WO2012024167A8 - Improving terephthalic acid purge filtration rate by controlling % water in filter feed slurry - Google Patents

Improving terephthalic acid purge filtration rate by controlling % water in filter feed slurry Download PDF

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Publication number
WO2012024167A8
WO2012024167A8 PCT/US2011/047500 US2011047500W WO2012024167A8 WO 2012024167 A8 WO2012024167 A8 WO 2012024167A8 US 2011047500 W US2011047500 W US 2011047500W WO 2012024167 A8 WO2012024167 A8 WO 2012024167A8
Authority
WO
WIPO (PCT)
Prior art keywords
terephthalic acid
controlling
water
filtration rate
feed slurry
Prior art date
Application number
PCT/US2011/047500
Other languages
French (fr)
Other versions
WO2012024167A1 (en
Inventor
Kenny Randolph Parker
Original Assignee
Grupo Petrotemex, S.A. De C.V.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Grupo Petrotemex, S.A. De C.V. filed Critical Grupo Petrotemex, S.A. De C.V.
Priority to EP11818589.1A priority Critical patent/EP2606156B1/en
Priority to EA201390263A priority patent/EA027339B1/en
Priority to CN201180050626.8A priority patent/CN103168108B/en
Priority to BR112013003893-4A priority patent/BR112013003893B1/en
Priority to LTEP11818589.1T priority patent/LT2606156T/en
Priority to PL11818589T priority patent/PL2606156T3/en
Priority to MX2013001960A priority patent/MX2013001960A/en
Priority to JP2013524885A priority patent/JP5973438B2/en
Priority to CA2808095A priority patent/CA2808095C/en
Priority to KR1020137006909A priority patent/KR101943115B1/en
Priority to ES11818589.1T priority patent/ES2681655T3/en
Priority to UAA201303397A priority patent/UA113395C2/en
Publication of WO2012024167A1 publication Critical patent/WO2012024167A1/en
Publication of WO2012024167A8 publication Critical patent/WO2012024167A8/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/40—Regeneration or reactivation
    • B01J31/4015—Regeneration or reactivation of catalysts containing metals
    • B01J31/4023—Regeneration or reactivation of catalysts containing metals containing iron group metals, noble metals or copper
    • B01J31/403—Regeneration or reactivation of catalysts containing metals containing iron group metals, noble metals or copper containing iron group metals or copper
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/50—Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C63/00—Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings
    • C07C63/14—Monocyclic dicarboxylic acids
    • C07C63/15—Monocyclic dicarboxylic acids all carboxyl groups bound to carbon atoms of the six-membered aromatic ring
    • C07C63/24—1,3 - Benzenedicarboxylic acid
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

The process relates improving the recovery of a metal catalyst from an oxidizer purge stream produced in the synthesis of carboxylic acid, typically terephthalic acid, while utilizing pressure filtration.
PCT/US2011/047500 2010-08-20 2011-08-12 Improving telephthalic acid purge filtration rate by controlling % water in filter feed slurry WO2012024167A1 (en)

Priority Applications (12)

Application Number Priority Date Filing Date Title
EP11818589.1A EP2606156B1 (en) 2010-08-20 2011-08-12 Improving terephthalic acid purge filtration rate by controlling % water in filter feed slurry
EA201390263A EA027339B1 (en) 2010-08-20 2011-08-12 Improving telephthalic acid purge filtration rate by controlling % water in filter feed slurry
CN201180050626.8A CN103168108B (en) 2010-08-20 2011-08-12 Improve p-phthalic acid by the percent of water in controlling filter feed slurry and clean filtering rate
BR112013003893-4A BR112013003893B1 (en) 2010-08-20 2011-08-12 Terephthalic Acid Purge Process
LTEP11818589.1T LT2606156T (en) 2010-08-20 2011-08-12 Improving terephthalic acid purge filtration rate by controlling % water in filter feed slurry
PL11818589T PL2606156T3 (en) 2010-08-20 2011-08-12 Improving terephthalic acid purge filtration rate by controlling % water in filter feed slurry
MX2013001960A MX2013001960A (en) 2010-08-20 2011-08-12 Improving telephthalic acid purge filtration rate by controlling % water in filter feed slurry
JP2013524885A JP5973438B2 (en) 2010-08-20 2011-08-12 Increasing terephthalic acid purge filtration rate by controlling the percentage of water in the filter feed slurry
CA2808095A CA2808095C (en) 2010-08-20 2011-08-12 Improving terephthalic acid purge filtration rate by controlling % water in filter feed slurry
KR1020137006909A KR101943115B1 (en) 2010-08-20 2011-08-12 Improving terephthalic acid purge filtration rate by controlling % water in filter feed slurry
ES11818589.1T ES2681655T3 (en) 2010-08-20 2011-08-12 Improved filtration rate of terephthalic acid purge by controlling the percentage of water in the filter feed suspension
UAA201303397A UA113395C2 (en) 2010-08-20 2011-12-08 IMPROVEMENT OF THE FILTERING SPEED BY PLEASE TREATTLE ACID BY CONTROLLING% WATER IN THE SUSPENSION SUBMITTED TO THE FILTER

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US12/860,135 US8167974B2 (en) 2010-08-20 2010-08-20 Terephthalic acid purge filtration rate by controlling % water in filter feed slurry
US12/860,135 2010-08-20

Publications (2)

Publication Number Publication Date
WO2012024167A1 WO2012024167A1 (en) 2012-02-23
WO2012024167A8 true WO2012024167A8 (en) 2013-03-21

Family

ID=45593006

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2011/047500 WO2012024167A1 (en) 2010-08-20 2011-08-12 Improving telephthalic acid purge filtration rate by controlling % water in filter feed slurry

Country Status (19)

Country Link
US (1) US8167974B2 (en)
EP (1) EP2606156B1 (en)
JP (1) JP5973438B2 (en)
KR (1) KR101943115B1 (en)
CN (1) CN103168108B (en)
AR (1) AR082485A1 (en)
BR (1) BR112013003893B1 (en)
CA (1) CA2808095C (en)
EA (1) EA027339B1 (en)
ES (1) ES2681655T3 (en)
LT (1) LT2606156T (en)
MX (1) MX2013001960A (en)
MY (1) MY159964A (en)
PL (1) PL2606156T3 (en)
PT (1) PT2606156T (en)
TR (1) TR201810739T4 (en)
TW (1) TWI554330B (en)
UA (1) UA113395C2 (en)
WO (1) WO2012024167A1 (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8466312B2 (en) * 2010-08-20 2013-06-18 Grupo Petrotemex, S.A. De C.V. Terephthalic acid purge filtration rate by controlling % water in filter feed slurry
US20140175025A1 (en) * 2012-12-21 2014-06-26 Eastman Chemical Company Generation of low-solids second mother liquor from terephthalic acid production filter
US9943834B2 (en) * 2014-05-08 2018-04-17 Eastman Chemical Company Furan-2,5-dicarboxylic acid purge process
CN110092715A (en) * 2019-06-06 2019-08-06 恒力石化（大连）有限公司 A kind of system of the BA recycled in PTA residue and catalyst

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4939297A (en) * 1989-06-05 1990-07-03 Eastman Kodak Company Extraction process for removal of impurities from terephthalic acid filtrate
US7196215B2 (en) * 2001-06-04 2007-03-27 Eastman Chemical Company Process for the production of purified terephthalic acid
US6779456B2 (en) * 2002-07-01 2004-08-24 Special Devices, Inc. Initiator with a bridgewire configured in an enhanced heat-sinking relationship
US7161027B2 (en) * 2002-12-09 2007-01-09 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
US7381386B2 (en) * 2003-06-05 2008-06-03 Eastman Chemical Company Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid
US7410632B2 (en) * 2003-06-05 2008-08-12 Eastman Chemical Company Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid
US7282151B2 (en) * 2003-06-05 2007-10-16 Eastman Chemical Company Process for removal of impurities from mother liquor in the synthesis of carboxylic acid using pressure filtration
US20070203359A1 (en) * 2006-03-01 2007-08-30 Philip Edward Gibson Versatile oxidation byproduct purge process
JP2010126455A (en) * 2008-11-26 2010-06-10 Mitsubishi Chemicals Corp Method for producing aromatic carboxylic acid

Also Published As

Publication number Publication date
BR112013003893A2 (en) 2016-06-07
EP2606156B1 (en) 2018-07-04
BR112013003893B1 (en) 2019-02-26
TW201213012A (en) 2012-04-01
CN103168108A (en) 2013-06-19
PL2606156T3 (en) 2018-11-30
TWI554330B (en) 2016-10-21
MX2013001960A (en) 2013-05-09
EA027339B1 (en) 2017-07-31
KR101943115B1 (en) 2019-01-28
MY159964A (en) 2017-02-15
EP2606156A4 (en) 2014-03-19
EA201390263A1 (en) 2013-08-30
ES2681655T3 (en) 2018-09-14
JP5973438B2 (en) 2016-08-23
JP2013537550A (en) 2013-10-03
PT2606156T (en) 2018-08-01
KR20130090897A (en) 2013-08-14
US20120042752A1 (en) 2012-02-23
CA2808095C (en) 2018-09-25
UA113395C2 (en) 2017-01-25
US8167974B2 (en) 2012-05-01
TR201810739T4 (en) 2018-08-27
CN103168108B (en) 2016-06-01
LT2606156T (en) 2018-08-10
CA2808095A1 (en) 2012-02-23
WO2012024167A1 (en) 2012-02-23
AR082485A1 (en) 2012-12-12
EP2606156A1 (en) 2013-06-26

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