WO2010100253A1 - Predictive rolling bearing maintenance - Google Patents
Predictive rolling bearing maintenance Download PDFInfo
- Publication number
- WO2010100253A1 WO2010100253A1 PCT/EP2010/052818 EP2010052818W WO2010100253A1 WO 2010100253 A1 WO2010100253 A1 WO 2010100253A1 EP 2010052818 W EP2010052818 W EP 2010052818W WO 2010100253 A1 WO2010100253 A1 WO 2010100253A1
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- signal
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- rolling bearing
- processing
- vibration
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Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01M—TESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
- G01M13/00—Testing of machine parts
- G01M13/04—Bearings
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01M—TESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
- G01M13/00—Testing of machine parts
- G01M13/04—Bearings
- G01M13/045—Acoustic or vibration analysis
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16C—SHAFTS; FLEXIBLE SHAFTS; ELEMENTS OR CRANKSHAFT MECHANISMS; ROTARY BODIES OTHER THAN GEARING ELEMENTS; BEARINGS
- F16C19/00—Bearings with rolling contact, for exclusively rotary movement
- F16C19/52—Bearings with rolling contact, for exclusively rotary movement with devices affected by abnormal or undesired conditions
- F16C19/527—Bearings with rolling contact, for exclusively rotary movement with devices affected by abnormal or undesired conditions related to vibration and noise
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01M—TESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
- G01M13/00—Testing of machine parts
- G01M13/02—Gearings; Transmission mechanisms
- G01M13/028—Acoustic or vibration analysis
Definitions
- the present invention relates in general to predictive rolling bearing maintenance, and in particular to maintenance-oriented, condition-based monitoring of rolling bearings in servomotors operating at an arbitrarily variable low speed and with (cyclic) motion inversions, such those employed in Filling Machines or Distribution Equipments of Packaging Lines designed to produce sealed packages containing a food product.
- Distribution Equipments such as, accumulators, straw applicators, film wrappers, and cardboard packers, connected to the Filling Machine via Conveyors, for the handling of the packages.
- a typical example of this type of packages is the parallelepiped-shaped package for liquid or pourable food products known as Tetra Brik Aseptic ®, which is made by folding and sealing a laminated web of packaging material.
- the packaging material has a multilayer sheet structure substantially comprising one or more stiffening and strengthening base layers typically made of a fibrous material, e.g. paper, or mineral-filled polypropylene material, covered on both sides with a number of heat-seal plastic material layers, e.g. polyethylene film.
- the packaging material also comprises a gas- and light-barrier material layer, e.g. aluminium foil or ethyl vinyl alcohol (EVOH) film, which is superimposed on a heat-seal plastic material layer, and is in turn covered with another heat-seal plastic material layer forming the inner face of the package eventually contacting the food product.
- a gas- and light-barrier material layer e.g. aluminium foil or ethyl vinyl alcohol (EVOH) film
- Packages of this sort are produced on fully automatic Filling Machines, wherein a continuous vertical tube is formed from the web-fed packaging material; which is sterilized by applying a chemical sterilizing agent such as a hydrogen peroxide solution, which, once sterilization is completed, is removed, e.g. evaporated by heating, from the surfaces of the packaging material; and the sterilized web is maintained in a closed, sterile environment, and is folded and sealed longitudinally to form the vertical tube.
- a chemical sterilizing agent such as a hydrogen peroxide solution
- the tube is then filled downwards with the sterilized or sterile-processed pourable food product, and is fed along a vertical path to a forming station, where it is gripped along equally spaced cross sections by a jaw system including two or more pairs of jaws, which act cyclically and successively on the tube, and seal the packaging material of tube to form a continuous strip of pillow packs connected to one another by transverse sealing strips.
- Pillow packs are separated from one another by cutting the relative sealing strips, and are conveyed to a final folding station where they are folded mechanically into the finished, e.g. substantially parallelepiped-shaped, packages.
- the packaging material may be cut into blanks, which are formed into packages on forming spindles, and the packages are filled with food product and sealed.
- the so-called "gable-top” package known as Tetra Rex ®.
- preventive periodic maintenance activities such as cleaning and lubrication
- contamination may come from the exterior (e.g. the bearing is placed in a hostile environment) but may also be due to internal causes (e.g. due to small flakes of material that the revolving elements lose during operation).
- vibration analysis is an important part of industrial predictive maintenance programs so that wear and damages in the rolling bearings can be discovered and repaired before the machine breaks down, thus reducing operating and maintenance costs.
- Empirical evaluation of the vibration level of a bearing is an error-prone activity that may lead to significantly underestimate or overestimate the remaining lifetime of the component, and also to mistake for a bearing damage a noise that is due to a completely different cause (e.g. a shaft imbalance). For this reason, the scientific community has striven to provide a scientific characterization of bearing faults, and nowadays a rich literature can be found on this topic.
- the basic idea is associating each failure mode of a bearing with a characteristic frequency signature, that can be extracted from a vibration signal via an appropriate analysis.
- traditional vibration analysis is based on the fact that if there is a localized damage on one of the bearing surfaces, it will cause a series of impacts during bearing rotation; moreover, such impacts are periodic assuming that the servomotor is rotating at constant speed.
- a kinematic analysis of the bearing shows that, assuming that no slip is present, the component is quite similar to an epicyclic gear; in other words there is a fixed "transmission ratio" between the servomotor shaft and all the other moving parts of the bearing, and this leads to the fundamental equation of vibration analysis:
- the damage frequency (which is actually the frequency of such impacts) depends linearly on the rotation frequency f by means of a damage coefficient k d which is none other than the transmission ratio between the servomotor shaft and the moving part on which the damage is located.
- k d which is none other than the transmission ratio between the servomotor shaft and the moving part on which the damage is located.
- Bd, Pd are ball and pitch diameter
- N is the number of revolving elements
- ⁇ is an angle that indicates a possible misalignment between inner and outer rings (or rings) as a result of mounting operations (typical values are between 0 and 10 degrees)
- subscript d relates in general to damage frequencies
- subscripts g, e, i and v relate to specific kinds of damage, namely in the inner and outer rings, in the balls evenly angularly spaced apart between the inner and outer rings, and in the cage which retains the balls and which rotates jointly, i.e., at the same speed, with the balls.
- forcing action u(t) will be a periodic repetition at the damage frequency of the original impulse d(t):
- G(f) is the transfer function of the mechanical assembly
- H(f) is the sensor (usually an accelerometer) sensitivity function
- N(f) is any kind of noise superimposed to the fault signal.
- the spectrum of Y(f) as such may not therefore be the best signal to look at in order to identify a damage signature; the usual procedure to obtain a signal with better signal-to-noise ratio is called envelope analysis and is based on the following assumptions: there exist a frequency band [fl, f2] such that:
- the damage causes a series of short-duration impacts, that generate a train of spikes in the frequency spectrum of the vibration signal with a certain periodicity
- OT Order Tracking
- R. Potter A new order tracking method for rotating machinery, Sound and Vibration 24, 1990, 30-34, and K. Fyfe, E. Munck, Analysis of computed order tracking, Mechanical System and Signal Processing 11(2), 1997, 187-205.
- Order Tracking is based on a constant spatial sampling approach, according to which the vibration signal is sampled at constant angular increments (i.e. uniform ⁇ ), and hence at a frequency proportional to the bearing rotation speed.
- Traditional order tracking accomplishes this task by using a variable-time data acquisition system, wherein a time-sampling is performed at a frequency which is varied proportionally to the bearing rotation speed.
- Computed order tracking (COT) instead, accomplishes this task by using a constant-time data acquisition system, wherein the vibration signal is first time-sampled at a constant frequency (i.e. constant-time sampling with uniform At), and then the sampled data are digitally spatially re-sampled at constant angular increments (i.e.
- Order Tracking maps real time reference t to a modified time reference ⁇ such that the vibration signal is seen as if it were generated piece-wise by a bearing rotating at a constant speed. This mapping results in a modified vibration signal where the frequency signature of a given typology of damage can be found, and in a rolling bearing fault being satisfactorily predicted.
- Computed Order Tracking is still based on further assumptions about the servomotor operation, such as operation at a high rotation speed (>500 rpm), several shaft revolutions needed for the fault detection, no motion inversions, which prevent its teaching from being satisfactorily applicable to servomotors which operate at arbitrarily variable low rotation speed, are subjected to cyclic motion inversions, and perform about one shaft revolution per cycle, such as those employed in the food product packaging field to operate the jaw systems.
- the objective of present invention is hence to provide a technique which allows the Computed Order Tracking to be applied also to servomotors which operate at arbitrarily variable low rotation speed, are subjected to cyclic motion inversions, and perform about one shaft revolution per cycle, such as those employed in the food product packaging field, to satisfactorily predict servomotor rolling bearing faults, so allowing the current machine maintenance programs to be effectively enhanced.
- This objective is achieved by the present invention in that it relates to a method of predicting faults in a rolling bearing, to a digital signal processing system programmed to implement the method, and to a software product designed to implement, when executed, the method, as defined in the appended claims.
- Figure 1 shows a general block diagram of a data acquisition system configured to implement a Modified Computed Order Tracking according to the present invention
- Figure 2 shows a general flowchart of the Modified Computed Order Tracking according to the present invention
- Figure 3 schematically shows a cross-section of an 8-ball bearing
- Figures 4 and 5 show a "cut & paste" operation according to a first embodiment of the present invention, to be performed on an acquired position signal x(t) and a filtered vibration signal y/t) to test a rolling bearing for a fault in the outer ring;
- Figures 6a and 6b show relative positions of an inner ring and, respectively, of a balls-cage assembly with respect to an outer ring of a rolling bearing plotted versus time;
- Figures 7 and 8 show a "cut & paste" operation according to a first embodiment of the present invention, to be performed on an acquired position signal x(t) and a filtered vibration signal y/t) to test a rolling bearing for a fault in the inner ring;
- Figures 9a and 9b show relative positions of an inner ring with respect to an outer ring and, respectively, of a balls-cage assembly with respect to an inner ring of a rolling bearing plotted versus time;
- Figures 10 and 11 show a "cut & paste" operation according to a second embodiment of the present invention, to be performed on an acquired position signal x(t) and a filtered vibration signal y/t);
- Figures 12a and 12b show a processed position signal x (t) obtained after a "cut & paste" operation and, respectively, a space-sampled position signal x (t) obtained by constant-space sampling a processed position signal x (t); • Figures 13, 14 and 15 show processed space-sampled position and vibration signals obtained by reversing portions of the space-sampled position and vibration signals x (t) and y (t) corresponding to the falling ramps of the space- sampled position signals x (t) shown in Figures 5, 7 and 11, respectively; and
- Figures 16 and 17 show frequency spectra of the reversed vibration signal shown in Figure 13, wherein the damage frequencies relating to an outer ring fault and an inner ring fault are depicted.
- Figure 1 shows a general block diagram of a data acquisition system configured to implement the MCOT according to the present invention.
- reference numeral 1 designates a servomotor with a shaft 2 rotatably supported by a rolling bearing 3 ( Figure 3) comprising an inner ring 3a, and outer ring 3b, and rolling bodies 3c retained and evenly angularly distributed between the inner and outer rings 3a, 3b by a cage 3d, and whose faults are to be predicted via the
- reference numeral 4 designates the servomotor drive, which supplies the servomotor 1 with electric power via a power cable 5, receives from the servomotor 1, via a feedback cable 6, a feedback signal generated by a high-resolution encoder (not shown) associated with the servomotor shaft 2, and outputs a position signal x(t) which is generated based on the feedback signal from the servomotor 1 and is indicative of the angular position of the servomotor shaft 2, and hence of the inner ring 3a with respect to the outer ring 3b of the rolling bearing 3; reference numeral 7 designates an accelerometer, which is associated with the monitored rolling bearing 3 and outputs a vibration signal y(t) which is indicative of the intensity of the vibrations in the rolling bearing 3; and reference numeral 8 designates a digital signal processing system configured to implement the MCOT according to the present invention.
- DSP digital signal processing
- the first step of the MCOT (block 100) is identifying a candidate bearing component to be tested for faults (e.g., inner ring fault, outer ring fault, etc.).
- a candidate bearing component to be tested for faults is indicated by an operator via a Graphical User Interface (GUI) implemented by the digital signal processing system 8, and is necessary because testing different bearing components for faults requires separate executions of the MCOT, as the reader will appreciate afterwards when the third step of the MCOT is described.
- GUI Graphical User Interface
- the second step of the MCOT (block 200) is identifying a suitable frequency band [/ ⁇ , /i] where the envelope analysis on the time-sampled vibration signal y(t) is performed: this means identifying a resonance frequency in the assembly wherein the servomotor is placed, and it can be done either by simulation or measurement. Such information is application-specific and therefore not likely to change by replacing the servomotor or even by moving to another machine of the same model.
- the time- sampled position signal x(t) and the time-sampled vibration signal y(t) are acquired over a given acquisition time period, for example of 50 s, and then the time-sampled vibration signal y(t) is band-pass filtered in [/ ⁇ , /i] and demodulated, so obtaining what hereinafter will be referred to as filtered vibration signal y/t).
- Filtering and demodulation of the time-sampled vibration signal y(t) is carried out because the filtered vibration signal y/t) has a bandwidth equal to/i-/), which is generally much lower than the one of the time-sampled vibration signal y(t), and this may improve significantly the readability of the results, especially in highly noisy environments.
- the third step of the MCOT (block 300) is processing the time-sampled position signal x(t) and the filtered time-sampled vibration signal y/t) according to two different, alternative embodiments of the present invention.
- a particular signal processing is performed which stems from an in-depth analysis of what happens in a faulted bearing during an operating cycle thereof.
- the rolling bearing is of an 8-ball type shown in Figure 3, wherein each pair of adjacent balls are spaced apart of an angular gap of 45°.
- Ri-c/45 and Ro-c/45 are not integers results in the operating cycles of the servomotor generally not ending with an impact, namely in the servomotor performing, after the last impact (third or fifth in the example considered above), an additional angular displacement before reversing the rotation direction.
- the signal processing according to the first embodiment of the present invention is aimed at causing the time-sampled position signal x(t) and the filtered vibration signal y/t) to look like as if they were generated by an inner ring that continuously rotates in one and the same direction, namely without any inversion of the rotation direction, with respect to the outer ring, and during which the balls-cage assembly performs angular displacements with respect to the inner and outer rings, respectively, each equal to an integer multiple of the angular displacement between two consecutive impacts in the rolling bearing.
- This aim is achieved by processing the time-sampled position signal x(t) and the filtered vibration signal y/t) such that, in each operating cycle of the servomotor, they correspond to angular displacements of the balls-cage assembly with respect to the inner ring and, respectively, to the outer ring, each of which is equal to a multiple integer of the angular gap between two adjacent rolling elements of the bearing.
- the aforementioned signal processing is accomplished by "cutting & pasting" the time-sampled position signal x(t) and the filtered vibration signal y/t) to remove (cut away) those portions thereof which allow the aforementioned result to be achieved.
- Figures 4 to 6 and in Figures 7 to 9 show the former three relate to a search for a fault in the outer ring, while the last three relate to a search for a fault in the inner ring.
- Figures 4 and 7 show the time- sampled position signals x(t), the filtered vibration signals y/t) and those parts thereof, bounded by gray-colored rectangles, to be cut away therefrom
- Figures 5 and 8 show the processed position and vibration signals x (t) and y (t), which are obtained by pasting one after the other (merging together) the remaining portions of the corresponding time-sampled position signal x(t) and the filtered vibration signal y/t) .
- the portions of the time-sampled position signal x(t) and of the filtered vibration signal y/t) that are to be cut away therefrom are those corresponding to both the initial and final portions of the operating cycles of the servomotor, in equal parts, in the example shown in Figure 4 those portions in the ranges 0° to 24.2° and 375.8° to 400°, so retaining those portions in the ranges 24.2° to 375.8°.
- the same computation may be made in the domain of the angular displacement of the balls-cage assembly instead of in the domain of the servomotor shaft.
- those portions in the ranges 0° to 9.3° and from 144.3° to 153.6° which, in the domain of the servomotor shaft, correspond to the previously indicated ranges 0° to 24.2° and 375.8° to 400°
- those portions in the ranges 9.3° to 144.3° which, in the domain of the servomotor shaft, correspond to the previously indicated ranges 24.2° to 375.8°
- the portions of the time-sampled position signal x(t) and of the filtered vibration signal y/t) that are to be cut away therefrom are those corresponding to both the initial and final portions of the operating cycles of the servomotor, in equal parts, in the example shown in Figure 7 those portions in the ranges 0° to 17.4° and 382.6° to 400°, so retaining those portions in the ranges 17.4° to 382.6°.
- the same computation may be made in the domain of the angular displacement of the balls-cage assembly instead of in the domain of the servomotor shaft.
- those portions in the ranges 0° to 10.7° and from 235.7° to 246.4° which, in the domain of the servomotor shaft, correspond to the previously indicated ranges 0° to 17.4° and 382.6° to 400°
- those portions in the ranges 10.7° to 235.7° which, in the domain of the servomotor shaft, correspond to the previously indicated ranges 17.4° to 382.6°
- the angular gap between two adjacent rolling elements of the bearing depends on the type and geometry of the rolling bearing, and hence that the aforementioned signal processing depends, in addition to which bearing component is to be tested for faults (inner ring or outer ring), also on the geometrical parameters of the bearing.
- the time-sampled position signal x(t) and the filtered vibration signal y/t) are processed such that they correspond to an integer number of complete rotations (360°) of the inner ring with respect to the outer ring, namely such that they look like as if they were generated by an inner ring that continuously rotates in the same direction, namely without any inversion of the rotation direction, with respect to the outer ring, and during which it performs an integer number of complete rotations with respect to the outer ring.
- the higher the number of complete rotations the richer the information based on which the vibration analysis will be performed.
- this task is accomplished by carrying out a "cut & paste" operation on the time-sampled position signal x(t) and the filtered vibration signal y/t) similar to that previously descried with reference to the first embodiment of the present invention.
- portions of the time-sampled position signal x(t) and of the filtered vibration signal y/t) corresponding to the initial portions of the original operating cycles namely the portions in the ranges 0° to 40°
- those portions of the time-sampled position signal x(t) and of the filtered vibration signal y/t) corresponding to both the initial and final portions of the original operating cycles conveniently in equal parts, for example those portions in the ranges 0° to 20° and 380° to 400°, so resulting in the retained portions of the time-sampled position signal x(t) and of the filtered vibration signal y/t) being centered in the respective operating cycles.
- rolling bearings that are structurally different from, but operatively equivalent to the one previously described, in particulars to rolling bearings wherein the rolling bodies are retained and evenly angularly spaced apart by retaining means other than the cage described above, or rolling bearings without either an inner or an outer ring, namely wherein the rolling bodies directly rest on, and are radially retained by either an inner or, respectively, an outer rotating member, which, hence, plays the role of the corresponding missing ring.
- the fourth step of the MCOT is space sampling, in particular constant-space sampling, the processed position and vibration signals x (t) and y (t), such that they are respectively transformed to space-sampled position and vibration signals x (t) and y (t) under a non-linear re-sampling law, defined as a mapping F: 9l"x9l"x9l — >
- ⁇ x represents the spatial sampling period, which is related to the minimum physical size of the fault that can be detected by the algorithm, and is in the order of magnitude of tenths or hundredths of degrees.
- mapping F is:
- mapping F it is thus possible to generate a space-sampled vibration signal y (t) where the frequency signature of a given typology of fault can be found (provided that the other previously mentioned assumptions hold).
- the damage frequency// based on (1) which computation requires the preliminary computation of the rotation frequency/- of the servomotor shaft (or, alternatively, of the inner ring with respect to the outer ring).
- the absolute value of the (constant) slope of the space-sampled position signal x (t) is the rotation frequency / sought, which also corresponds to the mean of the absolute value of the rotation speed in the acquisition period.
- the space-sampled position signal x (t) has a triangular time development whose slope is constant in modulus but different in sign.
- the fifth step of the MCOT (block 500) is reversing, i.e., overturning (turning upside down), those portions of the space-sampled position and vibration signals x (t) and y (t) corresponding to either of the two groups of rising and falling ramps in the space-sampled position signal x (t).
- the profile of the space-sampled position signal x (t) changes from a triangular one to a saw-toothed one, whose slope is constant both in modulus and in sign over the entire acquisition period, so ensuring a rotation frequency/- with a constant sign over the entire acquisition period.
- the sixth and last step of the MCOT (block 600) is computing the rotation frequency f r and then the damage frequency f ⁇ j based on the reversed position signal, computing the frequency spectrum of the reversed vibration signal by Fast Fourier Transforming the latter, and then by searching for peaks in the frequency spectrum of the reversed vibration signal that are separated in frequency by an amount equal to the damage frequency fd, as in the classical vibration analysis.
- Figures 15 and 16 show two frequency spectra of a reversed vibration signal obtained by implementing twice the MCOT according to the first embodiment of the present invention to test a rolling bearing for a fault in the inner ring and, respectively, in the outer ring.
- the frequency signature (damage frequency fd and the corresponding first higher harmonic thereof) relating to an inner ring fault is depicted by squares in Figure 15, while the frequency signature relating to an outer ring fault is depicted by circles in Figure 16.
- the damage frequency relating to an inner ring fault is at a value where the envelope of the frequency spectrum has a relative maximum, so being indicative of a fault in the inner ring
- the damage frequency relating to an outer ring fault is present at a value where the envelope of the frequency spectrum has a relative minimum, so being indicative of no fault in the outer ring.
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- Measurement Of Mechanical Vibrations Or Ultrasonic Waves (AREA)
Abstract
Description
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Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US13/201,336 US9182316B2 (en) | 2009-03-05 | 2010-03-05 | Predictive rolling bearing maintenance |
| JP2011552462A JP5690285B2 (en) | 2009-03-05 | 2010-03-05 | Predictive maintenance of rolling bearings |
| MX2011008675A MX2011008675A (en) | 2009-03-05 | 2010-03-05 | Predictive rolling bearing maintenance. |
| CN201080010966.3A CN102341687B (en) | 2009-03-05 | 2010-03-05 | predictive rolling bearing maintenance |
| BRPI1007871-1A BRPI1007871B1 (en) | 2009-03-05 | 2010-03-05 | METHOD FOR PREVENTING A FAILURE IN A BEARING BEARING, AND, COMPUTER-READABLE STORAGE MEDIA |
| RU2011140327/28A RU2534562C2 (en) | 2009-03-05 | 2010-03-05 | Proactive maintenance of roller bearings |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP09154474.2A EP2226621B1 (en) | 2009-03-05 | 2009-03-05 | Predictive rolling bearing maintenance |
| EP09154474.2 | 2009-03-05 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| WO2010100253A1 true WO2010100253A1 (en) | 2010-09-10 |
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ID=40929578
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/EP2010/052818 Ceased WO2010100253A1 (en) | 2009-03-05 | 2010-03-05 | Predictive rolling bearing maintenance |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US9182316B2 (en) |
| EP (1) | EP2226621B1 (en) |
| JP (1) | JP5690285B2 (en) |
| CN (1) | CN102341687B (en) |
| BR (1) | BRPI1007871B1 (en) |
| ES (1) | ES2775976T3 (en) |
| MX (1) | MX2011008675A (en) |
| RU (1) | RU2534562C2 (en) |
| WO (1) | WO2010100253A1 (en) |
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Also Published As
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| JP2012519837A (en) | 2012-08-30 |
| ES2775976T3 (en) | 2020-07-28 |
| CN102341687B (en) | 2014-10-22 |
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| MX2011008675A (en) | 2011-09-08 |
| JP5690285B2 (en) | 2015-03-25 |
| US20110301873A1 (en) | 2011-12-08 |
| CN102341687A (en) | 2012-02-01 |
| BRPI1007871A2 (en) | 2016-02-23 |
| RU2011140327A (en) | 2013-04-10 |
| BRPI1007871B1 (en) | 2020-01-07 |
| US9182316B2 (en) | 2015-11-10 |
| EP2226621A1 (en) | 2010-09-08 |
| EP2226621B1 (en) | 2020-01-01 |
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