WO2013116969A1 - Negative hydrogen ion powder and preparation process thereof - Google Patents

Negative hydrogen ion powder and preparation process thereof Download PDF

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Publication number
WO2013116969A1
WO2013116969A1 PCT/CN2012/001562 CN2012001562W WO2013116969A1 WO 2013116969 A1 WO2013116969 A1 WO 2013116969A1 CN 2012001562 W CN2012001562 W CN 2012001562W WO 2013116969 A1 WO2013116969 A1 WO 2013116969A1
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powder
hydrogen ion
negative hydrogen
temperature
sintered
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PCT/CN2012/001562
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French (fr)
Chinese (zh)
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姚鼎山
陈效庄
张丽
王绪珍
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Yao Dingshan
Chen Xiaozhuang
Zhang Li
Wang Xuzhen
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Publication of WO2013116969A1 publication Critical patent/WO2013116969A1/en

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K35/00Medicinal preparations containing materials or reaction products thereof with undetermined constitution
    • A61K35/56Materials from animals other than mammals
    • A61K35/612Crustaceans, e.g. crabs, lobsters, shrimps, krill or crayfish; Barnacles
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/70Polygonaceae (Buckwheat family), e.g. spineflower or dock
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P3/00Drugs for disorders of the metabolism
    • A61P3/02Nutrients, e.g. vitamins, minerals
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P3/00Drugs for disorders of the metabolism
    • A61P3/06Antihyperlipidemics
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P3/00Drugs for disorders of the metabolism
    • A61P3/08Drugs for disorders of the metabolism for glucose homeostasis
    • A61P3/10Drugs for disorders of the metabolism for glucose homeostasis for hyperglycaemia, e.g. antidiabetics
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P9/00Drugs for disorders of the cardiovascular system
    • A61P9/12Antihypertensives

Definitions

  • the invention relates to the field of health care products, in particular to a negative hydrogen ion powder and a preparation method thereof.
  • Negative hydrogen ion is the lightest substance in nature, but it is the strongest antioxidant.
  • the negative electrons possessed by a negative hydrogen ion capsule (net weight 0.35g) is equivalent to 863 coenzyme Ql (K10mg/piece).
  • 176 tablets of vitamin C 100mg / tablet
  • 431 vitamin E 10mg / tablet
  • its antioxidant effect is equivalent to 3500 apples, 1400 lemons.
  • An important factor in ATP It is well known that nutrients ingested by the human body must eventually enter the TCA circulatory system (ie, the Krebs cycle) and produce an electron "e", which is then transferred to the electron transport chain to ultimately produce energy ATP.
  • a glucose molecule can produce 36 ATPs through three stages of glycolysis, TCA circulatory system and oxidative phosphorylation. Among them, 30 ATPs are NAD (nicotinamide quinone dinucleotide) positive and negative hydrogen ions. "The other six were produced by coenzyme Q10.
  • H ⁇ is small (hydrogen atom diameter 0.064nm, hydrogen molecule diameter 0.128nm), the particle is smaller than the nanometer unit, the quality is extremely light (the lightest substance found at present), and it can quickly enter the cell, especially the micro cycle.
  • the human body can easily enter any tissue, such as the liver, heart, lungs, kidneys, brain, skin, muscles, bones, etc., and can act as an antioxidant and energy carrier.
  • the formation of a special biological environment in the body, so that bacteria, viruses, parasites can not survive, cancer cells are also daunting.
  • negative hydrogen ions have great health care value and are the most basic antioxidants on all life in the world. They may be the most superior antioxidants and energy carriers in various life forms to date. Therefore, the generation of negative hydrogen ions is quite significant.
  • the object of the present invention is to propose a negative hydrogen ion powder and a preparation method thereof.
  • the negative hydrogen ion powder of the present invention comprises: jellyfish powder, mother-of-pearl powder, wood fish stone powder, sea shrimp shell powder, buckwheat flour, and their weight percentage is 15-40: 18-38: 2-14: 1-7: 20-45.
  • sea bream powder and mother-of-pearl powder are prepared by washing and drying sea bream and mother-of-pearl, and grinding it to 500-700 mesh by a ball mill.
  • Muyu stone powder, sea shrimp shell powder, and buckwheat flour are all purchased directly from the market.
  • the method for preparing the negative hydrogen ion powder of the present invention has the following steps:
  • the dried cake is placed in a box type high temperature furnace, oxidized and sintered for 3-6 hours, and the temperature is 400-700.
  • the above oxidized and sintered block is placed in a box-type protective atmosphere furnace, and is subjected to a reduction reaction sintering for 3-6 hours, at a temperature of 400-700 ° C, and is taken out after cooling.
  • the protective atmosphere is hydrogen and is maintained at 1-2 atmospheres.
  • the above reaction is sintered into a gray mass and pulverized to 500-700 mesh, and UV-sterilized for 1 hour to prepare a capsule or a tablet or a sugar-coated tablet, which can be eaten.
  • the present invention is based on the fact that the calcium carbonate and magnesium carbonate contained in the above-mentioned formulation undergo a severe redox reaction by high-pressure, high-temperature oxidation sintering and reduction sintering, so that the H atom obtains an electron (e) into "H-".
  • H atom obtains an electron (e) into "H-”.
  • the biggest advantage of the negative hydrogen ion powder of the present invention is that the released negative hydrogen ion "" can improve the body immunity, enhance metabolism, improve sleep, anti-fatigue, anti-aging, and beauty. Improves high blood pressure, high blood fat, diabetes, prevention of obesity, cancer, Alzheimer's disease, and Parkinson's disease.
  • the dried cake is placed in a box-type high-temperature furnace, oxidized and sintered for 3-6 hours, at a temperature of 500-700 ° C, and taken out after cooling.
  • the box type high temperature furnace used in this embodiment is produced by Xi'an Electric Furnace Factory, model RX-60-9.
  • the above oxidized and sintered block is placed in a box-type protective atmosphere furnace, hydrogen gas is introduced, maintained at 1-2 atmospheres, and reduced and sintered for 3-6 hours, at a temperature of 400-700 ° C, and taken out after cooling.
  • the protective atmosphere furnace used in this embodiment is produced by Shanghai Minyue High Temperature Equipment Co., Ltd., model HMX1600-40.
  • the above reaction is sintered into a gray mass and pulverized to 500-700 mesh, and UV-sterilized for 1 hour to prepare a capsule or a tablet or a sugar-coated tablet, which can be eaten.
  • the preparation method is the same as above.
  • the preparation method is the same as above.
  • the sea otter in the above embodiment is a bone plate in the squid mantle film.
  • the original animal inhabits the sea floor. Alias thief bones.
  • the chemical composition of calcium carbonate is more than 85%, and its calcined content is increased. It also contains 6%-7% of the shell keratin, 10%-15% of the mucus, magnesium carbonate 3-5%, a small amount of calcium phosphate, sodium chloride and potassium. More than 10 inorganic elements such as zinc, copper and aluminum.
  • the inner shell contains 17 kinds of amino acids such as methionine, aspartic acid and glutamic acid.
  • the mother-of-pearl in the above embodiment is a shell-shell shell produced by pearls.
  • the chemical composition contains more than 92% of calcium carbonate, 5-7% of magnesium carbonate, and 5% of organic matter, among which keratin is mainly composed of aluminum and copper. Iron, sodium, zinc, phosphorus, antimony, sulfur, chlorine, potassium, silicon and other inorganic elements.
  • the shell nacre powder contains amino nitrogen 0.3.5%, and its shell hard protein is composed of threonine, glycine, proline and aspartic acid.
  • the Muyu Stone in the above examples is a rare Chinese herbal medicine.
  • the laboratory has identified that Muyu Stone contains 11.4% of magnesium carbonate, and also contains 0.09% of manganese, 2.4% of potassium, 23.2% of calcium, 0.01% of strontium, and molybdenum. 3.0%, lithium 0.03%, zinc 16%, selenium 0.01%, meta-silicic acid 0.01% and other trace elements beneficial to the human body, have a strong health and beauty effects.
  • the sea shrimp shell powder in the above embodiment is made of high quality sea shrimp, rich in chitin, protein, choline, phospholipid, cholesterol, astaxanthin, astaxanthin and phosphorus, calcium, iron, manganese, zinc, Copper and other
  • the buckwheat genus plant in the above embodiment has a long history of cultivation in China, and contains buckwheat flour. Protein 7%-13%, fat 3%, a total of 9 fatty acids, the most is oleic acid and linoleic acid; 72% carbohydrate, vitamin B1 and B2 3-4 times more than wheat; The effect of lowering blood fat and cholesterol; buckwheat also contains 2.1% minerals, especially phosphorus, calcium and magnesium.
  • Test method 300 mg of negative hydrogen ion powder was placed in 300 ml of tap water, stirred and dissolved, and compared with tap water.
  • the test results are as follows:

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Abstract

Disclosed are a negative hydrogen ion powder and a preparation process thereof. The raw materials of the powder consist of nacre powder, pearl oyster powder, mu-yu stone powder, sea shrimp shell powder and buckwheat powder, with the weight percentages thereof being 15-40:18-38:2-14:1-7:20-45. The preparation process of the powder comprises oxidative sintering and reductive sintering, with the negative hydrogen ion powder finally being prepared.

Description

一种负氢离子粉体及其制备方法  Negative hydrogen ion powder and preparation method thereof
技术领域 Technical field
本发明涉及保健品领域, 具体是指一种负氢离子粉体及其制备方法。  The invention relates to the field of health care products, in particular to a negative hydrogen ion powder and a preparation method thereof.
背景技术 Background technique
负氢离子" IT"又称氢化离子, 是氢原子上多带了一个电子, 因而带负电, 成为负离子 "ίΓ", 故而称负氢离子。 负氢离子有如下四大特点:  Negative hydrogen ion "IT", also known as hydrogen ion, is an electron with more electrons on the hydrogen atom, so it is negatively charged and becomes a negative ion. Therefore, it is called a negative hydrogen ion. Negative hydrogen ions have the following four characteristics:
1. 清除人体自由基  1. Eliminate free radicals in the body
负氢离子是自然界中最轻的物质, 但它却是抗氧化能力最强的一种, 一颗 负氢离子胶囊(净重 0.35g)所拥有的还原电子相当于 863颗辅酶 Ql(K10mg/颗)、 176片维生素 C(100mg/片)、431颗维生素 E (10mg/颗),其抗氧化效果相当于 3500 个苹果、 1400个柠檬。  Negative hydrogen ion is the lightest substance in nature, but it is the strongest antioxidant. The negative electrons possessed by a negative hydrogen ion capsule (net weight 0.35g) is equivalent to 863 coenzyme Ql (K10mg/piece). ), 176 tablets of vitamin C (100mg / tablet), 431 vitamin E (10mg / tablet), its antioxidant effect is equivalent to 3500 apples, 1400 lemons.
2. 提高人体细胞线粒体能量的合成  2. Improve the synthesis of mitochondrial energy in human cells
人的生命三大要素: 物质、 能量和信息, 其中能量是一切生命活动的动力, 人体细胞内线粒体是制造能量的工厂, 而负氢离子 "H~"则是线粒体的营养素, 是参与制造能量 ATP 的重要因子。 众所周知, 人体摄入的营养物质最终都必须 进入 TCA循环系统(即三羧酸循环) 中并产生电子 "e",然后此电子 "e"被递 转到电子传递链中, 最终生成能量 ATP。 一个葡萄糖分子经过酵解、 TCA循环系 统和氧化磷酸化三个阶段, 即可产生 36个 ATP, 其中 30个 ATP是依赖 NAD (烟 酰胺嘌呤二核苷酸)的正离子与负氢离子 "IT"产生的,其余 6个是由辅酶 Q10 参与产生的。  The three major elements of human life: matter, energy and information, where energy is the driving force of all life activities, the mitochondria in human cells are the factories that make energy, and the negative hydrogen ions "H~" are the nutrients of mitochondria, which are involved in the production of energy. An important factor in ATP. It is well known that nutrients ingested by the human body must eventually enter the TCA circulatory system (ie, the Krebs cycle) and produce an electron "e", which is then transferred to the electron transport chain to ultimately produce energy ATP. A glucose molecule can produce 36 ATPs through three stages of glycolysis, TCA circulatory system and oxidative phosphorylation. Among them, 30 ATPs are NAD (nicotinamide quinone dinucleotide) positive and negative hydrogen ions. "The other six were produced by coenzyme Q10.
由此可见, 线粒体在人体健康中的重要地位。 只有线粒体健康,才能保证能 量产生正常运转。 线粒体健康与否与细胞的膜电位密切相关, 而 "IT"是提高 膜电位的关键因素, 能起到提高并稳定膜电位而保证了线粒体的健康。 3. "H~"还是酶与基因中间的一个重要物质, "H~"进入细胞,还原性增强, 改善了细胞的内循环, 有利于器官的修复。 This shows that mitochondria plays an important role in human health. Only mitochondria are healthy to ensure proper energy production. The health of mitochondria is closely related to the membrane potential of cells, and "IT" is a key factor in increasing membrane potential, which can improve and stabilize membrane potential and ensure the health of mitochondria. 3. "H~" is also an important substance between the enzyme and the gene. "H~" enters the cell, and the reducing property is enhanced, which improves the inner circulation of the cell and is beneficial to the repair of the organ.
4. "H~"体积微小 (氢原子直径 0.064nm, 氢分子直径 0.128nm), 粒子比 纳米单位还小, 质量极轻(是目前发现最轻的物质), 能迅速进入细胞, 尤其是 微循环。 就人体而言, 它能轻松进入任何组织, 如肝、 心、 肺、 肾、 脑、 皮肤、 肌肉、 骨骼等, 无可不能, 充当抗氧化和能量载体的角色。 在体内形成一个特 殊的生物环境, 使细菌、 病毒、 寄生虫无法生存, 癌细胞也望而生畏。  4. "H~" is small (hydrogen atom diameter 0.064nm, hydrogen molecule diameter 0.128nm), the particle is smaller than the nanometer unit, the quality is extremely light (the lightest substance found at present), and it can quickly enter the cell, especially the micro cycle. As far as the human body is concerned, it can easily enter any tissue, such as the liver, heart, lungs, kidneys, brain, skin, muscles, bones, etc., and can act as an antioxidant and energy carrier. The formation of a special biological environment in the body, so that bacteria, viruses, parasites can not survive, cancer cells are also daunting.
综上所述, 负氢离子具有很大的医疗保健价值, 是地球上所有生命最基本 的抗氧化物质, 它可能成为迄今为止各种生命形式最优越的抗氧化剂和能量载 体。 因此, 幵发负氢离子意义颇大。  In summary, negative hydrogen ions have great health care value and are the most basic antioxidants on all life in the world. They may be the most superior antioxidants and energy carriers in various life forms to date. Therefore, the generation of negative hydrogen ions is quite significant.
发明内容 Summary of the invention
本发明的目的就是要提出一种负氢离子粉体及其制备方法。  The object of the present invention is to propose a negative hydrogen ion powder and a preparation method thereof.
本发明的负氢离子粉体, 包括: 海螵蛸粉体、 珍珠母贝粉体、 木鱼石粉体、 海虾壳粉体、 荞麦粉, 它们的重量百分比为 15-40: 18-38: 2-14: 1-7: 20-45。  The negative hydrogen ion powder of the present invention comprises: jellyfish powder, mother-of-pearl powder, wood fish stone powder, sea shrimp shell powder, buckwheat flour, and their weight percentage is 15-40: 18-38: 2-14: 1-7: 20-45.
其中海螵蛸粉体和珍珠母贝粉体是由将海螵蛸、 珍珠母贝洗净、 烘干, 用 球磨机将其研磨至 500~700目而制成的。 木鱼石粉体、 海虾壳粉体、 荞麦粉均 由市场直接购得。  Among them, sea bream powder and mother-of-pearl powder are prepared by washing and drying sea bream and mother-of-pearl, and grinding it to 500-700 mesh by a ball mill. Muyu stone powder, sea shrimp shell powder, and buckwheat flour are all purchased directly from the market.
本发明的负氢离子粉体的制备方法, 其步骤如下:  The method for preparing the negative hydrogen ion powder of the present invention has the following steps:
A. 按上述配方把原料放入容器内, 搅拌均匀后加水, 再搅拌, 形成面团, 捏成厚度为 0.3-0.5cm, 直径为 1.5-2cm圆形块状物, 再将其置于干燥炉内, 温 度为 50'C, 时间: 24h进行干燥。  A. Put the raw materials into the container according to the above formula, stir evenly, add water, stir, form the dough, and knead into a circular block with a thickness of 0.3-0.5cm and a diameter of 1.5-2cm, and then place it in a drying oven. Inside, the temperature was 50 ° C, and the time was: 24 h for drying.
B.把上述干燥后的块状物置于箱式高温炉内,氧化烧结 3-6h,温度 400-700 B. The dried cake is placed in a box type high temperature furnace, oxidized and sintered for 3-6 hours, and the temperature is 400-700.
V, 冷却后取出。 c. 把上述氧化烧结后的块状物置于箱式保护气氛炉内, 参与还原反应烧结 3-6h,温度 400-700°C, 冷却后取出。保护气氛为氢气, 维持在 1一 2个大气压。 V, remove after cooling. c. The above oxidized and sintered block is placed in a box-type protective atmosphere furnace, and is subjected to a reduction reaction sintering for 3-6 hours, at a temperature of 400-700 ° C, and is taken out after cooling. The protective atmosphere is hydrogen and is maintained at 1-2 atmospheres.
D. 把上述反应烧结呈灰色块状物粉碎至 500-700目, 经紫外线消毒 lh, 制 成胶囊或片剂或糖衣片, 即可食用。  D. The above reaction is sintered into a gray mass and pulverized to 500-700 mesh, and UV-sterilized for 1 hour to prepare a capsule or a tablet or a sugar-coated tablet, which can be eaten.
本发明是基于上述配方中含有的碳酸钙、 碳酸镁通过高压、 高温下的氧化 烧结和还原烧结发生了剧烈的氧化还原反应,使 H原子获得一个电子 (e)变成" H —"。 再看电负性: "Ca2+" =1.00, "Mg2+" =1.31 , "H~" =2.1。 "Ca2+"与 "『" 的电负性相差 1.1, "Mg2+"与 "IT"的电负性相差 0.79, "Ca2+"和 "Mg2+"与 "Ι " 的电负性相差均<1.7, 故 "Ca2+"和 "Mg2+"各自与 构成共价键, 并牢固地置入钙和镁的晶格中, 形成氢化钙和氢化镁, 一旦遇到水便释放出负 氢离子 "H""。 另外, 配方中荞麦粉、 海螵蛸粉体、 珍珠母贝粉体、 木鱼石粉体 和海虾壳粉体一起通过上述烧结后得到的最终粉体可溶于水。 The present invention is based on the fact that the calcium carbonate and magnesium carbonate contained in the above-mentioned formulation undergo a severe redox reaction by high-pressure, high-temperature oxidation sintering and reduction sintering, so that the H atom obtains an electron (e) into "H-". Look at the electronegativity: "Ca 2+ " = 1.00, "Mg 2+ " = 1.31 , "H~" = 2.1. The electronegativity of "Ca 2+ " and " 『 " differs by 1.1, the electronegativity of "Mg 2+ " and "IT" differs by 0.79, and the electrical charge of "Ca 2+ " and "Mg 2+ " and " Ι " The difference in properties is <1.7, so "Ca 2+ " and "Mg 2+ " each form a covalent bond and are firmly placed in the crystal lattice of calcium and magnesium to form calcium hydride and magnesium hydride. The negative hydrogen ion "H" is released. In addition, the final powder obtained by the above-mentioned sintering together with buckwheat flour, jellyfish powder, mother-of-pearl powder, wood fish stone powder and sea shrimp shell powder can be used. Dissolved in water.
本发明的负氢离子粉体的最大优点是: 释放出的负氢离子 "『"可提高机 体免疫力, 增强新陈代谢, 改善睡眠, 抗疲劳, 抗衰老, 美容。 改善高血压、 高血脂、 糖尿病, 预防肥胖、 癌症、 老年痴呆、 帕金森氏症。  The biggest advantage of the negative hydrogen ion powder of the present invention is that the released negative hydrogen ion "" can improve the body immunity, enhance metabolism, improve sleep, anti-fatigue, anti-aging, and beauty. Improves high blood pressure, high blood fat, diabetes, prevention of obesity, cancer, Alzheimer's disease, and Parkinson's disease.
具体实施方式 detailed description
下面通过实施例, 详细说明本发明的具体实施方式  DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS Hereinafter, specific embodiments of the present invention will be described in detail through embodiments.
实施例 1  Example 1
配方:  Recipe:
名称 粒径 (单位: 目) 色泽 重量百分比 (wt% ) 海螵蛸 500- 700 白色粉末 34  Name Particle size (Unit: mesh) Color Weight (wt%) Jellyfish 500- 700 White powder 34
珍珠母贝 500 700 白色粉末 20  Mother of pearl 500 700 white powder 20
木鱼石 500-700 棕色粉末 4 海虾壳 500 700 褐色粉末 1 Muyu Stone 500-700 Brown Powder 4 Sea prawn shell 500 700 brown powder 1
荞麦粉 500-700 白色粉末 41  Buckwheat flour 500-700 white powder 41
a. 按上述配方把原料放入容器内, 搅拌均匀后加水, 形成面团, 捏成厚度 为 0.3-0.5cm, 直径为 1.5-2cm圆形块状物, 置于干燥炉内, 干燥温度 50°C, 时 间: 24h进行干燥。  a. Put the raw materials into the container according to the above formula, stir evenly, add water, form the dough, and knead into a circular block with a thickness of 0.3-0.5cm and a diameter of 1.5-2cm, placed in a drying oven, and the drying temperature is 50°. C, Time: 24h for drying.
b.把上述干燥后的块状物置于箱式高温炉内,氧化烧结 3-6h,温度 500-700 °C ,冷却后取出。本实施例所用的箱式高温炉由西安电炉厂生产,型号 RX-60-9。  b. The dried cake is placed in a box-type high-temperature furnace, oxidized and sintered for 3-6 hours, at a temperature of 500-700 ° C, and taken out after cooling. The box type high temperature furnace used in this embodiment is produced by Xi'an Electric Furnace Factory, model RX-60-9.
C. 把上述氧化烧结后的块状物置于箱式保护气氛炉内, 通入氢气, 维持在 1-2个大气压, 还原反应烧结 3-6h, 温度 400-700'C, 冷却后取出。 本实施例所 用的保护气氛炉由上海皓越高温设备有限公司生产,型号 HMX1600-40。  C. The above oxidized and sintered block is placed in a box-type protective atmosphere furnace, hydrogen gas is introduced, maintained at 1-2 atmospheres, and reduced and sintered for 3-6 hours, at a temperature of 400-700 ° C, and taken out after cooling. The protective atmosphere furnace used in this embodiment is produced by Shanghai Minyue High Temperature Equipment Co., Ltd., model HMX1600-40.
d.把上述反应烧结呈灰色块状物粉碎至 500-700目,经紫外线消毒 lh,制成 胶囊或片剂或糖衣片, 即可食用。  d. The above reaction is sintered into a gray mass and pulverized to 500-700 mesh, and UV-sterilized for 1 hour to prepare a capsule or a tablet or a sugar-coated tablet, which can be eaten.
实施例 2  Example 2
配方:  Recipe:
名称 粒径 (单位:目) 色泽 重量百分比 (wt% ) 海螵蛸 500- 700 白色粉末 38  Name Particle size (Unit: mesh) Color Weight (wt%) Jellyfish 500- 700 White powder 38
珍珠母贝 500-700 白色粉末 28  Mother of pearl 500-700 white powder 28
木鱼石 500—700 棕色粉末  Muyu Stone 500-700 brown powder
海虾壳 500-700 褐色粉末  Sea shrimp shell 500-700 brown powder
荞麦粉 500-700 白色粉末 24  Buckwheat flour 500-700 white powder 24
制备方法同上。  The preparation method is the same as above.
实施例 3  Example 3
配方 名称 粒径 (单位:目) 色泽 重量百分比(wt% ) 海螵蛸 500- 700 白色粉末 36 Formula Name particle size (unit: mesh) Color weight percentage (wt%) jellyfish 500-700 white powder 36
珍珠母贝 500-700 白色粉末 26  Mother-of-pearl 500-700 white powder 26
木鱼石 500-700 棕色粉末 2  Muyu Stone 500-700 Brown Powder 2
海虾壳 500—700 褐色粉末 2  Sea prawn shell 500-700 brown powder 2
荞麦粉 500-700 白色粉末 34  Buckwheat Flour 500-700 White Powder 34
制备方法同上。  The preparation method is the same as above.
上述实施例中的海螵蛸为乌贼外套膜内的骨板。 原动物栖息于海底。 别名乌 贼骨。 化学成分碳酸钙 85%以上, 其煅品含量增大, 还含壳角质 6%-7%, 粘液 质 10%-15%, 碳酸镁 3-5%,少量磷酸钙、 氯化钠及钾、 锌、 铜、 铝等 10多种无 机元素。 此外, 内壳中含蛋氨酸、 天冬氨酸、 谷氨酸等 17种氨基酸。  The sea otter in the above embodiment is a bone plate in the squid mantle film. The original animal inhabits the sea floor. Alias thief bones. The chemical composition of calcium carbonate is more than 85%, and its calcined content is increased. It also contains 6%-7% of the shell keratin, 10%-15% of the mucus, magnesium carbonate 3-5%, a small amount of calcium phosphate, sodium chloride and potassium. More than 10 inorganic elements such as zinc, copper and aluminum. In addition, the inner shell contains 17 kinds of amino acids such as methionine, aspartic acid and glutamic acid.
上述实施例中的珍珠母贝为产珠贝类外壳贝壳. 化学成分含碳酸钙 92%以 上, 碳酸镁 5-7%,有机物 5%, 其中以角壳蛋白为主, 尚含铝、铜、铁、钠、锌、 磷、 钡、 硫、 氯、 钾、 硅等多种无机元素。 贝壳珍珠层粉含氨基氮 0. 35%, 其贝壳硬蛋白由苏氨酸, 甘氨酸, 脯氨酸,天冬氨酸组成。  The mother-of-pearl in the above embodiment is a shell-shell shell produced by pearls. The chemical composition contains more than 92% of calcium carbonate, 5-7% of magnesium carbonate, and 5% of organic matter, among which keratin is mainly composed of aluminum and copper. Iron, sodium, zinc, phosphorus, antimony, sulfur, chlorine, potassium, silicon and other inorganic elements. The shell nacre powder contains amino nitrogen 0.3.5%, and its shell hard protein is composed of threonine, glycine, proline and aspartic acid.
上述实施例中的木鱼石据《本草纲目》记载系珍稀中药材, 经实验室鉴定, 木鱼石含有碳酸镁 11.4%,还含有锰 0.09%、 钾 2.4%、 钙 23.2%、 锶 0.01%、 钼 3.0%、 锂 0.03%、 锌 16%、 硒 0.01%.偏硅酸 0.01%等十多种对人体有益的 微量元素, 有很强的保健和美容作用。  According to the "Compendium of Materia Medica", the Muyu Stone in the above examples is a rare Chinese herbal medicine. The laboratory has identified that Muyu Stone contains 11.4% of magnesium carbonate, and also contains 0.09% of manganese, 2.4% of potassium, 23.2% of calcium, 0.01% of strontium, and molybdenum. 3.0%, lithium 0.03%, zinc 16%, selenium 0.01%, meta-silicic acid 0.01% and other trace elements beneficial to the human body, have a strong health and beauty effects.
上述实施例中的海虾壳粉. 是以优质海虾为原料, 含有丰富甲壳素、 蛋白 质、 胆碱、 磷脂、 胆固醇、 虾青素、 虾红素及磷、 钙、 铁、 锰、 锌、 铜等多种 The sea shrimp shell powder in the above embodiment is made of high quality sea shrimp, rich in chitin, protein, choline, phospholipid, cholesterol, astaxanthin, astaxanthin and phosphorus, calcium, iron, manganese, zinc, Copper and other
Wii兀素。 Wii 兀素.
上述实施例中的荞麦属蓼科植物在我国有着悠久的栽培历史, 荞麦粉中含 蛋白质 7%-13%, 脂肪 3%, 共有 9种脂肪酸, 最多的是油酸和亚油酸; 碳水化 合物 72%, 维生素 B1和 B2比小麦多 3-4倍; 具有的芸香甙成分, 有降血脂、 胆固醇的功效; 荞麦中还含有 2.1%矿物质, 尤以磷、 钙、 镁较多。 The buckwheat genus plant in the above embodiment has a long history of cultivation in China, and contains buckwheat flour. Protein 7%-13%, fat 3%, a total of 9 fatty acids, the most is oleic acid and linoleic acid; 72% carbohydrate, vitamin B1 and B2 3-4 times more than wheat; The effect of lowering blood fat and cholesterol; buckwheat also contains 2.1% minerals, especially phosphorus, calcium and magnesium.
本发明的测试结果  Test result of the present invention
测试方法: 将 300毫克负氢离子粉体放入 300毫升自来水中, 搅拌待其溶 解后与自来水对照, 测试结果如下表:  Test method: 300 mg of negative hydrogen ion powder was placed in 300 ml of tap water, stirred and dissolved, and compared with tap water. The test results are as follows:
Figure imgf000007_0001
Figure imgf000007_0001
本实施例的原料供应商如下:  The raw material suppliers of this embodiment are as follows:
原料名称 供应商  Material Name Supplier
海螵蛸 安徽毫州市海螵蛸生产供应商  Haishu Anhui Wuzhou Haishu production supplier
珍珠母贝 深圳市爱特丽尔珠宝有限公司  Mother-of-pearl pearl Shenzhen Aitelier Jewelry Co., Ltd.
木鱼石 济南长清县长盛木鱼石公司  Muyushi Jinan Changqing County Changsheng Muyushi Company
虾壳粉 山东融丰青岛分公司  Shrimp Shell Powder Shandong Rongfeng Qingdao Branch
荞麦粉 天津港保税区爱信食品有限公司  Buckwheat flour Tianjin Port Free Trade Zone Aisin Food Co., Ltd.

Claims

权 利 要 求 Rights request
1. 一种负氢离子粉体, 其特征在于: 该粉体由海螵蛸粉体、 珍珠母贝粉体、 木鱼石粉体、海虾壳粉体、荞麦粉组成,它们的重量百分比为 15-40: 18-38: 2-14: 1-7: 20-45 o A negative hydrogen ion powder characterized in that: the powder consists of jellyfish powder, mother-of-pearl powder, wood fish stone powder, sea shrimp shell powder, buckwheat flour, and the weight percentage thereof is 15-40: 18-38: 2-14: 1-7: 20-45 o
2. 一种负氢离子粉体的制备方法, 其步骤如下:  2. A method for preparing a negative hydrogen ion powder, the steps of which are as follows:
首先将海螵蛸、 珍珠母贝洗净、 烘干, 用球磨机将其研磨至 500~700目成 粉体; 其余粉体为市场所购;  First, the jellyfish and mother-of-pearl are washed and dried, and ground to a powder of 500-700 mesh by a ball mill; the remaining powders are purchased by the market;
A. 按上述配方把原料放入容器内, 搅拌均匀后加水, 再搅拌, 形成面团, 捏成厚度为 0.3-0.5cm, 直径为 1.5-2cm圆形块状物, 再将其置于干燥炉内, 温 度为 50°C , 时间: 24h进行干燥;  A. Put the raw materials into the container according to the above formula, stir evenly, add water, stir, form the dough, and knead into a circular block with a thickness of 0.3-0.5cm and a diameter of 1.5-2cm, and then place it in a drying oven. Inside, the temperature is 50 ° C, time: 24h for drying;
B.把上述干燥后的块状物置于箱式高温炉内,氧化烧结 3-6h,温度 400-700 V, 冷却后取出;  B. The dried cake is placed in a box type high temperature furnace, oxidized and sintered for 3-6 hours, temperature 400-700 V, and taken out after cooling;
C. 把上述氧化烧结后的块状物置于箱式保护气氛炉内, 参与还原反应烧结 3-6h, 温度 400-700'C , 冷却后取出; 保护气氛为氢气, 维持在 1一 2个大气压;  C. The above oxidized and sintered block is placed in a box-type protective atmosphere furnace, and is subjected to reduction reaction sintering for 3-6 hours, temperature 400-700'C, and taken out after cooling; the protective atmosphere is hydrogen, maintained at 1 to 2 atmospheres. ;
D. 把上述反应烧结呈灰色块状物粉碎至 500-700目, 经紫外线消毒 lh,制 成胶囊或片剂或糖衣片, 即可食用。  D. The above reaction is sintered into a gray mass and pulverized to 500-700 mesh, and UV-sterilized for 1 hour to prepare a capsule or a tablet or a sugar-coated tablet, which can be eaten.
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