WO2014013397A3 - Katalysator zur herstellung von carbonsäuren und/oder carbonsäureanhydriden - Google Patents

Katalysator zur herstellung von carbonsäuren und/oder carbonsäureanhydriden Download PDF

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Publication number
WO2014013397A3
WO2014013397A3 PCT/IB2013/055729 IB2013055729W WO2014013397A3 WO 2014013397 A3 WO2014013397 A3 WO 2014013397A3 IB 2013055729 W IB2013055729 W IB 2013055729W WO 2014013397 A3 WO2014013397 A3 WO 2014013397A3
Authority
WO
WIPO (PCT)
Prior art keywords
catalyst
carboxylic
preparing
anhydrides
carboxylic acids
Prior art date
Application number
PCT/IB2013/055729
Other languages
English (en)
French (fr)
Other versions
WO2014013397A2 (de
Inventor
Michael Krämer
Jürgen ZÜHLKE
Stefan Altwasser
Nico Frederik FISCHER
Frank Rosowski
Hans-Martin Allmann
Original Assignee
Basf Se
Basf Schweiz Ag
Basf (China) Company Limited
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se, Basf Schweiz Ag, Basf (China) Company Limited filed Critical Basf Se
Priority to CN201380037094.3A priority Critical patent/CN104487164A/zh
Priority to JP2015522211A priority patent/JP2015530228A/ja
Priority to EP13820174.4A priority patent/EP2872251A4/de
Publication of WO2014013397A2 publication Critical patent/WO2014013397A2/de
Publication of WO2014013397A3 publication Critical patent/WO2014013397A3/de

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/20—Vanadium, niobium or tantalum
    • B01J23/22—Vanadium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B01J35/391—Physical properties of the active metal ingredient
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B01J35/391—Physical properties of the active metal ingredient
    • B01J35/393—Metal or metal oxide crystallite size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/613—10-100 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • B01J37/0225—Coating of metal substrates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/024—Multiple impregnation or coating
    • B01J37/0244—Coatings comprising several layers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/04—Mixing
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/77—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D307/87—Benzo [c] furans; Hydrogenated benzo [c] furans
    • C07D307/89—Benzo [c] furans; Hydrogenated benzo [c] furans with two oxygen atoms directly attached in positions 1 and 3

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Catalysts (AREA)
  • Furan Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Die vorliegende Erfindung betrifft einen Katalysator zur Herstellung von Carbonsäuren und/oder Carbonsäureanhydriden, der mehrere hintereinander angeordnete Katalysatorlagen aufweist, zu dessen Herstellung ein Vanadiumantimonat mit einem maximalen Gehalt an kristallinem Valentinit von 5 Gew.-% eingesetzt wurde. Ferner betrifft die vorliegende Erfindung ein Verfahren zur Gasphasenoxidation, bei dem man einen Gasstrom, der mindestens einen Kohlenwasserstoff und molekularen Sauerstoff umfasst, durch einen Katalysator leitet, der mehrere hintereinander angeordnete Katalysatorlagen aufweist und zu dessen Herstellung ein Vanadiumantimonat mit einem maximalen Gehalt an kristallinem Valentinit von 5 Gew.-% eingesetzt wurde.
PCT/IB2013/055729 2012-07-16 2013-07-12 Katalysator zur herstellung von carbonsäuren und/oder carbonsäureanhydriden WO2014013397A2 (de)

Priority Applications (3)

Application Number Priority Date Filing Date Title
CN201380037094.3A CN104487164A (zh) 2012-07-16 2013-07-12 制备羧酸和/或羧酸酐的催化剂
JP2015522211A JP2015530228A (ja) 2012-07-16 2013-07-12 カルボン酸および／またはカルボン酸無水物を製造するための触媒
EP13820174.4A EP2872251A4 (de) 2012-07-16 2013-07-12 Katalysator zur herstellung von carbonsäuren und/oder carbonsäureanhydriden

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP12176526.7 2012-07-16
EP12176526 2012-07-16

Publications (2)

Publication Number Publication Date
WO2014013397A2 WO2014013397A2 (de) 2014-01-23
WO2014013397A3 true WO2014013397A3 (de) 2014-03-06

Family

ID=49949314

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/IB2013/055729 WO2014013397A2 (de) 2012-07-16 2013-07-12 Katalysator zur herstellung von carbonsäuren und/oder carbonsäureanhydriden

Country Status (4)

Country Link
EP (1) EP2872251A4 (de)
JP (1) JP2015530228A (de)
CN (1) CN104487164A (de)
WO (1) WO2014013397A2 (de)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105992647A (zh) * 2014-02-17 2016-10-05 巴斯夫欧洲公司 用于将邻二甲苯和/或萘氧化成邻苯二甲酸酐的催化剂体系

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1054726A (zh) * 1990-03-16 1991-09-25 日本触媒化学工业株式会社 用于制造邻苯二甲酸酐的催化剂
CN1302294A (zh) * 1998-05-26 2001-07-04 巴斯福股份公司 邻二甲苯/萘混合物的气相催化氧化制备邻苯二甲酸酐的方法
US20110124885A1 (en) * 2009-11-20 2011-05-26 Basf Se Multilayer catalyst having vanadium antimonate in at least one catalyst layer for preparing carboxylic acids and/or carboxylic anhydrides and process for preparing phthalic anhydride having a low hot spot temperature
US20120029214A1 (en) * 2010-07-30 2012-02-02 Basf Se Catalyst for the oxidation of o-xylene and/or naphthalene to phthalic anhydride

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS57180430A (en) * 1981-04-30 1982-11-06 Nippon Shokubai Kagaku Kogyo Co Ltd Catalyst for production of phthalic acid anhydride
WO2012014154A1 (en) * 2010-07-30 2012-02-02 Basf Se Catalyst for oxidation of o-xylene and/or naphthalene to phthalic anhydride

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1054726A (zh) * 1990-03-16 1991-09-25 日本触媒化学工业株式会社 用于制造邻苯二甲酸酐的催化剂
CN1302294A (zh) * 1998-05-26 2001-07-04 巴斯福股份公司 邻二甲苯/萘混合物的气相催化氧化制备邻苯二甲酸酐的方法
US20110124885A1 (en) * 2009-11-20 2011-05-26 Basf Se Multilayer catalyst having vanadium antimonate in at least one catalyst layer for preparing carboxylic acids and/or carboxylic anhydrides and process for preparing phthalic anhydride having a low hot spot temperature
US20120029214A1 (en) * 2010-07-30 2012-02-02 Basf Se Catalyst for the oxidation of o-xylene and/or naphthalene to phthalic anhydride

Also Published As

Publication number Publication date
WO2014013397A2 (de) 2014-01-23
EP2872251A4 (de) 2016-03-02
JP2015530228A (ja) 2015-10-15
EP2872251A2 (de) 2015-05-20
CN104487164A (zh) 2015-04-01

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