WO2011018799A3 - A process for preparing vanadium oxide from vanadate sludge - Google Patents

A process for preparing vanadium oxide from vanadate sludge Download PDF

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Publication number
WO2011018799A3
WO2011018799A3 PCT/IN2010/000531 IN2010000531W WO2011018799A3 WO 2011018799 A3 WO2011018799 A3 WO 2011018799A3 IN 2010000531 W IN2010000531 W IN 2010000531W WO 2011018799 A3 WO2011018799 A3 WO 2011018799A3
Authority
WO
WIPO (PCT)
Prior art keywords
vanadate
vanadium oxide
sludge
preparing vanadium
aluminium
Prior art date
Application number
PCT/IN2010/000531
Other languages
French (fr)
Other versions
WO2011018799A2 (en
Inventor
Sanjaya Ranjana Mohapatra
Rahul Jadhav
Seema Salvi
Sadguru Kulkarni
Original Assignee
Aditya Birla Science & Technology Co. Ltd
Hindalco Industries Limited
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Aditya Birla Science & Technology Co. Ltd, Hindalco Industries Limited filed Critical Aditya Birla Science & Technology Co. Ltd
Publication of WO2011018799A2 publication Critical patent/WO2011018799A2/en
Publication of WO2011018799A3 publication Critical patent/WO2011018799A3/en

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Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G31/00Compounds of vanadium
    • C01G31/02Oxides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00Halogens; Halogen acids
    • C01B7/19Fluorine; Hydrogen fluoride
    • C01B7/191Hydrogen fluoride
    • C01B7/192Preparation from fluorspar
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D1/00Oxides or hydroxides of sodium, potassium or alkali metals in general
    • C01D1/04Hydroxides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F11/00Compounds of calcium, strontium, or barium
    • C01F11/46Sulfates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G31/00Compounds of vanadium
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G31/00Compounds of vanadium
    • C01G31/003Preparation involving a liquid-liquid extraction, an adsorption or an ion-exchange
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/70Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity

Abstract

Vanadate sludge obtained as a by-product during Bayer's process contains fairly higher quantity of precious metal vanadium as vanadium oxide ( 5- 20% ) along with other impurities like sodium, aluminium and phosphorus salt. The present invention relates to a process for recovering vanadium oxide from vanadate sludge obtained from Bayer's process. The effluent generated during the process is recycled and the impurities such as sodium, aluminium and calcium are recovered as valuable by-product.
PCT/IN2010/000531 2009-08-10 2010-08-10 A process for preparing vanadium oxide from vanadate sludge WO2011018799A2 (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
IN1837MU2009 2009-08-10
IN1837/MUM/2009 2009-08-10
IN1836MU2009 2009-08-10
IN1836/MUM/2009 2009-08-10

Publications (2)

Publication Number Publication Date
WO2011018799A2 WO2011018799A2 (en) 2011-02-17
WO2011018799A3 true WO2011018799A3 (en) 2011-05-05

Family

ID=43586592

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/IN2010/000531 WO2011018799A2 (en) 2009-08-10 2010-08-10 A process for preparing vanadium oxide from vanadate sludge

Country Status (1)

Country Link
WO (1) WO2011018799A2 (en)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106244828B (en) * 2016-09-21 2018-03-02 武汉科技大学 A kind of impurity-removing method containing vanadium leachate
CN107739826A (en) * 2017-10-31 2018-02-27 成都先进金属材料产业技术研究院有限公司 A kind of method of the reduction containing sodium content in vanadium leachate
CN112266017B (en) * 2020-09-11 2023-08-15 河钢承德钒钛新材料有限公司 Method for preparing sodium vanadate from vanadium-phosphorus-containing solid waste
CN114293016A (en) * 2021-12-29 2022-04-08 四川省绵阳市华意达化工有限公司 Method for clean vanadium extraction from vanadium-containing solution
CN115057474B (en) * 2022-07-27 2023-11-14 中国科学院过程工程研究所 Method for medium internal circulation in process of preparing ammonium metavanadate from calcium vanadate
CN116103518A (en) * 2022-12-20 2023-05-12 东北大学 Vanadium extraction method of vanadium slag by taking barium slag as additive

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2175681C1 (en) * 2000-08-30 2001-11-10 ОАО "Чусовской металлургический завод" Method for production of vanadium pentaoxide from man-made raw material
CN101215005A (en) * 2008-01-14 2008-07-09 攀钢集团攀枝花钢铁研究院有限公司 Method for producing vanadium pentoxide by utilizing vanadium slag
CN101412539A (en) * 2008-11-18 2009-04-22 攀钢集团研究院有限公司 Clean production process for vanadium oxide

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2175681C1 (en) * 2000-08-30 2001-11-10 ОАО "Чусовской металлургический завод" Method for production of vanadium pentaoxide from man-made raw material
CN101215005A (en) * 2008-01-14 2008-07-09 攀钢集团攀枝花钢铁研究院有限公司 Method for producing vanadium pentoxide by utilizing vanadium slag
CN101412539A (en) * 2008-11-18 2009-04-22 攀钢集团研究院有限公司 Clean production process for vanadium oxide

Also Published As

Publication number Publication date
WO2011018799A2 (en) 2011-02-17

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