WO2014098443A1 - Heating and ultra-high-pressure sterilisation method for ambient-temperature-sterile and refrigerated food - Google Patents

Heating and ultra-high-pressure sterilisation method for ambient-temperature-sterile and refrigerated food Download PDF

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WO2014098443A1
WO2014098443A1 PCT/KR2013/011726 KR2013011726W WO2014098443A1 WO 2014098443 A1 WO2014098443 A1 WO 2014098443A1 KR 2013011726 W KR2013011726 W KR 2013011726W WO 2014098443 A1 WO2014098443 A1 WO 2014098443A1
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food
ultra
sterilization
high pressure
heating
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PCT/KR2013/011726
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French (fr)
Korean (ko)
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문상영
이승환
이수현
김성균
강대익
최수희
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씨제이제일제당(주)
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/005Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by heating using irradiation or electric treatment
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/015Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with pressure variation, shock, acceleration or shear stress or cavitation

Definitions

  • the present invention relates to a method for sterilizing and heating ultra-high pressure sterilization of refrigerated foods, while having excellent sterilization effect, it is possible to maintain the taste and aroma immediately after cooking after sterilization, and preserves the appearance, color and texture as it is. And a method for sterilizing at room temperature and heating ultra-high pressure sterilization of refrigerated foods, which enables the production of refrigerated foods.
  • Retort food refers to foods that are cooked and processed at high temperatures, heated, sterilized and sealed for easy preservation, and can be eaten simply by pouring boiling water or heating in a microwave. Can be stored at room temperature or refrigerated for a certain period of time.
  • the conventional sterilization method used in the preparation of retort food is sterilization for 20 to 60 minutes at 110-130 ° C. using a conventional retort facility, and it takes several ten minutes or more to raise the temperature to the sterilization temperature and also reaches the sterilization temperature. After sterilizing for several ten minutes, excessive heat treatment causes the appearance of raw materials with high protein or sugar content such as meat, aquatic products, vegetables, intestines, and dairy products in the retort food. Deterioration occurred, there was a problem that the quality of the retort food is significantly reduced.
  • the sterilization method using the non-heating ultra-high pressure treatment process is a refrigerated food having a short shelf life, that is, juice and dressing. Only a limited number of the same product was inevitably used.
  • the sterilization effect is excellent, the taste and aroma immediately after cooking after sterilization can be maintained as it is, and the appearance, color and texture are preserved as it is, the sterilization method capable of manufacturing high quality room temperature sterilization and refrigerated food is urgently needed. .
  • Patent Document 1 KR 10-1006465 B1
  • the present invention has excellent sterilization effect, but can maintain the taste and aroma immediately after cooking after sterilization, appearance, color and texture are preserved as it is, high-quality room temperature sterilization and refrigerated foods It is an object of the present invention to provide a method for sterilizing at room temperature and heating ultra-high pressure sterilization of refrigerated foods.
  • the present invention relates to a method for sterilization and heating ultra-high pressure sterilization of refrigerated foods, and more particularly, a filling step of filling a pouch with cooked food; Preheating step of heating the food filled in the pouch to 60 ⁇ 100 °C; Ultra high pressure sterilization step of ultra-high pressure treatment of the preheated food to 500MPa ⁇ 700MPa; It provides a super-high pressure sterilization method of the normal temperature sterilization and refrigerated food comprising a cooling step of quenching the ultra-high pressure processed food.
  • the ultra-high pressure heating method of the present invention is about 90 seconds required for boosting by applying a high pressure after preheating the food to a temperature of about 20 to 30 ° C. lower than the desired sterilization temperature. Since the temperature of the food reaches a desired sterilization temperature within a short time, a temperature change time of 100 ° C. or more, which affects the deterioration of the food, is relatively short, thereby preventing deterioration of the food due to excessive heat treatment.
  • the method for sterilization and heating ultra-high pressure sterilization of refrigerated foods of the present invention because the ultra-high pressure treatment after the preheating process, the temperature inside the food rises uniformly at the same time without an additional heating process at the time of the ultra high pressure sterilization step, spores
  • the bactericidal effect is excellent also for the produced bacteria.
  • the ultra-high pressure sterilization method of the room temperature sterilization and refrigerated foods of the present invention because the ultra-high pressure without the additional heating step in the pre-heating step after the pre-heating step, the quality deviation according to the temperature difference between the plurality of food in the ultra-high pressure processor The effect is that there is no quality deviation inside the food.
  • the ultra-high pressure sterilization method of the normal temperature sterilization and refrigerated food of the present invention has excellent sterilization effect, the sterilized room temperature sterilization and refrigerated food can maintain the taste and aroma immediately after cooking, and the appearance, color, and texture are intact. It is preserved and has the effect of providing high quality room temperature sterilization and refrigerated foods.
  • Example 1 is a photograph comparing the beef rice bowl (Comparative Example 1) treated with a heating ultra-high pressure sterilization method of room temperature sterilization and refrigerated food of the present invention (Example 1) and the conventional retort sterilization method.
  • Figure 2 is a photograph comparing the spicy chicken rice sauce (Example 2) treated with a heating ultra-high pressure sterilization method of room temperature sterilization and refrigerated food of the present invention and the spicy chicken rice sauce (Comparative Example 2) treated by a conventional retort sterilization method
  • Example 3 is a photograph comparing the cream sauce (Example 3) treated with the heating ultra-high pressure sterilization method of the normal temperature sterilization and refrigerated food of the present invention and the cream sauce (Comparative Example 3) treated with the conventional retort sterilization method.
  • Figure 4 is a view showing a schematic configuration of an apparatus for performing a heating ultra-high pressure sterilization method of room temperature sterilization and refrigerated food of the present invention.
  • the present invention relates to a method for sterilizing and sterilizing a heated ultra-high pressure of refrigerated foods, and more specifically, to filling a pouch with a cooked food; Preheating step of heating the food filled in the pouch to 60 ⁇ 100 °C; Ultra high pressure sterilization step of ultra-high pressure treatment of the preheated food to 500MPa ⁇ 700MPa; It relates to a high temperature sterilization method of heating at room temperature sterilization and refrigerated food comprising a; cooling step of quenching the ultra-high pressure processed food.
  • the filling step is a step of filling the pouch with the cooked food.
  • the pouch in which the cooked food is filled is preferably made of a material that is sufficiently durable to accommodate temperature and pressure changes due to preheating and ultrahigh pressure treatment.
  • the heat-resistance, water resistance, and barrier properties should be excellent so that the lamination and sealing parts do not fall off or the strength decreases due to heat, and it is preferable to use a material having flexibility to accommodate shrinkage due to ultra high pressure.
  • the preheating step is a step of heating the food filled in the pouch to a temperature of 60 ⁇ 100 °C.
  • a water bath or to use a steam preheating or hydrothermal shower method, and more preferably a water bath (Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath).
  • the preheating step it is preferable to preheat the food to a temperature of 90 ⁇ 100 °C in order to make it suitable for room temperature distribution, it is preferable to preheat to a temperature of 60 ⁇ 90 °C to make the food suitable for refrigeration distribution. .
  • the ultra-high pressure sterilization step is a step of ultra-high pressure sterilization of the preheated food at a pressure of 500MPa ⁇ 700MPa.
  • the ultra-high pressure sterilization time is preferably about 1 to 10 minutes.
  • the preheated food is transferred to a high pressure processor (High Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel) without additional heating treatment.
  • a high pressure processor High Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel
  • the temperature inside the preheated food for a short time to increase the pressure quickly rises, characterized in that the food can be effectively sterilized within a short time.
  • the conventional retort sterilizer has a long time to reach the sterilization temperature, the food is exposed to heat for a long time until the sterilization temperature is reached, while the present invention is 20 ⁇ 30 °C than the sterilization temperature before the ultra-high pressure sterilization step
  • the present invention is 20 ⁇ 30 °C than the sterilization temperature before the ultra-high pressure sterilization step
  • the sterilization temperature is reached at 80-130 ° C. Therefore, the temperature change time of 100 ° C. or more, which affects the deterioration of the food, is relatively short, thereby effectively preventing the deterioration of the food due to excessive heat treatment.
  • the method for sterilization and heating ultra-high pressure sterilization of refrigerated foods of the present invention because the ultra-high pressure treatment after the preheating process, the temperature inside the food rises uniformly at the same time without the additional heating process during the ultra-high pressure sterilization step, spores
  • the bactericidal effect of the produced bacteria is superior to that of the conventional non-heating ultrahigh pressure sterilization method.
  • the ultra-high pressure sterilization method of the room temperature sterilization and refrigerated food of the present invention since only the ultra-high pressure without additional heating process in the ultra-high pressure sterilization step after the preheating step, the quality deviation according to the temperature difference between the plurality of food in the ultra-high pressure processor B, there is no effect of quality variation inside the food.
  • the cooling step is a step of rapidly cooling the ultra-high pressure processed food at about 5 ° C. or less for about 20 minutes.
  • Clostridium nigrificans a cause of blackening , is a thermophilic bacterium. Since the optimum growth temperature is 55 ° C, spores tend to germinate in this temperature range when gently cooled, and therefore, quenching is preferable.
  • the temperature of the product falls below the preheating temperature within a short time of 90 seconds required for the pressure to drop to 0.1 MPa. Quick cooling time is effective.
  • the movement for the preheating step, the ultrahigh pressure processing step, and the quenching step is automatically transferred through the conveyor belt.
  • Example A Experiment of confirming whether room temperature distribution or refrigeration distribution is possible for various processed foods sterilized by heating ultrahigh pressure sterilization method of room temperature sterilization and refrigerated food of the present invention
  • the initial number of bacteria was 1 ⁇ 10 1 level and all of them were heat resistant bacteria.
  • the initial bacterial count was 1 ⁇ 10 2 , and 1 ⁇ 10 1 was detected as heat-resistant bacteria.
  • the product temperature was raised to 95-99 ° C. during the 90 seconds of stepping up to 600 MPa, and in this state, ultrahigh pressure treatment was performed for 5 minutes.
  • the product was then quenched at 5 ° C. or lower for 20 minutes.
  • the quenched heated ultrahigh pressure sterilized food was stored in a 10 ° C. and 15 ° C. incubator, respectively, and the expiration date test was performed.
  • the cream sauce treated by the method of heating high-temperature sterilization of the room temperature sterilization and refrigerated food of the present invention was confirmed that refrigeration distribution is possible with a shelf life of 12 weeks.
  • the initial bacterial count was 2 ⁇ 10 2 , and 1.5 ⁇ 10 1 was detected as heat resistant bacteria.
  • the cream sauce was filled into the pouch and then preheated to 80 ° C. in a water bath (Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath). Subsequently, after being transferred to an ultra high pressure processor (Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel) was subjected to ultra high pressure at 600MPa for 5 minutes. The product temperature was raised to 105-109 ° C. during the 90 seconds stepped up to 600 MPa, and the ultrahigh pressure treatment was performed for 5 minutes in this state.
  • the product was then quenched at 5 ° C. or lower for 20 minutes.
  • the quenched heated ultrahigh pressure sterilized food was stored in a 10 ° C. and 15 ° C. incubator, respectively, and the expiration date test was performed.
  • the cream sauce treated by the method of heating high-temperature sterilization of the room temperature sterilization and refrigerated food of the present invention was confirmed that refrigeration distribution is possible with a shelf life of 12 weeks.
  • the total number of bacteria was 7 ⁇ 10 4 after preparation of the Jeok-yuk bowl sauce, of which 3 ⁇ 10 2 was detected as heat-resistant bacteria. .
  • the fleshed rice bowl was filled with a pouch and preheated to 70 ° C. in a water bath (Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath). Subsequently, after being transferred to an ultra high pressure processor (Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel) was subjected to ultra high pressure at 600MPa for 5 minutes. The product temperature was raised to 95-99 ° C. during the 90 seconds of stepping up to 600 MPa, and in this state, ultrahigh pressure treatment was performed for 5 minutes.
  • the product was then quenched for 20 minutes below 5 ° C.
  • the quenched heated ultrahigh pressure sterilized food was stored in a 10 ° C. and 15 ° C. incubator, respectively, and the expiration date test was performed.
  • the meat-covered rice sauce treated by the heating ultrahigh pressure sterilization method of the normal temperature sterilization and refrigerated food of the present invention can be refrigerated with a shelf life of 12 weeks.
  • the initial number of bacteria was 7 ⁇ 10 4 , of which 3 ⁇ 10 2 was detected as heat-resistant bacteria.
  • the product was then quenched at 5 ° C. or lower for 20 minutes.
  • the quenched heated ultrahigh pressure sterilized food was stored in a 10 ° C. and 15 ° C. incubator, respectively, and the expiration date test was performed.
  • the meat-covered rice sauce treated by the heating ultrahigh pressure sterilization method of the normal temperature sterilization and refrigerated food of the present invention can be refrigerated with a shelf life of 12 weeks.
  • the initial bacterial count was 1 ⁇ 10 1 , and all of them were detected as heat-resistant bacteria. .
  • the beef bowl sauce was filled into pouches and preheated to 80 ° C. in a water bath (Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath). Subsequently, after being transferred to an ultra high pressure processor (Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel) was subjected to ultra high pressure at 600MPa for 5 minutes. The product temperature was raised to 105-109 ° C. during the 90 seconds stepped up to 600 MPa, and the ultrahigh pressure treatment was performed for 5 minutes in this state.
  • the product was then quenched at 5 ° C. or lower for 20 minutes.
  • the beef bowl source treated with the heating ultrahigh pressure sterilization method of the normal temperature sterilization and refrigerated food of the present invention can be refrigerated with a shelf life of 12 weeks.
  • Example B Investigation of consumer's preference for processed food sterilized by heating ultrahigh pressure sterilization method of room temperature sterilization and refrigerated food of the present invention
  • the temperature was treated at a temperature of 90 °C in the preheating step and then quenched after treatment with a pressure of 600MPa, in the case of the comparative example sterilized after sterilization for 20 to 60 minutes at 110 ⁇ 130 °C, Examples and All of the comparative examples were sterilized under conditions in which normal temperature distribution was possible.
  • the consumer preference survey was conducted for 50 to 60 housewives aged 25 to 50 living in Gyeonggi-do, Seoul, and the survey was conducted with a consumer preference survey using the 5-point hedonic test.
  • Survey analysis method was performed by Mean / ANOVA / Open item analysis method, the results are shown in Table 1 to 3.
  • GAP means the difference in scores between the two sterilization methods for each item.
  • Beef bowl sauce (Example 1) treated by the heating ultra-high pressure sterilization method of the room temperature sterilization and refrigerated food of the present invention compared to the beef bowl sauce (Comparative Example 1) treated with the conventional retort sterilization method, the first sign, sauce color, meat It was confirmed that the chewing feeling is excellent.
  • Example 2 Compared to the spicy chicken rice sauce (Example 2) treated with the heating ultra-high pressure sterilization method of the present invention compared to the spicy chicken rice sauce (Comparative Example 2) treated with the conventional retort sterilization method, the taste of the sauce, the color of the chewing, etc. This excellence was confirmed.
  • the cream sauce (Example 3) treated by the heating ultrahigh pressure sterilization method of the present invention had superior first half symbol, appearance symbol, and cream flavor compared to the cream sauce (Comparative Example 3) treated by the conventional retort sterilization method.
  • Figure 1 is a photograph comparing the beef bowl sauce (Example 1) of the present invention and the beef bowl sauce (Comparative Example 1) treated by a conventional retort sterilization method. It can be seen that the color of the beef bowl sauce of Comparative Example 1 is darker than the beef bowl sauce of Example 1.
  • Example 2 is a photograph comparing the spicy chicken rice sauce (Example 2) of the present invention and the spicy chicken rice sauce (Comparative Example 2) treated by the conventional retort sterilization method. It can be seen that the color of the spicy chicken rice sauce of Comparative Example 2 is darker than the spicy chicken rice sauce of Example 2.
  • Example 3 is a photograph comparing the cream sauce (Example 3) of the present invention with the cream sauce (Comparative Example 3) treated by the conventional retort sterilization method. While the color of the cream sauce of Comparative Example 3 changed dark, it can be seen that the cream sauce of Example 3 maintains its original cream color.
  • the ultra-high pressure sterilization method of the room temperature sterilization and refrigerated foods of the present invention through the above experimental results is excellent in sterilization effect, while maintaining the original taste, aroma, texture and color of the product immediately after cooking, It can be seen that the production of food sterilization and refrigerated food.
  • Table 4 is the sterilization treatment under refrigeration distribution conditions (preheating temperature 70 °C after ultra-high pressure treatment)
  • Table 5 is the result of sterilization treatment at room temperature distribution conditions (preheating temperature 90 °C after ultra-high pressure treatment).
  • the investigation method was the same as the above B-1.
  • the beef rice sauce (Example 4) and cream sauce (Example 5) treated by the heating ultra-high pressure sterilization method of the room temperature sterilization and refrigerated foods of the present invention has an overall taste score of 3.8 or more In addition, it was confirmed that consumer preference was high.

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  • Life Sciences & Earth Sciences (AREA)
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Abstract

The present invention relates to a heating and ultra-high-pressure sterilisation method for an ambient-temperature-sterile and refrigerated food, and, more specifically, to a heating and ultra-high-pressure sterilisation method for an ambient-temperature-sterile and refrigerated food, the method comprising: a filling step in which a cooked food is filled into a pouch; a pre-heating step in which the food filled in the pouch is heated to between 60 and 100°C; an ultra-high-pressure sterilization step in which the pre-heated food is subjected to an ultra-high-pressure treatment of between 500 MPa and 700 MPa; and a cooling step in which the food that has been treated at ultra-high-pressure is rapidly cooled. The heating and ultra-high-pressure sterilisation method for an ambient-temperature sterile and refrigerated food of the present invention has the effect of allowing the production of a high-quality processed food of which the appearance, colour and texture are preserved unaltered even while the immediate post-cooking taste and aroma of the sterilised food are maintained unaltered, despite an outstanding sterilisation effect.

Description

상온멸균 및 냉장 식품의 가열 초고압 살균방법Sterilization and heating ultra-high pressure sterilization of refrigerated foods
본 발명은 상온멸균 및 냉장 식품의 가열 초고압 살균방법에 관한 것으로, 살균효과가 우수하면서도, 살균처리 후 조리 직후의 맛과 향을 그대로 유지할 수 있고, 외관, 색상 및 조직감이 그대로 보존되어 고품질 상온멸균 및 냉장 식품의 제조가 가능한 상온멸균 및 냉장 식품의 가열 초고압 살균방법에 관한 것이다.The present invention relates to a method for sterilizing and heating ultra-high pressure sterilization of refrigerated foods, while having excellent sterilization effect, it is possible to maintain the taste and aroma immediately after cooking after sterilization, and preserves the appearance, color and texture as it is. And a method for sterilizing at room temperature and heating ultra-high pressure sterilization of refrigerated foods, which enables the production of refrigerated foods.
레토르트 식품이란 조리하고 가공한 식품을 고온에서 가열, 살균, 밀봉하여 보존이 용이하고, 끓는 물을 붓거나 전자레인지에 덥히기만 하면 간편하게 먹을 수 있도록 한 음식을 통틀어 일컫는 것으로, 공기와 광선을 차단한 상태에서 상온 또는 냉장보관으로 일정 기간 보존할 수 있다. Retort food refers to foods that are cooked and processed at high temperatures, heated, sterilized and sealed for easy preservation, and can be eaten simply by pouring boiling water or heating in a microwave. Can be stored at room temperature or refrigerated for a certain period of time.
최근 식생활의 간편화를 추구하는 경향이 날로 증대되고 있어, 레토르트 식품의 종류는 소스, 죽, 카레, 국, 탕, 찌개, 파스타 등등 그 종류가 갈수록 늘어가고 있는 실정이다. In recent years, the tendency to simplify the diet is increasing day by day, the type of retort foods, sauces, porridge, curry, soup, soup, stew, pasta, etc. are increasingly increasing.
종래의 레토르트 식품 제조시 사용되는 살균방법은 통상적인 레토르트 설비를 이용하여 110~130℃에서 20분 내지 60분 살균하는 것으로, 상기 살균온도까지 승온하는데 몇 십분 이상 소요되고, 또한 상기 살균온도에 도달 후 몇 십분 간 살균하므로, 과다한 열처리로 인하여 레토르트 식품 내 육류, 수산물, 채소류, 장류, 유제품 등 단백질 또는/및 당분의 조성이 높은 원료들의 외관이 뭉그러지고, 조직감이 나빠지며, 색상이 흑변하는 등 열화가 발생하여, 레토르트 식품의 품질이 현저히 저하되는 문제점이 있었다. The conventional sterilization method used in the preparation of retort food is sterilization for 20 to 60 minutes at 110-130 ° C. using a conventional retort facility, and it takes several ten minutes or more to raise the temperature to the sterilization temperature and also reaches the sterilization temperature. After sterilizing for several ten minutes, excessive heat treatment causes the appearance of raw materials with high protein or sugar content such as meat, aquatic products, vegetables, intestines, and dairy products in the retort food. Deterioration occurred, there was a problem that the quality of the retort food is significantly reduced.
또한, 상기 살균방법에 이용되는 레토르트 설비는 중심부 온도가 가장 늦게 올라가므로, 중심부 온도와 외곽부분 온도의 편차로 인하여, 레토르트 설비 내에 동시에 투입된 복수의 식품 간에 온도 차이에 따른 품질편차가 있었으며, 심지어 한 개의 식품 내부에서도 품질편차가 있는 등의 문제점이 있었다. In addition, since the retort facility used in the sterilization method has the latest rise in the central temperature, there is a quality deviation according to the temperature difference between a plurality of foods simultaneously introduced into the retort facility due to the deviation of the central temperature and the outer temperature. There was a problem such as the quality deviation in the dog's food.
한편, 주스, 드레싱 등을 제조시 가열처리 대신 비가열초고압처리공정으로 살균하는 방법이 대한민국 등록특허공보 제10-1006465호에 개시되어 있다. 상기 비가열초고압처리공정은, 종래의 통상적인 레토르트 살균방식인, 열처리에 의한 살균방식의 문제점이었던 영양분의 손실, 가열취의 발생, 이상물질의 생성, 에너지의 대량소비와 같은 단점을 극복하면서, 미생물을 살균하고 원래의 제품의 품질을 유지할 수 있다는 장점이 있으나, 포자 생성균에 대해서는 살균효과가 낮아 이들에 대한 살균효과를 얻고자 할 경우 매우 높은 압력을 적용해야하는 단점이 있었다.On the other hand, a method of sterilizing the juice, dressing, etc. by a non-heating ultra-high pressure treatment process instead of heat treatment is disclosed in Korean Patent Publication No. 10-1006465. The non-heating ultra-high pressure treatment process, while overcoming disadvantages such as loss of nutrients, generation of heat odor, generation of abnormal substances, mass consumption of energy, which were problems of the sterilization method by heat treatment, which is a conventional conventional retort sterilization method, There is an advantage that can sterilize the microorganisms and maintain the quality of the original product, but for the spore-producing microorganisms had a low sterilization effect, if you want to get a sterilization effect on them had to have a very high pressure applied.
그러나 적용되는 압력이 높아질수록 장치비 및 운영비가 소요될 뿐 아니라 제품의 품질이 저하되는 문제점이 발생될 수 있으므로, 비가열초고압처리공정을 이용한 살균처리방식은 유통기간이 짧은 냉장식품, 즉, 주스, 드레싱 같은 일부 제품에만 제한적으로 이용될 수 밖에 없는 실정이었다. However, the higher the pressure applied, the higher the device cost and operating cost, and the lower the quality of the product. Therefore, the sterilization method using the non-heating ultra-high pressure treatment process is a refrigerated food having a short shelf life, that is, juice and dressing. Only a limited number of the same product was inevitably used.
따라서, 살균효과가 우수하고, 살균처리 후 조리 직후의 맛과 향을 그대로 유지할 수 있으며, 외관, 색상 및 조직감이 그대로 보존되어 고품질 상온멸균 및 냉장 식품의 제조가 가능한 살균방법이 절실히 요구되는 실정이다. Therefore, the sterilization effect is excellent, the taste and aroma immediately after cooking after sterilization can be maintained as it is, and the appearance, color and texture are preserved as it is, the sterilization method capable of manufacturing high quality room temperature sterilization and refrigerated food is urgently needed. .
[특허문헌][Patent Documents]
(특허문헌 1) KR 10-1006465 B1(Patent Document 1) KR 10-1006465 B1
상기의 종래기술의 문제점을 해결하기 위하여, 본 발명은 살균효과가 우수하면서도, 살균처리 후 조리 직후의 맛과 향을 그대로 유지할 수 있으며, 외관, 색상 및 조직감이 그대로 보존되어 고품질 상온멸균 및 냉장 식품의 제조가 가능한 상온멸균 및 냉장 식품의 가열 초고압 살균방법을 제공하는 것을 목적으로 한다. In order to solve the problems of the prior art, the present invention has excellent sterilization effect, but can maintain the taste and aroma immediately after cooking after sterilization, appearance, color and texture are preserved as it is, high-quality room temperature sterilization and refrigerated foods It is an object of the present invention to provide a method for sterilizing at room temperature and heating ultra-high pressure sterilization of refrigerated foods.
상기의 목적을 달성하기 위해, 본 발명은 상온멸균 및 냉장 식품의 가열 초고압 살균방법에 관한 것으로, 더욱 상세히는, 조리된 식품을 파우치에 충진하는 충진 단계; 상기 파우치에 충진된 식품을 60~100℃로 가열하는 예열 단계; 상기 예열된 식품을 500MPa~700MPa로 초고압 처리하는 초고압 살균 단계; 상기 초고압 처리된 식품을 급냉하는 냉각 단계;를 포함하는 상온멸균 및 냉장 식품의 가열 초고압 살균방법을 제공한다. In order to achieve the above object, the present invention relates to a method for sterilization and heating ultra-high pressure sterilization of refrigerated foods, and more particularly, a filling step of filling a pouch with cooked food; Preheating step of heating the food filled in the pouch to 60 ~ 100 ℃; Ultra high pressure sterilization step of ultra-high pressure treatment of the preheated food to 500MPa ~ 700MPa; It provides a super-high pressure sterilization method of the normal temperature sterilization and refrigerated food comprising a cooling step of quenching the ultra-high pressure processed food.
본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법은 원하는 살균 온도보다 20~30℃ 정도 낮은 온도가 되도록 식품을 예열 처리한 후 초고압의 압력을 가함으로써, 승압에 소요되는 약 90초 정도라는 매우 짧은 시간 내에 식품의 온도가 원하는 살균 온도에 도달하므로, 식품의 열화에 영향을 미치는 100℃ 이상의 온도변화 시간이 상대적으로 짧아 과도한 열처리에 의한 식품의 열화 현상을 방지할 수 있는 효과가 있다. In the method for sterilizing and refrigerated foods, the ultra-high pressure heating method of the present invention is about 90 seconds required for boosting by applying a high pressure after preheating the food to a temperature of about 20 to 30 ° C. lower than the desired sterilization temperature. Since the temperature of the food reaches a desired sterilization temperature within a short time, a temperature change time of 100 ° C. or more, which affects the deterioration of the food, is relatively short, thereby preventing deterioration of the food due to excessive heat treatment.
또한, 본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법은 예열 처리 후 초고압 처리를 함으로 인해, 초고압 살균 단계 시 별도의 추가 가열공정 없이도 압력 상승과 동시에 식품 내부의 온도가 균일하게 상승하므로, 포자 생성균에 대해서도 살균효과가 우수한 효과가 있다. In addition, the method for sterilization and heating ultra-high pressure sterilization of refrigerated foods of the present invention, because the ultra-high pressure treatment after the preheating process, the temperature inside the food rises uniformly at the same time without an additional heating process at the time of the ultra high pressure sterilization step, spores The bactericidal effect is excellent also for the produced bacteria.
또한, 본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법은 예열 단계 이후 초고압 살균 단계에서 별도의 추가 가열공정 없이 초고압의 압력만 가하므로, 초고압처리기 내 복수의 식품간의 온도 차이에 따른 품질 편차나, 식품 내부의 품질 편차가 없는 효과가 있는 것이다. In addition, the ultra-high pressure sterilization method of the room temperature sterilization and refrigerated foods of the present invention, because the ultra-high pressure without the additional heating step in the pre-heating step after the pre-heating step, the quality deviation according to the temperature difference between the plurality of food in the ultra-high pressure processor The effect is that there is no quality deviation inside the food.
따라서, 본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법은 살균효과가 우수하면서도, 살균처리 된 상온멸균 및 냉장 식품이 조리 직후의 맛과 향을 그대로 유지할 수 있고, 외관, 색상 및 조직감이 그대로 보존되어 고품질 상온멸균 및 냉장 식품을 제공할 수 있는 효과가 있는 것이다. Therefore, the ultra-high pressure sterilization method of the normal temperature sterilization and refrigerated food of the present invention has excellent sterilization effect, the sterilized room temperature sterilization and refrigerated food can maintain the taste and aroma immediately after cooking, and the appearance, color, and texture are intact. It is preserved and has the effect of providing high quality room temperature sterilization and refrigerated foods.
도 1은 본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법으로 처리한 소고기덮밥 소스(실시예 1)와 종래의 레토르트 살균방법으로 처리된 소고기덮밥 소스(비교예 1)를 비교한 사진이다.1 is a photograph comparing the beef rice bowl (Comparative Example 1) treated with a heating ultra-high pressure sterilization method of room temperature sterilization and refrigerated food of the present invention (Example 1) and the conventional retort sterilization method.
도 2는 본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법처리한 매운닭고기덮밥 소스(실시예 2)와 종래의 레토르트 살균방법으로 처리된 매운닭고기덮밥 소스(비교예 2)를 비교해 놓은 사진이다Figure 2 is a photograph comparing the spicy chicken rice sauce (Example 2) treated with a heating ultra-high pressure sterilization method of room temperature sterilization and refrigerated food of the present invention and the spicy chicken rice sauce (Comparative Example 2) treated by a conventional retort sterilization method
도 3은 본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법으로 처리한 크림소스(실시예 3)와 종래의 레토르트 살균방법으로 처리된 크림소스(비교예 3)를 비교해 놓은 사진이다.3 is a photograph comparing the cream sauce (Example 3) treated with the heating ultra-high pressure sterilization method of the normal temperature sterilization and refrigerated food of the present invention and the cream sauce (Comparative Example 3) treated with the conventional retort sterilization method.
도 4는 본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법을 수행하기 위한 장치의 개략적인 구성을 나타낸 도이다. Figure 4 is a view showing a schematic configuration of an apparatus for performing a heating ultra-high pressure sterilization method of room temperature sterilization and refrigerated food of the present invention.
본 발명은 상온멸균 및 냉장식품의 가열 초고압 살균방법에 관한 것으로, 더욱 상세히는, 조리된 식품을 파우치에 충진하는 충진 단계; 상기 파우치에 충진된 식품을 60~100℃로 가열하는 예열 단계; 상기 예열된 식품을 500MPa~700MPa로 초고압 처리하는 초고압 살균 단계; 상기 초고압 처리된 식품을 급냉하는 냉각 단계;를 포함하는 상온멸균 및 냉장 식품의 가열 초고압 살균방법에 관한 것이다. The present invention relates to a method for sterilizing and sterilizing a heated ultra-high pressure of refrigerated foods, and more specifically, to filling a pouch with a cooked food; Preheating step of heating the food filled in the pouch to 60 ~ 100 ℃; Ultra high pressure sterilization step of ultra-high pressure treatment of the preheated food to 500MPa ~ 700MPa; It relates to a high temperature sterilization method of heating at room temperature sterilization and refrigerated food comprising a; cooling step of quenching the ultra-high pressure processed food.
본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법에서, 상기 충진 단계는 조리된 식품을 파우치에 충진하는 단계이다. 상기 조리된 식품이 충진되는 파우치는 예열 처리 및 초고압 압력처리에 따른 온도 및 압력변화를 수용할 수 있도록 충분히 내구성이 있는 재질의 것을 사용하는 것이 바람직하다. 바람직하게는 열에 의하여 적층부나 밀봉부가 떨어져 나가거나 강도가 낮아지는 일이 없도록 열접착성, 내수성 및 차단성이 우수하여야 하고, 초고압에 의한 수축을 수용할 수 있는 유연성이 있는 재질을 사용하는 것이 바람직하다. 더욱 바람직하게는, 높은 기계적 강도와 치수안정성, 내수성, 질김성 등이 우수한 폴리에틸렌 테레프탈레이트 재질을 사용하는 것이 바람직하나, 반드시 이로 한정되는 것은 아니다.In the ultra-high pressure sterilization method of room temperature sterilization and refrigerated food of the present invention, the filling step is a step of filling the pouch with the cooked food. The pouch in which the cooked food is filled is preferably made of a material that is sufficiently durable to accommodate temperature and pressure changes due to preheating and ultrahigh pressure treatment. Preferably, the heat-resistance, water resistance, and barrier properties should be excellent so that the lamination and sealing parts do not fall off or the strength decreases due to heat, and it is preferable to use a material having flexibility to accommodate shrinkage due to ultra high pressure. Do. More preferably, it is preferable to use a polyethylene terephthalate material excellent in high mechanical strength, dimensional stability, water resistance, toughness, and the like, but is not limited thereto.
또한, 본 발명의 상온멸균 및 냉장식품의 가열 초고압 살균방법에서, 상기 예열 단계는 파우치에 충진된 식품이 60~100℃의 온도가 되도록 가열하는 단계이다. 예열 처리시, 워터배스를 이용하거나, 스팀예열 또는 열수샤워 방법 등을 이용하는 것이 바람직하고, 더욱 바람직하게는 워터 배스(Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath )를 이용하는 것이 바람직하다. In addition, in the ultra-high pressure sterilization method of room temperature sterilization and refrigerated foods of the present invention, the preheating step is a step of heating the food filled in the pouch to a temperature of 60 ~ 100 ℃. In the preheating process, it is preferable to use a water bath or to use a steam preheating or hydrothermal shower method, and more preferably a water bath (Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath). .
상기 예열 단계에서, 식품이 상온유통에 적합하도록 하기 위해서는 90~100℃의 온도가 되도록 예열하는 것이 바람직하고, 식품이 냉장유통에 적합하도록 하기 위해서는 60~90℃의 온도가 되도록 예열하는 것이 바람직하다. In the preheating step, it is preferable to preheat the food to a temperature of 90 ~ 100 ℃ in order to make it suitable for room temperature distribution, it is preferable to preheat to a temperature of 60 ~ 90 ℃ to make the food suitable for refrigeration distribution. .
또한, 본 발명의 상온멸균 및 냉장식품의 가열 초고압 살균방법에서, 상기 초고압 살균 단계는 상기 예열된 식품을 500MPa~700MPa의 압력으로 초고압 살균처리하는 단계이다. 상기 초고압 살균처리 시간은 1~10분 정도로 하는 것이 바람직하다. In addition, in the heating ultra-high pressure sterilization method of the normal temperature sterilization and refrigerated food of the present invention, the ultra-high pressure sterilization step is a step of ultra-high pressure sterilization of the preheated food at a pressure of 500MPa ~ 700MPa. The ultra-high pressure sterilization time is preferably about 1 to 10 minutes.
본 발명의 상온멸균 및 냉장식품의 가열 초고압 살균방법의 초고압 살균 단계에서는, 별도의 추가적인 가열처리 없이, 예열된 식품을 초고압 처리기(High Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel)로 이송하여 초고압의 압력을 가하는 것만으로, 승압되는 짧은 시간 동안 예열된 식품 내부의 온도가 빠르게 상승하여, 짧은 시간 내에 식품을 효과적으로 살균처리 할 수 있는 것을 특징으로 한다. In the ultra-high pressure sterilization step of the method of sterilization and heating ultra-high pressure sterilization of refrigerated foods of the present invention, the preheated food is transferred to a high pressure processor (High Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel) without additional heating treatment. Just by applying a very high pressure, the temperature inside the preheated food for a short time to increase the pressure quickly rises, characterized in that the food can be effectively sterilized within a short time.
즉, 종래의 레토르트 살균장치는 살균처리 온도까지 도달하는 시간이 길어, 상기 살균처리 온도에 도달하기까지 식품이 긴 시간 열에 노출되는데 반해, 본 발명은 초고압 살균 단계 이전에 살균 온도보다 20~30℃ 정도 낮은 온도가 되도록 식품을 예열 처리한 후, 초고압 살균 단계에서는 별도의 추가 가열공정 없이 초고압의 압력만을 가하는 것만으로, 승압에 소요되는 약 90초 정도라는 매우 짧은 시간 내에 예열된 식품의 온도가 원하는 살균 온도인 80~130℃에 도달하게 된다. 따라서, 식품의 열화에 영향을 미치는 100℃ 이상의 온도 변화 시간이 상대적으로 짧아 과도한 열처리에 의한 식품의 열화 현상을 효과적으로 방지할 수 있는 것이다. That is, the conventional retort sterilizer has a long time to reach the sterilization temperature, the food is exposed to heat for a long time until the sterilization temperature is reached, while the present invention is 20 ~ 30 ℃ than the sterilization temperature before the ultra-high pressure sterilization step After the food is preheated to a low temperature, in the ultra-high pressure sterilization step, only the ultra-high pressure is applied without any additional heating process, and the temperature of the food preheated within a very short time of about 90 seconds required for the boosting is desired. The sterilization temperature is reached at 80-130 ° C. Therefore, the temperature change time of 100 ° C. or more, which affects the deterioration of the food, is relatively short, thereby effectively preventing the deterioration of the food due to excessive heat treatment.
또한, 본 발명의 상온 멸균 및 냉장식품의 가열 초고압 살균방법은 예열 처리 후 초고압 처리를 함으로 인해, 초고압 살균 단계 시 별도의 추가 가열공정 없이도 압력 상승과 동시에 식품 내부의 온도가 균일하게 상승하므로, 포자 생성균에 대해 종래의 비가열식 초고압살균처리방식에 비해 살균효과가 우수한 효과가 있다. In addition, the method for sterilization and heating ultra-high pressure sterilization of refrigerated foods of the present invention, because the ultra-high pressure treatment after the preheating process, the temperature inside the food rises uniformly at the same time without the additional heating process during the ultra-high pressure sterilization step, spores The bactericidal effect of the produced bacteria is superior to that of the conventional non-heating ultrahigh pressure sterilization method.
또한, 본 발명의 상온 멸균 및 냉장식품의 가열 초고압 살균방법은, 예열 단계 이후 초고압 살균 단계에서 별도의 추가 가열공정 없이 초고압의 압력만 가하므로, 초고압처리기 내 복수의 식품간의 온도 차에 따른 품질 편차나, 식품 내부의 품질 편차가 없는 효과가 있는 것이다. In addition, the ultra-high pressure sterilization method of the room temperature sterilization and refrigerated food of the present invention, since only the ultra-high pressure without additional heating process in the ultra-high pressure sterilization step after the preheating step, the quality deviation according to the temperature difference between the plurality of food in the ultra-high pressure processor B, there is no effect of quality variation inside the food.
또한, 본 발명의 상온멸균 및 냉장식품의 가열 초고압 살균방법에서, 상기 냉각 단계는 초고압 처리된 식품을 5℃이하에서 약 20분 정도 급냉하는 단계이다. In addition, in the ultra-high pressure sterilization method of room temperature sterilization and refrigerated foods of the present invention, the cooling step is a step of rapidly cooling the ultra-high pressure processed food at about 5 ° C. or less for about 20 minutes.
살균처리 후 냉각속도를 완만히 하는 경우에는 식품 내 단백질로부터 황화수소의 발생량이 많아 흑변되기 쉽고, 또한, 이외에 흑변 현상을 야기하는 원인균인 클로스티리움 니그리피칸스(Clostridium nigrificans)가 호열성 균으로, 최적의 발육 온도가 55℃이므로, 완만하게 냉각할 경우 이 온도범위에서 포자가 발아하기 용이하므로, 급냉하는 것이 바람직하다. If the cooling rate is slow after sterilization, the amount of hydrogen sulfide from the protein in the food tends to be blackened, and in addition, Clostridium nigrificans , a cause of blackening , is a thermophilic bacterium. Since the optimum growth temperature is 55 ° C, spores tend to germinate in this temperature range when gently cooled, and therefore, quenching is preferable.
본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법에서는, 초고압의 압력을 제거하면 압력이 대기압인 0.1MPa까지 떨어지는데 소요되는 90초라는 짧은 시간 내에 제품의 온도가 예열 온도 이하로 내려가므로, 냉각단계시 빠른 시간 내에 급냉이 가능한 효과가 있다. In the method of sterilization and heating ultra high pressure sterilization of refrigerated foods of the present invention, when the ultra high pressure is removed, the temperature of the product falls below the preheating temperature within a short time of 90 seconds required for the pressure to drop to 0.1 MPa. Quick cooling time is effective.
본 발명의 상온멸균 및 냉장식품의 가열 초고압 살균방법에서 예열 단계, 초고압 처리 단계, 급냉 단계를 위한 이동은 컨베이어 벨트를 통해 자동으로 이송되게 하는 것이 바람직하다. In the heating ultrahigh pressure sterilization method of the room temperature sterilization and refrigerated food of the present invention, it is preferable that the movement for the preheating step, the ultrahigh pressure processing step, and the quenching step is automatically transferred through the conveyor belt.
이하에서는 실시예를 통하여 본 발명을 구체적으로 설명한다. 다만 이들 실시예는 본 발명을 구체적으로 설명하기 위한 예시일 뿐, 본 발명의 권리범위가 이들 실시예로 한정되는 것은 아니다. Hereinafter, the present invention will be described in detail through examples. However, these examples are merely illustrative for describing the present invention in detail, and the scope of the present invention is not limited to these examples.
실시예 A : 본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법으로 살균처리된 다양한 가공식품의 상온유통 또는 냉장유통 가능여부 확인 실험 Example A: Experiment of confirming whether room temperature distribution or refrigeration distribution is possible for various processed foods sterilized by heating ultrahigh pressure sterilization method of room temperature sterilization and refrigerated food of the present invention
A-1. 크림소스의 상온유통 또는 냉장유통A-1. Cold or cold distribution of cream sauce 가능여부 확인 실험Experiment to check the availability
크림소스를 다양한 예열 온도로 예열 처리 후 초고압 처리한 경우, 상온유통 또는 냉장유통이 가능한지 여부를 확인하기 위하여 아래와 같이 실험하였다. When the cream sauce was preheated to various preheating temperatures and then subjected to ultra-high pressure, the following experiment was conducted to determine whether room temperature distribution or refrigeration distribution is possible.
(1) 90?로 예열된 크림소스를 600MPa에서 5분간 초고압처리(1) Ultra high pressure treatment of cream sauce preheated to 90 ° at 600 MPa for 5 minutes.
크림소스 제조 후, 초기 균수는 1×101 수준이였으며, 이 균들은 모두 내열성 균이었다. After the preparation of the cream sauce, the initial number of bacteria was 1 × 10 1 level and all of them were heat resistant bacteria.
크림소스를 파우치에 충진 후, 워터 배스(water bath) (Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath.)에서 온도가 90℃가 되도록 예열하였다. 그후, 초고압 처리기(Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel)로 이송 후 600MPa에서 5분간 초고압 처리하였다. 600MPa까지 승압되는 90초의 시간 동안 제품 온도가 115~120℃까지 상승되었으며, 이 상태에서 5분간 초고압 처리하였다. After filling the cream sauce into the pouch, it was preheated to a temperature of 90 ℃ in a water bath (Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath.). Subsequently, after being transferred to an ultra high pressure processor (Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel) was subjected to ultra high pressure at 600MPa for 5 minutes. The product temperature was raised to 115-120 ° C. during the 90 seconds stepped up to 600 MPa, and the ultrahigh pressure treatment was performed for 5 minutes in this state.
그후 5℃ 이하에서 20분간 급냉시켰다. It was then quenched for 20 minutes at 5 DEG C or lower.
그후 상온유통 가능여부 확인을 위해 식품공전상에 명시되어 있는 레토르트 상온유통 제품 세균발육 테스트를 이용하였다. Then, the retort room temperature distribution product bacteria development test specified in the Food Code was used to confirm whether the room temperature distribution is possible.
35℃ 인큐베이터(incubator)에서 상기 급냉된 가열 초고압 살균 식품 10개의 샘플을 10일간 보관한 뒤 미생물 테스트를 진행하였다. 그 결과 10개의 샘플 모두 미생물 음성 결과가 나왔다. 10 samples of the quenched heated ultra-high pressure sterilized food were stored in a 35 ° C. incubator for 10 days and then microbiological test was performed. The result was microbial negative results for all 10 samples.
이는 본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법이, 특히, 예열 온도를 90℃이상으로 처리한 후 600MPa의 압력으로 처리한 경우, 상온유통 제품의 살균방법으로 적합함을 보여주는 결과라 하겠다. This is a result showing that the method of sterilization and heating ultra-high pressure sterilization of refrigerated food of the present invention is suitable as a sterilization method of the normal temperature distribution products, especially when the preheating temperature is treated at a pressure of 600MPa after the preheating temperature is higher than 90 ℃. .
(2) 70℃로 예열된 크림소스를 600MPa에서 5분간 초고압처리(2) Ultra high pressure treatment of cream sauce preheated at 70 ℃ for 5 minutes at 600MPa
크림소스 제조 후 초기 균수는 총 1×102 이였으며, 이 중 1×101 이 내열성 세균으로 검출되었다. After the preparation of the cream sauce, the initial bacterial count was 1 × 10 2 , and 1 × 10 1 was detected as heat-resistant bacteria.
크림소스를 파우치에 충진 후, 워터 배스(water bath) (Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath)에서 온도가 70℃가 되도록 예열하였다. 그후, 초고압 처리기(Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel)로 이송 후 600MPa에서 5분간 초고압 처리하였다.After filling the cream sauce into the pouch, it was preheated to a temperature of 70 ℃ in a water bath (Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath). Subsequently, after being transferred to an ultra high pressure processor (Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel) was subjected to ultra high pressure at 600MPa for 5 minutes.
600MPa까지 승압되는 90초의 시간 동안 제품 온도가 95~99℃까지 상승되었으며, 이 상태에서 5분간 초고압 처리하였다. The product temperature was raised to 95-99 ° C. during the 90 seconds of stepping up to 600 MPa, and in this state, ultrahigh pressure treatment was performed for 5 minutes.
그후 5℃ 이하에서 20분간 제품을 급냉시켰다. The product was then quenched at 5 ° C. or lower for 20 minutes.
그후 상기 급냉된 가열 초고압 살균 식품을 10℃, 15℃ 인큐베이터(incubator)에서 각각 저장하면서 유통기한 테스트를 진행하였다. Thereafter, the quenched heated ultrahigh pressure sterilized food was stored in a 10 ° C. and 15 ° C. incubator, respectively, and the expiration date test was performed.
살균 직후 내열성 세균을 포함한 세균이 검출되지 않았으며, 12주간의 저장기간 동안 세균이 검출되지 않았다. Immediately after sterilization, no bacteria, including heat-resistant bacteria, were detected and no bacteria were detected during the storage period of 12 weeks.
이를 통해 본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법으로 처리된 크림소스는 12주를 유통기한으로 냉장유통이 가능함을 확인할 수 있었다. Through this, the cream sauce treated by the method of heating high-temperature sterilization of the room temperature sterilization and refrigerated food of the present invention was confirmed that refrigeration distribution is possible with a shelf life of 12 weeks.
(3) 80℃로 예열된 크림소스를 600MPa에서 5분간 초고압처리(3) Ultra high pressure treatment for 5 minutes at 600MPa cream sauce preheated to 80 ℃
크림소스 제조 후 초기 균수는 총 2×102 이였으며, 이 중 1.5×101 이 내열성 세균으로 검출되었다. After the preparation of the cream sauce, the initial bacterial count was 2 × 10 2 , and 1.5 × 10 1 was detected as heat resistant bacteria.
크림소스를 파우치에 충진 후, 워터 배스(water bath) (Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath)에서 온도가 80℃가 되도록 예열하였다. 그후, 초고압 처리기(Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel)로 이송 후 600MPa에서 5분간 초고압 처리하였다. 600MPa까지 승압되는 90초의 시간 동안 제품 온도가 105~109℃까지 상승되었으며, 이 상태에서 5분간 초고압 처리하였다. The cream sauce was filled into the pouch and then preheated to 80 ° C. in a water bath (Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath). Subsequently, after being transferred to an ultra high pressure processor (Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel) was subjected to ultra high pressure at 600MPa for 5 minutes. The product temperature was raised to 105-109 ° C. during the 90 seconds stepped up to 600 MPa, and the ultrahigh pressure treatment was performed for 5 minutes in this state.
그후 5℃ 이하에서 20분간 제품을 급냉시켰다. The product was then quenched at 5 ° C. or lower for 20 minutes.
그후 상기 급냉된 가열 초고압 살균 식품을 10℃, 15℃ 인큐베이터(incubator)에서 각각 저장하면서 유통기한 테스트를 진행하였다. Thereafter, the quenched heated ultrahigh pressure sterilized food was stored in a 10 ° C. and 15 ° C. incubator, respectively, and the expiration date test was performed.
살균 직후 내열성 세균을 포함한 세균이 검출되지 않았으며, 12주간의 저장기간 동안 세균이 검출되지 않았다. Immediately after sterilization, no bacteria, including heat-resistant bacteria, were detected and no bacteria were detected during the storage period of 12 weeks.
이를 통해 본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법으로 처리된 크림소스는 12주를 유통기한으로 냉장유통이 가능함을 확인할 수 있었다. Through this, the cream sauce treated by the method of heating high-temperature sterilization of the room temperature sterilization and refrigerated food of the present invention was confirmed that refrigeration distribution is possible with a shelf life of 12 weeks.
A-2. 제육덮밥 소스의 냉장유통A-2. Refrigerated distribution of meat sauce 가능여부 확인 실험Experiment to check the availability
제육덮밥 소스를 다양한 예열 온도로 예열 처리 후 초고압 처리한 경우, 냉장유통이 가능한지 여부를 확인하기 위하여 아래와 같이 실험하였다. In the case of ultra-high pressure treatment after preheating the yukyukbap sauce at various preheating temperatures, the following experiments were conducted to determine whether refrigeration distribution is possible.
(1) 70℃로 예열된 제육덮밥 소스를 600MPa에서 5분간 초고압처리(1) Ultra-high pressure treatment for 5 minutes at 600MPa of the meat-covered rice sauce preheated to 70 ℃
제육덮밥 소스 제조 후 초기 균수는 총 7×104 이였으며, 이 중 3×102 이 내열성 세균으로 검출되었다. . The total number of bacteria was 7 × 10 4 after preparation of the Jeok-yuk bowl sauce, of which 3 × 10 2 was detected as heat-resistant bacteria. .
제육덮밥 소스를 파우치에 충진 후, 워터 배스(water bath) (Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath)에서 온도가 70℃가 되도록 예열하였다. 그후, 초고압 처리기(Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel)로 이송 후 600MPa에서 5분간 초고압 처리하였다. 600MPa까지 승압되는 90초의 시간 동안 제품 온도가 95~99℃까지 상승되었으며, 이 상태에서 5분간 초고압 처리하였다. The fleshed rice bowl was filled with a pouch and preheated to 70 ° C. in a water bath (Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath). Subsequently, after being transferred to an ultra high pressure processor (Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel) was subjected to ultra high pressure at 600MPa for 5 minutes. The product temperature was raised to 95-99 ° C. during the 90 seconds of stepping up to 600 MPa, and in this state, ultrahigh pressure treatment was performed for 5 minutes.
그후 5℃ 이하에 20분간 제품을 급냉시켰다. The product was then quenched for 20 minutes below 5 ° C.
그후 상기 급냉된 가열 초고압 살균 식품을 10℃, 15℃ 인큐베이터(incubator)에서 각각 저장하면서 유통기한 테스트를 진행하였다. Thereafter, the quenched heated ultrahigh pressure sterilized food was stored in a 10 ° C. and 15 ° C. incubator, respectively, and the expiration date test was performed.
살균 직후 내열성 세균을 포함한 세균이 검출되지 않았으며, 12주간의 저장기간 동안 세균이 검출되지 않았다. Immediately after sterilization, no bacteria, including heat-resistant bacteria, were detected and no bacteria were detected during the storage period of 12 weeks.
이를 통해 본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법으로 처리된 제육덮밥 소스는 12주를 유통기한으로 냉장유통이 가능함을 확인할 수 있었다. As a result, it was confirmed that the meat-covered rice sauce treated by the heating ultrahigh pressure sterilization method of the normal temperature sterilization and refrigerated food of the present invention can be refrigerated with a shelf life of 12 weeks.
(2) 80℃로 예열된 제육덮밥 소스를 600MPa에서 5분간 초고압처리(2) Ultra-high pressure treatment for 5 minutes at 600MPa of the meat-covered rice sauce preheated to 80 ℃
제육덮밥 소스 제조 후, 초기 균수는 총 7×104 이였으며, 이 중 3×102 이 내열성 세균으로 검출되었다. After preparation of the yukyukdonbap sauce, the initial number of bacteria was 7 × 10 4 , of which 3 × 10 2 was detected as heat-resistant bacteria.
제육덮밥 소스를 파우치에 충진 후, 워터 배스(water bath) (Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath)에서 온도가 80℃가 되도록 예열하였다. 그후, 초고압 처리기(Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel)로 이송 후 600MPa에서 5분간 초고압 처리하였다. 600MPa까지 승압되는 90초의 시간 동안 제품 온도가 105~109℃까지 상승되었으며, 이 상태에서 5분간 초고압 처리하였다. After filling the puffed rice sauce with a pouch, it was preheated to a temperature of 80 ° C. in a water bath (Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath). Subsequently, after being transferred to an ultra high pressure processor (Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel) was subjected to ultra high pressure at 600MPa for 5 minutes. The product temperature was raised to 105-109 ° C. during the 90 seconds stepped up to 600 MPa, and the ultrahigh pressure treatment was performed for 5 minutes in this state.
그후 5℃ 이하에서 20분간 제품을 급냉시켰다. The product was then quenched at 5 ° C. or lower for 20 minutes.
그후 상기 급냉된 가열 초고압 살균 식품을 10℃, 15℃ 인큐베이터(incubator)에서 각각 저장하면서 유통기한 테스트를 진행하였다. Thereafter, the quenched heated ultrahigh pressure sterilized food was stored in a 10 ° C. and 15 ° C. incubator, respectively, and the expiration date test was performed.
살균 직후 내열성 세균을 포함한 세균이 검출되지 않았으며, 12주간의 저장기간 동안 세균이 검출되지 않았다. Immediately after sterilization, no bacteria, including heat-resistant bacteria, were detected and no bacteria were detected during the storage period of 12 weeks.
이를 통해 본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법으로 처리된 제육덮밥 소스는 12주를 유통기한으로 냉장유통이 가능함을 확인할 수 있었다. As a result, it was confirmed that the meat-covered rice sauce treated by the heating ultrahigh pressure sterilization method of the normal temperature sterilization and refrigerated food of the present invention can be refrigerated with a shelf life of 12 weeks.
A-3. 소고기덮밥 소스의 냉장유통 가능여부 확인 실험A-3. Experiment to confirm whether cold distribution of beef bowl sauce is possible
소고기덮밥 소스를 일정 예열 온도로 예열 처리 후 초고압 처리한 경우, 냉장유통이 가능한지 여부를 확인하기 위하여 아래와 같이 실험하였다. When the beef bowl was preheated to a predetermined preheating temperature and then treated with ultra high pressure, the following experiment was conducted to determine whether refrigeration distribution is possible.
(1) 80℃로 예열된 소고기덮밥 소스를 600MPa 5분간 초고압처리(1) 600MPa 5 minutes ultra high pressure treatment of beef rice sauce preheated to 80 ℃
소고기덮밥 소스 제조 후, 초기 균수는 총 1×101 이였으며, 모두 내열성 세균으로 검출되었다. . After preparing the beef bowl sauce, the initial bacterial count was 1 × 10 1 , and all of them were detected as heat-resistant bacteria. .
소고기덮밥 소스를 파우치에 충진 후, 워터 배스(water bath) (Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath)에서 온도가 80℃가 되도록 예열하였다. 그후, 초고압 처리기(Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel)로 이송 후 600MPa에서 5분간 초고압 처리하였다. 600MPa까지 승압되는 90초의 시간 동안 제품 온도가 105~109℃까지 상승되었으며, 이 상태에서 5분간 초고압 처리하였다. The beef bowl sauce was filled into pouches and preheated to 80 ° C. in a water bath (Conditioning bath, Stansted Fluid Power, FPG 11500B 110 high pressure conditioning bath). Subsequently, after being transferred to an ultra high pressure processor (Vessel, Stansted Fluid Power, FPG 11500 System FPG 11570 110 Vessel) was subjected to ultra high pressure at 600MPa for 5 minutes. The product temperature was raised to 105-109 ° C. during the 90 seconds stepped up to 600 MPa, and the ultrahigh pressure treatment was performed for 5 minutes in this state.
그후 5℃ 이하에서 20분간 제품을 급냉시켰다. The product was then quenched at 5 ° C. or lower for 20 minutes.
그후 상기 급냉된 레토르트 식품을 10℃, 15℃ 인큐베이터(incubator)에서 각각 저장하면서 유통기한 테스트를 진행하였다. Thereafter, the quenched retort foods were stored in 10 ° C. and 15 ° C. incubators, respectively, and the expiration date test was performed.
살균 직후 내열성 세균을 포함한 세균이 검출되지 않았으며, 12주간의 저장기간 동안 세균이 검출되지 않았다. Immediately after sterilization, no bacteria, including heat-resistant bacteria, were detected and no bacteria were detected during the storage period of 12 weeks.
이를 통해 본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법으로 처리된 소고기덮밥 소스는 12주를 유통기한으로 냉장 유통이 가능함을 확인할 수 있었다.Through this, it was confirmed that the beef bowl source treated with the heating ultrahigh pressure sterilization method of the normal temperature sterilization and refrigerated food of the present invention can be refrigerated with a shelf life of 12 weeks.
실시예 B : 본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법으로 살균처리된 가공식품에 대한 소비자 기호도 조사 Example B: Investigation of consumer's preference for processed food sterilized by heating ultrahigh pressure sterilization method of room temperature sterilization and refrigerated food of the present invention
B-1. 통상적인 레토르트 처리 제품과의 소비자 기호도 비교 실험 및 색상 비 교 실험 B-1. Comparison of consumer preference and color comparison with conventional retort treatment products
본 발명의 가열 초고압 살균방법으로 처리된 가공 식품(실시예 1 내지 3)과 통상적인 레토르트 살균방법으로 처리된 레토르트 식품(비교예 1 내지 3)의 관능적 특성 및 제품 특성을 평가하기 위해, 소고기덮밥 소스, 매운닭고기덮밥 소스, 크림소스에 대한 소비자 기호도를 조사하였다. In order to evaluate the sensory properties and product characteristics of the processed foods (Examples 1 to 3) and the retort foods (Comparative Examples 1 to 3) treated by the conventional retort sterilization method, the beef rice bowl Consumer preference for sauce, spicy chicken rice sauce, and cream sauce was investigated.
실시예와 비교예의 가열 초고압 살균 및 레토르트 식품 모두 상온유통이 가능한 조건으로 진행하였다. Both the ultra-high pressure sterilization and the retort foods of Examples and Comparative Examples were conducted under conditions where normal temperature distribution was possible.
다시 말해 상기 실시예의 경우, 예열 단계에서 온도를 90℃로 처리한 후 600MPa의 압력으로 처리한 후 급냉하였고, 비교예의 경우 110~130℃에서 20분 내지 60분 살균한 후 급냉하여, 실시예 및 비교예 모두 상온유통이 가능한 조건으로 살균처리하였다. In other words, in the case of the above embodiment, the temperature was treated at a temperature of 90 ℃ in the preheating step and then quenched after treatment with a pressure of 600MPa, in the case of the comparative example sterilized after sterilization for 20 to 60 minutes at 110 ~ 130 ℃, Examples and All of the comparative examples were sterilized under conditions in which normal temperature distribution was possible.
소비자 기호도 조사는 서울, 경기권에 거주하는 만 25세~50세 주부 50~60명을 대상으로 실시하였으며, 조사형태는 기호척도법(5 point hedonic test)을 활용한 소비자 기호도 조사로 실시하였다. 조사분석방법은 Mean/ANOVA/Open 문항 분석방법으로 실시하였으며, 그 결과는 표 1 내지 3과 같다. GAP은 각 항목에 대한 두 살균법 사이의 점수차를 의미한다. The consumer preference survey was conducted for 50 to 60 housewives aged 25 to 50 living in Gyeonggi-do, Seoul, and the survey was conducted with a consumer preference survey using the 5-point hedonic test. Survey analysis method was performed by Mean / ANOVA / Open item analysis method, the results are shown in Table 1 to 3. GAP means the difference in scores between the two sterilization methods for each item.
표 1 소고기덮밥 소스에 대한 소비사 조사 결과
  비교예 1 실시예 1 GAP
전반기호도 3.38 3.63 0.25
소스색상 3.64 3.73 0.09
고기의 씹는느낌 3.24 3.81 0.57
Table 1 Consumer Survey on Beef Rice Sauce
Comparative Example 1 Example 1 GAP
First half diagram 3.38 3.63 0.25
Source color 3.64 3.73 0.09
Chewing of meat 3.24 3.81 0.57
본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법으로 처리된 소고기덮밥 소스(실시예 1)가 종래의 레토르트 살균방법으로 처리된 소고기 덮밥 소스(비교예 1)에 비해 전반기호도, 소스색상, 고기의 씹는 느낌 등이 우수함을 확인하였다. Beef bowl sauce (Example 1) treated by the heating ultra-high pressure sterilization method of the room temperature sterilization and refrigerated food of the present invention compared to the beef bowl sauce (Comparative Example 1) treated with the conventional retort sterilization method, the first sign, sauce color, meat It was confirmed that the chewing feeling is excellent.
표 2 매운닭고기덮밥 소스에 대한 소비사 조사 결과
  비교예 2 실시예 2 GAP
전반기호도 3.24 3.74 0.5
소스색상 2.97 3.78 0.77
고기의 씹는느낌 3.35 3.91 0.56
TABLE 2 Consumer Survey on Spicy Chicken Rice Sauce
Comparative Example 2 Example 2 GAP
First half diagram 3.24 3.74 0.5
Source color 2.97 3.78 0.77
Chewing of meat 3.35 3.91 0.56
본 발명의 가열 초고압 살균방법으로 처리된 매운닭고기덮밥 소스(실시예 2)가 종래의 레토르트 살균방법으로 처리된 매운닭고기덮밥 소스(비교예 2)에 비해 전반기호도, 소스색상, 고기의 씹는 느낌 등이 우수함을 확인하였다. Compared to the spicy chicken rice sauce (Example 2) treated with the heating ultra-high pressure sterilization method of the present invention compared to the spicy chicken rice sauce (Comparative Example 2) treated with the conventional retort sterilization method, the taste of the sauce, the color of the chewing, etc. This excellence was confirmed.
표 3 크림소스에 대한 소비사 조사 결과
  비교예 3 실시예 3 GAP
전반기호도 3.43 3.57 0.14
외관기호도 3.15 3.39 0.24
크림향미 기호도 3.59 3.62 0.03
TABLE 3 Consumer Survey Results for Cream Sauce
Comparative Example 3 Example 3 GAP
First half diagram 3.43 3.57 0.14
Exterior Symbol 3.15 3.39 0.24
Cream flavor symbol 3.59 3.62 0.03
본 발명의 가열 초고압 살균방법으로 처리된 크림소스(실시예 3)가 종래의 레토르트 살균방법으로 처리된 크림소스(비교예 3)에 비해 전반기호도, 외관기호도, 크림향미 등이 우수함을 확인하였다. It was confirmed that the cream sauce (Example 3) treated by the heating ultrahigh pressure sterilization method of the present invention had superior first half symbol, appearance symbol, and cream flavor compared to the cream sauce (Comparative Example 3) treated by the conventional retort sterilization method.
또한, 도 1는 본 발명의 소고기덮밥 소스(실시예 1)와 종래의 레토르트 살균방법으로 처리된 소고기덮밥 소스(비교예 1)를 비교해 놓은 사진이다. 비교예 1의 소고기덮밥 소스의 색상이 실시예 1의 소고기덮밥 소스에 비해 어둡게 변했음을 확인할 수 있다. In addition, Figure 1 is a photograph comparing the beef bowl sauce (Example 1) of the present invention and the beef bowl sauce (Comparative Example 1) treated by a conventional retort sterilization method. It can be seen that the color of the beef bowl sauce of Comparative Example 1 is darker than the beef bowl sauce of Example 1.
또한, 도 2는 본 발명의 매운닭고기덮밥 소스(실시예 2)와 종래의 레토르트 살균방법으로 처리된 매운닭고기덮밥 소스(비교예 2)를 비교한 사진이다. 비교예 2의 매운닭고기덮밥 소스의 색상이 실시예 2의 매운닭고기덮밥 소스에 비해 어둡게 변했음을 확인할 수 있다.2 is a photograph comparing the spicy chicken rice sauce (Example 2) of the present invention and the spicy chicken rice sauce (Comparative Example 2) treated by the conventional retort sterilization method. It can be seen that the color of the spicy chicken rice sauce of Comparative Example 2 is darker than the spicy chicken rice sauce of Example 2.
또한, 도 3은 본 발명의 크림소스(실시예 3)와 종래의 레토르트 살균방법으로 처리된 크림소스(비교예 3)를 비교해 놓은 사진이다. 비교예 3의 크림소스의 색상은 어둡게 변한 반면, 실시예 3의 크림소스는 본연의 크림 색상을 유지하고 있음을 확인할 수 있다. 3 is a photograph comparing the cream sauce (Example 3) of the present invention with the cream sauce (Comparative Example 3) treated by the conventional retort sterilization method. While the color of the cream sauce of Comparative Example 3 changed dark, it can be seen that the cream sauce of Example 3 maintains its original cream color.
따라서 상기와 같은 실험결과를 통해 본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법은 살균효과가 우수하면서도, 살균 후에도 조리 직후의 제품 본연의 맛, 향, 조직감 및 색상이 그대로 유지되어, 고품질의 상온멸균 및 냉장 식품의 제조가 가능함을 알 수 있다. Therefore, the ultra-high pressure sterilization method of the room temperature sterilization and refrigerated foods of the present invention through the above experimental results is excellent in sterilization effect, while maintaining the original taste, aroma, texture and color of the product immediately after cooking, It can be seen that the production of food sterilization and refrigerated food.
B-2. 배합조건을 상이하게 한 경우 소비자 기호도 실험 B-2. Experiment with consumer preference when different mixing conditions
상기 표 1 내지 3의 제품의 배합을 바탕으로 품질력을 극대화 하여 본 발명의 가열 초고압 살균방법으로 살균처리한 제품만 소비자 조사를 진행한 결과는 표 4, 표 5 이다.Based on the formulation of the products of Tables 1 to 3, the results of the consumer survey of only products sterilized by the heating ultra-high pressure sterilization method of the present invention are Table 4 and Table 5.
살균방법은 표 4는 냉장유통 조건(예열온도 70 ℃ 처리 후 초고압 처리)으로 살균처리한 것이고, 표 5은 상온유통 조건(예열온도 90℃ 처리 후 초고압 처리)으로 살균처리한 결과이다. Sterilization method Table 4 is the sterilization treatment under refrigeration distribution conditions (preheating temperature 70 ℃ after ultra-high pressure treatment), Table 5 is the result of sterilization treatment at room temperature distribution conditions (preheating temperature 90 ℃ after ultra-high pressure treatment).
표 1에서는 레토르트 살균은 고기 조직감에 많은 영향을 주기 때문에 고기를 5mm정도로 사용했었으나, 본 발명의 가열 초고압 살균방법이 조직감에 미치는 영향이 작다는 것에 착안하여 표 4에서는 고기의 두께는 3mm로 줄여서 건더기 씹힘 기호도를 상승시켰다. 또한, 레토르트에 약한 야채의 함량을 5% 상승시키고 고기의 함량을 5% 감소시켜 전체적인 맛을 상승시켰다. 크림소스는 가열 초고압 살균할 경우 유화안정성이 깨지며 살균 후 점도가 레토르트 대비 낮아지는 단점이 있다. 표 5에서는 이를 개선하기 위하여 전분의 함량을 증가시키고 산탄검의 첨가로 유화안정성을 확보하고 점도가 낮아지는 현상을 방지하였다. 표 3에서는 레토르트 제품용 배합으로 가열초고압 및 레토르트 처리를 하였으나 표 5에서는 크림과 우유, 베이컨의 함량을 올린 가열 초고압 살균 전용 배합을 사용하였다.In Table 1, since the retort sterilization had a large effect on meat texture, the meat was used at about 5 mm. However, in view of the fact that the heating ultra-high pressure sterilization method of the present invention had a small effect on the texture, the thickness of the meat was reduced to 3 mm. Increased chewing preference. In addition, the content of vegetables that are weak in retort was increased by 5% and the meat content was reduced by 5% to increase the overall taste. Cream sauce has the disadvantage that the emulsification stability is broken when the ultra-high pressure sterilization is heated, the viscosity is lower than the retort after sterilization. In Table 5, to improve this, the content of starch was increased, and the addition of xanthan gum ensured the emulsion stability and prevented the phenomenon of low viscosity. In Table 3, the super high pressure and retort treatment were used as the formulation for the retort product, but in Table 5, only the super high pressure sterilization formulation with the content of cream, milk, and bacon was used.
조사방법은 위 B-1과 동일하게 하였다.The investigation method was the same as the above B-1.
표 4 소고기덮밥 소스 소비자 조사 결과
  전반적인 맛 점수
전반기호도 3.86
외관기호도 3.97
향기호도 3.84
건더기 씹힘 기호도 4.03
소스의 맛 기호도 3.73
Table 4 Beef Rice Sauce Consumer Survey
Overall taste score
First half diagram 3.86
Exterior Symbol 3.97
Fragrance 3.84
Dried Chew Symbol 4.03
Taste taste of sauce 3.73
표 5 크림소스 소비자 조사 결과
  전반적인 맛 점수
전반기호도 3.82
외관기호도 3.8
소스의 맛 기호도 3.9
크림 향미 기호도 3.84
치즈맛 기호도 3.76
뒷맛 기호고 3.82
Table 5 Cream Sauce Consumer Survey
Overall taste score
First half diagram 3.82
Exterior Symbol 3.8
Taste taste of sauce 3.9
Cream flavor symbol 3.84
Cheese flavor 3.76
Aftertaste sign 3.82
상기 표 4 내지 5의 결과를 통해, 본 발명의 상온멸균 및 냉장 식품의 가열 초고압 살균방법으로 처리된 소고기 덮밥 소스(실시예 4) 및 크림소스(실시예 5)가 전반적인 맛 점수가 3.8이상으로, 소비자 기호도가 높음을 확인할 수 있었다. Through the results of the above Tables 4 to 5, the beef rice sauce (Example 4) and cream sauce (Example 5) treated by the heating ultra-high pressure sterilization method of the room temperature sterilization and refrigerated foods of the present invention has an overall taste score of 3.8 or more In addition, it was confirmed that consumer preference was high.

Claims (6)

  1. 상온멸균 및 냉장 식품의 가열 초고압 살균방법에 있어서, In the ultra-high pressure sterilization method of room temperature sterilization and refrigerated food,
    조리된 식품을 파우치에 충진하는 충진 단계;A filling step of filling the pouch with cooked food;
    상기 파우치에 충진된 식품을 60~100℃로 가열하는 예열 단계;Preheating step of heating the food filled in the pouch to 60 ~ 100 ℃;
    상기 예열된 식품을 500MPa~700MPa로 초고압 처리하는 초고압 살균 단계;Ultra high pressure sterilization step of ultra-high pressure treatment of the preheated food to 500MPa ~ 700MPa;
    상기 초고압 살균처리된 식품을 급냉하는 냉각 단계;를 포함하는 상온멸균 및 냉장 식품식품의 가열 초고압 살균방법.Sterilizing the food at room temperature sterilization and refrigerated food comprising a cooling step of quenching the ultra-high pressure sterilized food.
  2. 제1항에 있어서, The method of claim 1,
    상기 예열 단계는 워터 배스(water bath), 스팀 터널, 열수 샤워 방법 중 선택된 하나의 방법을 사용하는 것을 특징으로 하는 상온멸균 및 냉장 식품의 가열 초고압 살균방법. The preheating step is a method for heating ultra-high pressure sterilization of the normal temperature sterilization and refrigerated food, characterized in that using one of the water bath (water bath), steam tunnel, hot water shower method.
  3. 제1항에 있어서, The method of claim 1,
    상기 예열 단계는 워터 배스(water bath)로 이루어지는 것을 특징으로 하는 상온멸균 및 냉장 식품의 가열초고압 살균방법.The preheating step is a heating ultrahigh pressure sterilization method of the normal temperature sterilization and refrigerated food, characterized in that the water bath (water bath).
  4. 제1항에 있어서, The method of claim 1,
    상온유통 가능 조건을 위해 상기 예열 단계에서 식품의 온도가 90~100℃ 가 되도록 예열하는 것을 특징으로 하는 상온멸균 및 냉장 식품의 가열 초고압 살균방법. Method for sterilization and refrigeration of cold foods, characterized in that the preheating step so that the temperature of the food in the preheating step to the ambient temperature distribution possible conditions.
  5. 제1항에 있어서, The method of claim 1,
    냉장유통 가능 조건을 위해 상기 예열 단계에서 식품의 온도가 60~90℃가 되도록 예열하는 것을 특징으로 하는 상온멸균 및 냉장 식품의 가열 초고압 살균방법. Sterilization method for heating and normal temperature sterilization and refrigerated foods, characterized in that the preheating step so that the temperature of the food in the preheating step for the refrigerated distribution possible conditions.
  6. 제1항에 있어서, The method of claim 1,
    상기 초고압 살균 단계의 처리시간은 1분 내지 10분인 것을 특징으로 하는 상온멸균 및 냉장 식품식품의 가열 초고압 살균방법. The treatment time of the ultra-high pressure sterilization step is a heating ultra-high pressure sterilization method of room temperature sterilization and refrigerated foods, characterized in that 1 to 10 minutes.
PCT/KR2013/011726 2012-12-17 2013-12-17 Heating and ultra-high-pressure sterilisation method for ambient-temperature-sterile and refrigerated food WO2014098443A1 (en)

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CN110637987A (en) * 2019-09-11 2020-01-03 中国农业大学 Preparation method and application of pork ribs with fermented soybean juice based on ultrahigh pressure
CN112914058A (en) * 2021-03-16 2021-06-08 中国农业大学 Method for making crisp and tasty pot-stewed lotus roots
CN113662144A (en) * 2021-07-19 2021-11-19 山西农业大学山西功能食品研究院 Preparation method of sauced meat

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JPH11169103A (en) * 1997-12-11 1999-06-29 Shikoku Kakoki Co Ltd Production of prepared food by high pressure treatment
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Publication number Priority date Publication date Assignee Title
CN110637987A (en) * 2019-09-11 2020-01-03 中国农业大学 Preparation method and application of pork ribs with fermented soybean juice based on ultrahigh pressure
CN112914058A (en) * 2021-03-16 2021-06-08 中国农业大学 Method for making crisp and tasty pot-stewed lotus roots
CN113662144A (en) * 2021-07-19 2021-11-19 山西农业大学山西功能食品研究院 Preparation method of sauced meat

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