크팩 구조체에 포함된 타마린드씨 검의 -OH 기와 다가알코올의 수소결합에 의해 겔화가 이루어지므로 강도가 더욱 향상되며, 에센스에 온도에 약한 유효성분을 추가하는 데 제한이 없고 온도에 민감한 펩타이드 류를 첨가할 수 있다.According to the conventional method of manufacturing a hydrogel mask pack, a process of heating to high temperature is required in order to make a hydrogel mask pack and is heated to 60 ~ 90 ℃, there was a limit to adding a weak active ingredient to the temperature. However, according to the present invention, by filling an essence containing polyhydric alcohol in a gel-shaped molded article prepared by heating and cooling, strength is improved, and at the same time, a peptide sensitive to temperature can be added. More specifically, since the essence is filled on the molded body of the hydrogel mask pack composition, gelation is performed by hydrogen bonding of -OH group and polyhydric alcohol of tamarind gum included in the hydrogel mask pack structure to further improve strength. In addition, there is no limitation in adding an active ingredient having a weak temperature to the essence, and temperature sensitive peptides can be added.
이하, 본 발명을 하기 실시예를 통해 보다 상세하게 설명한다. 하기 실시예는 본 발명을 예시하기 위하여 제시되는 것이며, 본 발명의 권리범위가 이에 한정되는 것은 아니다.Hereinafter, the present invention will be described in more detail with reference to the following examples. The following examples are presented to illustrate the present invention, but the scope of the present invention is not limited thereto.
[[ 실시예Example ]]
실시예Example 1.  One. 하이드로겔Hydrogel 마스크팩의Mask pack 제조 1 Manufacture 1
정제수 96.7 g, 카라기난 0.9 g, 로커스트빈 검 1.2 g, 잔탄검 0.9 g 및 타마린드씨 검 0.3 g 을 혼합한 후 교반기를 이용하여 250 rpm으로 180 분간 교반하여 혼합물을 제조한 후, 80℃로 가열하고, 상기 가열된 혼합물을 랩코터를 이용하여 박막 위에 700 ㎛ 두께로 도포하였다. 이후, 25℃에서 냉각하여 성형체를 제조하였다. 상기 성형체를 마스크 형태로 재단한 후, 정제수 39.99 g, 글리세린 20 g, 부틸렌 글라이콜 40 g 및 sh-oligopeptide-1 0.01 g을 혼합하여 제조한 에센스를 15 ml 충진하여 하이드로겔 마스크팩을 완성하였다.96.7 g of purified water, 0.9 g of carrageenan, 1.2 g of locust bean gum, 0.9 g of xanthan gum and 0.3 g of tamarind seed gum were mixed, and then stirred at 250 rpm for 180 minutes using a stirrer to prepare a mixture, which was then heated to 80 ° C. The heated mixture was applied to the thin film using a lab coater to a thickness of 700 μm. Then, it cooled at 25 degreeC and manufactured the molded object. After cutting the molded product in the form of a mask, 15 ml of an essence prepared by mixing 39.99 g of purified water, 20 g of glycerin, 40 g of butylene glycol, and 0.01 g of sh-oligopeptide-1 was filled to complete the hydrogel mask pack. It was.
실시예Example 2 ~  2 to 실시예Example 12.  12. 하이드로겔Hydrogel 마스크팩의Mask pack 제조 Produce
하기 표 1 및 표 2와 같은 조성으로 하이드로겔 마스크팩 조성물 및 에센스를 제조한 것을 제외하고는, 상기 실시예 1과 동일한 방법으로 하이드로겔 마스크팩을 제조하였다.A hydrogel mask pack was prepared in the same manner as in Example 1, except that the hydrogel mask pack composition and the essence were prepared in the same composition as in Table 1 and Table 2.
원료명Raw material name 실시예 1Example 1 실시예 2Example 2 실시예 3Example 3 실시예 4Example 4 실시예 5Example 5 실시예 6Example 6
하이드로겔Hydrogel 정제수Purified water 96.796.7 96.796.7 96.796.7 96.796.7 96.796.7 96.796.7
카라기난Carrageenan 0.90.9 0.90.9 0.90.9 0.90.9 0.90.9 0.90.9
로커스트빈검Locust Bean Sword 1.21.2 1.21.2 1.21.2 1.21.2 1.21.2 1.21.2
잔탄검Xanthan Gum 0.70.7 0.70.7 0.70.7 0.70.7 0.70.7 0.70.7
타마린드씨검Tamarind Sea Sword 0.30.3 0.30.3 0.30.3 0.30.3 0.30.3 0.30.3
에센스essence 정제수Purified water 39.9939.99 39.9939.99 39.9939.99 39.9939.99 39.9939.99 39.9939.99
글리세린glycerin 2020 2020 2020 2020 4040 4040
부틸렌글라이콜Butylene Glycol 4040 4040 4040 4040 2020 2020
sh-oligopeptide-1sh-oligopeptide-1 0.010.01 0.010.01 0.010.01 0.010.01 0.010.01 0.010.01
원료명Raw material name 실시예 7Example 7 실시예 8Example 8 실시예 9Example 9 실시예 10Example 10 실시예 11Example 11 실시예 12Example 12
하이드로겔Hydrogel 정제수Purified water 96.796.7 96.796.7 96.796.7 96.796.7 96.796.7 96.796.7
카라기난Carrageenan 0.90.9 0.90.9 0.90.9 0.90.9 0.90.9 0.90.9
로커스트빈검Locust Bean Sword 1.21.2 1.21.2 1.21.2 1.21.2 1.21.2 1.21.2
잔탄검Xanthan Gum 0.70.7 0.70.7 0.70.7 0.70.7 0.70.7 0.70.7
타마린드씨검Tamarind Sea Sword 0.30.3 0.60.6 0.30.3 0.30.3 0.30.3 0.30.3
에센스essence 정제수Purified water 39.9939.99 39.9939.99 69.9969.99 69.9969.99 69.9969.99 69.9969.99
글리세린glycerin 4040 4040 1010 1010 1010 1010
부틸렌글라이콜Butylene Glycol 2020 2020 2020 2020 2020 2020
sh-oligopeptide-1sh-oligopeptide-1 0.010.01 0.010.01 0.010.01 0.010.01 0.010.01 0.010.01
비교예Comparative example 1 ~  1 to 비교예Comparative example 4.  4. 하이드로겔Hydrogel 마스크팩의Mask pack 제조 Produce
하기 표 3과 같은 조성으로 하이드로겔 조성물 및 에센스를 혼합하여 제조한 것을 제외하고는, 상기 실시예 1과 동일한 방법으로 하이드로겔 마스크팩을 제조하였다.A hydrogel mask pack was prepared in the same manner as in Example 1, except that the hydrogel composition and the essence were mixed with the composition shown in Table 3 below.
원료명Raw material name 비교예 1Comparative Example 1 비교예 2Comparative Example 2 비교예 3Comparative Example 3 비교예 4Comparative Example 4
하이드로겔Hydrogel 정제수Purified water 9797 9797 97.297.2 97.497.4
카라기난Carrageenan 0.90.9 0.90.9 0.50.5 0.90.9
로커스트빈검Locust Bean Sword 1.21.2 1.11.1 1.21.2 1One
잔탄검Xanthan Gum 0.90.9 1One 1.11.1 0.70.7
타마린드씨검Tamarind Sea Sword 00 00 00 00
에센스essence 정제수Purified water 99.9999.99 99.9999.99 99.9999.99 99.9999.99
sh-oligopeptide-1sh-oligopeptide-1 0.010.01 0.010.01 0.010.01 0.010.01
실험예Experimental Example 1.  One. 하이드로겔Hydrogel 마스크팩의Mask pack 강도측정 Strength measurement
상기 실시예 1 내지 12 및 비교예 1 내지 4에서 제조된 하이드로겔 마스크팩의 열단장 및 파열강도를 UTM(Instron 5544, USA)을 이용하여 측정하였고, 그 결과를 하기 표 4에 나타내었다.Thermal shortening and burst strength of the hydrogel mask packs prepared in Examples 1 to 12 and Comparative Examples 1 to 4 were measured using UTM (Instron 5544, USA), and the results are shown in Table 4 below.
열단장(breaking length)(단위: m)Breaking length in m 비파열강도(burst factor)(단위: kg/cm2)Burst factor (kg / cm 2 )
실시예 1Example 1 3.63.6 6.76.7
실시예 2Example 2 3.73.7 6.76.7
실시예 3Example 3 3.53.5 6.66.6
실시예 4Example 4 3.33.3 6.56.5
실시예 5Example 5 3.23.2 6.76.7
실시예 6Example 6 3.33.3 6.76.7
실시예 7Example 7 3.43.4 6.56.5
실시예 8Example 8 3.33.3 6.36.3
실시예 9Example 9 3.53.5 6.86.8
실시예 10Example 10 3.73.7 6.46.4
실시예 11Example 11 3.63.6 6.76.7
실시예 12Example 12 3.53.5 6.26.2
비교예 1Comparative Example 1 2.72.7 4.34.3
비교예 2Comparative Example 2 2.92.9 4.24.2
비교예 3Comparative Example 3 2.62.6 4.14.1
비교예 4Comparative Example 4 2.52.5 4.04.0

Claims (17)

  1. 정제수, 카라기난, 로커스트빈 검, 잔탄검 및 타마린드씨검을 함유하는 하이드로겔 마스크팩 조성물.Hydrogel mask pack composition containing purified water, carrageenan, locust bean gum, xanthan gum and tamarind seed gum.
  2. 제1항에 있어서, 상기 하이드로겔 마스크팩 조성물은 정제수 90 ~ 99중량%, 카라기난 0.1 ~ 2 중량%, 로커스트빈 검 0.1 ~ 2 중량%, 잔탄검 0.1 ~ 1 중량% 및 타마린드씨 검 0.005 ~ 7 중량%를 함유하는 것을 특징으로 하는 하이드로겔 마스크팩 조성물.According to claim 1, wherein the hydrogel mask pack composition is 90 to 99% by weight purified water, 0.1 to 2% by weight carrageenan, 0.1 to 2% by weight locust bean gum, 0.1 to 1% by weight xanthan gum and tamarind seed gum 0.005 ~ Hydrogel mask pack composition comprising 7% by weight.
  3. 제1항 또는 제2항 중 한 항의 하이드로겔 마스크팩 조성물의 성형체를 포함하는 것을 특징으로 하는 하이드로겔 마스크팩.A hydrogel mask pack comprising a molded body of the hydrogel mask pack composition of claim 1.
  4. 제3항에 있어서, 상기 성형체 100 중량부에 대하여 정제수, 다가 알코올, 천연추출물 및 기능성 첨가제로 이루어진 군으로부터 선택되는 1종 이상을 함유하는 에센스 30 ~ 70 중량부를 포함하는 것을 특징으로 하는 하이드로겔 마스크팩.The hydrogel mask according to claim 3, comprising 30 to 70 parts by weight of an essence containing at least one selected from the group consisting of purified water, polyhydric alcohols, natural extracts and functional additives based on 100 parts by weight of the molded body. pack.
  5. 제4항에 있어서, 상기 에센스는 정제수 100 중량부에 대해서, 다가알코올 40 ~ 300 중량부를 함유하는 것을 특징으로 하는 하이드로겔 마스크팩.The hydrogel mask pack of claim 4, wherein the essence contains 40 to 300 parts by weight of polyhydric alcohol with respect to 100 parts by weight of purified water.
  6. 제5항에 있어서, 상기 다가 알코올은 글리세린 및 부틸렌 글라이콜을 1:0.1 ~ 2.5의 중량비로 포함하는 것을 특징으로 하는 하이드로겔 마스크팩.The hydrogel mask pack of claim 5, wherein the polyhydric alcohol comprises glycerin and butylene glycol in a weight ratio of 1: 0.1 to 2.5.
  7. 제4항에 있어서, 상기 성형체에 포함된 타마린드씨 검과 에센스에 포함된 다가알코올을 1:20 ~ 80의 중량비로 포함하는 것을 특징으로 하는 하이드로겔 마스크팩.[5] The hydrogel mask pack of claim 4, wherein the tamarind seed gum and polyhydric alcohol included in the essence are included in a weight ratio of 1:20 to 80.
  8. 제4항에 있어서, 상기 에센스는 정제수 100 중량부에 대해서, 천연추출물 0.01 ~ 20 중량부를 함유하는 것을 특징으로 하는 하이드로겔 마스크팩.The hydrogel mask pack of claim 4, wherein the essence contains 0.01 to 20 parts by weight of natural extract, based on 100 parts by weight of purified water.
  9. 제4항에 있어서, 상기 에센스는 정제수 100 중량부에 대해서, 기능성 첨가제 0.001 ~ 20 중량부를 함유하는 것을 특징으로 하는 하이드로겔 마스크팩.      The hydrogel mask pack of claim 4, wherein the essence contains 0.001 to 20 parts by weight of a functional additive based on 100 parts by weight of purified water.
  10. 제4항에 있어서, 상기 천연추출물은 녹차추출물, 감초추출물, 닥나무추출물, 상백피추출물, 황금추출물, 푸에리라리아추출물, 홍삼추출물, 살구추출물, 오일추출물, 오렌지추출물, 레몬추출물, 대나무추출물, 구아바추출물, 로즈마리추출물, 산수유추출물, 영지추출물, 은행추출물, 서시옥욕산추출물, 자음단추출물, 모과추출물, 백련초추출물, 파프리카추출물, 알로에추출물, 수세미추출물, 해초추출물, 당근추출물, 대두추출물, 자몽씨추출물, 포도씨추출물, 마치현추출물, 캐비어추출물, 석류추출물, 인삼추출물, 복숭아추출물, 천궁추출물, 병풀추출물, 캐모마일추출물, 자초근추출물, 고삼추출물, 당귀추출물, 박하추출물, 삼백초추출물, 어성초추출물, 작약추출물, 목초액, 민들레추출물, 카렌듈라추출물, 황백피추출물, 탱자추출물, 황금추출물, 회향추출물, 컴푸리추출물, 율피추출물, ROE(로즈마리오일추출물) 및 자몽씨추출물로 이루어진 군으로부터 선택되는 1종 이상을 포함하는 것을 특징으로 하는 하이드로겔 마스크팩.The extract of claim 4, wherein the natural extract is green tea extract, licorice extract, medicinal extract, lettuce extract, golden extract, pueraria extract, red ginseng extract, apricot extract, oil extract, orange extract, lemon extract, bamboo extract, guava Extract, rosemary extract, cornus extract, ganoderma lucidum extract, ginkgo extract, seookoksan acid extract, consonant extract, quince extract, white lotus extract, paprika extract, aloe extract, scrubber extract, seaweed extract, carrot extract, soybean extract, grapefruit seed Extract, Portulaca oleracea extract, Caviar extract, Pomegranate extract, Ginseng extract, Peach extract, Cheongung extract, Centella asiatica extract, Chamomile extract, Licorice root extract, Red ginseng extract, Angelica extract, Peppermint extract, Sambaekcho extract, Echo vinegar extract, Dancho extract Extract, calendula extract, yellow skin extract, tanza extract, golden extract, ash Hydrogel mask pack, characterized in that it comprises at least one selected from the group consisting of fragrance extract, extract extract, yulpi extract, ROE (Rose Mario oil extract) and grapefruit seed extract.
  11. 제4항에 있어서, 상기 기능성 첨가제는 글리세린, 판테놀, 히아루론산, 세라마이드, 베타글루칸, 알부틴, 비타민C, 화이텐스, 레티놀, 엘라스틴, 콜라겐, 코엔자임Q10, 이펙틴, EGF, 프로폴리스, 알란토인, 피토스탄, 인프라산 및 항산화제 비타민E(천연토코페롤)으로 이루어진 군으로부터 선택되는 1종 이상을 포함하는 것을 특징으로 하는 하이드로겔 마스크팩.The method according to claim 4, wherein the functional additive is glycerin, panthenol, hyaluronic acid, ceramide, betaglucan, arbutin, vitamin C, whiten, retinol, elastin, collagen, coenzyme Q10, effectin, EGF, propolis, allantoin, phytostane Hydrogel mask pack, characterized in that it comprises at least one selected from the group consisting of infra acid and antioxidant vitamin E (natural tocopherol).
  12. 제11항에 있어서, 상기 기능성 첨가제는 펩타이드를 더 함유하고, 상기 펩타이드는 rh-Polypeptide-64, rh-Oligopeptide-33, sh-oligopeptide-1, sh-Polypeptide-11, sh-Polypeptide-1, rh-Polypeptide-7, rh-Polypeptide-62, rh-Oligopeptide-2, sh-Polypeptide-31, rh-Polypeptide-3, rh-Polypeptide-14, sh-Polypeptide-13, rh-Polypeptide-8, sh-Polypeptide-59, sh-Polypeptide-16, rh-Polypeptide-4, rh-Polypeptide-66, rh-Polypeptide-67, rh-Polypeptide-60, rh-Polypeptide-51, rh-Polypeptide-58, sh-Polypeptide-19, sh-Polypeptide-22, sh-Polypeptide-5, rh-Polypeptide-33, rh-Oligopeptide-4, 및 rh-Polypeptide-9으로 이루어진 군으로부터 선택되는 1종 이상인 것을 특징으로 하는 하이드로겔 마스크팩.The method of claim 11, wherein the functional additive further contains a peptide, wherein the peptide is rh-Polypeptide-64, rh-Oligopeptide-33, sh-oligopeptide-1, sh-Polypeptide-11, sh-Polypeptide-1, rh -Polypeptide-7, rh-Polypeptide-62, rh-Oligopeptide-2, sh-Polypeptide-31, rh-Polypeptide-3, rh-Polypeptide-14, sh-Polypeptide-13, rh-Polypeptide-8, sh-Polypeptide -59, sh-Polypeptide-16, rh-Polypeptide-4, rh-Polypeptide-66, rh-Polypeptide-67, rh-Polypeptide-60, rh-Polypeptide-51, rh-Polypeptide-58, sh-Polypeptide-19 Hydrogel mask pack, characterized in that at least one selected from the group consisting of, sh-Polypeptide-22, sh-Polypeptide-5, rh-Polypeptide-33, rh-Oligopeptide-4, and rh-Polypeptide-9.
  13. 제1항 또는 제2항 중에서 선택되는 어느 한 항의 하이드로겔 마스크팩 조성물을 혼합하여 혼합물을 제조하는 1단계;1 step of preparing a mixture by mixing the hydrogel mask pack composition of any one of claims 1 or 2;
    상기 1단계에서 제조된 혼합물을 60 ~ 90℃로 가열한 후 박막 위에 도포하는 2단계;Heating the mixture prepared in step 1 to 60 to 90 ° C. and then applying the same on a thin film;
    상기 2단계에서 박막 위에 도포된 혼합물을 냉각 및 건조하여 성형체를 제조하는 3단계;Step 3 of producing a molded body by cooling and drying the mixture applied on the thin film in the step 2;
    상기 성형체를 마스크 형태로 재단하는 4단계; 및4 steps of cutting the molded body in the form of a mask; And
    상기 마스크 형태의 성형체에 정제수, 다가 알코올, 천연추출물 및 기능성 첨가제로 이루어진 군으로부터 선택되는 1종 이상을 함유하는 에센스를 충진하는 단계; 를 포함하는 하이드로겔 마스크팩의 제조방법.Filling an essence containing at least one member selected from the group consisting of purified water, a polyhydric alcohol, a natural extract, and a functional additive in the molded article in a mask form; Method for producing a hydrogel mask pack comprising a.
  14. 제13항에 있어서, 상기 2단계에서 혼합물을 랩코팅 방법으로 박막 위에 500 ~ 2000 ㎛ 두께로 도포하는 것을 특징으로 하는 하이드로겔 마스크팩의 제조방법.The method of manufacturing a hydrogel mask pack according to claim 13, wherein the mixture is coated on the thin film by a wrap coating method in a thickness of 500 to 2000 μm in the second step.
  15. 제13항에 있어서, 상기 3단계에서 박막 위에 도포된 혼합물을 0 ~ 30℃에서 냉각하는 것을 특징으로 하는 하이드로겔 마스크팩의 제조방법.The method of claim 13, wherein the mixture applied on the thin film in the step 3 is cooled at 0 ~ 30 ℃.
  16. 제13항에 있어서, 상기 3단계에서 박막 위에 도포된 혼합물을 70 ~110℃ 에서 건조하는 것을 특징으로 하는 하이드로겔 마스크팩의 제조방법.The method of claim 13, wherein the mixture applied to the thin film in the step 3 is dried at 70 ~ 110 ℃ method of producing a hydrogel mask pack.
  17. 제13항에 있어서, 상기 3단계에서 제조된 성형체는 두께가 100 ~ 1000㎛인 것을 특징으로 하는 하이드로겔 마스크팩의 제조방법.The method of claim 13, wherein the molded article prepared in step 3 has a thickness of 100 to 1000 µm.
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