WO2013035083A3 - Storage stable premixed hydraulic cement compositions, cements, methods, and articles - Google Patents

Storage stable premixed hydraulic cement compositions, cements, methods, and articles Download PDF

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Publication number
WO2013035083A3
WO2013035083A3 PCT/IB2012/054701 IB2012054701W WO2013035083A3 WO 2013035083 A3 WO2013035083 A3 WO 2013035083A3 IB 2012054701 W IB2012054701 W IB 2012054701W WO 2013035083 A3 WO2013035083 A3 WO 2013035083A3
Authority
WO
WIPO (PCT)
Prior art keywords
hydraulic cement
aqueous
cement compositions
liquid
methods
Prior art date
Application number
PCT/IB2012/054701
Other languages
French (fr)
Other versions
WO2013035083A2 (en
Inventor
Håkan ENGQVIST
Jonas ÅBERG
Original Assignee
Oss-Q Ab
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US13/229,534 external-priority patent/US20130066327A1/en
Priority claimed from US13/229,539 external-priority patent/US20130066324A1/en
Priority claimed from US13/229,545 external-priority patent/US8591645B2/en
Application filed by Oss-Q Ab filed Critical Oss-Q Ab
Priority to GB1405031.4A priority Critical patent/GB2513477A/en
Priority to US14/343,105 priority patent/US9676665B2/en
Publication of WO2013035083A2 publication Critical patent/WO2013035083A2/en
Publication of WO2013035083A3 publication Critical patent/WO2013035083A3/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B40/00Processes, in general, for influencing or modifying the properties of mortars, concrete or artificial stone compositions, e.g. their setting or hardening ability
    • C04B40/06Inhibiting the setting, e.g. mortars of the deferred action type containing water in breakable containers ; Inhibiting the action of active ingredients
    • C04B40/0683Inhibiting the setting, e.g. mortars of the deferred action type containing water in breakable containers ; Inhibiting the action of active ingredients inhibiting by freezing or cooling
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B40/00Processes, in general, for influencing or modifying the properties of mortars, concrete or artificial stone compositions, e.g. their setting or hardening ability
    • C04B40/06Inhibiting the setting, e.g. mortars of the deferred action type containing water in breakable containers ; Inhibiting the action of active ingredients
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/34Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing cold phosphate binders
    • C04B28/344Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing cold phosphate binders the phosphate binder being present in the starting composition solely as one or more phosphates
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00034Physico-chemical characteristics of the mixtures
    • C04B2111/00181Mixtures specially adapted for three-dimensional printing (3DP), stereo-lithography or prototyping
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474Uses not provided for elsewhere in C04B2111/00
    • C04B2111/00836Uses not provided for elsewhere in C04B2111/00 for medical or dental applications

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Materials For Medical Uses (AREA)

Abstract

Refrigerated hydraulic cement compositions comprise a mixture of (a) β-tricalcium phosphate powder, (b) monocalcium phosphate comprising monocalcium phosphate anhydrous (MCPA), monocalcium phosphate monohydrate (MCPM), or a combination thereof, wherein a 0.1 g/ml saturated aqueous solution of the monocalcium phosphate has a pH less than 3.0, (c) non-aqueous water-miscible liquid, and (d) an aqueous hydrating liquid. The aqueous hydrating liquid is included in an amount of about 1-50 volume percent, based on the combined volume of the non-aqueous water-miscible liquid and the aqueous hydration liquid, and the refrigerated hydraulic cement composition is storage stable for greater than one day, without setting. Methods of forming hardened cements in vivo and/or for forming implants for use in vivo employ the hydraulic cement compositions.
PCT/IB2012/054701 2011-09-09 2012-09-10 Storage stable premixed hydraulic cement compositions, cements, methods, and articles WO2013035083A2 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
GB1405031.4A GB2513477A (en) 2011-09-09 2012-09-10 Storage stable premixed hydraulic cement compositions, cements, methods, and articles
US14/343,105 US9676665B2 (en) 2011-09-09 2012-09-10 Storage stable premixed hydraulic cement compositions, cements, methods, and articles

Applications Claiming Priority (8)

Application Number Priority Date Filing Date Title
US201161533064P 2011-09-09 2011-09-09
US13/229,534 US20130066327A1 (en) 2011-09-09 2011-09-09 Hydraulic cement compositions with low ph methods, articles and kits
US13/229,534 2011-09-09
US13/229,539 US20130066324A1 (en) 2011-09-09 2011-09-09 Hydraulic cements, methods and products
US61/533,064 2011-09-09
US13/229,545 2011-09-09
US13/229,539 2011-09-09
US13/229,545 US8591645B2 (en) 2011-09-09 2011-09-09 Hydraulic cements with optimized grain size distribution, methods, articles and kits

Publications (2)

Publication Number Publication Date
WO2013035083A2 WO2013035083A2 (en) 2013-03-14
WO2013035083A3 true WO2013035083A3 (en) 2013-07-18

Family

ID=47116126

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/IB2012/054701 WO2013035083A2 (en) 2011-09-09 2012-09-10 Storage stable premixed hydraulic cement compositions, cements, methods, and articles

Country Status (2)

Country Link
GB (1) GB2513477A (en)
WO (1) WO2013035083A2 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2855009T3 (en) * 2014-08-14 2021-09-23 Ossdsign Ab Bone implants to correct bone defects
EP3866711B1 (en) 2018-10-16 2024-10-02 OssDsign AB Implants for filling bore holes in bone

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01100049A (en) * 1987-10-13 1989-04-18 Asahi Optical Co Ltd Production of calcium phosphate-based set material
US5683667A (en) * 1994-11-04 1997-11-04 Norian Corporation Reactive tricalcium phosphate compositions
US6117456A (en) * 1995-05-19 2000-09-12 Etex Corporation Methods and products related to the physical conversion of reactive amorphous calcium phosphate
WO2002011781A1 (en) * 2000-08-04 2002-02-14 Orthogem Limited Porous synthetic bone graft and method of manufacture thereof
WO2004093734A2 (en) * 2002-01-23 2004-11-04 Ada Foundation Premixed self-hardening bone graft pastes
WO2005074453A2 (en) * 2004-01-16 2005-08-18 Ada Foundation Rapid-hardening calcium phosphate cement compositions
US20060263443A1 (en) * 2001-01-24 2006-11-23 Ada Foundation Premixed self-hardening bone graft pastes
CN1919357A (en) * 2006-09-19 2007-02-28 天津大学 Premix plaster calcium phosphate bone cement
WO2010055483A2 (en) * 2008-11-12 2010-05-20 Engqvist Haakan Hydraulic cements, methods and products

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9101436B2 (en) 2005-10-21 2015-08-11 Ada Foundation Dental and endodontic filling materials and methods

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01100049A (en) * 1987-10-13 1989-04-18 Asahi Optical Co Ltd Production of calcium phosphate-based set material
US5683667A (en) * 1994-11-04 1997-11-04 Norian Corporation Reactive tricalcium phosphate compositions
US6117456A (en) * 1995-05-19 2000-09-12 Etex Corporation Methods and products related to the physical conversion of reactive amorphous calcium phosphate
WO2002011781A1 (en) * 2000-08-04 2002-02-14 Orthogem Limited Porous synthetic bone graft and method of manufacture thereof
US20060263443A1 (en) * 2001-01-24 2006-11-23 Ada Foundation Premixed self-hardening bone graft pastes
WO2004093734A2 (en) * 2002-01-23 2004-11-04 Ada Foundation Premixed self-hardening bone graft pastes
WO2005074453A2 (en) * 2004-01-16 2005-08-18 Ada Foundation Rapid-hardening calcium phosphate cement compositions
CN1919357A (en) * 2006-09-19 2007-02-28 天津大学 Premix plaster calcium phosphate bone cement
WO2010055483A2 (en) * 2008-11-12 2010-05-20 Engqvist Haakan Hydraulic cements, methods and products

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
BOHNER M ET AL: "Technological issues for the development of more efficient calcium phosphate bone cements: A critical assessment", BIOMATERIALS, ELSEVIER SCIENCE PUBLISHERS BV., BARKING, GB, vol. 26, no. 33, 1 November 2005 (2005-11-01), pages 6423 - 6429, XP027767608, ISSN: 0142-9612, [retrieved on 20051101] *
HAN ET AL.: "beta-TCP/MCPM-based premixed calcium phosphate cements", ACTA BIOMATERIALIA, vol. 5, 2009, pages 3165 - 3177, XP002692082 *
HOCKIN H K XU ET AL: "Premixed macroporous calcium phosphate cement scaffold", JOURNAL OF MATERIALS SCIENCE: MATERIALS IN MEDICINE, KLUWER ACADEMIC PUBLISHERS, BO, vol. 18, no. 7, 3 February 2007 (2007-02-03), pages 1345 - 1353, XP019503760, ISSN: 1573-4838, DOI: 10.1007/S10856-007-0146-X *

Also Published As

Publication number Publication date
GB2513477A (en) 2014-10-29
WO2013035083A2 (en) 2013-03-14
GB201405031D0 (en) 2014-05-07

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