WO2015037743A1 - New multifunctional colloidal cleaning agent composition using vegetable fatty acid and lecithin, and low-cost method for manufacturing same - Google Patents
New multifunctional colloidal cleaning agent composition using vegetable fatty acid and lecithin, and low-cost method for manufacturing same Download PDFInfo
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- WO2015037743A1 WO2015037743A1 PCT/JP2014/074752 JP2014074752W WO2015037743A1 WO 2015037743 A1 WO2015037743 A1 WO 2015037743A1 JP 2014074752 W JP2014074752 W JP 2014074752W WO 2015037743 A1 WO2015037743 A1 WO 2015037743A1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/0004—Preparation of sols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/44—Vegetable products
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Definitions
- the present invention relates to a new multifunctional active colloidal fatty acid detergent excellent in environment and a method for producing the same.
- Multifunctional activated colloidal fatty acid detergents that are excellent for the environment, human health, and beauty have traditionally been manufactured by mixing lecithin with plant fatty acids and cutting the molecules using the cutting force of the blades. Shear stirring is necessary, and sufficient mixing is not possible, so mixing with water is insufficient, so it is necessary to use a large amount of many types of emulsifiers. There wasn't. SUMMARY OF THE INVENTION Problems to be Solved by the Invention The present invention is intended to solve such problems, and its purpose is to easily remove dirt adhering to the surface of various organic and inorganic substances including skin, and to penetrate, moisturize and emulsify.
- An object of the present invention is to provide a cleaning agent having multiple functions such as dispersion, washing, decomposition, deodorization, sterilization and the like with an inexpensive and efficient production method.
- those production methods involve shear stirring with a shearing stirrer using blades at a rotation speed of about 4,000 rotations for a long time, and then mixing necessary components to nanosize capable of Brownian motion up to 5,000. Because it is a manufacturing method that stirs for a long time with a shearing stirrer of rotating blades and refines to nanoparticles, 1. Long production time 2. All cannot be cut completely, cutting efficiency is poor, and activation power is low. 3. Since the mixing power with water is low, many kinds of emulsifiers and solvents are required. 4. Therefore, the manufacturing price is high and the product price is also high. If the above items are solved, high-quality and high-quality production can be achieved in a short time, and the cost can be kept low.
- the problem to be solved by the present invention is to meet the above-mentioned conventional needs.
- the stirring ability can be increased by a shear stirring method capable of performing high-efficiency shear stirring in a short time.
- the type and amount of the mixed solvent can be reduced as much as possible, the manufacturing cost can be reduced, and the shear stirring ability can be greatly increased.
- the purpose is to provide the market with all product cost factors kept low, such as reducing cutting residue and improving performance.
- Means for Solving the Problem This problem is important in that the shear force of the shear stirring technique is improved, the cutting residue is eliminated, and the production can be performed with or without the addition of a minimum amount of emulsifier.
- the stirring time can be greatly shortened, the entire manufacturing time can be greatly shortened and the manufacturing cost can be greatly reduced.
- inertial force due to rapid forward / reverse rotation of the stirrer and shearing force due to centrifugal force are generated around the inner wall of the container, and after that, it is almost completely completed in a short time using a technique that allows shear stirring so that there is no residual shear due to convection. It was found that shear stirring was performed. Since this shear stirrer does not require a stirrer or a stirring blade, the inside of the stirrer is completely hollow, so that cleaning can be performed in a short time. Further, if water can be mixed and complete shear stirring can be performed, the amount of a solvent such as an emulsifier for mixing with water may be small or unnecessary.
- the solution of the present invention basically comprises the means ⁇ circle around (1) ⁇ .
- (1). Mix plant fatty acid and lecithin (2). Cut the plant fatty acid molecule with a shearing stirrer (3). Mix water, emulsifier and pH adjuster (4). Shear stirring to nano size with a shear stirrer.
- Vegetable fatty acids include corn oil fatty acids, canola oil fatty acids, soybean oil fatty acids, olive oil fatty acids, ben flower oil fatty acids, pine oil fatty acids, grape seed oil fatty acids and all other fatty acids such as pine nut oil fatty acids and nut oil fatty acids. It can be illustrated.
- Lecithin is egg yolk lecithin and soybean lecithin, peanut or yeast lecithin.
- the shear stirrer can use the Q mix stirrer without stirring rod and stirring blade and other forward / reverse rotating reaction that rapidly forward and reverse rotate and shear the contents by inertial force and centrifugal force.
- Water is purified water or distilled water using an ion exchange resin.
- the emulsifier is propylene glycol or 1.3-butylene glycol, but 1.3-butylene glycol with high safety is suitable.
- Examples of the pH adjusting agent and the saponifying agent include caustic potash and caustic soda. It can be cut to a particle size of 8 nm to 20 nm with a shear stirrer, and the natural motion is washed by Brownian motion, so that it can be soaked and washed.
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Abstract
[Problem] To provide a new multifunctional colloidal cleaning agent composition using vegetable fatty acid and lecithin, and a low-cost method for manufacturing the same. [Solution] 35-45 parts by weight of soybean fatty acid, 3-5 parts by weight of lecithin, 3-5 parts by weight of 1.3-butylene glycol, and 45-59 parts by weight of purified water are mixed and then stirred for several minutes using a rapid forward/reverse rotation shear stirrer. In this stage, a colloidal mixture that has been almost entirely shear stirred and emulsified is obtained. 3-5 parts by weight of α-tocopherol, which prevents oxidation, and 5-10 parts by weight of caustic potash, which serves as a saponification agent, are added to the colloidal mixture, which is then stirred for several minutes using the rapid forward/reverse rotation shear stirrer in order to obtain the completed colloidal multifunctional vegetable cleaning agent.
Description
本発明は、環境に優れた新しい多機能活性コロイド状脂肪酸洗浄剤とその製法に関するものである。
The present invention relates to a new multifunctional active colloidal fatty acid detergent excellent in environment and a method for producing the same.
環境と人の健康・美容に優れた多機能活性化コロイド脂肪酸洗浄剤は、従来その製法は、植物脂肪酸にレシチンを混合し羽根の切断力を利用して分子の切断を行うので、長時間のせん断撹拌が必要であり、また充分な撹拌が出来ないため水との混合が不足となり多種類の乳化剤を多量に使用する必要が有り、しかも分子の切断残りが有り全ての分子が有効に使用出来なかった。
発明が解決しようとする課題
本発明は、かかる問題を解決するためのもので、その目的は、皮膚を始め各種の有機物や無機物の表面に付着した汚れを容易に除去し、浸透、保湿、乳化、分散、洗浄、分解、消臭、除菌などの複合的な機能を有する洗浄剤を低価格で効率の良い製造方法で提供することにある。 Multifunctional activated colloidal fatty acid detergents that are excellent for the environment, human health, and beauty have traditionally been manufactured by mixing lecithin with plant fatty acids and cutting the molecules using the cutting force of the blades. Shear stirring is necessary, and sufficient mixing is not possible, so mixing with water is insufficient, so it is necessary to use a large amount of many types of emulsifiers. There wasn't.
SUMMARY OF THE INVENTION Problems to be Solved by the Invention The present invention is intended to solve such problems, and its purpose is to easily remove dirt adhering to the surface of various organic and inorganic substances including skin, and to penetrate, moisturize and emulsify. An object of the present invention is to provide a cleaning agent having multiple functions such as dispersion, washing, decomposition, deodorization, sterilization and the like with an inexpensive and efficient production method.
発明が解決しようとする課題
本発明は、かかる問題を解決するためのもので、その目的は、皮膚を始め各種の有機物や無機物の表面に付着した汚れを容易に除去し、浸透、保湿、乳化、分散、洗浄、分解、消臭、除菌などの複合的な機能を有する洗浄剤を低価格で効率の良い製造方法で提供することにある。 Multifunctional activated colloidal fatty acid detergents that are excellent for the environment, human health, and beauty have traditionally been manufactured by mixing lecithin with plant fatty acids and cutting the molecules using the cutting force of the blades. Shear stirring is necessary, and sufficient mixing is not possible, so mixing with water is insufficient, so it is necessary to use a large amount of many types of emulsifiers. There wasn't.
SUMMARY OF THE INVENTION Problems to be Solved by the Invention The present invention is intended to solve such problems, and its purpose is to easily remove dirt adhering to the surface of various organic and inorganic substances including skin, and to penetrate, moisturize and emulsify. An object of the present invention is to provide a cleaning agent having multiple functions such as dispersion, washing, decomposition, deodorization, sterilization and the like with an inexpensive and efficient production method.
本発明は、今や石油系合成界面活性剤による河川や海洋の汚染は、どんどん進んでおり、それらに代わる食用洗浄剤で、植物脂肪酸分子を切ることにより、洗浄力、除菌力、消臭力、静電気防止力、抗カビ力などを有し、１週間以内に９９．９％生分解する新しい環境洗浄剤が、工業分野から医療、美容分野まで幅広く応用されつつある。
In the present invention, pollution of rivers and the ocean by petroleum-based synthetic surfactants is now progressing rapidly, and it is an edible cleaning agent that replaces them. By cutting plant fatty acid molecules, detergency, disinfecting power, deodorizing power New environmental cleaners that have antistatic and antifungal properties and biodegrade 99.9% within a week are being widely applied from industrial to medical and beauty fields.
しかし、それらの製法は、羽根を利用したせん断撹拌機で４．０００回転前後の回転数で長時間せん断撹拌し、その後必要な組成分を混合してブラウン運動が可能なナノサイズまで５，０００回転の羽根のせん断撹拌機で長時間かけて撹拌し、ナノ粒子まで微細化すると言う製法であるため、
１、製造時間が長くかかる
２、全てが完全に切断出来ず、切断効率が悪く、活性化力が低い。
３、水との混合力が低いため、多種の乳化剤や溶剤が多く必要とする。
４、従って、製造価格が高く、製品価格も高価格なものになる。
上記の項目を解決すれば、短時間に高効率で高品質な製造が出来、コストも低く抑えることが出来る。
発明が解決しようとする課題
従って本発明が解決しようとする課題は、従来の上記要望に応えることである。すなわち、短時間に高効率なせん断撹拌を行えるせん断撹拌方法により撹拌能力を上げ、したがって、可能な限り混合溶剤の種類と使用量を削減でき製造コストの低減とせん断撹拌能力を大きく上げて分子の切断残りを少なくして性能を上げることなど全ての製品コスト要因を低く抑えて市場に提供することにある。
課題を解決するための手段
この課題は、そのせん断撹拌技術のせん断力を向上させ、切断残りを無くし、また最小限の乳化剤の添加かもしくは無添加で製造出来ることが重要である。同時に撹拌時間を大幅に短縮出来れば、全体の製造時間を大きく短縮でき製造コストを大幅に下げることが出来る。
そのためには、撹拌機の急速正逆回転による慣性力と遠心力によるせん断力が容器内壁周辺に発生し、その後対流によりせん断残りが無いようにせん断撹拌出来る技術を活用し短時間に殆ど完全にせん断撹拌することが判った。
このせん断撹拌機は、撹拌棒も撹拌羽根も不要のため、撹拌機内が完全な中空になるため清掃も短時間に出来る。
また、水を混合して完全なせん断撹拌が出来れば、水との混合のための乳化剤など溶剤の使用量が少量で済むか、もしくは不要となる可能性もある。 However, those production methods involve shear stirring with a shearing stirrer using blades at a rotation speed of about 4,000 rotations for a long time, and then mixing necessary components to nanosize capable of Brownian motion up to 5,000. Because it is a manufacturing method that stirs for a long time with a shearing stirrer of rotating blades and refines to nanoparticles,
1. Long production time 2. All cannot be cut completely, cutting efficiency is poor, and activation power is low.
3. Since the mixing power with water is low, many kinds of emulsifiers and solvents are required.
4. Therefore, the manufacturing price is high and the product price is also high.
If the above items are solved, high-quality and high-quality production can be achieved in a short time, and the cost can be kept low.
SUMMARY OF THE INVENTION Accordingly, the problem to be solved by the present invention is to meet the above-mentioned conventional needs. In other words, the stirring ability can be increased by a shear stirring method capable of performing high-efficiency shear stirring in a short time.Therefore, the type and amount of the mixed solvent can be reduced as much as possible, the manufacturing cost can be reduced, and the shear stirring ability can be greatly increased. The purpose is to provide the market with all product cost factors kept low, such as reducing cutting residue and improving performance.
Means for Solving the Problem This problem is important in that the shear force of the shear stirring technique is improved, the cutting residue is eliminated, and the production can be performed with or without the addition of a minimum amount of emulsifier. At the same time, if the stirring time can be greatly shortened, the entire manufacturing time can be greatly shortened and the manufacturing cost can be greatly reduced.
For that purpose, inertial force due to rapid forward / reverse rotation of the stirrer and shearing force due to centrifugal force are generated around the inner wall of the container, and after that, it is almost completely completed in a short time using a technique that allows shear stirring so that there is no residual shear due to convection. It was found that shear stirring was performed.
Since this shear stirrer does not require a stirrer or a stirring blade, the inside of the stirrer is completely hollow, so that cleaning can be performed in a short time.
Further, if water can be mixed and complete shear stirring can be performed, the amount of a solvent such as an emulsifier for mixing with water may be small or unnecessary.
１、製造時間が長くかかる
２、全てが完全に切断出来ず、切断効率が悪く、活性化力が低い。
３、水との混合力が低いため、多種の乳化剤や溶剤が多く必要とする。
４、従って、製造価格が高く、製品価格も高価格なものになる。
上記の項目を解決すれば、短時間に高効率で高品質な製造が出来、コストも低く抑えることが出来る。
発明が解決しようとする課題
従って本発明が解決しようとする課題は、従来の上記要望に応えることである。すなわち、短時間に高効率なせん断撹拌を行えるせん断撹拌方法により撹拌能力を上げ、したがって、可能な限り混合溶剤の種類と使用量を削減でき製造コストの低減とせん断撹拌能力を大きく上げて分子の切断残りを少なくして性能を上げることなど全ての製品コスト要因を低く抑えて市場に提供することにある。
課題を解決するための手段
この課題は、そのせん断撹拌技術のせん断力を向上させ、切断残りを無くし、また最小限の乳化剤の添加かもしくは無添加で製造出来ることが重要である。同時に撹拌時間を大幅に短縮出来れば、全体の製造時間を大きく短縮でき製造コストを大幅に下げることが出来る。
そのためには、撹拌機の急速正逆回転による慣性力と遠心力によるせん断力が容器内壁周辺に発生し、その後対流によりせん断残りが無いようにせん断撹拌出来る技術を活用し短時間に殆ど完全にせん断撹拌することが判った。
このせん断撹拌機は、撹拌棒も撹拌羽根も不要のため、撹拌機内が完全な中空になるため清掃も短時間に出来る。
また、水を混合して完全なせん断撹拌が出来れば、水との混合のための乳化剤など溶剤の使用量が少量で済むか、もしくは不要となる可能性もある。 However, those production methods involve shear stirring with a shearing stirrer using blades at a rotation speed of about 4,000 rotations for a long time, and then mixing necessary components to nanosize capable of Brownian motion up to 5,000. Because it is a manufacturing method that stirs for a long time with a shearing stirrer of rotating blades and refines to nanoparticles,
1. Long production time 2. All cannot be cut completely, cutting efficiency is poor, and activation power is low.
3. Since the mixing power with water is low, many kinds of emulsifiers and solvents are required.
4. Therefore, the manufacturing price is high and the product price is also high.
If the above items are solved, high-quality and high-quality production can be achieved in a short time, and the cost can be kept low.
SUMMARY OF THE INVENTION Accordingly, the problem to be solved by the present invention is to meet the above-mentioned conventional needs. In other words, the stirring ability can be increased by a shear stirring method capable of performing high-efficiency shear stirring in a short time.Therefore, the type and amount of the mixed solvent can be reduced as much as possible, the manufacturing cost can be reduced, and the shear stirring ability can be greatly increased. The purpose is to provide the market with all product cost factors kept low, such as reducing cutting residue and improving performance.
Means for Solving the Problem This problem is important in that the shear force of the shear stirring technique is improved, the cutting residue is eliminated, and the production can be performed with or without the addition of a minimum amount of emulsifier. At the same time, if the stirring time can be greatly shortened, the entire manufacturing time can be greatly shortened and the manufacturing cost can be greatly reduced.
For that purpose, inertial force due to rapid forward / reverse rotation of the stirrer and shearing force due to centrifugal force are generated around the inner wall of the container, and after that, it is almost completely completed in a short time using a technique that allows shear stirring so that there is no residual shear due to convection. It was found that shear stirring was performed.
Since this shear stirrer does not require a stirrer or a stirring blade, the inside of the stirrer is completely hollow, so that cleaning can be performed in a short time.
Further, if water can be mixed and complete shear stirring can be performed, the amount of a solvent such as an emulsifier for mixing with water may be small or unnecessary.
本発明の溶液は、基本的には▲１▼~の手段から成っている。
▲１▼．植物脂肪酸とレシチンを混合し
▲２▼．せん断撹拌機で植物脂肪酸の分子を切り
▲３▼．水と乳化剤とＰＨ調整材を混合し
▲４▼．せん断撹拌機でナノサイズまでせん断撹拌する。
植物脂肪酸は、コーン油脂肪酸、キャノーラ油脂肪酸、大豆油脂肪酸、オリーブ油脂肪酸、べに花油脂肪酸、パイン油脂肪酸、グレープシードオイル脂肪酸などの植物脂肪酸や松の実油脂肪酸やナッツ油脂肪酸などあらゆる脂肪酸等も例示出来る。
レシチンは、卵卵黄レシチンおよび大豆レシチン、ピーナツや酵母レシチンである。
せん断撹拌機は、急速正回転と急速逆回転を行い内容物を慣性力と遠心力によりせん断する、撹拌棒や撹拌羽根の無い株式会社Ｑミックスの撹拌機やその他の正逆回転反応を利用出来るせん断撹拌機を使用する。
水はイオン交換樹脂を使用した精製水や蒸留水である。
乳化剤はプロピレングリコールや１．３−ブチレングリコールなどであるが、安全性の高い１．３−ブチレングリコールが適している。
ＰＨ調整剤と鹸化剤は、苛性カリや苛性ソーダー、が例示出来る。
せん断撹拌機で、８ｎｍ~２０ｎｍの粒子径まで切断でき、ブラウン運動により自然運動が
洗浄を行うため、漬け置き洗浄が可能となる。 The solution of the present invention basically comprises the means {circle around (1)}.
(1). Mix plant fatty acid and lecithin (2). Cut the plant fatty acid molecule with a shearing stirrer (3). Mix water, emulsifier and pH adjuster (4). Shear stirring to nano size with a shear stirrer.
Vegetable fatty acids include corn oil fatty acids, canola oil fatty acids, soybean oil fatty acids, olive oil fatty acids, ben flower oil fatty acids, pine oil fatty acids, grape seed oil fatty acids and all other fatty acids such as pine nut oil fatty acids and nut oil fatty acids. It can be illustrated.
Lecithin is egg yolk lecithin and soybean lecithin, peanut or yeast lecithin.
The shear stirrer can use the Q mix stirrer without stirring rod and stirring blade and other forward / reverse rotating reaction that rapidly forward and reverse rotate and shear the contents by inertial force and centrifugal force. Use a shear stirrer.
Water is purified water or distilled water using an ion exchange resin.
The emulsifier is propylene glycol or 1.3-butylene glycol, but 1.3-butylene glycol with high safety is suitable.
Examples of the pH adjusting agent and the saponifying agent include caustic potash and caustic soda.
It can be cut to a particle size of 8 nm to 20 nm with a shear stirrer, and the natural motion is washed by Brownian motion, so that it can be soaked and washed.
▲１▼．植物脂肪酸とレシチンを混合し
▲２▼．せん断撹拌機で植物脂肪酸の分子を切り
▲３▼．水と乳化剤とＰＨ調整材を混合し
▲４▼．せん断撹拌機でナノサイズまでせん断撹拌する。
植物脂肪酸は、コーン油脂肪酸、キャノーラ油脂肪酸、大豆油脂肪酸、オリーブ油脂肪酸、べに花油脂肪酸、パイン油脂肪酸、グレープシードオイル脂肪酸などの植物脂肪酸や松の実油脂肪酸やナッツ油脂肪酸などあらゆる脂肪酸等も例示出来る。
レシチンは、卵卵黄レシチンおよび大豆レシチン、ピーナツや酵母レシチンである。
せん断撹拌機は、急速正回転と急速逆回転を行い内容物を慣性力と遠心力によりせん断する、撹拌棒や撹拌羽根の無い株式会社Ｑミックスの撹拌機やその他の正逆回転反応を利用出来るせん断撹拌機を使用する。
水はイオン交換樹脂を使用した精製水や蒸留水である。
乳化剤はプロピレングリコールや１．３−ブチレングリコールなどであるが、安全性の高い１．３−ブチレングリコールが適している。
ＰＨ調整剤と鹸化剤は、苛性カリや苛性ソーダー、が例示出来る。
せん断撹拌機で、８ｎｍ~２０ｎｍの粒子径まで切断でき、ブラウン運動により自然運動が
洗浄を行うため、漬け置き洗浄が可能となる。 The solution of the present invention basically comprises the means {circle around (1)}.
(1). Mix plant fatty acid and lecithin (2). Cut the plant fatty acid molecule with a shearing stirrer (3). Mix water, emulsifier and pH adjuster (4). Shear stirring to nano size with a shear stirrer.
Vegetable fatty acids include corn oil fatty acids, canola oil fatty acids, soybean oil fatty acids, olive oil fatty acids, ben flower oil fatty acids, pine oil fatty acids, grape seed oil fatty acids and all other fatty acids such as pine nut oil fatty acids and nut oil fatty acids. It can be illustrated.
Lecithin is egg yolk lecithin and soybean lecithin, peanut or yeast lecithin.
The shear stirrer can use the Q mix stirrer without stirring rod and stirring blade and other forward / reverse rotating reaction that rapidly forward and reverse rotate and shear the contents by inertial force and centrifugal force. Use a shear stirrer.
Water is purified water or distilled water using an ion exchange resin.
The emulsifier is propylene glycol or 1.3-butylene glycol, but 1.3-butylene glycol with high safety is suitable.
Examples of the pH adjusting agent and the saponifying agent include caustic potash and caustic soda.
It can be cut to a particle size of 8 nm to 20 nm with a shear stirrer, and the natural motion is washed by Brownian motion, so that it can be soaked and washed.
大豆脂肪酸３５~４５重量部、レシチン３~５重量部、１．３−ブチレングリコール３~５重量部、精製水４５~５９重量部を混合し、急速正逆回転せん断撹拌機で数分間撹拌する。この段階で殆ど完全にせん断撹拌され、乳化されコロイド状の混合物が出来る。
コロイド状の混合物に、酸化を防ぐα—トコフェロール１０重量部と鹸化剤として苛性カリ１０重量部を入れて急速正逆回転せん断撹拌機で数分間撹拌し完全なコロイド状多機能植物洗浄剤を得る。
効能試験（コロイド洗浄剤４．５倍希釈液）
Mix 35-45 parts by weight of soybean fatty acid, 3-5 parts by weight of lecithin, 3-5 parts by weight of 1.3-butylene glycol, 45-59 parts by weight of purified water, and stir for several minutes with a rapid forward / reverse rotating shear stirrer. . At this stage, it is almost completely sheared and emulsified to produce a colloidal mixture.
Into the colloidal mixture, 10 parts by weight of α-tocopherol for preventing oxidation and 10 parts by weight of caustic potash as a saponifying agent are added and stirred for several minutes with a rapid forward / reverse rotating shear stirrer to obtain a complete colloidal multifunctional plant cleaner.
Efficacy test (colloid detergent 4.5 times dilution)
コロイド状の混合物に、酸化を防ぐα—トコフェロール１０重量部と鹸化剤として苛性カリ１０重量部を入れて急速正逆回転せん断撹拌機で数分間撹拌し完全なコロイド状多機能植物洗浄剤を得る。
効能試験（コロイド洗浄剤４．５倍希釈液）
Into the colloidal mixture, 10 parts by weight of α-tocopherol for preventing oxidation and 10 parts by weight of caustic potash as a saponifying agent are added and stirred for several minutes with a rapid forward / reverse rotating shear stirrer to obtain a complete colloidal multifunctional plant cleaner.
Efficacy test (colloid detergent 4.5 times dilution)
Claims (2)
- 大豆油、コーン油、菜種油、オリーブ油、米油、ごま油、べに花油、ひまわり油、綿実油、パイン油、グレープシードオイルなどの植物脂肪酸や松の実油やナッツ油の植物脂肪酸のうち１つ以上とレシチン、１．３−ブチレングリコール、苛性カリ、精製水を混合した多機能活性水溶性植物コロイド状洗浄剤組成物。 With one or more of vegetable fatty acids such as soybean oil, corn oil, rapeseed oil, olive oil, rice oil, sesame oil, benflower oil, sunflower oil, cottonseed oil, pine oil, grape seed oil, and vegetable fatty acids of pine nut oil and nut oil A multifunctional active water-soluble plant colloidal detergent composition in which lecithin, 1.3-butylene glycol, caustic potash and purified water are mixed.
- 植物脂肪酸の分子をレシチンなどで切る場合に使用する撹拌機を急速正回転と急速逆回転の繰り返しにより容器内の回転方向を維持しようとして発生する「せん断力」で短時間にしかも分子切断残しの無いように切断撹拌し、高い効率の製造が出来るだけでなく、切断羽根を使用しないため清掃など簡便に出来る高効率製造と製造時間短縮し使用溶剤の種類と量の低減によるより天然性を上げた低コストの請求項１の組成物についての製造方法。 A stirrer used for cutting plant fatty acid molecules with lecithin or the like is a "shearing force" generated by trying to maintain the rotation direction in the container by repeating rapid forward rotation and rapid reverse rotation. Not only can it be cut and agitated so that it can be produced with high efficiency, but also because it does not use cutting blades, high efficiency production that can be easily performed such as cleaning and shortening the production time and reducing the type and amount of solvent used increase the naturalness. A process for producing the composition of claim 1 at low cost.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2013208606A JP2015054966A (en) | 2013-09-13 | 2013-09-13 | Novel multifunctional colloidal detergent composition using plant fatty acid and lecithin and low cost manufacturing method therefor |
| JP2013-208606 | 2013-09-13 |
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|---|---|
| WO2015037743A1 true WO2015037743A1 (en) | 2015-03-19 |
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| PCT/JP2014/074752 WO2015037743A1 (en) | 2013-09-13 | 2014-09-03 | New multifunctional colloidal cleaning agent composition using vegetable fatty acid and lecithin, and low-cost method for manufacturing same |
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| JP (1) | JP2015054966A (en) |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2022210888A1 (en) * | 2021-03-30 | 2022-10-06 | 株式会社Nexting | Bactericidal agent |
| JP2022155564A (en) * | 2021-03-30 | 2022-10-13 | 株式会社Nexting | Bactericidal agent |
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| JPH10310798A (en) * | 1997-05-09 | 1998-11-24 | Noevir Co Ltd | Detergent composition |
| JP2002068961A (en) * | 2000-08-28 | 2002-03-08 | Noevir Co Ltd | Skin cleanser |
| JP2004224726A (en) * | 2003-01-23 | 2004-08-12 | Pola Chem Ind Inc | Cleansing cosmetic composition |
| JP2005028292A (en) * | 2003-07-14 | 2005-02-03 | Bbc Soft:Kk | Stirring apparatus |
| JP2008307498A (en) * | 2007-06-18 | 2008-12-25 | Bbc Soft:Kk | Stirring device |
| JP2009072746A (en) * | 2007-09-25 | 2009-04-09 | Bbc Soft:Kk | Apparatus for stirring with temperature adjusting function |
| JP3153460U (en) * | 2008-12-23 | 2009-09-10 | 株式会社ウイット | Medium and large containers with a bellows-injection bellows containing environmental and health-friendly multifunctional plant cleaner and cleaner |
| JP2010229066A (en) * | 2009-03-26 | 2010-10-14 | Kose Corp | Detergent composition |
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- 2013-09-13 JP JP2013208606A patent/JP2015054966A/en active Pending
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- 2014-09-03 WO PCT/JP2014/074752 patent/WO2015037743A1/en active Application Filing
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH10310798A (en) * | 1997-05-09 | 1998-11-24 | Noevir Co Ltd | Detergent composition |
| JP2002068961A (en) * | 2000-08-28 | 2002-03-08 | Noevir Co Ltd | Skin cleanser |
| JP2004224726A (en) * | 2003-01-23 | 2004-08-12 | Pola Chem Ind Inc | Cleansing cosmetic composition |
| JP2005028292A (en) * | 2003-07-14 | 2005-02-03 | Bbc Soft:Kk | Stirring apparatus |
| JP2008307498A (en) * | 2007-06-18 | 2008-12-25 | Bbc Soft:Kk | Stirring device |
| JP2009072746A (en) * | 2007-09-25 | 2009-04-09 | Bbc Soft:Kk | Apparatus for stirring with temperature adjusting function |
| JP3153460U (en) * | 2008-12-23 | 2009-09-10 | 株式会社ウイット | Medium and large containers with a bellows-injection bellows containing environmental and health-friendly multifunctional plant cleaner and cleaner |
| JP2010229066A (en) * | 2009-03-26 | 2010-10-14 | Kose Corp | Detergent composition |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2022210888A1 (en) * | 2021-03-30 | 2022-10-06 | 株式会社Nexting | Bactericidal agent |
| JP2022155564A (en) * | 2021-03-30 | 2022-10-13 | 株式会社Nexting | Bactericidal agent |
| JP7178069B2 (en) | 2021-03-30 | 2022-11-25 | 株式会社Nexting | Disinfectant |
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| JP2015054966A (en) | 2015-03-23 |
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