WO2011140477A3 - Procédé de séparation de l'acétaldéhyde dans des mélanges contenant de l'éthanol - Google Patents
Procédé de séparation de l'acétaldéhyde dans des mélanges contenant de l'éthanol Download PDFInfo
- Publication number
- WO2011140477A3 WO2011140477A3 PCT/US2011/035577 US2011035577W WO2011140477A3 WO 2011140477 A3 WO2011140477 A3 WO 2011140477A3 US 2011035577 W US2011035577 W US 2011035577W WO 2011140477 A3 WO2011140477 A3 WO 2011140477A3
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- ethanol
- acetaldehyde
- recovery
- purifying
- crude ethanol
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
- C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
- C07C29/147—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof
- C07C29/149—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof with hydrogen or hydrogen-containing gases
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Cette invention concerne la purification et/ou la récupération d'éthanol à partir d'un produit d'éthanol brut obtenu par hydrogénation de l'acide acétique. Les procédés de séparation et de purification d'un mélange d'éthanol brut sont utilisés pour récupérer l'éthanol et éliminer les impuretés. En particulier, les extrémités légères sont séparées dans une colonne d'extraction d'acétaldéhyde fonctionnant à une pression supérieure à la pression atmosphérique pour récupérer l'acétaldéhyde susceptible d'être renvoyé vers le réacteur et pour réduire les concentrations en acétaldéhyde dans un courant d'acétate d'éthyle.
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP11720937A EP2566837A2 (fr) | 2010-05-07 | 2011-05-06 | Procédé de purification d'ethanol |
CN201180011550.8A CN102918013B (zh) | 2010-05-07 | 2011-05-06 | 纯化乙醇的方法 |
Applications Claiming Priority (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US33269910P | 2010-05-07 | 2010-05-07 | |
US61/332,699 | 2010-05-07 | ||
US12/852,269 | 2010-08-06 | ||
US12/852,269 US8304586B2 (en) | 2010-02-02 | 2010-08-06 | Process for purifying ethanol |
US13/078,754 US8754267B2 (en) | 2010-05-07 | 2011-04-01 | Process for separating acetaldehyde from ethanol-containing mixtures |
US13/078,754 | 2011-04-01 |
Publications (2)
Publication Number | Publication Date |
---|---|
WO2011140477A2 WO2011140477A2 (fr) | 2011-11-10 |
WO2011140477A3 true WO2011140477A3 (fr) | 2012-03-01 |
Family
ID=46761372
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2011/035577 WO2011140477A2 (fr) | 2010-05-07 | 2011-05-06 | Procédé de séparation de l'acétaldéhyde dans des mélanges contenant de l'éthanol |
Country Status (4)
Country | Link |
---|---|
EP (1) | EP2566837A2 (fr) |
CN (1) | CN102918013B (fr) |
TW (1) | TW201204695A (fr) |
WO (1) | WO2011140477A2 (fr) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8304586B2 (en) * | 2010-02-02 | 2012-11-06 | Celanese International Corporation | Process for purifying ethanol |
CN112920015A (zh) * | 2019-12-06 | 2021-06-08 | 陶氏技术投资有限责任公司 | 用于精炼由醛的氢化衍生的醇的方法 |
CN113429261B (zh) * | 2021-06-18 | 2023-03-21 | 国家能源投资集团有限责任公司 | 从乙醇粗品中分离提纯乙醇的系统、方法和应用 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0990638A1 (fr) * | 1998-10-01 | 2000-04-05 | Kvaerner Process Technology Limited | Procédé |
Family Cites Families (30)
Publication number | Priority date | Publication date | Assignee | Title |
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US2882244A (en) | 1953-12-24 | 1959-04-14 | Union Carbide Corp | Molecular sieve adsorbents |
US3130007A (en) | 1961-05-12 | 1964-04-21 | Union Carbide Corp | Crystalline zeolite y |
US5026908A (en) | 1984-05-03 | 1991-06-25 | Hoechst Celanese Corporation | Methanol carbonylation process |
US5001259A (en) | 1984-05-03 | 1991-03-19 | Hoechst Celanese Corporation | Methanol carbonylation process |
US5144068A (en) | 1984-05-03 | 1992-09-01 | Hoechst Celanese Corporation | Methanol carbonylation process |
CA1299195C (fr) | 1986-06-16 | 1992-04-21 | G. Paull Torrence | Ajout d'hydrogene a un gaz d'alimentation contenant du monoxyde de carboneen vue de produire de l'acide acetique par carbonylateur du methanol |
US5821111A (en) | 1994-03-31 | 1998-10-13 | Bioengineering Resources, Inc. | Bioconversion of waste biomass to useful products |
USRE35377E (en) | 1993-05-27 | 1996-11-12 | Steinberg; Meyer | Process and apparatus for the production of methanol from condensed carbonaceous material |
US5599976A (en) | 1995-04-07 | 1997-02-04 | Hoechst Celanese Corporation | Recovery of acetic acid from dilute aqueous streams formed during a carbonylation process |
IN192600B (fr) | 1996-10-18 | 2004-05-08 | Hoechst Celanese Corp | |
BR0010379A (pt) | 1999-03-11 | 2001-12-26 | Dan Verser | Processo para a produção de etanol |
US7074603B2 (en) | 1999-03-11 | 2006-07-11 | Zeachem, Inc. | Process for producing ethanol from corn dry milling |
US6232352B1 (en) | 1999-11-01 | 2001-05-15 | Acetex Limited | Methanol plant retrofit for acetic acid manufacture |
US6627770B1 (en) | 2000-08-24 | 2003-09-30 | Celanese International Corporation | Method and apparatus for sequesting entrained and volatile catalyst species in a carbonylation process |
US6657078B2 (en) | 2001-02-07 | 2003-12-02 | Celanese International Corporation | Low energy carbonylation process |
US6685754B2 (en) | 2001-03-06 | 2004-02-03 | Alchemix Corporation | Method for the production of hydrogen-containing gaseous mixtures |
US7115772B2 (en) | 2002-01-11 | 2006-10-03 | Celanese International Corporation | Integrated process for producing carbonylation acetic acid, acetic anhydride, or coproduction of each from a methyl acetate by-product stream |
US7005541B2 (en) | 2002-12-23 | 2006-02-28 | Celanese International Corporation | Low water methanol carbonylation process for high acetic acid production and for water balance control |
NZ549320A (en) | 2004-01-29 | 2010-10-29 | Zeachem Inc | Recovery of organic acids |
US7208624B2 (en) | 2004-03-02 | 2007-04-24 | Celanese International Corporation | Process for producing acetic acid |
CN101646776A (zh) | 2007-02-09 | 2010-02-10 | 齐凯姆公司 | 制造产物的高能效方法 |
US7923405B2 (en) | 2007-09-07 | 2011-04-12 | Range Fuels, Inc. | Cobalt-molybdenum sulfide catalyst materials and methods for ethanol production from syngas |
EP2060553A1 (fr) | 2007-11-14 | 2009-05-20 | BP p.l.c. | Procédé pour la conversion d'hydrocarbures en alcool |
WO2009137708A1 (fr) | 2008-05-07 | 2009-11-12 | Zeachem Inc. | Récupération d'acides organiques |
US7863489B2 (en) | 2008-07-31 | 2011-01-04 | Celanese International Corporation | Direct and selective production of ethanol from acetic acid utilizing a platinum/tin catalyst |
US8501652B2 (en) | 2008-07-31 | 2013-08-06 | Celanese International Corporation | Catalysts for making ethanol from acetic acid |
US7608744B1 (en) | 2008-07-31 | 2009-10-27 | Celanese International Corporation | Ethanol production from acetic acid utilizing a cobalt catalyst |
US20100030002A1 (en) | 2008-07-31 | 2010-02-04 | Johnston Victor J | Ethylene production from acetic acid utilizing dual reaction zone process |
US20100030001A1 (en) | 2008-07-31 | 2010-02-04 | Laiyuan Chen | Process for catalytically producing ethylene directly from acetic acid in a single reaction zone |
US7884253B2 (en) | 2008-12-11 | 2011-02-08 | Range Fuels, Inc. | Methods and apparatus for selectively producing ethanol from synthesis gas |
-
2011
- 2011-05-06 TW TW100115921A patent/TW201204695A/zh unknown
- 2011-05-06 CN CN201180011550.8A patent/CN102918013B/zh not_active Expired - Fee Related
- 2011-05-06 EP EP11720937A patent/EP2566837A2/fr not_active Withdrawn
- 2011-05-06 WO PCT/US2011/035577 patent/WO2011140477A2/fr active Application Filing
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0990638A1 (fr) * | 1998-10-01 | 2000-04-05 | Kvaerner Process Technology Limited | Procédé |
Also Published As
Publication number | Publication date |
---|---|
CN102918013A (zh) | 2013-02-06 |
CN102918013B (zh) | 2014-12-24 |
TW201204695A (en) | 2012-02-01 |
EP2566837A2 (fr) | 2013-03-13 |
WO2011140477A2 (fr) | 2011-11-10 |
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