Classifications

• • A—HUMAN NECESSITIES
  • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
  • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
  • A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
  • A01N47/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides
• • A—HUMAN NECESSITIES
  • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
  • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
  • A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
  • A01N33/26—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds containing nitrogen-to-nitrogen bonds, e.g. azides, diazo-amino compounds, diazonium compounds, hydrazine derivatives
• • A—HUMAN NECESSITIES
  • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
  • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
  • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
  • A01N37/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
  • A01N37/22—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof the nitrogen atom being directly attached to an aromatic ring system, e.g. anilides
  • A01N37/24—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof the nitrogen atom being directly attached to an aromatic ring system, e.g. anilides containing at least one oxygen or sulfur atom being directly attached to the same aromatic ring system
• • A—HUMAN NECESSITIES
  • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
  • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
  • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
  • A01N37/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
  • A01N37/28—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof containing the group; Thio analogues thereof
• • A—HUMAN NECESSITIES
  • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
  • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
  • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
  • A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
  • A01N37/38—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system
  • A01N37/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system having at least one carboxylic group or a thio analogue, or a derivative thereof, and one oxygen or sulfur atom attached to the same aromatic ring system
• • A—HUMAN NECESSITIES
  • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
  • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
  • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
  • A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
  • A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
  • A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
  • A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
• • A—HUMAN NECESSITIES
  • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
  • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
  • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
  • A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
  • A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles

Definitions

• the present invention relates to a harmful arthropod control composition and a method for controlling harmful arthropods.
• a harmful arthropod control composition comprising a cyanamide compound represented by formula (1), one or more insect growth control compounds selected from the group (A), and one or more blight control compounds selected from the group (B) object.
• the blight control compound is flutolanil, pencyclon, or N- [2- (1,3-dimethylbutyl) phenyl] -5-fluoro-1,3-dimethyl-1H-pyrazole-4-carboxamide.
• a method for controlling harmful arthropods comprising a step of applying an effective amount of the composition for controlling harmful arthropods according to any one of [1] to [4] to a plant or a plant cultivation site.
• the harmful arthropod control composition of the present invention is a cyanamide compound represented by the following formula (1) (hereinafter sometimes referred to as the present cyanamide compound) and one or more selected from the following group (A).
• Insect growth control compound hereinafter may be referred to as the present insect growth control compound
• one or more blight control compounds selected from the following group (B) hereinafter referred to as the present blight control compound Is included.
• Group (B) Group consisting of flutolanil, pencyclone, N- [2- (1,3-dimethylbutyl) phenyl] -5-fluoro-1,3-dimethyl-1H-pyrazole-4-carboxamide, flametopyr and validamycin A .
• the present cyanamide compound is a known compound and can be produced, for example, by the method described in International Publication No. 2007/095229.
• Methoxyphenozide, chromafenozide, tebufenozide, flutolanil, pencyclon, furamethpyr, and validamycin A are all known compounds, for example, “The Pesticide Manual-15th edition (BCPC); ISBN 978-1901396-18-8”, 764.
• N- [2- (1,3-dimethylbutyl) phenyl] -5-fluoro-1,3-dimethyl-1H-pyrazole-4-carboxamide (hereinafter referred to as the present active compound (I)) is a known compound. For example, it can be produced by the method described in International Publication No. 2003/010149 pamphlet.
• the blight control compound flutolanil, pencyclon and the active compound (I) are preferable.
• the content ratio of the present cyanamide compound, the present insect growth control compound, and the main blight control compound is not particularly limited, but is 100 parts by weight of the present cyanamide compound.
• the present insect growth control compound is usually 0.2 to 50000 parts by weight, preferably 2 to 5000 parts by weight, more preferably 5 to 2000 parts by weight. It is ⁇ 100,000 parts by weight, preferably 2 to 10,000 parts by weight, more preferably 5 to 5,000 parts by weight.
• the weight ratio of the present cyanamide compound to the present insect growth control compound (the present cyanamide compound: the present insect growth control compound) in the harmful arthropod control composition of the present invention is usually 500: 1 to 1: 500, preferably 50: 1 to 1:50, more preferably 20: 1 to 1:20.
• the weight ratio of the present cyanamide compound to the main blight control compound (the present cyanamide compound: main blight control compound) is usually 500: 1 to 1: 1000, The ratio is preferably 50: 1 to 1: 100, more preferably 20: 1 to 1:50.
• the harmful arthropod control composition of the present invention may be a mixture of the present cyanamide compound, the present insect growth control compound, and the present blight control compound, but usually the present cyanamide compound and the present insect growth control compound.
• a compound for controlling blight of this coat and an inert carrier is added, and if necessary, surfactants and other formulation adjuvants are added to obtain oils, emulsions, flowables, wettable powders, and granular wettable powders. , Powders, granules and the like are used.
• the formulated arthropod pest control composition can be used as it is or by adding other inactive ingredients (water, sand, vegetable oil, etc.).
• the total amount of the present cyanamide compound, the present insect growth control compound and the main blight control compound is usually 0.01 to 99% by weight, preferably 0.1 to 90% by weight. %, More preferably 0.5 to 70% by weight.
• the inert carrier include a solid carrier and a liquid carrier.
• solid carriers include kaolin clay, attapulgite clay, bentonite, montmorillonite, acid clay, pyrophyllite, talc, diatomaceous earth, calcite, and other natural organic substances such as corn cob powder and walnut shell powder, urea, and the like.
• Examples thereof include fine powders or granular materials composed of synthetic organic substances, salts such as calcium carbonate and ammonium sulfate, and synthetic inorganic substances such as synthetic hydrous silicon oxide.
• the liquid carrier include aromatic hydrocarbons such as xylene, alkylbenzene, and methylnaphthalene; alcohols such as 2-propanol, ethylene glycol, propylene glycol, and ethylene glycol monoethyl ether; ketones such as acetone, cyclohexanone, and isophorone;
• Examples include vegetable oils such as soybean oil and cottonseed oil, petroleum aliphatic hydrocarbons, esters, dimethyl sulfoxide, acetonitrile and water.
• surfactants include anionic interfaces such as alkyl sulfate esters, alkylaryl sulfonates, dialkyl sulfosuccinates, polyoxyethylene alkylaryl ether phosphate esters, lignin sulfonates, naphthalene sulfonate formaldehyde polycondensates, and the like.
• Nonionic surfactants such as activators and polyoxyethylene alkyl aryl ethers, polyoxyethylene alkyl polyoxypropylene block copolymers, sorbitan fatty acid esters, and cationic surfactants such as alkyltrimethylammonium salts.
• Examples of other adjuvants for preparation include water-soluble polymers such as polyvinyl alcohol and polyvinylpyrrolidone, gum arabic, alginic acid and salts thereof, polysaccharides such as CMC (carboxymethylcellulose) and xanthan gum, inorganic substances such as aluminum magnesium silicate and alumina sol. , Preservatives, colorants and stabilizers such as PAP (isopropyl acid phosphate) and BHT (dibutylhydroxytoluene).
• the harmful arthropod control composition of the present invention can be used to protect a plant from harm by a harmful arthropod that causes feeding, sucking or the like to the plant.
• Examples of the harmful arthropods having the controlling effect of the harmful arthropod control composition of the present invention include the following. Hemiptera: small brown planthopper (Laodelphax striatellus), brown planthopper (Nilaparvata lugens), planthopper such Sejirounka (Sogatella furcifera), green rice leafhopper (Nephotettix cincticeps), Taiwan green rice leafhopper (Nephotettix virescens), Inazuma leafhopper (Recilia dorsalis), Chanomidorihime Leafhoppers such as leafhopper (Empoasca onukii), cotton aphid (Aphis gossypi), peach aphid (Myzus persicae), radish aphid (Brevicorine brassicae), snowy spruce (Aphasianis spruce) la), tulip beetle aphids (Macrosiphum euporbiae),
• Lepidoptera rice stem borer (Chilo suppressalis), Sankameiga (Tryporyza incertulas), leaf roller (Cnaphalocrocis medinalis), Watanomeiga (Notarcha derogata), Indian meal moth (Plodia interpunctella), the European corn borer (Ostrinia furnacalis), high Madara Roh moth (Hellula undalis), Common moths such as Pediasia teterrellus, Spodoptera litura, Spodoptera exigua, Pseudoteria sepata, Seiyoto ferens), mushroom brassicae, agrotis ipsilon, tamanagiwawa (plusia nigrisigna), cervus genus, trichoplusia ni White butterflies, genus Adoxofies, papaver moth (Graphophrita molesta), leguminivola glycinivolorella, azusayamashi
• Kibaga such as, Tiger Moth such as the United States White Arctiidae (Hyphantria cunea), clothes moth (Tinea translucens), Hirozukoga such as webbing clothes moth (Tineola bisselliella), Tuta absolute diluter (Tuta absoluta) and the like.
• Thysanoptera western flower thrips (Frankliniella occidentalis), Minami thrips (Thrips peri), yellow tea thrips (Scirtothrips dorsalis), green onion thrips (Thrips tabaci), Hirazuhanaazamiuma (Frankliniella intonsa), tobacco thrips (Frankliniella fusca), onion thrips Thrips such as (Thrips tabaci), rice thrips (Stenchaethotrips biformis), and rice thrips (Haplotrips acculeatus), etc .; Diptera: onion maggot (Hylemya antiqua), seedcorn maggot (Hylemya platura), rice leafminer (Agromyza oryzae), rice Hime leafminer (Hydrellia griseola), Inekimoguribae (Chlorops oryzae), leafminer such as beans leafminer (Liriomyza trifolii), melon fly
• the harmful arthropods preferred examples include planthoppers, leafhoppers, aphids, stink bugs, rice weevil, rice beetles, moths, and moths.
• the harmful arthropod control composition of the present invention can also control plant diseases such as rice blight (Rhizoctonia solani).
• the harmful arthropod control composition of the present invention can be used in agricultural fields such as fields, paddy fields, dry fields, lawns, orchards, or non-cultivated areas.
• Agricultural crops corn, rice, wheat, barley, rye, oat, sorghum, cotton, soybean, peanut, buckwheat, sugar beet, rapeseed, sunflower, sugarcane, tobacco, etc.
• Vegetables Solanum vegetables (eggplants, tomatoes, peppers, peppers, potatoes, etc.), Cucurbitaceae vegetables (cucumbers, pumpkins, zucchini, watermelons, melons, etc.), Brassicaceae vegetables (radish, turnip, horseradish, kohlrabi, Chinese cabbage, cabbage) , Mustard, broccoli, cauliflower, rape, etc.), asteraceae vegetables (burdock, shungiku, artichoke, lettuce, etc.), liliaceae vegetables (eg, leek, onion, garlic, asparagus), celery family vegetables (carrot, parsley, celery, American Bow Fu etc.), Rubiaceae vegetables (spinach, chard, etc.), Lamiaceae vegetables (shiso, mint
• Fruit trees berries (apples, pears, Japanese pears, quince, quince, etc.), nuclear fruits (peaches, plums, nectarines, ume, sweet cherry, apricots, prunes, etc.), citrus (satsuma mandarin, orange, lemon, lime, grapefruit) ), Nuts (chestnut, walnut, hazel, almond, pistachio, cashew nut, macadamia nut, etc.), berries (blueberry, cranberry, blackberry, raspberry, etc.), grape, oyster, olive, loquat, banana, coffee, Date palm, coconut palm, oil palm etc.
• Trees other than fruit trees tea, mulberry, flowering trees (Satsuki, camellia, hydrangea, sasanqua, shikimi, sakura, yurinoki, crape myrtle, snapdragon, etc.), roadside trees (ash, birch, dogwood, eucalyptus, ginkgo, lilac, maple, oak) , Poplar, redwood, fu, sycamore, zelkova, blackfish, Japanese amberjack, moths, pine, pine, spruce, yew, elm, Japanese cypress, etc.), coral jug, dogwood, cedar, cypress, croton, masaki, kanamochi, etc.
• Lawn Shiba (Nasis, Pleurotus, etc.), Bermudagrass (Neurodonidae, etc.), Bentgrass (Oleoptera, Hykonukagusa, Odonoptera, etc.), Bluegrass (Nagahagusa, Oosuzunokatabira, etc.), Fescue (Oonishi nokegusa, Drosophila, etc.) , Grass, etc.), ryegrass (rat, wheat, etc.), anemonefish, blue whale, etc.
• the “plant” may be a plant imparted with resistance by a genetic recombination technique or a breeding method by crossing.
• the harmful arthropod control composition of the present invention can control harmful arthropods, for example, by applying it to plants or plant cultivation areas.
• the plant can be applied to plant foliage, plant flowers, plant nuts, plant seeds, and the like.
• the method for controlling harmful arthropods according to the present invention includes a step of applying an effective amount of the composition for controlling harmful arthropods to a plant or a plant cultivation site.
• the method for controlling harmful arthropods of the present invention is performed by applying the composition for controlling harmful arthropods of the present invention.
• Specific application methods include treatment of plant foliage such as foliage spraying, treatment of plant seeds, soil treatment, treatment of plant cultivation areas such as water surface application, and the like. Plants cultivated by ground spraying using a human sprayer, power sprayer, boom sprayer or cruckle sprayer, aerial spraying using an unmanned helicopter, etc. The method of processing to the surface of this is mentioned.
• Examples of the treatment for plant seeds include dipping treatment, spraying treatment, smearing treatment, film coating treatment, and pellet coating treatment.
• Plant planting treatment includes planting hole treatment, plant root treatment, grooving treatment, rowing treatment, full surface treatment, side row treatment, seedling box treatment, nursery bed treatment, soil mixing, bed soil mixing, paste fertilizer mixing , Water surface treatment, water spraying and the like.
• the application amount is the type of plant, the type and degree of occurrence of harmful arthropods to be controlled, the form of preparation, the processing time.
• the total amount of the present cyanamide compound, the present insect growth control compound and the present blight control compound is usually 0.5 to 3000 g per 1000 m 2 where the plant is cultivated, preferably 5 to 300 g.
• the effective amount means the total dose of the cyanamide compound, the insect growth control compound and the blight control compound, and the dose necessary for controlling harmful arthropods.
• the harmful arthropod composition of the present invention is an emulsion, wettable powder, flowable preparation or the like, it is usually applied by diluting with water and spraying.
• the total concentration of the present cyanamide compound, the present insect growth control compound and the present blight control compound is usually 0.00001 to 10% by weight, preferably 0.0001 to 5% by weight.
• the harmful arthropod composition of the present invention is a powder, granule or the like, it is usually applied as it is without dilution.
• Formulation Example 1 Add 5 parts of this cyanamide compound, 20 parts of methoxyphenozide and 2 parts of flutolanil to a mixture of 4 parts of sodium lauryl sulfate, 2 parts of calcium lignin sulfonate, 20 parts of synthetic silicon hydroxide fine powder and the remainder of diatomaceous earth and mix well. To obtain 100 parts of wettable powder.
• Formulation Examples 2-5 It replaces with 2 parts of flutolanil, and except having applied each compound and usage-amount of the [Table 1] description, operation similar to the formulation example 1 is performed, and 100 parts of each wettable powder is obtained.
• Formulation Example 6 Add 5 parts of this cyanamide compound, 20 parts of chromafenozide and 2 parts of flutolanil to a mixture of 4 parts of sodium lauryl sulfate, 2 parts of calcium lignin sulfonate, 20 parts of synthetic silicon hydroxide fine powder and the remainder of diatomaceous earth and mix well. To obtain 100 parts of wettable powder.
• Formulation Examples 7-10 It replaces with 2 parts of flutolanil, and except having applied each compound and usage-amount of the [Table 2] description, operation similar to the formulation example 6 is performed, and 100 parts of each wettable powder is obtained.
• Formulation Example 11 Add 5 parts of the present cyanamide compound, 40 parts of tebufenozide and 2 parts of flutolanil to a mixture of 4 parts of sodium lauryl sulfate, 2 parts of calcium lignin sulfonate, 20 parts of synthetic silicon hydroxide-containing fine powder and the remainder of diatomaceous earth and mix well. To obtain 100 parts of wettable powder.
• Formulation Examples 12-15 It replaces with 2 parts of flutolanil, and except having applied each compound and usage-amount of the [Table 3] description, operation similar to the formulation example 11 is performed, and 100 parts of each wettable powder is obtained.
• Formulation Example 16 By thoroughly pulverizing and mixing 0.35 part of the present cyanamide compound, 0.5 part of methoxyphenozide, 2 parts of flutolanil, 10 parts of talc and the remainder of kaolin clay, 100 parts of a powder is obtained.
• Formulation Examples 17-20 It replaces with 2 parts of flutolanil, and except having applied each compound and usage-amount of the [Table 4] description, operation similar to the formulation example 16 is performed, and 100 parts of each powder agent is obtained.
• Formulation Example 21 By thoroughly pulverizing and mixing 0.35 part of the present cyanamide compound, 0.5 part of chromafenozide, 2 parts of flutolanil, 10 parts of talc and the remainder of kaolin clay, 100 parts of a powder is obtained.
• Formulation Examples 22-25 It replaces with 2 parts of flutolanil, and except having applied each compound and usage-amount of [Table 5], operation similar to the formulation example 21 is performed, and 100 parts of each powder agent is obtained.
• Formulation Example 26 By thoroughly pulverizing and mixing 0.35 parts of the present cyanamide compound, 0.75 parts of tebufenozide, 2 parts of flutolanil, 10 parts of talc and the remainder of kaolin clay, 100 parts of a powder is obtained.
• Formulation Examples 27-30 It replaces with 2 parts of flutolanil, and except having applied each compound and usage-amount of the [Table 6] description, operation similar to the formulation example 26 is performed, and 100 parts of each powder agent is obtained.
• Formulation Example 31 By finely pulverizing 100 parts of a mixture of 2 parts of the present cyanamide compound, 4 parts of methoxyphenozide, 16 parts of flutolanil, 30 parts of white carbon containing 50 parts of polyoxyethylene alkyl ether sulfate ammonium salt and the remainder of the water by a wet grinding method, Obtain a flowable agent.
• white carbon containing 50 parts of polyoxyethylene alkyl ether sulfate ammonium salt means a 1: 1 weight ratio mixture of polyoxyethylene alkyl ether sulfate ammonium salt and white carbon.
• Formulation Examples 32-35 It replaces with 16 parts of flutolanil, and except having applied each compound and usage-amount of the [Table 7] description, operation similar to the formulation example 31 is performed, and 100 parts of each flowable agent is obtained.
• Formulation Example 36 By finely pulverizing 100 parts of a mixture obtained by mixing 2 parts of the present cyanamide compound, 4 parts of chromafenozide, 16 parts of flutolanil, 30 parts of white carbon containing 50 parts of polyoxyethylene alkyl ether sulfate ammonium salt and the remainder of water by a wet pulverization method, Obtain a flowable agent.
• Formulation Examples 37-40 It replaces with 16 parts of flutolanil, and except having applied each compound and usage-amount of the [Table 8] description, operation similar to the formulation example 36 is performed, and 100 parts of each flowable agent is obtained.
• Formulation Example 41 By finely pulverizing 100 parts of a mixture of 2 parts of the present cyanamide compound, 8 parts of tebufenozide, 16 parts of flutolanil, 30 parts of white carbon containing 50 parts of polyoxyethylene alkyl ether sulfate ammonium salt and the remainder of the water by a wet grinding method, Obtain a flowable agent.
• Formulation Examples 42 to 45 It replaces with 16 parts of flutolanil, and except having applied each compound and usage-amount of [Table 9], operation similar to the formulation example 41 is performed, and 100 parts of each flowable agent is obtained. Next, the effect of the present invention will be shown by test examples.
• Test example 1 After dissolving 6 mg of this cyanamide compound in 0.2 ml of acetone (manufactured by Wako Pure Chemical Industries, Ltd.) each containing Sorgen TW-20 (manufactured by Daiichi Kogyo Seiyaku), a spreading agent (trade name: Dyne) (Registered trademark, manufactured by Sumika Takeda Horticulture) was diluted with water containing 0.02% by volume.
• a water diluted solution of the present cyanamide compound, an aqueous diluted solution of methoxyphenozide, chromafenozide or tebufenozide, and an aqueous diluted solution of flutolanil, pencyclon or the active compound (I) were mixed to prepare a test drug solution.
• 2.5 ml of paper pot planted rice (Oryza sativa, variety: Hoshino Yume) seedlings were sprayed with 10 ml of the test chemical per strain.
• the rice seedlings were air-dried and placed in a glass test tube (diameter 30 mm, height 200 mm) containing 4.8 ml of water.
• harmful arthropods can be controlled.

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• Zoology (AREA)
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• Agricultural Chemicals And Associated Chemicals (AREA)

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• 2011
  • 2011-04-15 JP JP2011090796A patent/JP5776293B2/ja not_active Expired - Fee Related
• 2012
  • 2012-03-28 KR KR1020137029980A patent/KR101879902B1/ko active IP Right Grant
  • 2012-03-28 WO PCT/JP2012/059133 patent/WO2012141049A1/ja active Application Filing
  • 2012-03-28 CN CN2012800179701A patent/CN103458693A/zh active Pending
  • 2012-04-03 TW TW101111812A patent/TWI524847B/zh not_active IP Right Cessation

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