WO2009009595A3 - Process for determining viscous, elastic, plastic, and adhesive (vepa) properties of materials using afm-based or conventional nano-indentation - Google Patents

Process for determining viscous, elastic, plastic, and adhesive (vepa) properties of materials using afm-based or conventional nano-indentation Download PDF

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Publication number
WO2009009595A3
WO2009009595A3 PCT/US2008/069530 US2008069530W WO2009009595A3 WO 2009009595 A3 WO2009009595 A3 WO 2009009595A3 US 2008069530 W US2008069530 W US 2008069530W WO 2009009595 A3 WO2009009595 A3 WO 2009009595A3
Authority
WO
WIPO (PCT)
Prior art keywords
plastic
vepa
afm
indentation
adhesive
Prior art date
Application number
PCT/US2008/069530
Other languages
French (fr)
Other versions
WO2009009595A2 (en
Inventor
Valeriy V Ginzburg
Gregory Frederick Meyers
Hamed Lakrout
Robert K Mcintyre
Original Assignee
Dow Global Technologies Inc
Valeriy V Ginzburg
Gregory Frederick Meyers
Hamed Lakrout
Robert K Mcintyre
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Global Technologies Inc, Valeriy V Ginzburg, Gregory Frederick Meyers, Hamed Lakrout, Robert K Mcintyre filed Critical Dow Global Technologies Inc
Publication of WO2009009595A2 publication Critical patent/WO2009009595A2/en
Publication of WO2009009595A3 publication Critical patent/WO2009009595A3/en

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Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00—Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/40—Investigating hardness or rebound hardness
    • G01N3/42—Investigating hardness or rebound hardness by performing impressions under a steady load by indentors, e.g. sphere, pyramid
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01Q—SCANNING-PROBE TECHNIQUES OR APPARATUS; APPLICATIONS OF SCANNING-PROBE TECHNIQUES, e.g. SCANNING PROBE MICROSCOPY [SPM]
    • G01Q60/00—Particular types of SPM [Scanning Probe Microscopy] or microscopes; Essential components thereof
    • G01Q60/24—AFM [Atomic Force Microscopy] or apparatus therefor, e.g. AFM probes
    • G01Q60/36—DC mode
    • G01Q60/366—Nanoindenters, i.e. wherein the indenting force is measured
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0058—Kind of property studied
    • G01N2203/0069—Fatigue, creep, strain-stress relations or elastic constants
    • G01N2203/0075—Strain-stress relations or elastic constants
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0058—Kind of property studied
    • G01N2203/0076—Hardness, compressibility or resistance to crushing
    • G01N2203/0078—Hardness, compressibility or resistance to crushing using indentation
    • G01N2203/0082—Indentation characteristics measured during load
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00—Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0058—Kind of property studied
    • G01N2203/0092—Visco-elasticity, solidification, curing, cross-linking degree, vulcanisation or strength properties of semi-solid materials
    • G01N2203/0094—Visco-elasticity

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  • General Physics & Mathematics (AREA)
  • General Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Radiology & Medical Imaging (AREA)
  • Engineering & Computer Science (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Nanotechnology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)

Abstract

A process is described for determining elastic modulus, plastic yield strain, and viscosity of a material, and the work of adhesion between the material and an indenter tip, using Atomic Force Microscopy-based or conventional nanoindentation. Specifically, the process includes a measurement method whereby a sequence of load-unload quasistatic indentations are performed in the vicinity of each chosen point on a sample. The loading- unloading curves are analyzed using a specific modeling algorithm to calculate multiple mechanical properties of the sample.
PCT/US2008/069530 2007-07-10 2008-07-09 Process for determining viscous, elastic, plastic, and adhesive (vepa) properties of materials using afm-based or conventional nano-indentation WO2009009595A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US94873107P 2007-07-10 2007-07-10
US60/948,731 2007-07-10

Publications (2)

Publication Number Publication Date
WO2009009595A2 WO2009009595A2 (en) 2009-01-15
WO2009009595A3 true WO2009009595A3 (en) 2009-03-12

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2008/069530 WO2009009595A2 (en) 2007-07-10 2008-07-09 Process for determining viscous, elastic, plastic, and adhesive (vepa) properties of materials using afm-based or conventional nano-indentation

Country Status (2)

Country Link
TW (1) TW200909792A (en)
WO (1) WO2009009595A2 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7352121B2 (en) 2020-06-25 2023-09-28 富士通株式会社 Material evaluation equipment, material evaluation method, and material evaluation program

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102011115519B4 (en) 2011-10-11 2014-10-02 HS - Technische Beratung Method for material testing
CN103383330B (en) * 2012-05-04 2015-08-26 宏启胜精密电子(秦皇岛)有限公司 The method for making of material cured Tachistoscope system, method of testing and welding resisting layer
RU2561788C1 (en) * 2014-06-17 2015-09-10 Федеральное государственное автономное образовательное учреждение высшего профессионального образования "Национальный исследовательский технологический университет "МИСиС" Method of determination of coefficient of viscosity of microdestruction of thin films from multicomponent amorphous and nanocrystal metal alloys (versions)
US9541575B2 (en) * 2014-11-26 2017-01-10 Tufts University Exploitation of second-order effects in atomic force microscopy
CN111735728B (en) * 2020-05-22 2023-03-31 扬州市舜意机械有限公司 Method and device for identifying mechanical property of vibration damping coating
GB2615332B (en) * 2022-02-03 2024-04-03 Plastometrex Ltd Indentation plastometry
CN114544876B (en) * 2022-02-23 2022-11-25 上海大学 Method and system for determining characteristics of viscoelastic material
CN115472248B (en) * 2022-09-23 2023-06-13 哈尔滨工业大学 Molecular dynamics simulation calculation method for nano indentation test of CuZrAl amorphous alloy

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20030080721A1 (en) * 2001-07-23 2003-05-01 Lee Hyung Yil Ball indenter utilizing fea solutions for property evaluation
US6581446B1 (en) * 1999-04-13 2003-06-24 The University Of Houston Determination of adhesion strength of HVOF coating by spherical indentation
WO2006013450A2 (en) * 2004-07-30 2006-02-09 S.M. Scienzia Machinale Srl Method and apparatus for determining mechanical features of a material with comparison to reference database

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6581446B1 (en) * 1999-04-13 2003-06-24 The University Of Houston Determination of adhesion strength of HVOF coating by spherical indentation
US20030080721A1 (en) * 2001-07-23 2003-05-01 Lee Hyung Yil Ball indenter utilizing fea solutions for property evaluation
WO2006013450A2 (en) * 2004-07-30 2006-02-09 S.M. Scienzia Machinale Srl Method and apparatus for determining mechanical features of a material with comparison to reference database

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
ANDREAS JÄGER ET AL: "Identification of viscoelastic properties by means of nanoindentation taking the real tip geometry into account", 2 May 2007, MECCANICA, KLUWER ACADEMIC PUBLISHERS, DO, PAGE(S) 293 - 306, ISSN: 1572-9648, XP019506177 *
BELIKOV, MAGONOV ET AL: "Theoretical modelling and implementation of elastic modulus measurement at the nanoscale using atomic foce microscope", JOURNAL OF PHYSICS: CONFERENCE SERIES, vol. 61, 2007, pages 1303 - 1307, XP002502966 *
FANG T-H ET AL: "Nanoindentation characteristics on polycarbonate polymer film", 1 July 2004, MICROELECTRONICS JOURNAL, MACKINTOSH PUBLICATIONS LTD. LUTON, GB, PAGE(S) 595 - 599, ISSN: 0026-2692, XP004510105 *
LIU CHIEN-KUO ET AL: "Load-displacement relations for nanoindentation of viscoelastic materials", 1 August 2006, JOURNAL OF APPLIED PHYSICS, AMERICAN INSTITUTE OF PHYSICS. NEW YORK, US, PAGE(S) 33503 - 033503, ISSN: 0021-8979, XP012089572 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7352121B2 (en) 2020-06-25 2023-09-28 富士通株式会社 Material evaluation equipment, material evaluation method, and material evaluation program

Also Published As

Publication number Publication date
TW200909792A (en) 2009-03-01
WO2009009595A2 (en) 2009-01-15

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