WO2009099008A1 - Method of preserving cut flower, kit for preserving cut flower, method of producing processed cut flower and processed cut flower - Google Patents

Method of preserving cut flower, kit for preserving cut flower, method of producing processed cut flower and processed cut flower Download PDF

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Publication number
WO2009099008A1
WO2009099008A1 PCT/JP2009/051572 JP2009051572W WO2009099008A1 WO 2009099008 A1 WO2009099008 A1 WO 2009099008A1 JP 2009051572 W JP2009051572 W JP 2009051572W WO 2009099008 A1 WO2009099008 A1 WO 2009099008A1
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Prior art keywords
organic solvent
hydrophilic organic
cut
cut flower
cut flowers
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PCT/JP2009/051572
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French (fr)
Japanese (ja)
Inventor
Yasunori Yomo
Mami Furukawa
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Suntory Flowers Limited
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Application filed by Suntory Flowers Limited filed Critical Suntory Flowers Limited
Priority to JP2009552455A priority Critical patent/JPWO2009099008A1/en
Publication of WO2009099008A1 publication Critical patent/WO2009099008A1/en

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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N3/00Preservation of plants or parts thereof, e.g. inhibiting evaporation, improvement of the appearance of leaves or protection against physical influences such as UV radiation using chemical compositions; Grafting wax

Definitions

  • the present invention relates to a method for preserving cut flowers that improves the longevity of the cut flowers by replacing the tissue water in the cut flowers with a preservative solution, and a method for producing processed cut flowers with a long shelf life.
  • preserved flowers are the ones that replace the moisture in the tissues (hereinafter referred to as tissue fluids) with cut stocks such as roses and carnations, and are more similar to fresh flowers than dried flowers (shape, texture, As a unique floral material, it is often used for wedding bouquets, ordinary household entrances, and living room arrangements.
  • tissue fluids tissue fluids
  • cut stocks such as roses and carnations
  • Patent Document 1 has a problem that the flower is severely deteriorated under high temperature and high humidity, and the color of the petal changes to white or becomes partially transparent. .
  • the step of replacing the hydrophilic organic solvent substituted with the tissue fluid in the cut flower with the preservation solution is not always successful. In some cases, the shape (size and shape) could not be sufficiently maintained.
  • This invention is made
  • the first characteristic means of the method for preserving cut flowers according to the present invention is a method for preserving the cut flowers by replacing the tissue fluid in the cut flowers with the preservative solution, and the following steps are as follows: 1. a first replacing step of replacing the tissue fluid in the cut flowers with a hydrophilic organic solvent;
  • the hydrophilic organic solvent substituted with the tissue fluid in the cut flowers contains a storage solution that is compatible with the hydrophilic organic solvent and is a non-volatile or hardly volatile organic solvent, and the hydrophilic organic solvent
  • a second substitution step of substituting with the mixed solution is a first replacing step of replacing the tissue fluid in the cut flowers with a hydrophilic organic solvent.
  • the second characteristic means of the method for preserving cut flowers according to the present invention is a method for preserving the cut flowers by substituting the tissue fluid in the cut flowers with the preservative solution.
  • a first replacing step of replacing the tissue fluid in the cut flowers with a hydrophilic organic solvent The hydrophilic organic solvent substituted with the tissue fluid in the cut flowers contains a storage solution that is compatible with the hydrophilic organic solvent and is a non-volatile or hardly volatile organic solvent, and the hydrophilic organic solvent 2.
  • the first mixed liquid in the cut flowers is a mixed liquid containing the hydrophilic organic solvent and the preservative liquid, and the second mixed liquid having a larger content of the preservative liquid than the first mixed liquid is replaced.
  • Including a third substitution step The first mixed liquid in the cut flowers is a mixed liquid containing the hydrophilic organic solvent and the preservative liquid, and the second mixed liquid having a larger content of the preservative liquid than the first mixed liquid is replaced.
  • the present invention relates to a second substitution step of substituting a first liquid mixture containing a preservation solution that is a non-volatile or hardly volatile organic solvent having affinity with a hydrophilic organic solvent, and a hydrophilic organic solvent, and
  • the first mixed liquid in the cut flowers is a mixed liquid containing the hydrophilic organic solvent and the preservative liquid, and the second mixed liquid having a larger content of the preservative liquid than the first mixed liquid is replaced.
  • Including a third substitution step That is, the present invention is capable of carrying out a plurality of substitution steps step by step while increasing the content of the preservation solution in the mixed solution to be used.
  • the shape of the cut flower is easily maintained, and it is resistant to drying, and it is possible to store the cut flower in a shape close to the original fresh flower more stably.
  • the third characteristic means of the method for preserving cut flowers according to the present invention is that the hydrophilic organic solvent contains at least one liquid selected from the group consisting of ethanol, normal propyl alcohol, and isopropyl alcohol.
  • the hydrophilic organic solvent containing at least one liquid selected from the group consisting of ethanol, normal propyl alcohol, and isopropyl alcohol is immersed in cut flowers in the hydrophilic organic solvent as shown in Example 1 described later.
  • the natural pigment contained in the cut flower is difficult to be leached and the cut flower is also difficult to contract.
  • the fourth characteristic means of the method for storing cut flowers according to the present invention is that the storage solution is polypropylene glycol.
  • the mixed solution containing polypropylene glycol can store cut flowers in a form (shape, texture, flower color, etc.) close to the original fresh flowers for a long period of time.
  • the mixed solution is difficult to leach natural pigments (anthocyanins, etc.) contained in cut flowers, and natural pigments are easily retained in the cut flowers, so the flower color of the cut flowers is close to the original flower color or an equivalent flower color. Can be held in.
  • the fifth characteristic means of the method for preserving cut flowers according to the present invention is that the content of polypropylene glycol in the mixed solution is 1% by volume to 80% by volume.
  • the sixth characteristic means of the method for preserving cut flowers according to the present invention is that the content of polypropylene glycol in the first mixed solution is 1% to 40% by volume, and the content of polypropylene glycol in the second mixed solution Is 41 to 80% by volume.
  • the seventh characteristic means of the method for preserving cut flowers according to the present invention is that the method further comprises a step of rinsing the surface of the cut flowers with a hydrophilic organic solvent or a hydrophilic organic solvent other than the hydrophilic organic solvent.
  • Cut flowers that have undergone a replacement step with a mixed solution containing a hydrophilic organic solvent and a preservative solution may have unnatural color and texture due to the preservative solution adhering to the surface thereof. Therefore, according to the present invention, the color and texture of the cut flower can be made closer to the original fresh flower by rinsing the preservative solution adhering to the cut flower surface with a hydrophilic organic solvent and washing it away.
  • a feature of the cut flower preservation kit according to the present invention is that it can be used in the method for preserving cut flowers provided with the feature means, and includes at least the hydrophilic organic solvent and the preservation solution.
  • the first characteristic means of the method for producing a processed cut flower according to the present invention is a method for manufacturing a processed cut flower by substituting the tissue fluid in the cut flower with a preservation solution, which comprises the following steps: 1. a first replacing step of replacing the tissue fluid in the cut flowers with a hydrophilic organic solvent;
  • the hydrophilic organic solvent substituted with the tissue fluid in the cut flowers contains a storage solution that is compatible with the hydrophilic organic solvent and is a non-volatile or hardly volatile organic solvent, and the hydrophilic organic solvent
  • a second substitution step of substituting with the mixed solution is a first replacing step of replacing the tissue fluid in the cut flowers with a hydrophilic organic solvent.
  • the second characteristic means of the method for producing a processed cut flower according to the present invention is a method for manufacturing a processed cut flower by replacing the tissue fluid in the cut flower with a preservation solution, which comprises the following steps: 1. a first replacing step of replacing the tissue fluid in the cut flowers with a hydrophilic organic solvent;
  • the hydrophilic organic solvent substituted with the tissue fluid in the cut flowers contains a storage solution that is compatible with the hydrophilic organic solvent and is a non-volatile or hardly volatile organic solvent, and the hydrophilic organic solvent 2.
  • the first mixed liquid in the cut flowers is a mixed liquid containing the hydrophilic organic solvent and the preservative liquid, and the second mixed liquid having a larger content of the preservative liquid than the first mixed liquid is replaced.
  • the present invention relates to a second substitution step of substituting a first liquid mixture containing a preservation solution that is a non-volatile or hardly volatile organic solvent having affinity with a hydrophilic organic solvent, and a hydrophilic organic solvent, and
  • the first mixed liquid in the cut flowers is a mixed liquid containing the hydrophilic organic solvent and the preservative liquid, and the second mixed liquid having a larger content of the preservative liquid than the first mixed liquid is replaced.
  • Including a third substitution step That is, the present invention is capable of carrying out a plurality of substitution steps step by step while increasing the content of the preservation solution in the mixed solution to be used.
  • the shape of the cut flower is easily maintained, and it is resistant to drying, and it is possible to store the cut flower in a shape close to the original fresh flower more stably.
  • the third characteristic means of the method for producing a processed cut flower according to the present invention is that the hydrophilic organic solvent contains at least one liquid selected from the group consisting of ethanol, normal propyl alcohol, and isopropyl alcohol.
  • the hydrophilic organic solvent containing at least one liquid selected from the group consisting of ethanol, normal propyl alcohol, and isopropyl alcohol is immersed in cut flowers in the hydrophilic organic solvent as shown in Example 1 described later.
  • the natural pigment contained in the cut flower is difficult to be leached and the cut flower is also difficult to contract.
  • the fourth characteristic means of the method for producing a processed cut flower according to the present invention is that the preservation solution is polypropylene glycol.
  • the mixed solution containing polypropylene glycol can store cut flowers in a form (shape, texture, flower color, etc.) close to the original fresh flowers for a long period of time.
  • the mixed solution is difficult to leach natural pigments (anthocyanins, etc.) contained in cut flowers, and natural pigments are easily retained in the cut flowers, so the flower color of the cut flowers is close to the original flower color or an equivalent flower color. Can be held in.
  • the fifth characteristic means of the method for producing a processed cut flower according to the present invention is that the content of polypropylene glycol in the mixed solution is 1% by volume to 80% by volume.
  • the content of polypropylene glycol in the first mixed solution is 1% by volume to 40% by volume
  • the content of polypropylene glycol in the second mixed solution is The amount is from 41% to 80% by volume.
  • the seventh characteristic means of the method for producing a processed cut flower according to the present invention is that it further includes a step of rinsing the surface of the cut flower with a hydrophilic organic solvent or a hydrophilic organic solvent other than the hydrophilic organic solvent.
  • Cut flowers that have undergone a replacement step with a mixed solution containing a hydrophilic organic solvent and a preservative solution may have unnatural color and texture due to the preservative solution adhering to the surface thereof. Therefore, according to the present invention, the color and texture of the cut flower can be made closer to the original fresh flower by rinsing the preservative solution adhering to the cut flower surface with a hydrophilic organic solvent and washing it away.
  • the characteristic configuration of the processed cut flower according to the present invention is that it is manufactured by a method for manufacturing a processed cut flower provided with the characteristic means.
  • the processed cut flower of the present invention can maintain a shape close to the original fresh flower over a long period of time.
  • Cut flowers Examples of cut flowers to which the present invention can be applied include Vietnamese Kyocera (Symphony Marine, King of Blue Picot, Picco Rosa Pink Picot, Diamond Peach, Eucosa White, Rosina Pink), Delphinium (Aurora Blue Imp, Triton Light Blue), etc. However, it is not limited to these.
  • tissue fluid in the present invention means a fluid (mainly moisture) present in cut flower tissue.
  • the processed cut flowers in the present invention are those obtained by performing at least a first replacement step and a second replacement step, which will be described later, on the aforementioned cut flowers, and further performing a washing step and a drying step as necessary.
  • the water held by the fresh flower is substantially replaced by the preservation solution, and the preservation is improved as compared with the fresh flower.
  • the hydrophilic organic solvent in the present invention means an organic solvent having at least an affinity for water and a property that it can be replaced with a cut tissue fluid.
  • a hydrophilic organic solvent the natural pigment contained in the cut flower is hardly leached, and the cut flower is not easily contracted when the cut flower is immersed in the first substitution step described later.
  • a hydrophilic organic solvent having a partition coefficient logP (parameter indicating the hydrophilicity / hydrophobicity of a molecule) in the vicinity of ⁇ 0.271 to 0.344 and low viscosity is preferable.
  • hydrophilic organic solvent applicable to the present invention examples include those containing at least one liquid selected from the group consisting of ethanol, normal propyl alcohol, and isopropyl alcohol. That is, as the hydrophilic organic solvent in the present invention, any one of the above-mentioned ethanol, normal propyl alcohol, and isopropyl alcohol may be selected and used, or these alcohols may be used as necessary. A plurality of alcohols may be arbitrarily selected and mixed, and the mixture may be used. In particular, when the cut flower is a white flower, in order to maintain a better flower color, a product obtained by adding a certain amount of methanol to the alcohols or a mixture thereof may be used.
  • the preservation solution in the present invention means at least an organic solvent that has affinity with the hydrophilic organic solvent and is non-volatile or hardly volatile.
  • an organic solvent having a property that it is difficult to leach out a natural pigment contained in cut flowers is preferable.
  • it is non-volatile has a partition coefficient logP (parameter indicating the hydrophilicity / hydrophobicity of the molecule) of around ⁇ 0.236 to 2.8266, and a liquid storage solution at room temperature can improve the storage stability of the petal shape. It is preferable because it is excellent.
  • Examples of the preservation solution that can be applied to the present invention include polypropylene glycol, but are not limited thereto.
  • Embodiments of the present invention (a method for storing cut flowers and a method for producing processed cut flowers) will be described below.
  • This embodiment includes the following (1) first substitution step and (2) second substitution step, and (3) a washing step and (4) a drying step are performed as necessary. May be.
  • (1) First substitution step First, the prepared cut flowers are immersed in the above-mentioned hydrophilic organic solvent for a predetermined time (for example, about 4 to 24 hours), so that the tissue fluid in the cut flower tissue is hydrophilic. Replace with organic solvent.
  • the content of polypropylene glycol in the mixed solution is preferably 1% by volume to 80% by volume.
  • washing step After the second replacement step, the surface of the cut flower is lightly rinsed with a washing solution described later to wash away the preservative solution adhering to the surface.
  • This washing step is effective in removing the non-volatile organic solvent adhering to the surface of the cut flower in the second substitution step, particularly when a non-volatile organic solvent is used as the preservation solution.
  • cleaning liquid that can be used in the present invention, any solvent can be used as long as it can wash off the preservative liquid adhering to the cut flower surface with a solvent other than water. Examples of such cleaning liquid include, but are not limited to, the aforementioned hydrophilic organic solvents.
  • the hydrophilic organic solvent used as the cleaning liquid is not limited to the hydrophilic organic solvent used in the first substitution step, and other hydrophilic organic solvents other than the hydrophilic organic solvent are used as necessary. Also good.
  • the drying method is a temperature / humidity condition (for example, a room temperature of 35 ° C. and a humidity of 70) that does not affect the shape of the cut flowers (processed cut flowers) that have undergone the above-described processing steps, such as standing, air drying, and warm air blowing. % Or less) is desirable.
  • the drying time can be arbitrarily set from several minutes to several weeks.
  • the shape of a cut flower is easy to be maintained, and a cut flower can be preserve
  • the specific gravity difference between the mixed liquid of the hydrophilic organic solvent and the preservation liquid and the hydrophilic organic solvent is smaller than the specific gravity difference between the preservation liquid and the hydrophilic organic solvent. This is probably because the replacement of the mixed solution and the hydrophilic organic solvent is performed more quickly than the replacement of the above.
  • the present embodiment includes the following (1) first substitution step, (2) second substitution step, and (3) third substitution step, and (3) a washing step and (4) as necessary. ) You may make it implement a drying process.
  • (1) First substitution step First, the prepared cut flowers are immersed in the above-mentioned hydrophilic organic solvent for a predetermined time (for example, about 4 to 24 hours), so that the tissue fluid in the cut flower tissue is hydrophilic. Replace with organic solvent.
  • the first mixed solution containing the hydrophilic organic solvent used in the first substitution step and the above-described preservative solution is added to the cut flowers dehydrated in the first substitution step.
  • the container is immersed in a container for a predetermined time (for example, about 10 to 24 hours), and the hydrophilic organic solvent in the cut flower tissue is replaced with the first mixed solution.
  • the content of polypropylene glycol in the first mixed solution is preferably 1% by volume to 80% by volume, more preferably 10% by volume to 50% by volume, and even more. Preferably, it is 20 volume% to 40 volume%.
  • the cut flower treated in the second substitution step is a mixed solution containing the hydrophilic organic solvent used in the second substitution step and the preservation solution, and the preservation solution
  • the first mixed solution in the cut flower tissue is immersed in a container containing the second mixed solution whose content is higher than that of the first mixed solution for a predetermined time (for example, about 10 to 24 hours). Replace with.
  • the content of polypropylene glycol in the second mixed solution is preferably 1% by volume to 80% by volume, more preferably 41% by volume to 80% by volume, and even more. Preferably, it is 60 volume% to 80 volume%.
  • the content of the preservation solution in the mixed solution is increased and further substitution step (fourth substitution step, second substitution step) is performed. 5 substitution step etc.) may be carried out (the content of the preservative in the first mixture used in the second substitution step ⁇ the content of the preservative in the second mixture used in the third substitution step) Content ⁇ Content of preservation solution in third mixed solution used in fourth substitution step ⁇ ).
  • washing solution As the cleaning liquid that can be used in the present invention, any solvent can be used as long as it can wash off the preservative liquid adhering to the cut flower surface with a solvent other than water. Examples of such cleaning liquid include, but are not limited to, the aforementioned hydrophilic organic solvents. Moreover, the hydrophilic organic solvent used as the cleaning liquid is not limited to the hydrophilic organic solvent used in the first substitution step, and other hydrophilic organic solvents other than the hydrophilic organic solvent are used as necessary. Also good.
  • the drying method is a temperature / humidity condition (for example, a room temperature of 35 ° C. and a humidity of 70) that does not affect the shape of the cut flowers (processed cut flowers) that have undergone the above-described processing steps, such as standing, air drying, and warm air blowing. % Or less) is desirable.
  • the drying time can be arbitrarily set from several minutes to several weeks.
  • the shape of the cut flower is easily maintained, and it is resistant to drying, and the cut flower can be stored more stably in a shape close to the original fresh flower. .
  • the specific gravity difference between the mixed liquid of the hydrophilic organic solvent and the preservation liquid and the hydrophilic organic solvent is smaller than the specific gravity difference between the preservation liquid and the hydrophilic organic solvent.
  • the present invention is not limited to the above-described embodiment, and if necessary, a step of re-dying cut flowers by adding an artificial dye to the preservation solution may be added.
  • the present invention may be carried out by using a cut flower preservation kit (at least in a suitable container) comprising at least a hydrophilic organic solvent and a preservation solution.
  • Example 1 Examination of hydrophilic organic solvent applicable to the present invention As a cut flower, diamond peach of Turkish Falcon and aurora blue imp of delphinium were used, and various hydrophilic organic solvents shown in Table 1 below were used. After 4 hours of immersion (first substitution step), the dehydrated state, petal hardness, stem hardness, petal thickness, and color change were compared with fresh flowers. (Results and discussion) Preservation of the dye was observed in all the hydrophilic organic solvents shown in Table 1 below. In Example 2 and Example 3 described later, the third mixed ethanol (ethanol 85.5% by volume, normal propyl alcohol 9.6% by volume, isopropyl alcohol 4.9% by volume) was used. .
  • Example 2 Example of the first embodiment From the result of the comparative example, the second substitution step is not performed only with polypropylene glycol, but the specific gravity difference is obtained by mixing the third mixed ethanol and polypropylene glycol of Example 1 above. Based on the knowledge that it is effective to reduce the concentration, the state when the concentration of polypropylene glycol in the mixed liquid of the third mixed ethanol and polypropylene glycol is 30% by volume, 50% by volume, 70% by volume A comparative test was performed. As a cut flower, Turkish Kyocera's Picco Rosa Pink Picot, Minimoni Blue Picot and Rosina Blue were used to perform the first substitution step by immersing in 3rd mixed ethanol for 4 hours.
  • Cut flowers that have undergone the second substitution process using liquid mixtures 1 to 3 are more effective in improving the shape of the cut flowers than the control (conventional method using the preservation solution as it is).
  • the liquid mixture 1 polypropylene glycol concentration: 30% by volume
  • the polypropylene glycol concentration must be higher than 50% by volume to improve the storage condition after drying. I understood.
  • Example 3 Example of the second embodiment From the results shown in the above Example 2, the specific gravity difference between the hydrophilic organic solvent and the mixed solution is within 0.08, but there is no large diffusion / substitution ability. It was suggested that when the specific gravity difference was 0.1 or more, uneven diffusion from the inside of the petal to the outside of the petal was likely to occur. For this reason, it was considered that sufficient substitution proceeds without breaking the shape by setting the difference in specific gravity within 0.08 and moving the polypropylene glycol concentration of the mixed solution from 30 vol% to a thick solution stepwise. Two cut varieties of Rosina blue, Piccolosa pink picoty, and Minimoni blue picoty were used as cut flowers, and test groups 1 to 4 shown below were set.
  • Test Zone 1 In test group 1, the cut flowers were treated according to the following steps. 1. First substitution step: The cut flowers were immersed in the third mixed ethanol for 4 hours. 2. Second substitution step: The cut flowers subjected to the first substitution step were immersed in the first mixed liquid (third mixed ethanol 70% by volume, polypropylene glycol 30% by volume) for 3 hours. 3. Third substitution step: The cut flowers subjected to the second substitution step were immersed in a second mixed liquid (third mixed ethanol 50% by volume, polypropylene glycol 50% by volume) for 21 hours. 4). Washing step: The cut flowers subjected to the third replacement step were washed for 10 seconds using the third mixed ethanol. 5). Drying step: The cut flowers subjected to the washing step were dried by forcedly circulating air with a stirring fan in a drying room maintaining a room temperature of 35 ° C. and a humidity of 70% or less.
  • Test Zone 2 In test group 2, the cut flowers were treated according to the following steps. 1. First substitution step: The cut flowers were immersed in the third mixed ethanol for 4 hours. 2. Second substitution step: The cut flowers subjected to the first substitution step were immersed in the first mixed liquid (third mixed ethanol 70% by volume, polypropylene glycol 30% by volume) for 3 hours. 3. Third substitution step: The cut flowers subjected to the second substitution step were immersed in the second mixed liquid (third mixed ethanol 50% by volume, polypropylene glycol 50% by volume) for 4 hours. 4). Fourth substitution step: Cut flowers subjected to the third substitution step were immersed in a third mixed solution (30% by volume of third mixed ethanol, 70% by volume of polypropylene glycol) for 17 hours. 5).
  • Washing step The cut flowers subjected to the fourth substitution step were washed with the third mixed ethanol for 30 seconds (10 seconds was washed three times). 6). Drying step: The cut flowers subjected to the washing step were dried by forcedly circulating air with a stirring fan in a drying room maintaining a room temperature of 35 ° C. and a humidity of 70% or less.
  • Test Zone 3 In test group 3, the cut flowers were treated according to the following steps. 1. First substitution step: The cut flowers were immersed in the third mixed ethanol for 4 hours. 2. Second substitution step: The cut flowers subjected to the first substitution step were immersed in the first mixed liquid (third mixed ethanol 70% by volume, polypropylene glycol 30% by volume) for 3 hours. 3. Third substitution step: The cut flowers subjected to the second substitution step were immersed in the second mixed liquid (third mixed ethanol 50% by volume, polypropylene glycol 50% by volume) for 4 hours. 4). Fourth substitution step: Cut flowers subjected to the third substitution step were immersed in a third mixed solution (40% by volume of third mixed ethanol, 60% by volume of polypropylene glycol) for 17 hours. 5).
  • Washing step The cut flowers subjected to the fourth substitution step were washed with third mixed ethanol for 20 seconds (twice for 10 seconds). 6). Drying step: The cut flowers subjected to the washing step were dried by forcedly circulating air with a stirring fan in a drying room maintaining a room temperature of 35 ° C. and a humidity of 70% or less.
  • Test Zone 4 In test group 4, the cut flowers were treated according to the following steps. 1. First substitution step: The cut flowers were immersed in the third mixed ethanol for 4 hours. 2. Second substitution step: The cut flowers subjected to the first substitution step were immersed in the first mixed liquid (third mixed ethanol 70% by volume, polypropylene glycol 30% by volume) for 3 hours. 3. Third substitution step: The cut flowers subjected to the second substitution step were immersed in a second mixed liquid (third mixed ethanol 40% by volume, polypropylene glycol 60% by volume) for 21 hours. 4). Washing step: The cut flowers subjected to the third replacement step were washed with the third mixed ethanol for 20 seconds (twice for 10 seconds). 5). Drying step: The cut flowers subjected to the washing step were dried by forcedly circulating air with a stirring fan in a drying room maintaining a room temperature of 35 ° C. and a humidity of 70% or less.
  • (+ and ⁇ ) in Table 3 mean the magnitude of cut flower shape abnormality (minimization, curl (curving), post-drying atrophy), and the more +, the greater the degree. Large (ie, ( ⁇ ) ⁇ (+ ⁇ ) ⁇ (+) ⁇ (++) ⁇ (++++)).
  • test plots 1 to 4 cut flower dwarfing and petal curl were less than in the control plot. Only Test Zone 3 was slightly smaller than the other Test Zones. During cleaning, test group 1 was the easiest to clean, and test group 2 took three times as much cleaning time as test group 1. Test area 3 and test area 4 required more cleaning time than test area 1. The control area could not be cleaned well. As described above, in any of the test groups 1 to 4, the shape of the cut flower is easily maintained as compared to the control group (conventional method using the preservation solution as it is), and the resistance to drying is equal to or higher than that of the control group. The result was that it could have
  • the present invention is useful when storing cut flowers and manufacturing processed cut flowers, and is suitable for maintaining the shape of cut flowers stably over a long period of time.

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Abstract

A method of preserving a cut flower by substituting the tissue liquid in the cut flower by a preserving solution to thereby preserve the cut flower, which comprises the following steps: (1) a first substitution step of substituting the tissue liquid in the cut flower as described above by a hydrophilic organic solvent; and (2) a second substitution step of substituting the above-described hydrophilic organic solvent, by which the tissue liquid as described above in the cut flower as described above has been substituted, by a mixed solution containing a preserving solution, which is a non-volatile or hardly volatile organic solvent being compatible with the above-described hydrophilic organic solvent, and the hydrophilic organic solvent as described above.

Description

切花の保存方法、切花保存用キット、加工切花の製造方法及び加工切花Cut flower preservation method, cut flower preservation kit, processed cut flower production method and processed cut flower
 本発明は、切花中の組織水を保存液と置換することによってその切花の日持ちを良くする切花の保存方法、並びに日持ちの良い加工切花の製造方法に関する。 The present invention relates to a method for preserving cut flowers that improves the longevity of the cut flowers by replacing the tissue water in the cut flowers with a preservative solution, and a method for producing processed cut flowers with a long shelf life.
 近年、プリザーブドフラワーと呼ばれる加工切花が注目を集めている。プリザーブドフラワーとは、バラやカーネーション等の切花について、その組織中の水分(以下、組織液と称する)を保存液で置換したものであり、ドライフラワーに比べてより生花に近い形態(形状、質感、花色等)を残しているので、ユニークな花材として結婚式のブーケや一般家庭の玄関・居間のアレンジメント等に使われることが多くなっている。
 こうしたプリザーブドフラワーの従来の作製方法としては、例えば、以下の特許文献1や特許文献2に開示される方法が知られている。
特許第3548744号公報 特開2007-119459号公報
In recent years, processed cut flowers called preserved flowers have attracted attention. Preserved flowers are the ones that replace the moisture in the tissues (hereinafter referred to as tissue fluids) with cut stocks such as roses and carnations, and are more similar to fresh flowers than dried flowers (shape, texture, As a unique floral material, it is often used for wedding bouquets, ordinary household entrances, and living room arrangements.
As a conventional method for producing such a preserved flower, for example, methods disclosed in Patent Document 1 and Patent Document 2 below are known.
Japanese Patent No. 3548744 JP 2007-11959 A
 しかしながら、上記特許文献1に記載される方法においては、高温多湿の条件下では花の劣化が激しく、花弁の色調が白く変化したり、部分的に透明になってしまうなどの問題点があった。また、上記特許文献2に記載される方法においては、処理する切花の品種によっては、切花中の組織液と置換した親水性有機溶媒を、保存液と置換する工程が必ずしもうまくいかず、その切花の形状(大きさ、及び形)を十分に維持できない場合があった。
 本発明は、上記実情に鑑みてなされたものであって、その目的は、切花の形状をより安定して維持し得る切花の保存方法、及び加工切花の製造方法を提供することにある。
However, the method described in Patent Document 1 has a problem that the flower is severely deteriorated under high temperature and high humidity, and the color of the petal changes to white or becomes partially transparent. . In the method described in Patent Document 2, depending on the type of cut flower to be treated, the step of replacing the hydrophilic organic solvent substituted with the tissue fluid in the cut flower with the preservation solution is not always successful. In some cases, the shape (size and shape) could not be sufficiently maintained.
This invention is made | formed in view of the said situation, The objective is to provide the preservation method of the cut flower which can maintain the shape of a cut flower more stably, and the manufacturing method of a processed cut flower.
 本発明に係る切花の保存方法の第1特徴手段は、切花中の組織液を保存液と置換することによってその切花を保存する方法であって、以下の工程:1.前記切花中の組織液を親水性有機溶媒と置換する第1置換工程;2.前記切花中の前記組織液と置換した前記親水性有機溶媒を、前記親水性有機溶媒と親和性があり且つ不揮発性又は難揮発性の有機溶媒である保存液と、前記親水性有機溶媒とを含有する混合液と置換する第2置換工程;を包含する点にある。 The first characteristic means of the method for preserving cut flowers according to the present invention is a method for preserving the cut flowers by replacing the tissue fluid in the cut flowers with the preservative solution, and the following steps are as follows: 1. a first replacing step of replacing the tissue fluid in the cut flowers with a hydrophilic organic solvent; The hydrophilic organic solvent substituted with the tissue fluid in the cut flowers contains a storage solution that is compatible with the hydrophilic organic solvent and is a non-volatile or hardly volatile organic solvent, and the hydrophilic organic solvent A second substitution step of substituting with the mixed solution.
〔作用及び効果〕
 後述する実施例2に示されるように、本発明においては、親水性有機溶媒と親和性があり且つ不揮発性又は難揮発性の有機溶媒である保存液と、親水性有機溶媒とを含有する混合液を使用しており、保存液をそのまま使用する従来方法と比べると、切花の形状が維持され易く、切花を元の生花に近い形状でより安定に保存することが可能である。
[Action and effect]
As shown in Example 2 to be described later, in the present invention, a mixture containing a preservative solution that is a non-volatile or hardly volatile organic solvent that is compatible with a hydrophilic organic solvent and a hydrophilic organic solvent. Compared with the conventional method using the solution and using the preservation solution as it is, the shape of the cut flower is easily maintained, and the cut flower can be stored more stably in a shape close to the original fresh flower.
 本発明に係る切花の保存方法の第2特徴手段は、切花中の組織液を保存液と置換することによってその切花を保存する方法であって、以下の工程:1.前記切花中の組織液を親水性有機溶媒と置換する第1置換工程;2.前記切花中の前記組織液と置換した前記親水性有機溶媒を、前記親水性有機溶媒と親和性があり且つ不揮発性又は難揮発性の有機溶媒である保存液と、前記親水性有機溶媒とを含有する第1混合液と置換する第2置換工程;3.前記切花中の第1混合液を、前記親水性有機溶媒と前記保存液とを含有する混合液であって、前記保存液の含有量が前記第1混合液よりも多い第2混合液と置換する第3置換工程;を包含する点にある。 The second characteristic means of the method for preserving cut flowers according to the present invention is a method for preserving the cut flowers by substituting the tissue fluid in the cut flowers with the preservative solution. 1. a first replacing step of replacing the tissue fluid in the cut flowers with a hydrophilic organic solvent; The hydrophilic organic solvent substituted with the tissue fluid in the cut flowers contains a storage solution that is compatible with the hydrophilic organic solvent and is a non-volatile or hardly volatile organic solvent, and the hydrophilic organic solvent 2. a second substitution step of substituting with the first mixed liquid; The first mixed liquid in the cut flowers is a mixed liquid containing the hydrophilic organic solvent and the preservative liquid, and the second mixed liquid having a larger content of the preservative liquid than the first mixed liquid is replaced. Including a third substitution step.
〔作用及び効果〕
 本発明は、親水性有機溶媒と親和性があり且つ不揮発性又は難揮発性の有機溶媒である保存液と、親水性有機溶媒とを含有する第1混合液と置換する第2置換工程、並びに前記切花中の第1混合液を、前記親水性有機溶媒と前記保存液とを含有する混合液であって、前記保存液の含有量が前記第1混合液よりも多い第2混合液と置換する第3置換工程を包含する。
 即ち、本発明は、段階的に、使用する混合液中の保存液の含有量を増加させつつ、複数の置換工程を実施し得るものであり、後述する実施例3に示されるように、保存液をそのまま使用する従来方法と比べると、切花の形状が維持され易く、且つ乾燥にも強く、切花を元の生花に近い形状でより安定に保存することが可能である。
[Action and effect]
The present invention relates to a second substitution step of substituting a first liquid mixture containing a preservation solution that is a non-volatile or hardly volatile organic solvent having affinity with a hydrophilic organic solvent, and a hydrophilic organic solvent, and The first mixed liquid in the cut flowers is a mixed liquid containing the hydrophilic organic solvent and the preservative liquid, and the second mixed liquid having a larger content of the preservative liquid than the first mixed liquid is replaced. Including a third substitution step.
That is, the present invention is capable of carrying out a plurality of substitution steps step by step while increasing the content of the preservation solution in the mixed solution to be used. Compared with the conventional method using the liquid as it is, the shape of the cut flower is easily maintained, and it is resistant to drying, and it is possible to store the cut flower in a shape close to the original fresh flower more stably.
 本発明に係る切花の保存方法の第3特徴手段は、前記親水性有機溶媒が、エタノール、ノルマルプロピルアルコール、イソプロピルアルコールからなる群から選択される少なくとも1種の液体を含有する点にある。 The third characteristic means of the method for preserving cut flowers according to the present invention is that the hydrophilic organic solvent contains at least one liquid selected from the group consisting of ethanol, normal propyl alcohol, and isopropyl alcohol.
〔作用及び効果〕
 エタノール、ノルマルプロピルアルコール、イソプロピルアルコールからなる群から選択される少なくとも1種の液体を含有する親水性有機溶媒は、後述する実施例1に示されるように、当該親水性有機溶媒中に切花を浸漬した際、切花に含まれる天然色素が溶脱し難く、尚且つ切花も収縮し難い。
 尚、前記親水性有機溶媒が有するこうした性質は、本発明者らの鋭意研究によって初めて見出されたものである。
[Action and effect]
The hydrophilic organic solvent containing at least one liquid selected from the group consisting of ethanol, normal propyl alcohol, and isopropyl alcohol is immersed in cut flowers in the hydrophilic organic solvent as shown in Example 1 described later. In this case, the natural pigment contained in the cut flower is difficult to be leached and the cut flower is also difficult to contract.
These properties of the hydrophilic organic solvent have been found for the first time by the inventors' diligent research.
 本発明に係る切花の保存方法の第4特徴手段は、前記保存液が、ポリプロピレングリコールである点にある。 The fourth characteristic means of the method for storing cut flowers according to the present invention is that the storage solution is polypropylene glycol.
〔作用及び効果〕
 後述する実施例2及び実施例3に記載されるように、ポリプロピレングリコールを含む混合液は、切花を元の生花に近い形態(形状、質感、花色等)で長期間保存することが可能である。特に、当該混合液は、切花に含まれる天然色素(アントシアニン等)を溶脱し難く、天然色素がそのまま切花中に保持され易いので、切花の花色を元の花に近い花色か、又は同等の花色で保持することができる。
[Action and effect]
As described in Example 2 and Example 3 described later, the mixed solution containing polypropylene glycol can store cut flowers in a form (shape, texture, flower color, etc.) close to the original fresh flowers for a long period of time. . In particular, the mixed solution is difficult to leach natural pigments (anthocyanins, etc.) contained in cut flowers, and natural pigments are easily retained in the cut flowers, so the flower color of the cut flowers is close to the original flower color or an equivalent flower color. Can be held in.
 本発明に係る切花の保存方法の第5特徴手段は、前記混合液中のポリプロピレングリコールの含有量が1容積%~80容積%である点にある。 The fifth characteristic means of the method for preserving cut flowers according to the present invention is that the content of polypropylene glycol in the mixed solution is 1% by volume to 80% by volume.
〔作用及び効果〕
 ポリプロピレングリコール100%使用では、(1)小花及び花弁の萎縮の進行が起こり、(2)置換後の洗浄工程で洗浄不良が起きやすく、(3)ポリプロピレングリコールの吸湿力の高さから起こる形状の崩れ、(4)常に濡れたような状態となるなど、解決しなければならない問題がいくつかあるが、エタノール、イソプロピルアルコール、ノルマルプロピルアルコールなどのアルコール類との混合液で置換を行うことで、これらの問題が解決される。
[Action and effect]
When 100% polypropylene glycol is used, (1) Progression of floret and petal atrophy occurs, (2) Deterioration of washing tends to occur in the washing process after replacement, and (3) Shape caused by the high hygroscopicity of polypropylene glycol. There are some problems that need to be solved, such as collapse and (4) always wet, but by replacing with a mixture of alcohols such as ethanol, isopropyl alcohol, normal propyl alcohol, These problems are solved.
 本発明に係る切花の保存方法の第6特徴手段は、前記第1混合液中のポリプロピレングリコールの含有量が1容積%~40容積%であり、前記第2混合液中のポリプロピレングリコールの含有量が41容積%~80容積%である点にある。 The sixth characteristic means of the method for preserving cut flowers according to the present invention is that the content of polypropylene glycol in the first mixed solution is 1% to 40% by volume, and the content of polypropylene glycol in the second mixed solution Is 41 to 80% by volume.
〔作用及び効果〕
 1容積%~40容積%のポリプロピレングリコール濃度を有する第1混合液で置換した後に、41容積%~80容積%のポリプロピレングリコール濃度を有する第2混合液で再度置換することによって、花弁の萎縮が抑えられ、切花の形状をより安定に維持することができる。
[Action and effect]
Replacing with a first mixture having a polypropylene glycol concentration of 1% to 40% by volume and then replacing again with a second mixture having a polypropylene glycol concentration of 41% to 80% by volume reduces petal atrophy. It is suppressed and the shape of the cut flower can be maintained more stably.
 本発明に係る切花の保存方法の第7特徴手段は、前記親水性有機溶媒又は前記親水性有機溶媒以外の親水性有機溶媒によって前記切花の表面をすすぐ洗浄工程をさらに包含する点にある。 The seventh characteristic means of the method for preserving cut flowers according to the present invention is that the method further comprises a step of rinsing the surface of the cut flowers with a hydrophilic organic solvent or a hydrophilic organic solvent other than the hydrophilic organic solvent.
〔作用及び効果〕
 親水性有機溶媒と保存液とを含む混合液による置換工程を経た切花は、その表面に付着した保存液によって不自然な色合いや質感を有する場合がある。
 そこで、本発明によれば、切花の表面に付着した保存液を、親水性有機溶媒ですすいで洗い流すことによって、その切花の花色や質感をより元の生花に近いものとすることができる。
[Action and effect]
Cut flowers that have undergone a replacement step with a mixed solution containing a hydrophilic organic solvent and a preservative solution may have unnatural color and texture due to the preservative solution adhering to the surface thereof.
Therefore, according to the present invention, the color and texture of the cut flower can be made closer to the original fresh flower by rinsing the preservative solution adhering to the cut flower surface with a hydrophilic organic solvent and washing it away.
 本発明に係る切花保存用キットの特徴構成は、前記特徴手段を備えた切花の保存方法に使用可能であって、少なくとも、前記親水性有機溶媒と前記保存液とを備える点にある。 A feature of the cut flower preservation kit according to the present invention is that it can be used in the method for preserving cut flowers provided with the feature means, and includes at least the hydrophilic organic solvent and the preservation solution.
〔作用及び効果〕
 本発明の切花保存用キットを使用すれば、前記特徴手段を備えた切花の保存方法を簡便に実施することができる。
[Action and effect]
If the kit for preserving cut flowers of the present invention is used, the method for preserving cut flowers provided with the above characteristic means can be easily carried out.
 本発明に係る加工切花の製造方法の第1特徴手段は、切花中の組織液を保存液と置換することによって加工切花を製造する方法であって、以下の工程:1.前記切花中の組織液を親水性有機溶媒と置換する第1置換工程;2.前記切花中の前記組織液と置換した前記親水性有機溶媒を、前記親水性有機溶媒と親和性があり且つ不揮発性又は難揮発性の有機溶媒である保存液と、前記親水性有機溶媒とを含有する混合液と置換する第2置換工程;を包含する点にある。 The first characteristic means of the method for producing a processed cut flower according to the present invention is a method for manufacturing a processed cut flower by substituting the tissue fluid in the cut flower with a preservation solution, which comprises the following steps: 1. a first replacing step of replacing the tissue fluid in the cut flowers with a hydrophilic organic solvent; The hydrophilic organic solvent substituted with the tissue fluid in the cut flowers contains a storage solution that is compatible with the hydrophilic organic solvent and is a non-volatile or hardly volatile organic solvent, and the hydrophilic organic solvent A second substitution step of substituting with the mixed solution.
〔作用及び効果〕
 後述する実施例2に示されるように、本発明においては、親水性有機溶媒と親和性があり且つ不揮発性又は難揮発性の有機溶媒である保存液と、親水性有機溶媒とを含有する混合液を使用しており、保存液をそのまま使用する従来方法と比べると、切花の形状が維持され易く、切花を元の生花に近い形状でより安定に保存することが可能である。
[Action and effect]
As shown in Example 2 to be described later, in the present invention, a mixture containing a preservative solution that is a non-volatile or hardly volatile organic solvent that is compatible with a hydrophilic organic solvent and a hydrophilic organic solvent. Compared with the conventional method using the solution and using the preservation solution as it is, the shape of the cut flower is easily maintained, and the cut flower can be stored more stably in a shape close to the original fresh flower.
 本発明に係る加工切花の製造方法の第2特徴手段は、切花中の組織液を保存液と置換することによって加工切花を製造する方法であって、以下の工程:1.前記切花中の組織液を親水性有機溶媒と置換する第1置換工程;2.前記切花中の前記組織液と置換した前記親水性有機溶媒を、前記親水性有機溶媒と親和性があり且つ不揮発性又は難揮発性の有機溶媒である保存液と、前記親水性有機溶媒とを含有する第1混合液と置換する第2置換工程;3.前記切花中の第1混合液を、前記親水性有機溶媒と前記保存液とを含有する混合液であって、前記保存液の含有量が前記第1混合液よりも多い第2混合液と置換する第3置換工程;を包含する点にある。 The second characteristic means of the method for producing a processed cut flower according to the present invention is a method for manufacturing a processed cut flower by replacing the tissue fluid in the cut flower with a preservation solution, which comprises the following steps: 1. a first replacing step of replacing the tissue fluid in the cut flowers with a hydrophilic organic solvent; The hydrophilic organic solvent substituted with the tissue fluid in the cut flowers contains a storage solution that is compatible with the hydrophilic organic solvent and is a non-volatile or hardly volatile organic solvent, and the hydrophilic organic solvent 2. a second substitution step of substituting with the first mixed liquid; The first mixed liquid in the cut flowers is a mixed liquid containing the hydrophilic organic solvent and the preservative liquid, and the second mixed liquid having a larger content of the preservative liquid than the first mixed liquid is replaced. Including a third substitution step.
〔作用及び効果〕
 本発明は、親水性有機溶媒と親和性があり且つ不揮発性又は難揮発性の有機溶媒である保存液と、親水性有機溶媒とを含有する第1混合液と置換する第2置換工程、並びに前記切花中の第1混合液を、前記親水性有機溶媒と前記保存液とを含有する混合液であって、前記保存液の含有量が前記第1混合液よりも多い第2混合液と置換する第3置換工程を包含する。
 即ち、本発明は、段階的に、使用する混合液中の保存液の含有量を増加させつつ、複数の置換工程を実施し得るものであり、後述する実施例3に示されるように、保存液をそのまま使用する従来方法と比べると、切花の形状が維持され易く、且つ乾燥にも強く、切花を元の生花に近い形状でより安定に保存することが可能である。
[Action and effect]
The present invention relates to a second substitution step of substituting a first liquid mixture containing a preservation solution that is a non-volatile or hardly volatile organic solvent having affinity with a hydrophilic organic solvent, and a hydrophilic organic solvent, and The first mixed liquid in the cut flowers is a mixed liquid containing the hydrophilic organic solvent and the preservative liquid, and the second mixed liquid having a larger content of the preservative liquid than the first mixed liquid is replaced. Including a third substitution step.
That is, the present invention is capable of carrying out a plurality of substitution steps step by step while increasing the content of the preservation solution in the mixed solution to be used. Compared with the conventional method using the liquid as it is, the shape of the cut flower is easily maintained, and it is resistant to drying, and it is possible to store the cut flower in a shape close to the original fresh flower more stably.
 本発明に係る加工切花の製造方法の第3特徴手段は、前記親水性有機溶媒が、エタノール、ノルマルプロピルアルコール、イソプロピルアルコールからなる群から選択される少なくとも1種の液体を含有する点にある。 The third characteristic means of the method for producing a processed cut flower according to the present invention is that the hydrophilic organic solvent contains at least one liquid selected from the group consisting of ethanol, normal propyl alcohol, and isopropyl alcohol.
〔作用及び効果〕
 エタノール、ノルマルプロピルアルコール、イソプロピルアルコールからなる群から選択される少なくとも1種の液体を含有する親水性有機溶媒は、後述する実施例1に示されるように、当該親水性有機溶媒中に切花を浸漬した際、切花に含まれる天然色素が溶脱し難く、尚且つ切花も収縮し難い。
 尚、前記親水性有機溶媒が有するこうした性質は、本発明者らの鋭意研究によって初めて見出されたものである。
[Action and effect]
The hydrophilic organic solvent containing at least one liquid selected from the group consisting of ethanol, normal propyl alcohol, and isopropyl alcohol is immersed in cut flowers in the hydrophilic organic solvent as shown in Example 1 described later. In this case, the natural pigment contained in the cut flower is difficult to be leached and the cut flower is also difficult to contract.
These properties of the hydrophilic organic solvent have been found for the first time by the inventors' diligent research.
 本発明に係る加工切花の製造方法の第4特徴手段は、前記保存液が、ポリプロピレングリコールである点にある。 The fourth characteristic means of the method for producing a processed cut flower according to the present invention is that the preservation solution is polypropylene glycol.
〔作用及び効果〕
 後述する実施例2及び実施例3に記載されるように、ポリプロピレングリコールを含む混合液は、切花を元の生花に近い形態(形状、質感、花色等)で長期間保存することが可能である。特に、当該混合液は、切花に含まれる天然色素(アントシアニン等)を溶脱し難く、天然色素がそのまま切花中に保持され易いので、切花の花色を元の花に近い花色か、又は同等の花色で保持することができる。
[Action and effect]
As described in Example 2 and Example 3 described later, the mixed solution containing polypropylene glycol can store cut flowers in a form (shape, texture, flower color, etc.) close to the original fresh flowers for a long period of time. . In particular, the mixed solution is difficult to leach natural pigments (anthocyanins, etc.) contained in cut flowers, and natural pigments are easily retained in the cut flowers, so the flower color of the cut flowers is close to the original flower color or an equivalent flower color. Can be held in.
 本発明に係る加工切花の製造方法の第5特徴手段は、前記混合液中のポリプロピレングリコールの含有量が1容積%~80容積%であるにある。 The fifth characteristic means of the method for producing a processed cut flower according to the present invention is that the content of polypropylene glycol in the mixed solution is 1% by volume to 80% by volume.
〔作用及び効果〕
 ポリプロピレングリコール100%使用では、(1)小花及び花弁の萎縮の進行が起こり、(2)置換後の洗浄工程で洗浄不良が起きやすく、(3)ポリプロピレングリコールの吸湿力の高さから起こる形状の崩れ、(4)常に濡れたような状態となるなど、解決しなければならない問題がいくつかあるが、エタノール、イソプロピルアルコール、ノルマルプロピルアルコールなどのアルコール類との混合液で置換を行うことで、これらの問題が解決される。
[Action and effect]
When 100% polypropylene glycol is used, (1) Progression of floret and petal atrophy occurs, (2) Deterioration of washing tends to occur in the washing process after replacement, and (3) Shape caused by the high hygroscopicity of polypropylene glycol. There are some problems that need to be solved, such as collapse and (4) always wet, but by replacing with a mixture of alcohols such as ethanol, isopropyl alcohol, normal propyl alcohol, These problems are solved.
 本発明に係る加工切花の製造方法の第6特徴手段は、前記第1混合液中のポリプロピレングリコールの含有量が1容積%~40容積%であり、前記第2混合液中のポリプロピレングリコールの含有量が41容積%~80容積%である点にある。 According to a sixth feature of the method for producing a processed cut flower according to the present invention, the content of polypropylene glycol in the first mixed solution is 1% by volume to 40% by volume, and the content of polypropylene glycol in the second mixed solution is The amount is from 41% to 80% by volume.
〔作用及び効果〕
 1容積%~40容積%のポリプロピレングリコール濃度を有する第1混合液で置換した後に、41容積%~80容積%のポリプロピレングリコール濃度を有する第2混合液で再度置換することによって、花弁の萎縮が抑えられ、切花の形状をより安定に維持することができる。
[Action and effect]
Replacing with a first mixture having a polypropylene glycol concentration of 1% to 40% by volume and then replacing again with a second mixture having a polypropylene glycol concentration of 41% to 80% by volume reduces petal atrophy. It is suppressed and the shape of the cut flower can be maintained more stably.
 本発明に係る加工切花の製造方法の第7特徴手段は、前記親水性有機溶媒又は前記親水性有機溶媒以外の親水性有機溶媒によって前記切花の表面をすすぐ洗浄工程をさらに包含する点にある。 The seventh characteristic means of the method for producing a processed cut flower according to the present invention is that it further includes a step of rinsing the surface of the cut flower with a hydrophilic organic solvent or a hydrophilic organic solvent other than the hydrophilic organic solvent.
〔作用及び効果〕
 親水性有機溶媒と保存液とを含む混合液による置換工程を経た切花は、その表面に付着した保存液によって不自然な色合いや質感を有する場合がある。
 そこで、本発明によれば、切花の表面に付着した保存液を、親水性有機溶媒ですすいで洗い流すことによって、その切花の花色や質感をより元の生花に近いものとすることができる。
[Action and effect]
Cut flowers that have undergone a replacement step with a mixed solution containing a hydrophilic organic solvent and a preservative solution may have unnatural color and texture due to the preservative solution adhering to the surface thereof.
Therefore, according to the present invention, the color and texture of the cut flower can be made closer to the original fresh flower by rinsing the preservative solution adhering to the cut flower surface with a hydrophilic organic solvent and washing it away.
 本発明に係る加工切花の特徴構成は、前記特徴手段を備えた加工切花の製造方法によって製造される点にある。 The characteristic configuration of the processed cut flower according to the present invention is that it is manufactured by a method for manufacturing a processed cut flower provided with the characteristic means.
〔作用及び効果〕
 本発明の加工切花は、元の生花に近い形状が長期にわたって維持され得る。
[Action and effect]
The processed cut flower of the present invention can maintain a shape close to the original fresh flower over a long period of time.
  本発明の実施の形態を説明する前に、特許請求の範囲及び明細書にて用いられる用語について以下に説明する。 Before describing the embodiments of the present invention, terms used in the claims and specification will be described below.
 (切花)
 本発明を適用し得る切花としては、例えば、トルコキキョウ(シンフォニーマリン、キングオブブルーピコティー、ピッコローサピンクピコティ、ダイアモンドピーチ、エクローサホワイト、ロジーナピンク)、デルフィニウム(オーロラブルーインプ、トリトンライトブルー)等が挙げられるが、これらに限定されるものではない。
(Cut flowers)
Examples of cut flowers to which the present invention can be applied include Turkish Kyocera (Symphony Marine, King of Blue Picot, Picco Rosa Pink Picot, Diamond Peach, Eucosa White, Rosina Pink), Delphinium (Aurora Blue Imp, Triton Light Blue), etc. However, it is not limited to these.
 (組織液)
 本発明における組織液とは、切花組織中に存在する液体(主として、水分)を意味するものである。
(Tissue fluid)
The tissue fluid in the present invention means a fluid (mainly moisture) present in cut flower tissue.
 (加工切花)
 本発明における加工切花とは、前述の切花に対して、少なくとも後述する第1置換工程及び第2置換工程が施されたものであり、また必要に応じて更に洗浄工程や乾燥工程を施された切花の加工品をいう。本発明における加工切花は、生花が持っていた水分が実質的に保存液に置き換わっており、生花に比較して保存性が向上している。
(Processed cut flowers)
The processed cut flowers in the present invention are those obtained by performing at least a first replacement step and a second replacement step, which will be described later, on the aforementioned cut flowers, and further performing a washing step and a drying step as necessary. A processed product of cut flowers. In the processed cut flower according to the present invention, the water held by the fresh flower is substantially replaced by the preservation solution, and the preservation is improved as compared with the fresh flower.
 (親水性有機溶媒)
 本発明における親水性有機溶媒とは、少なくとも、水と親和性があり、且つ切花の組織液と置換可能であるという性質を有する有機溶媒を意味する。尚、そのような親水性有機溶媒としては、さらに切花中に含まれる天然色素を溶脱し難く、尚且つ後述する第1置換工程で切花を浸漬する際の切花の収縮を発生させ難い性質を有するものが好ましい。詳細には、分配係数logP(分子の親疎水性を示すパラメータ)が-0.271~0.344付近で粘性が低い親水性有機溶媒が好ましい。
(Hydrophilic organic solvent)
The hydrophilic organic solvent in the present invention means an organic solvent having at least an affinity for water and a property that it can be replaced with a cut tissue fluid. In addition, as such a hydrophilic organic solvent, the natural pigment contained in the cut flower is hardly leached, and the cut flower is not easily contracted when the cut flower is immersed in the first substitution step described later. Those are preferred. Specifically, a hydrophilic organic solvent having a partition coefficient logP (parameter indicating the hydrophilicity / hydrophobicity of a molecule) in the vicinity of −0.271 to 0.344 and low viscosity is preferable.
 本発明に適用可能な親水性有機溶媒としては、例えば、エタノール、ノルマルプロピルアルコール、イソプロピルアルコールからなる群から選択される少なくとも1種の液体を含有するものが挙げられる。即ち、本発明における親水性有機溶媒として、上述のエタノール、ノルマルプロピルアルコール、イソプロピルアルコールの中からいずれか一つを選んで使用しても良いし、あるいはこれらのアルコール類の中から必要に応じて任意に複数のアルコールを選択して混合して、その混合物を使用するようにしても良い。また特に切花が白い花の場合には、より良い花色の保持のために上記アルコール類やそれらの混合物にさらに一定量のメタノールを加えたものを用いても良い。 Examples of the hydrophilic organic solvent applicable to the present invention include those containing at least one liquid selected from the group consisting of ethanol, normal propyl alcohol, and isopropyl alcohol. That is, as the hydrophilic organic solvent in the present invention, any one of the above-mentioned ethanol, normal propyl alcohol, and isopropyl alcohol may be selected and used, or these alcohols may be used as necessary. A plurality of alcohols may be arbitrarily selected and mixed, and the mixture may be used. In particular, when the cut flower is a white flower, in order to maintain a better flower color, a product obtained by adding a certain amount of methanol to the alcohols or a mixture thereof may be used.
 (保存液)
 本発明における保存液とは、少なくとも、上記親水性有機溶媒と親和性があり、且つ不揮発性又は難揮発性の有機溶媒を意味する。尚、そのような保存液としては、さらに切花中に含まれる天然色素を溶脱し難くい性質を有する有機溶媒が好ましい。詳細には、不揮発性で、分配係数logP(分子の親疎水性を示すパラメータ)が-0.236~2.8266付近であり、尚且つ常温で液体の保存液が、花弁の形状の保存性に優れるため好ましい。
 本発明に適用し得る保存液としては、例えば、ポリプロピレングリコール等が挙げられるが、これに限定されるものではない。
(Preservation solution)
The preservation solution in the present invention means at least an organic solvent that has affinity with the hydrophilic organic solvent and is non-volatile or hardly volatile. In addition, as such a preservation solution, an organic solvent having a property that it is difficult to leach out a natural pigment contained in cut flowers is preferable. Specifically, it is non-volatile, has a partition coefficient logP (parameter indicating the hydrophilicity / hydrophobicity of the molecule) of around −0.236 to 2.8266, and a liquid storage solution at room temperature can improve the storage stability of the petal shape. It is preferable because it is excellent.
Examples of the preservation solution that can be applied to the present invention include polypropylene glycol, but are not limited thereto.
 以下に本発明(切花の保存方法及び加工切花の製造方法)の実施の形態を説明する。
〔第1実施形態〕
 本実施形態は、以下の(1)第1置換工程、及び(2)第2置換工程を包含するものであり、必要に応じて(3)洗浄工程及び(4)乾燥工程を実施するようにしても良い。
(1)第1置換工程
 先ず、用意した切花を、前述の親水性有機溶媒を入れた容器内に所定時間(例えば、4時間~24時間程度)浸漬させ、切花の組織中の組織液を親水性有機溶媒に置換する。
Embodiments of the present invention (a method for storing cut flowers and a method for producing processed cut flowers) will be described below.
[First Embodiment]
This embodiment includes the following (1) first substitution step and (2) second substitution step, and (3) a washing step and (4) a drying step are performed as necessary. May be.
(1) First substitution step First, the prepared cut flowers are immersed in the above-mentioned hydrophilic organic solvent for a predetermined time (for example, about 4 to 24 hours), so that the tissue fluid in the cut flower tissue is hydrophilic. Replace with organic solvent.
(2)第2置換工程
 次いで、上記第1置換工程にて脱水処理した切花を、上記第1置換工程で使用した親水性有機溶媒と、前述の保存液とを含有する混合液を入れた容器内に所定時間(例えば、10時間~24時間程度)浸漬させ、切花の組織中の親水性有機溶媒を混合液に置換する。
(2) Second replacement step Next, a container containing a mixed solution containing the hydrophilic organic solvent used in the first replacement step and the above-described preservative solution of the cut flowers dehydrated in the first replacement step. It is immersed in the inside for a predetermined time (for example, about 10 to 24 hours), and the hydrophilic organic solvent in the cut flower tissue is replaced with the mixed solution.
 尚、本実施形態において保存液としてポリプロピレングリコールを使用した場合、混合液中のポリプロピレングリコールの含有量は、1容積%~80容積%であることが好ましい。 In this embodiment, when polypropylene glycol is used as the preservation solution, the content of polypropylene glycol in the mixed solution is preferably 1% by volume to 80% by volume.
(3)洗浄工程
 上記第2置換工程の後、その切花の表面を、後述の洗浄液を用いて軽くすすいで、表面に付着している保存液を洗い流す。尚、この洗浄工程は、上記第2置換工程において、特に保存液として不揮発性の有機溶媒を用いた場合、切花の表面に付着しているその不揮発性有機溶媒を除去するのに有効である。
 (洗浄液)
 本発明に使用可能な洗浄液としては、水以外の溶媒で、切花表面に付着している保存液を洗い落すことが可能な溶媒であれば、任意の溶媒を使用することができる。
 そのような洗浄液としては、例えば、前述の親水性有機溶媒が挙げられるが、これらに限定されるものではない。また、洗浄液として使用する親水性有機溶媒は、上記第1置換工程にて使用した親水性有機溶媒に限らず、必要に応じて当該親水性有機溶媒以外のその他の親水性有機溶媒を使用しても良い。
(3) Washing step After the second replacement step, the surface of the cut flower is lightly rinsed with a washing solution described later to wash away the preservative solution adhering to the surface. This washing step is effective in removing the non-volatile organic solvent adhering to the surface of the cut flower in the second substitution step, particularly when a non-volatile organic solvent is used as the preservation solution.
(Cleaning solution)
As the cleaning liquid that can be used in the present invention, any solvent can be used as long as it can wash off the preservative liquid adhering to the cut flower surface with a solvent other than water.
Examples of such cleaning liquid include, but are not limited to, the aforementioned hydrophilic organic solvents. Moreover, the hydrophilic organic solvent used as the cleaning liquid is not limited to the hydrophilic organic solvent used in the first substitution step, and other hydrophilic organic solvents other than the hydrophilic organic solvent are used as necessary. Also good.
(4)乾燥工程
 最後に、上記洗浄工程にてすすぎ終えた切花を乾燥して、その表面に残存している洗浄液を除去する。尚、乾燥方法は、静置、風乾、温風の送風など、上述の各処理工程を経た切花(加工切花)の形態に影響を与えない温度・湿度条件下(例えば、室温35℃、湿度70%以下)での乾燥が望ましい。乾燥時間は、数分~数週間程度で任意に設定することができる。
(4) Drying process Finally, the cut flowers that have been rinsed in the above washing process are dried to remove the cleaning liquid remaining on the surface. The drying method is a temperature / humidity condition (for example, a room temperature of 35 ° C. and a humidity of 70) that does not affect the shape of the cut flowers (processed cut flowers) that have undergone the above-described processing steps, such as standing, air drying, and warm air blowing. % Or less) is desirable. The drying time can be arbitrarily set from several minutes to several weeks.
 本実施形態によれば、保存液をそのまま使用する従来方法と比べて、切花の形状が維持され易く、切花を元の生花に近い形状でより安定に保存することができる。
 これは、親水性有機溶媒と保存液との混合液と、親水性有機溶媒との比重差は、保存液と親水性有機溶媒との比重差よりも小さいので、保存液と親水性有機溶媒との置換よりも、混合液と親水性有機溶媒との置換の方がより速やかに実施されるためと考えられる。
According to this embodiment, compared with the conventional method using a preservation | save liquid as it is, the shape of a cut flower is easy to be maintained, and a cut flower can be preserve | saved more stably by the shape close | similar to the original fresh flower.
This is because the specific gravity difference between the mixed liquid of the hydrophilic organic solvent and the preservation liquid and the hydrophilic organic solvent is smaller than the specific gravity difference between the preservation liquid and the hydrophilic organic solvent. This is probably because the replacement of the mixed solution and the hydrophilic organic solvent is performed more quickly than the replacement of the above.
〔第2実施形態〕
 本実施形態は、以下の(1)第1置換工程、(2)第2置換工程、及び(3)第3置換工程を包含するものであり、必要に応じて(3)洗浄工程及び(4)乾燥工程を実施するようにしても良い。
[Second Embodiment]
The present embodiment includes the following (1) first substitution step, (2) second substitution step, and (3) third substitution step, and (3) a washing step and (4) as necessary. ) You may make it implement a drying process.
(1)第1置換工程
 先ず、用意した切花を、前述の親水性有機溶媒を入れた容器内に所定時間(例えば、4時間~24時間程度)浸漬させ、切花の組織中の組織液を親水性有機溶媒に置換する。
(1) First substitution step First, the prepared cut flowers are immersed in the above-mentioned hydrophilic organic solvent for a predetermined time (for example, about 4 to 24 hours), so that the tissue fluid in the cut flower tissue is hydrophilic. Replace with organic solvent.
(2)第2置換工程
 次いで、上記第1置換工程にて脱水処理した切花を、上記第1置換工程で使用した親水性有機溶媒と、前述の保存液とを含有する第1混合液を入れた容器内に所定時間(例えば、10時間~24時間程度)浸漬させ、切花の組織中の親水性有機溶媒を第1混合液に置換する。
 保存液としてポリプロピレングリコールを使用した場合、第1混合液中のポリプロピレングリコールの含有量は、好ましくは1容積%~80容積%であり、より好ましくは10容積%~50容積%であり、さらにより好ましくは、20容積%~40容積%である。
(2) Second Substitution Step Next, the first mixed solution containing the hydrophilic organic solvent used in the first substitution step and the above-described preservative solution is added to the cut flowers dehydrated in the first substitution step. The container is immersed in a container for a predetermined time (for example, about 10 to 24 hours), and the hydrophilic organic solvent in the cut flower tissue is replaced with the first mixed solution.
When polypropylene glycol is used as the preservation solution, the content of polypropylene glycol in the first mixed solution is preferably 1% by volume to 80% by volume, more preferably 10% by volume to 50% by volume, and even more. Preferably, it is 20 volume% to 40 volume%.
(3)第3置換工程
 次いで、上記第2置換工程にて処理した切花を、上記第2置換工程で使用した親水性有機溶媒と保存液とを含有する混合液であって、その保存液の含有量が上記第1混合液よりも多い第2混合液を入れた容器内に所定時間(例えば、10時間~24時間程度)浸漬させ、切花の組織中の第1混合液を第2混合液に置換する。
 保存液としてポリプロピレングリコールを使用した場合、第2混合液中のポリプロピレングリコールの含有量は、好ましくは1容積%~80容積%であり、より好ましくは41容積%~80容積%であり、さらにより好ましくは、60容積%~80容積%である。
(3) Third substitution step Next, the cut flower treated in the second substitution step is a mixed solution containing the hydrophilic organic solvent used in the second substitution step and the preservation solution, and the preservation solution The first mixed solution in the cut flower tissue is immersed in a container containing the second mixed solution whose content is higher than that of the first mixed solution for a predetermined time (for example, about 10 to 24 hours). Replace with.
When polypropylene glycol is used as the preservation solution, the content of polypropylene glycol in the second mixed solution is preferably 1% by volume to 80% by volume, more preferably 41% by volume to 80% by volume, and even more. Preferably, it is 60 volume% to 80 volume%.
 尚、本実施形態においては、必要に応じて、上記第2置換工程及び第3置換工程の後に、混合液中の保存液の含有量を増加させつつ、さらなる置換工程(第4置換工程、第5置換工程等・・・)を実施しても良い(第2置換工程で使用する第1混合液中の保存液の含有量<第3置換工程で使用する第2混合液中の保存液の含有量<第4置換工程で使用する第3混合液中の保存液の含有量<・・・)。 In the present embodiment, if necessary, after the second substitution step and the third substitution step, the content of the preservation solution in the mixed solution is increased and further substitution step (fourth substitution step, second substitution step) is performed. 5 substitution step etc.) may be carried out (the content of the preservative in the first mixture used in the second substitution step <the content of the preservative in the second mixture used in the third substitution step) Content <Content of preservation solution in third mixed solution used in fourth substitution step <...).
(4)洗浄工程
 上記第3置換工程の後、その切花の表面を、後述の洗浄液を用いて軽くすすいで、表面に付着している保存液を洗い流す。尚、この洗浄工程は、上記第2置換工程及び第3置換工程において、特に保存液として不揮発性の有機溶媒を用いた場合、切花の表面に付着しているその不揮発性有機溶媒を除去するのに有効である。
 (洗浄液)
 本発明に使用可能な洗浄液としては、水以外の溶媒で、切花表面に付着している保存液を洗い落すことが可能な溶媒であれば、任意の溶媒を使用することができる。
 そのような洗浄液としては、例えば、前述の親水性有機溶媒が挙げられるが、これらに限定されるものではない。また、洗浄液として使用する親水性有機溶媒は、上記第1置換工程にて使用した親水性有機溶媒に限らず、必要に応じて当該親水性有機溶媒以外のその他の親水性有機溶媒を使用しても良い。
(4) Washing step After the third replacement step, the surface of the cut flower is lightly rinsed with a washing solution described later to wash away the preservative solution adhering to the surface. In addition, this washing process removes the non-volatile organic solvent adhering to the cut flower surface in the second substitution process and the third substitution process, particularly when a non-volatile organic solvent is used as a preservation solution. It is effective for.
(Cleaning solution)
As the cleaning liquid that can be used in the present invention, any solvent can be used as long as it can wash off the preservative liquid adhering to the cut flower surface with a solvent other than water.
Examples of such cleaning liquid include, but are not limited to, the aforementioned hydrophilic organic solvents. Moreover, the hydrophilic organic solvent used as the cleaning liquid is not limited to the hydrophilic organic solvent used in the first substitution step, and other hydrophilic organic solvents other than the hydrophilic organic solvent are used as necessary. Also good.
(5)乾燥工程
 最後に、上記洗浄工程にてすすぎ終えた切花を乾燥して、その表面に残存している洗浄液を除去する。尚、乾燥方法は、静置、風乾、温風の送風など、上述の各処理工程を経た切花(加工切花)の形態に影響を与えない温度・湿度条件下(例えば、室温35℃、湿度70%以下)での乾燥が望ましい。乾燥時間は、数分~数週間程度で任意に設定することができる。
(5) Drying process Finally, the cut flowers that have been rinsed in the above washing process are dried to remove the cleaning liquid remaining on the surface. The drying method is a temperature / humidity condition (for example, a room temperature of 35 ° C. and a humidity of 70) that does not affect the shape of the cut flowers (processed cut flowers) that have undergone the above-described processing steps, such as standing, air drying, and warm air blowing. % Or less) is desirable. The drying time can be arbitrarily set from several minutes to several weeks.
 本実施形態によれば、保存液をそのまま使用する従来方法と比べて、切花の形状が維持され易く、且つ乾燥にも強く、切花を元の生花に近い形状でより安定に保存することができる。
 これは、親水性有機溶媒と保存液との混合液と、親水性有機溶媒との比重差は、保存液と親水性有機溶媒との比重差よりも小さいので、保存液と親水性有機溶媒との置換よりも、混合液と親水性有機溶媒との置換の方がより速やかに実施されることに加えて、段階的に使用する混合液中の保存液の含有量を増加させつつ、複数の置換工程を実施することによって、従来方法と比べて、親水性有機溶媒と保存液との置換がよりスムーズに実施され得るためと考えられる。
According to this embodiment, compared with the conventional method using the preservation solution as it is, the shape of the cut flower is easily maintained, and it is resistant to drying, and the cut flower can be stored more stably in a shape close to the original fresh flower. .
This is because the specific gravity difference between the mixed liquid of the hydrophilic organic solvent and the preservation liquid and the hydrophilic organic solvent is smaller than the specific gravity difference between the preservation liquid and the hydrophilic organic solvent. In addition to the fact that the replacement of the mixed liquid and the hydrophilic organic solvent is performed more quickly than the replacement of the above, in addition to increasing the content of the storage liquid in the mixed liquid used stepwise, a plurality of By performing the substitution step, it is considered that the substitution of the hydrophilic organic solvent and the preservation solution can be carried out more smoothly than in the conventional method.
〔その他の実施形態〕
 1.本発明は上記の実施形態に限定されるものではなく、必要に応じて、保存液に人工色素を添加して切花を再染色する工程を追加しても良い。
 2.本発明は、少なくとも親水性有機溶媒と保存液とを備える(それぞれ適当な容器に入れられている)切花保存用キットを用いて実施するようにしても良い。
[Other Embodiments]
1. The present invention is not limited to the above-described embodiment, and if necessary, a step of re-dying cut flowers by adding an artificial dye to the preservation solution may be added.
2. The present invention may be carried out by using a cut flower preservation kit (at least in a suitable container) comprising at least a hydrophilic organic solvent and a preservation solution.
 以下、本発明について、実施例により具体的に説明するが、本発明はこれらに限定されるものではない。 Hereinafter, the present invention will be specifically described with reference to examples, but the present invention is not limited thereto.
〔比較例〕
 親水性有機溶媒として、エタノール、ノルマルプロピルアルコール、及びイロプロピルアルコールを混合して調製したミックスエタノール(エタノール85.5容積%、ノルマルプロピルアルコール9.6容積%、イロプロピルアルコール4.9容積%)を用いて第1置換工程を実施した後、保存液としてポリプロピレングリコール(100容積%)を用いてで第2置換工程を実施し、さらに、ミックスエタノールで洗浄して自然乾燥するという、従来のプリザーブドフラワー作製方法を、100L容器での大量生産で再現できるかを試験した。
[Comparative example]
Mixed ethanol prepared by mixing ethanol, normal propyl alcohol, and isopropyl alcohol as a hydrophilic organic solvent (ethanol 85.5 vol%, normal propyl alcohol 9.6 vol%, isopropyl alcohol 4.9 vol%) After carrying out the first substitution step using a conventional preserved solution, the second substitution step is carried out using polypropylene glycol (100% by volume) as a preservative solution, followed by washing with mixed ethanol and natural drying. It was tested whether the flower production method could be reproduced by mass production in a 100 L container.
 切花として、トルコキキョウ(シンフォニーマリン、キングオブブルーピコティー、ピッコローサピンクピコティ、ダイアモンドピーチ、エクローサホワイト、ロジーナピンク)、デルフィニウム(オーロラブルーインプ、トリトンライトブルー)を使用し、カゴバットにこれらの切花を並べ、100Lのコンテナを薬剤容器とし1コンテナ当り200輪~400輪を同時処理した。
 第1置換工程は、上記ミックスエタノールを使用し、6時間浸漬することで行った。
 第2置換工程は、上記第1置換工程と同型のコンテナを使用してポリプロピレングリコールを100L入れ、第1置換工程を施した切花をポリプロピレングリコール入りのコンテナに移して15時間浸漬させた。
 第2置換工程後に、切花を上記ミックスエタノールで数回洗浄し(洗浄工程)、室内で自然乾燥した(乾燥工程)。
As cut flowers, we use Turkish Kyoko (Symphony Marine, King of Blue Picot, Picco Rosa Pink Picot, Diamond Peach, Ecrosa White, Rosina Pink), Delphinium (Aurora Blue Imp, Triton Light Blue) and use these cut flowers on the basket. A 100 L container was used as a drug container, and 200 to 400 wheels per container were simultaneously processed.
The 1st substitution process was performed by using the above-mentioned mixed ethanol and immersing for 6 hours.
In the second substitution step, 100 L of polypropylene glycol was added using the same type of container as the first substitution step, and the cut flowers subjected to the first substitution step were transferred to a container containing polypropylene glycol and immersed for 15 hours.
After the second substitution step, the cut flowers were washed several times with the above mixed ethanol (washing step) and naturally dried indoors (drying step).
(結果及び考察)
 第2置換工程直後から、花弁内からのアルコールの浸出がはっきりと見られ、浸出が進むにつれて、花のサイズが最大40%程度縮小した。また、花弁先端がカールした。
 洗浄工程においては、花の基部部分に付いたポリプロピレングリコールを洗い流すために5分以上の時間を必要とした。しかし、花弁先端部分は、20秒程度ですでに洗浄過多となり、乾燥直後から萎縮が始まり商品にならなかった。
 これらの問題は、ポリプロピレングリコールを100容積%で使用することによって、親水性有機溶媒との比重差(親水性有機溶媒:ポリプロピレングリコール=0.8:1.004)が大きくなるために起こると予想できた。したがって、比重差を小さくする(即ち、ポリプロピレングリコールとミックスエタノールを混合して使用する)ことで回避できる可能性が高いと考えられた。
(Results and discussion)
Immediately after the second substitution step, alcohol leaching was clearly seen from within the petals, and as leaching progressed, the flower size was reduced by up to about 40%. The petal tip curled.
In the washing process, it took 5 minutes or more to wash away the polypropylene glycol attached to the flower base. However, the tip of the petal was already overwashed in about 20 seconds, and atrophy started immediately after drying and did not become a product.
These problems are expected to occur because the specific gravity difference from the hydrophilic organic solvent (hydrophilic organic solvent: polypropylene glycol = 1.004) is increased by using 100% by volume of polypropylene glycol. did it. Therefore, it was considered that there is a high possibility that this can be avoided by reducing the specific gravity difference (that is, using a mixture of polypropylene glycol and mixed ethanol).
〔実施例1〕本発明に適用可能な親水性有機溶媒の検討
 切花として、トルコキキョウのダイアモンドピーチ、及びデルフィニウムのオーロラブルーインプを使用し、以下の表1に示される種々の親水性有機溶媒中に4時間浸漬後(第1置換工程)、その脱水状態、花弁の硬さ、茎の硬さ、花弁厚、色変化を生花と比較観察した。
(結果及び考察)
 以下の表1に示す全ての親水性有機溶媒において色素の保存が見られた。
尚、後述する実施例2及び実施例3においては、第3ミックスエタノール(エタノール85.5容積%、ノルマルプロピルアルコール9.6容積%、イロプロピルアルコール4.9容積%)を使用することとした。
[Example 1] Examination of hydrophilic organic solvent applicable to the present invention As a cut flower, diamond peach of Turkish Falcon and aurora blue imp of delphinium were used, and various hydrophilic organic solvents shown in Table 1 below were used. After 4 hours of immersion (first substitution step), the dehydrated state, petal hardness, stem hardness, petal thickness, and color change were compared with fresh flowers.
(Results and discussion)
Preservation of the dye was observed in all the hydrophilic organic solvents shown in Table 1 below.
In Example 2 and Example 3 described later, the third mixed ethanol (ethanol 85.5% by volume, normal propyl alcohol 9.6% by volume, isopropyl alcohol 4.9% by volume) was used. .
Figure JPOXMLDOC01-appb-T000001
Figure JPOXMLDOC01-appb-T000001
〔実施例2〕上記第1実施形態の実施例
 上記比較例の結果から、第2置換工程をポリプロピレングリコールだけで行わず、上記実施例1の第3ミックスエタノールとポリプロピレングリコールとの混用によって比重差を小さくすることが有効ではないかとの知見を元に、第3ミックスエタノールとポリプロピレングリコールとの混合液中のポリプロピレングリコールの濃度を30容積%、50容積%、70容積%としたときの状態を比較試験した。
 切花として、トルコキキョウのピッコローサピンクピコティ、ミニモニブルーピコティー、ロジーナブルーを用い、第3ミックスエタノール中に4時間浸漬して第1置換工程を実施して、次いで、以下の表2に示される種々のポリプロピレングリコール濃度を有する混合液1~3中に15時間浸漬して第2置換工程を実施した後、洗浄・乾燥した。
 尚、コントロールとして、第2置換工程をポリプロピレングリコールだけで実施したものを用意した。結果を以下の表2に示した。尚、表2中の記号(+及び-)は、切花の形状異常(矮小化、カール(反り返り)、乾燥後萎縮)の程度の大きさを意味しており、+が多いほど、その程度が大きい(即ち、(-)<(+-)<(+)<(++)<(+++))。
[Example 2] Example of the first embodiment From the result of the comparative example, the second substitution step is not performed only with polypropylene glycol, but the specific gravity difference is obtained by mixing the third mixed ethanol and polypropylene glycol of Example 1 above. Based on the knowledge that it is effective to reduce the concentration, the state when the concentration of polypropylene glycol in the mixed liquid of the third mixed ethanol and polypropylene glycol is 30% by volume, 50% by volume, 70% by volume A comparative test was performed.
As a cut flower, Turkish Kyocera's Picco Rosa Pink Picot, Minimoni Blue Picot and Rosina Blue were used to perform the first substitution step by immersing in 3rd mixed ethanol for 4 hours. After performing the second substitution step by immersing in the mixed liquids 1 to 3 having a polypropylene glycol concentration of 15 hours for 15 hours, washing and drying were performed.
In addition, what performed the 2nd substitution process only with polypropylene glycol was prepared as control. The results are shown in Table 2 below. The symbols (+ and −) in Table 2 mean the magnitude of cut flower shape abnormalities (minimization, curl (warping), atrophy after drying), and the more +, the more Large (ie, (−) <(+ −) <(+) <(++) <(++++)).
(結果及び考察)
 混合液1(ポリプロピレングリコール濃度:30容積%)では花弁のカールも花全体の矮小化も起きなかった。しかし、乾燥後に花全体は干乾びてしまった。
 混合液2(ポリプロピレングリコール濃度:50容積%)では花弁のカールは見られたが、花のサイズの矮小化は見られなかった。しかし、乾燥後は、混合液1同様に干乾びた。
 混合液3(ポリプロピレングリコール濃度:70容積%)では、コントロールとほぼ同様に花弁のカールと花全体の矮小化が起き、コントロールと同様の仕上がりとなったが、乾燥後の花の萎縮においてはコントロールよりも幾分改善されていた。
 混合液1~3を使用して第2置換工程を施した切花においては、程度に差はあるものの、コントロール(保存液をそのまま使用する従来方法)よりも切花の形状が維持され易くなり改善効果が見受けられた。
 尚、特に、切花の形状維持には混合液1(ポリプロピレングリコール濃度:30容積%)が良く、乾燥後の保存状態を良くするためにはポリプロピレングリコール濃度が50容積%よりも多くなければならないことがわかった。
(Results and discussion)
In the mixed solution 1 (polypropylene glycol concentration: 30% by volume), neither the petal curl nor the whole flower dwarf occurred. However, after drying, the entire flower has dried up.
In the mixed solution 2 (polypropylene glycol concentration: 50% by volume), the petal curl was observed, but the flower size was not reduced. However, after drying, it was dried like the liquid mixture 1.
In mixed solution 3 (polypropylene glycol concentration: 70% by volume), the curl of the petals and the dwarf of the whole flower occurred in the same manner as in the control, and the result was the same as in the control. It was somewhat improved.
Cut flowers that have undergone the second substitution process using liquid mixtures 1 to 3 are more effective in improving the shape of the cut flowers than the control (conventional method using the preservation solution as it is). Was found.
In particular, the liquid mixture 1 (polypropylene glycol concentration: 30% by volume) is good for maintaining the shape of cut flowers, and the polypropylene glycol concentration must be higher than 50% by volume to improve the storage condition after drying. I understood.
Figure JPOXMLDOC01-appb-T000002
Figure JPOXMLDOC01-appb-T000002
〔実施例3〕上記第2実施形態の実施例
 上記実施例2に示される結果から、親水性有機溶媒と混合液との比重差が0.08以内では大きな拡散・置換能を持たないが、比重差が0.1以上となると、花弁内から花弁外への偏った拡散が起こり易いことが示唆された。
 そのため、比重差を0.08以内として、混合液のポリプロピレングリコール濃度を30容積%から段階的に濃い溶液に移すことで、形状を崩さずに十分な置換が進むと考えられた。
 切花として、トルコキキョウのロジーナブルー、ピッコローサピンクピコティ、ミニモニブルーピコティーをそれぞれ2品種ずつ用いて、以下に示す試験区1~4を設定した。
[Example 3] Example of the second embodiment From the results shown in the above Example 2, the specific gravity difference between the hydrophilic organic solvent and the mixed solution is within 0.08, but there is no large diffusion / substitution ability. It was suggested that when the specific gravity difference was 0.1 or more, uneven diffusion from the inside of the petal to the outside of the petal was likely to occur.
For this reason, it was considered that sufficient substitution proceeds without breaking the shape by setting the difference in specific gravity within 0.08 and moving the polypropylene glycol concentration of the mixed solution from 30 vol% to a thick solution stepwise.
Two cut varieties of Rosina blue, Piccolosa pink picoty, and Minimoni blue picoty were used as cut flowers, and test groups 1 to 4 shown below were set.
 (試験区1)
 試験区1では、以下の工程に従って上記切花を処理した。
 1.第1置換工程:上記切花を、第3ミックスエタノール中に4時間浸漬した。
 2.第2置換工程:前記第1置換工程を実施した切花を、第1混合液(第3ミックスエタノール70容積%、ポリプロピレングリコール30容積%)中に3時間浸漬した。
 3.第3置換工程:前記第2置換工程を実施した切花を、第2混合液(第3ミックスエタノール50容積%、ポリプロピレングリコール50容積%)中に21時間浸漬した。
 4.洗浄工程:前記第3置換工程を実施した切花を、第3ミックスエタノールを用いて10秒間洗浄した。
 5.乾燥工程:前記洗浄工程を実施した切花を、室温35℃、湿度70%以下を維持する乾燥室において、攪拌扇で空気を強制循環させて乾燥させた。
(Test Zone 1)
In test group 1, the cut flowers were treated according to the following steps.
1. First substitution step: The cut flowers were immersed in the third mixed ethanol for 4 hours.
2. Second substitution step: The cut flowers subjected to the first substitution step were immersed in the first mixed liquid (third mixed ethanol 70% by volume, polypropylene glycol 30% by volume) for 3 hours.
3. Third substitution step: The cut flowers subjected to the second substitution step were immersed in a second mixed liquid (third mixed ethanol 50% by volume, polypropylene glycol 50% by volume) for 21 hours.
4). Washing step: The cut flowers subjected to the third replacement step were washed for 10 seconds using the third mixed ethanol.
5). Drying step: The cut flowers subjected to the washing step were dried by forcedly circulating air with a stirring fan in a drying room maintaining a room temperature of 35 ° C. and a humidity of 70% or less.
 (試験区2)
 試験区2では、以下の工程に従って上記切花を処理した。
 1.第1置換工程:上記切花を、第3ミックスエタノール中に4時間浸漬した。
 2.第2置換工程:前記第1置換工程を実施した切花を、第1混合液(第3ミックスエタノール70容積%、ポリプロピレングリコール30容積%)中に3時間浸漬した。
 3.第3置換工程:前記第2置換工程を実施した切花を、第2混合液(第3ミックスエタノール50容積%、ポリプロピレングリコール50容積%)中に4時間浸漬した。
 4.第4置換工程:前記第3置換工程を実施した切花を、第3混合液(第3ミックスエタノール30容積%、ポリプロピレングリコール70容積%)中に17時間浸漬した。
 5.洗浄工程:前記第4置換工程を実施した切花を、第3ミックスエタノールを用いて30秒間(10秒間洗浄を3回)洗浄した。
 6.乾燥工程:前記洗浄工程を実施した切花を、室温35℃、湿度70%以下を維持する乾燥室において、攪拌扇で空気を強制循環させて乾燥させた。
(Test Zone 2)
In test group 2, the cut flowers were treated according to the following steps.
1. First substitution step: The cut flowers were immersed in the third mixed ethanol for 4 hours.
2. Second substitution step: The cut flowers subjected to the first substitution step were immersed in the first mixed liquid (third mixed ethanol 70% by volume, polypropylene glycol 30% by volume) for 3 hours.
3. Third substitution step: The cut flowers subjected to the second substitution step were immersed in the second mixed liquid (third mixed ethanol 50% by volume, polypropylene glycol 50% by volume) for 4 hours.
4). Fourth substitution step: Cut flowers subjected to the third substitution step were immersed in a third mixed solution (30% by volume of third mixed ethanol, 70% by volume of polypropylene glycol) for 17 hours.
5). Washing step: The cut flowers subjected to the fourth substitution step were washed with the third mixed ethanol for 30 seconds (10 seconds was washed three times).
6). Drying step: The cut flowers subjected to the washing step were dried by forcedly circulating air with a stirring fan in a drying room maintaining a room temperature of 35 ° C. and a humidity of 70% or less.
 (試験区3)
 試験区3では、以下の工程に従って上記切花を処理した。
 1.第1置換工程:上記切花を、第3ミックスエタノール中に4時間浸漬した。
 2.第2置換工程:前記第1置換工程を実施した切花を、第1混合液(第3ミックスエタノール70容積%、ポリプロピレングリコール30容積%)中に3時間浸漬した。
 3.第3置換工程:前記第2置換工程を実施した切花を、第2混合液(第3ミックスエタノール50容積%、ポリプロピレングリコール50容積%)中に4時間浸漬した。
 4.第4置換工程:前記第3置換工程を実施した切花を、第3混合液(第3ミックスエタノール40容積%、ポリプロピレングリコール60容積%)中に17時間浸漬した。
 5.洗浄工程:前記第4置換工程を実施した切花を、第3ミックスエタノールを用いて20秒間(10秒間洗浄を2回)洗浄した。
 6.乾燥工程:前記洗浄工程を実施した切花を、室温35℃、湿度70%以下を維持する乾燥室において、攪拌扇で空気を強制循環させて乾燥させた。
(Test Zone 3)
In test group 3, the cut flowers were treated according to the following steps.
1. First substitution step: The cut flowers were immersed in the third mixed ethanol for 4 hours.
2. Second substitution step: The cut flowers subjected to the first substitution step were immersed in the first mixed liquid (third mixed ethanol 70% by volume, polypropylene glycol 30% by volume) for 3 hours.
3. Third substitution step: The cut flowers subjected to the second substitution step were immersed in the second mixed liquid (third mixed ethanol 50% by volume, polypropylene glycol 50% by volume) for 4 hours.
4). Fourth substitution step: Cut flowers subjected to the third substitution step were immersed in a third mixed solution (40% by volume of third mixed ethanol, 60% by volume of polypropylene glycol) for 17 hours.
5). Washing step: The cut flowers subjected to the fourth substitution step were washed with third mixed ethanol for 20 seconds (twice for 10 seconds).
6). Drying step: The cut flowers subjected to the washing step were dried by forcedly circulating air with a stirring fan in a drying room maintaining a room temperature of 35 ° C. and a humidity of 70% or less.
 (試験区4)
 試験区4では、以下の工程に従って上記切花を処理した。
 1.第1置換工程:上記切花を、第3ミックスエタノール中に4時間浸漬した。
 2.第2置換工程:前記第1置換工程を実施した切花を、第1混合液(第3ミックスエタノール70容積%、ポリプロピレングリコール30容積%)中に3時間浸漬した。
 3.第3置換工程:前記第2置換工程を実施した切花を、第2混合液(第3ミックスエタノール40容積%、ポリプロピレングリコール60容積%)中に21時間浸漬した。
 4.洗浄工程:前記第3置換工程を実施した切花を、第3ミックスエタノールを用いて20秒間(10秒間洗浄を2回)洗浄した。
 5.乾燥工程:前記洗浄工程を実施した切花を、室温35℃、湿度70%以下を維持する乾燥室において、攪拌扇で空気を強制循環させて乾燥させた。
(Test Zone 4)
In test group 4, the cut flowers were treated according to the following steps.
1. First substitution step: The cut flowers were immersed in the third mixed ethanol for 4 hours.
2. Second substitution step: The cut flowers subjected to the first substitution step were immersed in the first mixed liquid (third mixed ethanol 70% by volume, polypropylene glycol 30% by volume) for 3 hours.
3. Third substitution step: The cut flowers subjected to the second substitution step were immersed in a second mixed liquid (third mixed ethanol 40% by volume, polypropylene glycol 60% by volume) for 21 hours.
4). Washing step: The cut flowers subjected to the third replacement step were washed with the third mixed ethanol for 20 seconds (twice for 10 seconds).
5). Drying step: The cut flowers subjected to the washing step were dried by forcedly circulating air with a stirring fan in a drying room maintaining a room temperature of 35 ° C. and a humidity of 70% or less.
 (コントロール区)
 コントロール区では、以下の工程に従って上記切花を処理した。
 1.第1置換工程:上記切花を、第3ミックスエタノール中に4時間浸漬した。
 2.第2置換工程:前記第1置換工程を実施した切花を、ポリプロピレングリコール100容積%中に15時間浸漬した。
 3.洗浄工程:前記第2置換工程を実施した切花を、第3ミックスエタノールを用いて洗浄したがうまくできなかった。
 4.乾燥工程:前記洗浄工程を実施した切花を、室温35℃、湿度70%以下を維持する乾燥室において、攪拌扇で空気を強制循環させて乾燥させた。
 結果を以下の表3に示した。尚、表3中の記号(+及び-)は、切花の形状異常(矮小化、カール(反り返り)、乾燥後萎縮)の程度の大きさを意味しており、+が多いほど、その程度が大きい(即ち、(-)<(+-)<(+)<(++)<(+++))。
(Control area)
In the control group, the cut flowers were treated according to the following steps.
1. First substitution step: The cut flowers were immersed in the third mixed ethanol for 4 hours.
2. Second substitution step: Cut flowers subjected to the first substitution step were immersed in 100% by volume of polypropylene glycol for 15 hours.
3. Washing step: The cut flower subjected to the second replacement step was washed with the third mixed ethanol, but was not successful.
4). Drying step: The cut flowers subjected to the washing step were dried by forcedly circulating air with a stirring fan in a drying room maintaining a room temperature of 35 ° C. and a humidity of 70% or less.
The results are shown in Table 3 below. The symbols (+ and −) in Table 3 mean the magnitude of cut flower shape abnormality (minimization, curl (curving), post-drying atrophy), and the more +, the greater the degree. Large (ie, (−) <(+ −) <(+) <(++) <(++++)).
(結果及び考察)
 試験区1~4までの全ての試験区で、コントロール区よりも切花の矮小化、及び花弁のカールは少なくなった。試験区3のみが、他の試験区に比べてやや矮小化が進んだ。洗浄時は、試験区1が最も洗浄が簡単で、試験区2は試験区1の3倍の洗浄時間がかかった。 試験区3と試験区4は、試験区1よりも1回洗浄時間が多く必要となった。
 コントロール区は、洗浄がうまく出来なかった。
 以上より、いずれの試験区1~4でも、コントロール区(保存液をそのまま使用する従来方法)と比べて、切花の形状が維持され易く、また、乾燥に対してもコントロール区と同等以上の強さを有し得るという結果が得られた。
(Results and discussion)
In all of the test plots 1 to 4, cut flower dwarfing and petal curl were less than in the control plot. Only Test Zone 3 was slightly smaller than the other Test Zones. During cleaning, test group 1 was the easiest to clean, and test group 2 took three times as much cleaning time as test group 1. Test area 3 and test area 4 required more cleaning time than test area 1.
The control area could not be cleaned well.
As described above, in any of the test groups 1 to 4, the shape of the cut flower is easily maintained as compared to the control group (conventional method using the preservation solution as it is), and the resistance to drying is equal to or higher than that of the control group. The result was that it could have
Figure JPOXMLDOC01-appb-T000003
Figure JPOXMLDOC01-appb-T000003
  以上説明したように、本発明は、切花の保存、及び加工切花の製造の際に有用であり、切花の形状を長期にわたって安定に維持する場合に適している。 As described above, the present invention is useful when storing cut flowers and manufacturing processed cut flowers, and is suitable for maintaining the shape of cut flowers stably over a long period of time.

Claims (16)

  1.   切花中の組織液を保存液と置換することによってその切花を保存する方法であって、以下の工程:
     1.前記切花中の組織液を親水性有機溶媒と置換する第1置換工程;
     2.前記切花中の前記組織液と置換した前記親水性有機溶媒を、前記親水性有機溶媒と親和性があり且つ不揮発性又は難揮発性の有機溶媒である保存液と、前記親水性有機溶媒とを含有する混合液と置換する第2置換工程;
    を包含する切花の保存方法。
    A method for preserving a cut flower by replacing the tissue fluid in the cut flower with a preservative solution comprising the following steps:
    1. A first replacement step of replacing the tissue fluid in the cut flowers with a hydrophilic organic solvent;
    2. The hydrophilic organic solvent substituted with the tissue fluid in the cut flowers contains a storage solution that is compatible with the hydrophilic organic solvent and is a non-volatile or hardly volatile organic solvent, and the hydrophilic organic solvent A second substituting step of substituting with the mixed liquid
    A method for preserving cut flowers.
  2.  切花中の組織液を保存液と置換することによってその切花を保存する方法であって、以下の工程:
     1.前記切花中の組織液を親水性有機溶媒と置換する第1置換工程;
     2.前記切花中の前記組織液と置換した前記親水性有機溶媒を、前記親水性有機溶媒と親和性があり且つ不揮発性又は難揮発性の有機溶媒である保存液と、前記親水性有機溶媒とを含有する第1混合液と置換する第2置換工程;
     3.前記切花中の第1混合液を、前記親水性有機溶媒と前記保存液とを含有する混合液であって、前記保存液の含有量が前記第1混合液よりも多い第2混合液と置換する第3置換工程;
    を包含する切花の保存方法。
    A method for preserving a cut flower by replacing the tissue fluid in the cut flower with a preservative solution comprising the following steps:
    1. A first replacement step of replacing the tissue fluid in the cut flowers with a hydrophilic organic solvent;
    2. The hydrophilic organic solvent substituted with the tissue fluid in the cut flowers contains a storage solution that is compatible with the hydrophilic organic solvent and is a non-volatile or hardly volatile organic solvent, and the hydrophilic organic solvent A second substituting step for substituting with the first liquid mixture;
    3. The first mixed liquid in the cut flowers is a mixed liquid containing the hydrophilic organic solvent and the preservative liquid, and the second mixed liquid having a larger content of the preservative liquid than the first mixed liquid is replaced. A third replacement step;
    A method for preserving cut flowers.
  3.  前記親水性有機溶媒が、エタノール、ノルマルプロピルアルコール、イソプロピルアルコールからなる群から選択される少なくとも1種の液体を含有する請求項1又は2に記載の切花の保存方法。 The method for preserving cut flowers according to claim 1 or 2, wherein the hydrophilic organic solvent contains at least one liquid selected from the group consisting of ethanol, normal propyl alcohol, and isopropyl alcohol.
  4.  前記保存液が、ポリプロピレングリコールである請求項1~3のいずれか1項に記載の切花の保存方法。 The method for preserving cut flowers according to any one of claims 1 to 3, wherein the preservative solution is polypropylene glycol.
  5.  前記混合液中のポリプロピレングリコールの含有量が1容積%~80容積%である請求項4に記載の切花の保存方法。 The method for preserving cut flowers according to claim 4, wherein the content of polypropylene glycol in the mixed solution is 1% by volume to 80% by volume.
  6.  前記第1混合液中のポリプロピレングリコールの含有量が1容積%~40容積%であり、前記第2混合液中のポリプロピレングリコールの含有量が41容積%~80容積%である請求項5に記載の切花の保存方法。 The content of polypropylene glycol in the first mixed solution is 1% by volume to 40% by volume, and the content of polypropylene glycol in the second mixed solution is 41% by volume to 80% by volume. To save the cut flowers.
  7.  前記親水性有機溶媒又は前記親水性有機溶媒以外の親水性有機溶媒によって前記切花の表面をすすぐ洗浄工程をさらに包含する請求項1~6のいずれか1項に記載の切花の保存方法。 The method for preserving cut flowers according to any one of claims 1 to 6, further comprising a step of rinsing the surface of the cut flowers with a hydrophilic organic solvent other than the hydrophilic organic solvent or the hydrophilic organic solvent.
  8.  請求項1~7のいずれか1項に記載される切花の保存方法に使用可能であって、少なくとも、前記親水性有機溶媒と前記保存液とを備える切花保存用キット。 A cut flower storage kit that can be used in the cut flower storage method according to any one of claims 1 to 7 and includes at least the hydrophilic organic solvent and the storage solution.
  9.  切花中の組織液を保存液と置換することによって加工切花を製造する方法であって、以下の工程:
     1.前記切花中の組織液を親水性有機溶媒と置換する第1置換工程;
     2.前記切花中の前記組織液と置換した前記親水性有機溶媒を、前記親水性有機溶媒と親和性があり且つ不揮発性又は難揮発性の有機溶媒である保存液と、前記親水性有機溶媒とを含有する混合液と置換する第2置換工程;
    を包含する加工切花の製造方法。
    A method for producing a processed cut flower by replacing the tissue fluid in a cut flower with a preservation solution comprising the following steps:
    1. A first replacement step of replacing the tissue fluid in the cut flowers with a hydrophilic organic solvent;
    2. The hydrophilic organic solvent substituted with the tissue fluid in the cut flowers contains a storage solution that is compatible with the hydrophilic organic solvent and is a non-volatile or hardly volatile organic solvent, and the hydrophilic organic solvent A second substituting step of substituting with the mixed liquid
    A method for producing a processed cut flower comprising:
  10.  切花中の組織液を保存液と置換することによって加工切花を製造する方法であって、以下の工程:
     1.前記切花中の組織液を親水性有機溶媒と置換する第1置換工程;
     2.前記切花中の前記組織液と置換した前記親水性有機溶媒を、前記親水性有機溶媒と親和性があり且つ不揮発性又は難揮発性の有機溶媒である保存液と、前記親水性有機溶媒とを含有する第1混合液と置換する第2置換工程;
     3.前記切花中の第1混合液を、前記親水性有機溶媒と前記保存液とを含有する混合液であって、前記保存液の含有量が前記第1混合液よりも多い第2混合液と置換する第3置換工程;
    を包含する加工切花の製造方法。
    A method for producing a processed cut flower by replacing the tissue fluid in a cut flower with a preservation solution comprising the following steps:
    1. A first replacement step of replacing the tissue fluid in the cut flowers with a hydrophilic organic solvent;
    2. The hydrophilic organic solvent substituted with the tissue fluid in the cut flowers contains a storage solution that is compatible with the hydrophilic organic solvent and is a non-volatile or hardly volatile organic solvent, and the hydrophilic organic solvent A second substituting step for substituting with the first liquid mixture;
    3. The first mixed liquid in the cut flowers is a mixed liquid containing the hydrophilic organic solvent and the preservative liquid, and the second mixed liquid having a larger content of the preservative liquid than the first mixed liquid is replaced. A third replacement step;
    A method for producing a processed cut flower comprising:
  11.  前記親水性有機溶媒が、エタノール、ノルマルプロピルアルコール、イソプロピルアルコールからなる群から選択される少なくとも1種の液体を含有する請求項9又は10のいずれか1項に記載の加工切花の製造方法。 The method for producing a processed cut flower according to any one of claims 9 and 10, wherein the hydrophilic organic solvent contains at least one liquid selected from the group consisting of ethanol, normal propyl alcohol, and isopropyl alcohol.
  12.  前記保存液が、ポリプロピレングリコールである請求項9~11のいずれか1項に記載の加工切花の製造方法。 The process for producing a processed cut flower according to any one of claims 9 to 11, wherein the preservation solution is polypropylene glycol.
  13.  前記混合液中のポリプロピレングリコールの含有量が1容積%~80容積%である請求項12に記載の加工切花の製造方法。 The method for producing a processed cut flower according to claim 12, wherein the content of polypropylene glycol in the mixed solution is 1% by volume to 80% by volume.
  14.  前記第1混合液中のポリプロピレングリコールの含有量が1容積%~40容積%であり、前記第2混合液中のポリプロピレングリコールの含有量が41容積%~80容積%である請求項13に記載の加工切花の製造方法。 The polypropylene glycol content in the first mixed solution is 1 to 40% by volume, and the polypropylene glycol content in the second mixed solution is 41 to 80% by volume. Method of processing cut flowers.
  15.    前記親水性有機溶媒又は前記親水性有機溶媒以外の親水性有機溶媒によって前記切花の表面をすすぐ洗浄工程をさらに包含する請求項9~14のいずれか1項に記載の加工切花の製造方法。 The method for producing a processed cut flower according to any one of claims 9 to 14, further comprising a step of rinsing the surface of the cut flower with a hydrophilic organic solvent other than the hydrophilic organic solvent or the hydrophilic organic solvent.
  16.  請求項9~15のいずれか1項に記載される加工切花の製造方法によって製造される加工切花。 A processed cut flower produced by the method for producing a processed cut flower according to any one of claims 9 to 15.
PCT/JP2009/051572 2008-02-06 2009-01-30 Method of preserving cut flower, kit for preserving cut flower, method of producing processed cut flower and processed cut flower WO2009099008A1 (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010168291A (en) * 2009-01-20 2010-08-05 Harue Sudo Method for producing preserved flower

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04290801A (en) * 1991-03-19 1992-10-15 Keiichi Honda Method for maintaining original color and shape of plant by chemical treatment
JP2004099605A (en) * 2002-08-19 2004-04-02 Yoshihisa Sakamoto Method for preserving cut flower
JP2007106707A (en) * 2005-10-14 2007-04-26 Yoshihisa Sakamoto Method for preserving cut flower
JP2007119459A (en) * 2005-09-30 2007-05-17 Suntory Ltd Method for preservation of cut flower, cut flower preservation kit, method for producing processed cut flower, and processed cut flower

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04290801A (en) * 1991-03-19 1992-10-15 Keiichi Honda Method for maintaining original color and shape of plant by chemical treatment
JP2004099605A (en) * 2002-08-19 2004-04-02 Yoshihisa Sakamoto Method for preserving cut flower
JP2007119459A (en) * 2005-09-30 2007-05-17 Suntory Ltd Method for preservation of cut flower, cut flower preservation kit, method for producing processed cut flower, and processed cut flower
JP2007106707A (en) * 2005-10-14 2007-04-26 Yoshihisa Sakamoto Method for preserving cut flower

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010168291A (en) * 2009-01-20 2010-08-05 Harue Sudo Method for producing preserved flower

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