WO2013163571A3 - Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto - Google Patents

Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto Download PDF

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Publication number
WO2013163571A3
WO2013163571A3 PCT/US2013/038452 US2013038452W WO2013163571A3 WO 2013163571 A3 WO2013163571 A3 WO 2013163571A3 US 2013038452 W US2013038452 W US 2013038452W WO 2013163571 A3 WO2013163571 A3 WO 2013163571A3
Authority
WO
WIPO (PCT)
Prior art keywords
methods
systems related
biomass particulates
densified biomass
hydrolyzing pretreated
Prior art date
Application number
PCT/US2013/038452
Other languages
French (fr)
Other versions
WO2013163571A2 (en
Inventor
Bryan Bals
Farzaneh Teymouri
Timothy J. Campbell
Bruce E. Dale
Original Assignee
The Michigan Biotechnology Institute D/B/A Mbi
Board Of Trustees Of Michigan State University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US13/458,830 external-priority patent/US8945245B2/en
Priority to SG11201406820TA priority Critical patent/SG11201406820TA/en
Priority to CA2870758A priority patent/CA2870758C/en
Priority to CN201380022053.7A priority patent/CN104284983A/en
Priority to EP13725503.0A priority patent/EP2841588A2/en
Priority to MX2014012737A priority patent/MX356553B/en
Application filed by The Michigan Biotechnology Institute D/B/A Mbi, Board Of Trustees Of Michigan State University filed Critical The Michigan Biotechnology Institute D/B/A Mbi
Priority to KR1020147033096A priority patent/KR101970859B1/en
Priority to BR112014026818-5A priority patent/BR112014026818B1/en
Priority to JP2015509190A priority patent/JP6243899B2/en
Publication of WO2013163571A2 publication Critical patent/WO2013163571A2/en
Publication of WO2013163571A3 publication Critical patent/WO2013163571A3/en
Priority to PH12014502401A priority patent/PH12014502401A1/en

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00—Preparation of compounds containing saccharide radicals
    • C12P19/02—Monosaccharides
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00—Preparation of compounds containing saccharide radicals
    • C12P19/14—Preparation of compounds containing saccharide radicals produced by the action of a carbohydrase (EC 3.2.x), e.g. by alpha-amylase, e.g. by cellulase, hemicellulase
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/02—Preparation of oxygen-containing organic compounds containing a hydroxy group
    • C12P7/04—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic
    • C12P7/06—Ethanol, i.e. non-beverage
    • C12P7/08—Ethanol, i.e. non-beverage produced as by-product or from waste or cellulosic material substrate
    • C12P7/10—Ethanol, i.e. non-beverage produced as by-product or from waste or cellulosic material substrate substrate containing cellulosic material
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C1/00—Pretreatment of the finely-divided materials before digesting
    • D21C1/06—Pretreatment of the finely-divided materials before digesting with alkaline reacting compounds
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C1/00—Pretreatment of the finely-divided materials before digesting
    • D21C1/10—Physical methods for facilitating impregnation
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C5/00—Other processes for obtaining cellulose, e.g. cooking cotton linters ; Processes characterised by the choice of cellulose-containing starting materials
    • D21C5/005—Treatment of cellulose-containing material with microorganisms or enzymes
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P2201/00—Pretreatment of cellulosic or lignocellulosic material for subsequent enzymatic treatment or hydrolysis
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel

Abstract

A method is provided in which pretreated and densified cellulosic biomass particulates can hydrolyzed at a high solids loading rate as compared with the solids loading rate of loose hydrolysable cellulosic biomass fibers. The resulting high concentration sugar-containing stream can be easily converted to biofuels or an entire suite of other useful bioproducts.
PCT/US2013/038452 2012-04-27 2013-04-26 Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto WO2013163571A2 (en)

Priority Applications (9)

Application Number Priority Date Filing Date Title
JP2015509190A JP6243899B2 (en) 2012-04-27 2013-04-26 Pretreatment densified biomass particulate hydrolysis method and related system
CA2870758A CA2870758C (en) 2012-04-27 2013-04-26 Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto
CN201380022053.7A CN104284983A (en) 2012-04-27 2013-04-26 Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto
EP13725503.0A EP2841588A2 (en) 2012-04-27 2013-04-26 Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto
MX2014012737A MX356553B (en) 2012-04-27 2013-04-26 Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto.
SG11201406820TA SG11201406820TA (en) 2012-04-27 2013-04-26 Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto
KR1020147033096A KR101970859B1 (en) 2012-04-27 2013-04-26 Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto
BR112014026818-5A BR112014026818B1 (en) 2012-04-27 2013-04-26 METHOD FOR PRODUCING A CHAIN CONTAINING SUGAR
PH12014502401A PH12014502401A1 (en) 2012-04-27 2014-10-24 Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US13/458,830 US8945245B2 (en) 2009-08-24 2012-04-27 Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto
US13/458,830 2012-04-27

Publications (2)

Publication Number Publication Date
WO2013163571A2 WO2013163571A2 (en) 2013-10-31
WO2013163571A3 true WO2013163571A3 (en) 2014-03-06

Family

ID=48534478

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2013/038452 WO2013163571A2 (en) 2012-04-27 2013-04-26 Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto

Country Status (12)

Country Link
EP (1) EP2841588A2 (en)
JP (1) JP6243899B2 (en)
KR (1) KR101970859B1 (en)
CN (1) CN104284983A (en)
AR (1) AR094993A1 (en)
BR (1) BR112014026818B1 (en)
CA (1) CA2870758C (en)
MX (1) MX356553B (en)
MY (1) MY174524A (en)
PH (1) PH12014502401A1 (en)
SG (1) SG11201406820TA (en)
WO (1) WO2013163571A2 (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8945245B2 (en) 2009-08-24 2015-02-03 The Michigan Biotechnology Institute Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto
US9039792B2 (en) 2009-08-24 2015-05-26 Board Of Trustees Of Michigan State University Methods for producing and using densified biomass products containing pretreated biomass fibers
US9206446B2 (en) 2006-05-01 2015-12-08 Board Of Trustees Of Michigan State University Extraction of solubles from plant biomass for use as microbial growth stimulant and methods related thereto

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8968515B2 (en) 2006-05-01 2015-03-03 Board Of Trustees Of Michigan State University Methods for pretreating biomass
BRPI0722418B1 (en) 2006-05-01 2023-10-10 Dartmouth College Process for treating lignocellulosic biomass with ammonia and water vapors
US10457810B2 (en) 2009-08-24 2019-10-29 Board Of Trustees Of Michigan State University Densified biomass products containing pretreated biomass fibers
CN102939388B (en) 2010-04-19 2016-08-03 密歇根州立大学董事会 Lignocellulose biomass and extract and preparation method thereof can be digested
WO2013131015A1 (en) 2012-03-02 2013-09-06 Board Of Trustees Of Michigan State University Methods for increasing sugar yield with size-adjusted lignocellulosic biomass particles
CA2982187A1 (en) 2015-04-10 2016-10-13 Comet Biorefining Inc. Glucose-rich sugar streams and methods for making the same
GB201506701D0 (en) * 2015-04-20 2015-06-03 Univ York Method for converting waste lignocellulosic materials derived from converting lignocellulose to ethanol into levoglucosenone
JP5982549B1 (en) * 2015-10-01 2016-08-31 新日鉄住金エンジニアリング株式会社 Pretreatment method and pretreatment apparatus for lignocellulosic biomass
FI130510B (en) * 2016-03-24 2023-10-13 Upm Kymmene Corp A method for an enzymatic hydrolysis
JP6788034B2 (en) * 2016-12-22 2020-11-18 日本コーンスターチ株式会社 Manufacturing method of raw materials for saccharification
US11440999B2 (en) 2017-07-07 2022-09-13 Board Of Trustees Of Michigan State University De-esterification of biomass prior to ammonia pretreatment
CN112367853A (en) 2018-05-10 2021-02-12 彗星生物炼制公司 Composition containing glucose and hemicellulose and application thereof
CN111793662A (en) * 2019-04-08 2020-10-20 南京理工大学 Method for pretreating lignocellulose by adding alkaline reagent in densification process
CN112111540B (en) * 2019-06-20 2023-05-09 南京理工大学 Method for pretreatment and bioconversion by adding acidic reagent in lignocellulose raw material densification process
EP3954779A4 (en) * 2019-04-08 2023-08-16 Nanjing University Of Science And Technology Methods for pre-treatment of lignocellulose by adding alkali or acid reagent during densification thereof and for biotransformation thereof

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US20080256851A1 (en) * 2007-04-23 2008-10-23 Lumb Kevin D Compressed Fuel Product Using Flax Straw Derivative
US20090042259A1 (en) * 2007-08-09 2009-02-12 Board Of Trustees Of Michigan State University Process for enzymatically converting a plant biomass
WO2010121348A1 (en) * 2009-04-20 2010-10-28 Greenfield Ethanol Inc. Pretreatment of lignocellulosic biomass through removal of inhibitory compounds
WO2011028543A2 (en) * 2009-08-24 2011-03-10 Board Of Trustees Of Michigan State University Pretreated densified biomass products and methods of making and using same

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US4600590A (en) 1981-10-14 1986-07-15 Colorado State University Research Foundation Method for increasing the reactivity and digestibility of cellulose with ammonia
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FR2876863B1 (en) 2004-10-19 2007-01-12 Saint Gobain DEVICE FOR ETCHING A CONDUCTIVE LAYER AND ETCHING METHOD
US7187176B2 (en) 2005-02-08 2007-03-06 Bruker Biospin Corp. NMR probe circuit with nodal impedance bridge
WO2011157427A1 (en) * 2010-06-17 2011-12-22 Borregaard Industries Limited, Norge Enzymatic hydrolysis of cellulose
BR112013009003A2 (en) * 2010-10-15 2016-07-05 Andritz Tech & Asset Man Gmbh high solids enzyme reactor or mixer and method

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080256851A1 (en) * 2007-04-23 2008-10-23 Lumb Kevin D Compressed Fuel Product Using Flax Straw Derivative
US20090042259A1 (en) * 2007-08-09 2009-02-12 Board Of Trustees Of Michigan State University Process for enzymatically converting a plant biomass
WO2010121348A1 (en) * 2009-04-20 2010-10-28 Greenfield Ethanol Inc. Pretreatment of lignocellulosic biomass through removal of inhibitory compounds
WO2011028543A2 (en) * 2009-08-24 2011-03-10 Board Of Trustees Of Michigan State University Pretreated densified biomass products and methods of making and using same

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9206446B2 (en) 2006-05-01 2015-12-08 Board Of Trustees Of Michigan State University Extraction of solubles from plant biomass for use as microbial growth stimulant and methods related thereto
US8945245B2 (en) 2009-08-24 2015-02-03 The Michigan Biotechnology Institute Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto
US9039792B2 (en) 2009-08-24 2015-05-26 Board Of Trustees Of Michigan State University Methods for producing and using densified biomass products containing pretreated biomass fibers
US9458482B2 (en) 2009-08-24 2016-10-04 The Michigan Biotechnology Institute Methods of hydrolyzing pretreated densified biomass particulates and systems related thereto

Also Published As

Publication number Publication date
WO2013163571A2 (en) 2013-10-31
EP2841588A2 (en) 2015-03-04
CA2870758C (en) 2018-01-16
CA2870758A1 (en) 2013-10-31
KR20150028959A (en) 2015-03-17
PH12014502401A1 (en) 2015-01-12
SG11201406820TA (en) 2014-11-27
MY174524A (en) 2020-04-23
MX356553B (en) 2018-06-04
JP2015516157A (en) 2015-06-11
BR112014026818B1 (en) 2021-09-28
MX2014012737A (en) 2015-03-19
BR112014026818A2 (en) 2018-11-27
KR101970859B1 (en) 2019-04-19
CN104284983A (en) 2015-01-14
AR094993A1 (en) 2015-09-16
JP6243899B2 (en) 2017-12-06

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