WO2010106417A2 - Formulations de soin personnel à base de plantes et procédé de préparation de celui-ci - Google Patents

Formulations de soin personnel à base de plantes et procédé de préparation de celui-ci Download PDF

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Publication number
WO2010106417A2
WO2010106417A2 PCT/IB2010/000548 IB2010000548W WO2010106417A2 WO 2010106417 A2 WO2010106417 A2 WO 2010106417A2 IB 2010000548 W IB2010000548 W IB 2010000548W WO 2010106417 A2 WO2010106417 A2 WO 2010106417A2
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WO
WIPO (PCT)
Prior art keywords
herbs
extract
blend
formulation according
formulation
Prior art date
Application number
PCT/IB2010/000548
Other languages
English (en)
Other versions
WO2010106417A3 (fr
Inventor
Ramesh Surianarayanan
Krishnan Manral
Uddagiri Venkanna Babu
Ekta Saxena
Chandrika Mahendra
Original Assignee
Himalaya Global Holdings Ltd.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Himalaya Global Holdings Ltd. filed Critical Himalaya Global Holdings Ltd.
Publication of WO2010106417A2 publication Critical patent/WO2010106417A2/fr
Publication of WO2010106417A3 publication Critical patent/WO2010106417A3/fr

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Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A61K36/484—Glycyrrhiza (licorice)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/58—Meliaceae (Chinaberry or Mahogany family), e.g. Azadirachta (neem)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/59—Menispermaceae (Moonseed family), e.g. hyperbaena or coralbead
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
    • A61K36/8965—Asparagus, e.g. garden asparagus or asparagus fern
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/906—Zingiberaceae (Ginger family)
    • A61K36/9066—Curcuma, e.g. common turmeric, East Indian arrowroot or mango ginger
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9794—Liliopsida [monocotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/10—Washing or bathing preparations

Definitions

  • This invention in general relates to a herbal personal care formulation.
  • the present invention provides a herbal personal care formulation comprising extracts of herbs and enzyme based preservatives and essential oil blend, along with cosmeceutically acceptable excipients and method of preparing the same.
  • Herbs are highly susceptible to bacterial and fungal contamination, therefore herbal personal care products require good preservatives to withstand the shelf life without any micro contamination. This is also because Personal care products like shampoos kept in the bathroom and used over a period of few weeks and therefore there is a possibility of contamination during use. Traditionally preservatives used like
  • US Patent no. 7,083,779B2 by Behl et al. discloses a synergistic herbal formulation comprising herbal extract of Azadirechta indica, Citrullus colocynthis, Cucumis sativus and pharmaceutically acceptable carriers.
  • the herbal formulation is non-toxic and biodegradable and useful in the form of lotion, cream, mouthwash, toothpaste or similar forms of application in daily life.
  • US Patent no. 7,279,151 by Pushpangadan et al. disclose a herbal dental care formulation comprising herbs such as Citrus karna, Zanthoxylum armatum, and
  • Azadirachta indica thereof which can be combined with pharmaceutically acceptable carriers or diluents to be administered in the form of powder, paste, gel, mouthwash and chewing gum etc.
  • the formulation also contains Mint.
  • Further object is to provide a method of preparing a personal care formulation comprising extracts of herbs and enzyme based preservatives and essential oil blend, wherein said method is devoid of using any solvent.
  • a personal care formulation comprising extracts of herbs and enzyme-based preservatives and essential oil blend, along with other cosmeceutically acceptable excipients, wherein the extract is prepared employing a super critical fluid extraction and water extraction.
  • a personal care formulation comprising extracts of herbs and enzyme-based preservatives and essential oil blend, along with other cosmeceutically acceptable excipients, wherein the extract of herbs is obtained from a blend of herbs selected from Azadirachta indica, Curcuma longa, Glycyrrhiza glabra, Asparagus racemosus, Tinospora cordifolia and Sida cordifolia and in various combinations thereof.
  • a personal care formulation comprising extracts of herbs and enzyme-based preservatives and essential oil blend, along with other cosmeceutically acceptable excipients, wherein the extract of herbs is obtained from a blend of herbs selected from Azadirachta indica and Curcuma longa.
  • a personal care formulation comprising extracts of herbs and enzyme-based preservatives and essential oil blend, along with other cosmeceutically acceptable excipients, wherein the extract of herbs is obtained from a blend of herbs selected from Glycyrrhiza glabra, Asparagus racemosus, Tinospora cordifolia and Sida cordifolia and in various combinations thereof.
  • a personal care formulation comprising extracts of herbs and enzyme-based preservatives and essential oil blend, along with other cosmecutically acceptable excipients, wherein the blend extract is used in the range of 0.5% to 2%.
  • a personal care formulation comprising extracts of herbs and enzyme-based preservatives and essential oil blend, along with other cosmecutically acceptable excipients, wherein the preservatives are natural, two-part "system", based on an enzyme solution containing lactoperoxidase and glucose oxidase and a substrate solution containing glucose, thiocyanate and iodide ions, and essential oil blends.
  • a personal care formulation comprising extracts of herbs and enzyme-based preservatives and, .essential oil blend, along with other cosmeceutically acceptable exdipjdftS; Stfheteifr the preservative is used in the range of 0.05% to 1.05%. ⁇ . ⁇ • ⁇ " l !
  • a personal care formulation comprising extracts of herbs and enzyme-based preservatives and essential oil blend, along with other cosmeceutically acceptable excipients, wherein said formulation is in the form of any kind of personal care formulation, preferably, Face wash, Revitalizing hand wash and Revitalizing Body Lotion.
  • a personal care formulation comprising extracts of herbs and enzyme-based preservatives and essential' ⁇ irbiend, along with other cosmeceutically acceptable excipients, wherein said formulation is prepared by a method comprising blending the organically certified herbs and extracting the resultant herbs employing super critical fluid extraction (SCFE), mixing the resultant extract of blend with enzyme based preservatives and essential oil blend, along with cosmeceutically acceptable excipients.
  • SCFE super critical fluid extraction
  • a personal care formulation comprising extracts of herbs and enzyme-based preservatives and essential oil blend, along with other cosmeceutically acceptable excipients, wherein said formulation is prepared by a method comprising blending the organically certified herbs and extracting the resultant herbs employing percolation or soxhlation using water, mixing the resultant extract of blend with enzymes based preservatives and essential oil blend, along with cosmeceutically acceptable excipients.
  • the present invention discloses a personal care formulation comprising extracts of herbs and enzyme-based preservatives and essential oil blend, along with other cosmeceutically acceptable excipients
  • the present invention describes the preparation of various types of herbal personal care formulation. According to one of the example, wherein various Face Washes are developed preferably Neem and Turmeric Face wash.'
  • the said extract of herbs is obtained from a blend of herbs selected from Azadirachta indica, Curcuma longa, Glycyrrhiza glabra, Asparagus racemosus, Tinospora cordifolia and Sida cordifoliaand.
  • a method of preparing the extract from said herbs wherein process is performed using suitable extraction technique, preferably super critical fluid extraction, cold percolation method, hot-soxhlation method or percolation method.
  • suitable extraction technique preferably super critical fluid extraction, cold percolation method, hot-soxhlation method or percolation method.
  • said extract of herbs can be prepared by using any parts of herbs, preferably leaf of Azadirachta indica, rhizomes of Curcuma longa, root of Glycyrrhiza glabra, root of Asparagus racemosus, stem of Tinospora cordifolia and root of Sida cordifoliaand.
  • This invention discloses a synergistic combination of preservatives containing enzyme based preservatives like Biovert*, nature identical preservatives like Sorbates and essential oil blends maximun ⁇ ttp ⁇ to ⁇ A'CBiovert is enzyme based preservative sold by Arch chemicals,
  • Example 1 We have evaluated face washes with use of biovert, potassium sorbate and other herbal materials /oils for total microbial count.
  • Decyl Glucoside and Coco Glucoside is weighed in the side vessel and mixed well for 10 minutes. The mixture pH is adjusted by 20% citric acid solution around 5.50.
  • Glycerin is taken in a separate SS Vessel and Amaze-XT is dispersed in it using Karl Homogeniser.
  • DM water is taken in the main vessel and to it is added the slurry of glycerine & tart-XT to form gum dispersion.
  • the surfactant mixture from the step 1 is then transferred to the main vessel under vacuum. This is mixed for 20 minutes to ensure complete mixing.
  • Natural Vitamin E is added into the main vessel and mixed well.
  • the vortexed samples were spread on the prescribed media agar plate (Hi-Media) in duplicate for bacteria and fungi, using turntable and sterile spreader uniformly, maintaining aseptic conditions, in the Laminar Air Flow cabinet.
  • examined the plates for growth count the number of colonies manually or using colony counter , and express the average of two plates in terms of colony forming units per gram or per ml of the test substance (CFU/gm or CFU/ml), using the following formula: Average number of colonies from ⁇ 2 plates X dilution factor
  • the dried material of leaves of Azhadirachta indica was pulverized to coarse powder and about 25 Kg of powdered material was placed in a SCF extractor at the temperature of 40-50C at high pressure of 280-320 bar using carbon dioxide as super critical fluid for extraction upto 4 to 6 hours and then the extract was collected in the collection vessel and evaporated at room temperature to remove any further residues of carbon dioxide.
  • the extract thus obtained was free from any solvent residues and in highest pure form.
  • the dried materials of leaves of Azadirachta indica was pulverized to coarse powder and 25 Kg of powdered material was placed in percolator soaked with purified water for 24 hours at room temperature. The next day the extract was decanted from the percolator and filtered through musclin cloth and dried to fine powder.
  • the dried material of rhizomes of Curcuma longa was pulverized to coarse powder and about 25 Kg of powdered material was placed in a SCF extractor at the temperature of 40-50C at high pressure of 280-320 bar using carbon dioxide as super critical fluid for extraction upto 4 to 6 hours and then the extract was collected in the collection vessel and evaporated at room temperature to remove any further residues of carbon dioxide.
  • the extract thus obtained was free from any solvent residues and in highest pure form.
  • the dried materials of leaves of Curcuma longa was pulverized to coarse powder and 25 Kg of powdered material was placed in soxhlator and refluxed with purified water at steam temperature for 4-6 hours. The process was repeated for three cycles and the resultant extracts were filtered through musclin cloth and concentrated to dryness.
  • the dried materials of leaves of Glycyrrhiza glabra was pulverized to coarse powder and 25 Kg of powdered material was placed in percolator soaked with purified water for 24 hours at room temperature. The next day the extract was decanted from the percolator and filtered through musclin cloth and dried to fine powder
  • Example 16 Preparation of water extract from Glycyrrhiza glabra by hot-soxhlation method powder and 25 Kg of powdered material was placed in soxhlator and refluxed with purified water at steam temperature for 4-6 hours. The process was repeated for three cycles and the resultant extracts were filtered through musclin cloth and concentrated to dryness.
  • Example 17 Preparation of water extract from Glycyrrhiza glabra by hot-soxhlation method powder and 25 Kg of powdered material was placed in soxhlator and refluxed with purified water at steam temperature for 4-6 hours. The process was repeated for three cycles and the resultant extracts were filtered through musclin cloth and concentrated to dryness.
  • Example 17 Preparation of water extract from Glycyrrhiza glabra by hot-soxhlation method powder and 25 Kg of powdered material was placed in soxhlator and refluxed with purified water at steam temperature for 4-6 hours. The process was repeated for three cycles
  • the dried materials of leaves of Asparagus racemosus was pulverized to coarse powder and 25 Kg of powdered material was placed in percolator soaked with purified water for 24 hours The next day the extract was decanted from the percolator and filtered through musclin cloth and dried to fine powder.
  • the dried materials of leaves of Asparagus racemosus was pulverized to coarse powder and 25 Kg of powdered material was placed in soxhlator and refluxed with purified water at steam temperature for 4-6 hours. The process was repeated for three cycles and the resultant extracts were filtered through musclin cloth and concentrated to dryness.
  • the dried material of stem was pulverized to coarse powder and about 25 Kg of powdered material was placed in a SCF extractor at the temperature of 40-50C at high pressure of 280-320 bar using carbon dioxide as super critical fluid for extraction upto 4 to 6 hours and then the extract was collected in the collection vessel and evaporated at room temperature to remove any further residues of carbon dioxide.
  • the extract thus obtained was free from any solvent residues and in highest pure form.
  • the dried materials of leaves of Tinospora cordifolia was pulverized to coarse powder and 25 Kg of powdered material was placed in percolator soaked with purified water for 24 hours at room temperature. The next day the extract was decanted from the percolator and filtered through musclin cloth and dried to fine powder.
  • the dried material of Sida cordifolia roots was pulverized to coarse powder and about 25 Kg of powdered material was placed in a SCF extractor at the temperature of 40-50C at high pressure of 280-320 bar using carbon dioxide as super critical fluid for extraction upto 4 to 6 hours and then the extract was collected in the collection vessel and evaporated at room temperature to remove any further residues of carbon dioxide.
  • the extract thus obtained was free from any solvent residues and in highest pure form.
  • the shade dried material of herbal blend of Glycyrrhiza glabra roots and/or Asparagus racemosus roots and /or Tinospora cordifolia stem and/or Sida cordifolia roots in the ratio of 1 : 1 : 1 : 1 respectively was pulverized to coarse powder and about 100 Kg of powdered herbal blend was placed in a SCF extractor at the temperature of 40-50C at high pressure of 300-350 bar using carbon dioxide as super critical fluid for extraction upto 4 to 6 hours and then the extract was collected in the collection vessel and evaporated at room any further residues of carbon dioxide. The extract thus obtained was free from any solvent residues and in highest pure form.

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Mycology (AREA)
  • Engineering & Computer Science (AREA)
  • Botany (AREA)
  • Chemical & Material Sciences (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Medicinal Chemistry (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Medical Informatics (AREA)
  • Birds (AREA)
  • Dermatology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Cosmetics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

La présente invention concerne une formulation de soin personnel à base de plantes comprenant des extraits de plantes et des conservateurs à base d'enzyme, un mélange d'huiles essentielles, et des excipients acceptables en cosmétique, et un procédé de préparation de celui-ci.
PCT/IB2010/000548 2009-03-16 2010-03-16 Formulations de soin personnel à base de plantes et procédé de préparation de celui-ci WO2010106417A2 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
IN504/DEL/2009 2009-03-16
IN504DE2009 2009-03-16

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Publication Number Publication Date
WO2010106417A2 true WO2010106417A2 (fr) 2010-09-23
WO2010106417A3 WO2010106417A3 (fr) 2011-03-31

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PCT/IB2010/000548 WO2010106417A2 (fr) 2009-03-16 2010-03-16 Formulations de soin personnel à base de plantes et procédé de préparation de celui-ci

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012011892A1 (fr) * 2010-07-19 2012-01-26 Colgate-Palmolive Company Composition de nettoyage avec des décyl- et coco-glucosides
CN108130234A (zh) * 2018-01-19 2018-06-08 北京麦恩缇斯国际商贸有限公司 天然抑菌洗手液及其制备方法

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6080401A (en) * 1998-11-19 2000-06-27 Reddy; Malireddy S. Herbal and pharmaceutical drugs enhanced with probiotics
US20040156920A1 (en) * 2000-07-14 2004-08-12 Kane Shantaram Govind Extracts from plant and non-plant biomass and uses thereof
US20070122492A1 (en) * 2004-11-18 2007-05-31 Stephen Behr Plant extracts and dermatological uses thereof
WO2007074349A2 (fr) * 2005-12-29 2007-07-05 Robert Basic Régulation de réaction allergique
US20070253943A1 (en) * 2004-06-22 2007-11-01 Ali Altunkaya Compositions for Topical Treatment
US20080226568A1 (en) * 2007-03-13 2008-09-18 Playtex Products, Inc. Synergistic preservative systems and their use in topical compositions

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6080401A (en) * 1998-11-19 2000-06-27 Reddy; Malireddy S. Herbal and pharmaceutical drugs enhanced with probiotics
US20040156920A1 (en) * 2000-07-14 2004-08-12 Kane Shantaram Govind Extracts from plant and non-plant biomass and uses thereof
US20070253943A1 (en) * 2004-06-22 2007-11-01 Ali Altunkaya Compositions for Topical Treatment
US20070122492A1 (en) * 2004-11-18 2007-05-31 Stephen Behr Plant extracts and dermatological uses thereof
WO2007074349A2 (fr) * 2005-12-29 2007-07-05 Robert Basic Régulation de réaction allergique
US20080226568A1 (en) * 2007-03-13 2008-09-18 Playtex Products, Inc. Synergistic preservative systems and their use in topical compositions

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012011892A1 (fr) * 2010-07-19 2012-01-26 Colgate-Palmolive Company Composition de nettoyage avec des décyl- et coco-glucosides
US8877184B2 (en) 2010-07-19 2014-11-04 Colgate-Palmolive Company Cleaning composition with decyl and coco glucosides
US9504635B2 (en) 2010-07-19 2016-11-29 Colgate-Palmolive Company Composition containing 4-oxovaleric acid and leuconostoc/radish root ferment filtrat
CN108130234A (zh) * 2018-01-19 2018-06-08 北京麦恩缇斯国际商贸有限公司 天然抑菌洗手液及其制备方法
CN108130234B (zh) * 2018-01-19 2020-05-15 北京麦恩缇斯国际商贸有限公司 天然抑菌洗手液及其制备方法

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