WO2007064285A1 - A method of discovering leakage in a heat exchanger - Google Patents

A method of discovering leakage in a heat exchanger Download PDF

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Publication number
WO2007064285A1
WO2007064285A1 PCT/SE2006/001378 SE2006001378W WO2007064285A1 WO 2007064285 A1 WO2007064285 A1 WO 2007064285A1 SE 2006001378 W SE2006001378 W SE 2006001378W WO 2007064285 A1 WO2007064285 A1 WO 2007064285A1
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WO
WIPO (PCT)
Prior art keywords
heat exchanger
pressure
section
leakage
period
Prior art date
Application number
PCT/SE2006/001378
Other languages
French (fr)
Inventor
Mats Gustafsson
Max Leufstedt
Original Assignee
Tetra Laval Holdings & Finance Sa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tetra Laval Holdings & Finance Sa filed Critical Tetra Laval Holdings & Finance Sa
Priority to US12/083,562 priority Critical patent/US7975529B2/en
Priority to DK06824508.3T priority patent/DK1957951T3/en
Priority to PL06824508T priority patent/PL1957951T3/en
Priority to AU2006321018A priority patent/AU2006321018B2/en
Priority to NZ567238A priority patent/NZ567238A/en
Priority to EP06824508.3A priority patent/EP1957951B1/en
Priority to CN2006800448026A priority patent/CN101317079B/en
Priority to JP2008543236A priority patent/JP2009517689A/en
Priority to CA2630230A priority patent/CA2630230C/en
Publication of WO2007064285A1 publication Critical patent/WO2007064285A1/en

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Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01M—TESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
    • G01M3/00—Investigating fluid-tightness of structures
    • G01M3/02—Investigating fluid-tightness of structures by using fluid or vacuum
    • G01M3/26—Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors
    • G01M3/32—Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors for containers, e.g. radiators
    • G01M3/3227—Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors for containers, e.g. radiators for radiators
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01M—TESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
    • G01M3/00—Investigating fluid-tightness of structures
    • G01M3/02—Investigating fluid-tightness of structures by using fluid or vacuum
    • G01M3/26—Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors
    • G01M3/32—Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors for containers, e.g. radiators
    • G01M3/3236—Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors for containers, e.g. radiators by monitoring the interior space of the containers
    • G01M3/3263—Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors for containers, e.g. radiators by monitoring the interior space of the containers using a differential pressure detector

Definitions

  • the present invention relates to a methocLof diseoyeringJeakage in a heat exchanger, the heat exchanger being, together with surrounding conduits, filled with water, and the method comprising the steps that, in each section of the heat exchanger, an excess pressure is applied on the one side and is closed in across the section during a period of time, while the other side in the section is at normal pressure, and that the pressure difference is monitored during the period of time.
  • heat exchangers In order to heat treat liquid products use is made of various types of heat exchangers in indirect heating.
  • the commonest types of heat exchangers are plate heat exchangers and tube heat exchangers.
  • the method according to the present invention is applicable to both types, but is preferably intended for plate heat exchangers.
  • Heat exchangers are also used to a considerable extent within the food industry, such as in dairies and in juice factories. Depending upon the temperature to which the product is heated, a pasteurised or a sterile product will be obtained.
  • a heat exchanger normally consists of different sections which all have two sides - one side for product and one side for a heating medium, such as water or other liquid at different temperature, or steam.
  • the sections may be disposed regeneratively, so that a cold product is heated up by an already heated product.
  • One object of the present invention is to realise a method which is rapid and reliable.
  • a further object of the present invention is to realise a method which may be carried out routinely, for example in connection with washing of the plant.
  • Fig. 1 shows a part of a flow diagram with a heat exchanger.
  • the drawing shows only those details and parts essential to an understanding of the present invention, and the remaining part of the plant in which the heat exchanger is included has been omitted. DESCRIPTION OF PREFERRED EMBODIMENT
  • the method according to the present invention is intended to be employed to detect leakage in a heat exchanger.
  • the method is primarily intended for a plate heat exchanger,, as shown in Fig. l ⁇ but the method may also be used for other types of heat exchangers, such as tube heat exchangers, which process liquid foods.
  • the method may be employed in connection with an existing heat exchanger without it needing to be dismounted or without the need to dismount connecting conduits.
  • the method may be used directly in conjunction with washing of the plant in which the heat exchanger is included. Directly in conjunction with the washing, the heat exchanger and connecting conduits are filled with rinsing water from the washing operation.
  • the method may be carried into effect on other occasions, for example before start up of production, but then conduits and the heat exchanger must first be filled with water.
  • the heat exchanger 1 in Fig. 1 has three sections 2, 3, 4, but the method may naturally also be employed for both more and fewer sections 2, 3, 4.
  • Each section
  • the pressure indicator 5-10 is preferably electric, but also other types of pressure indicators 5-10 may occur.
  • the pressure indicators 5-10 emit signals to the master or control unit of the plant.
  • Conventional heat exchangers 1 may perhaps need to be retrofitted with pressure indicators 5-10, but in those cases where one or more of the sections 2, 3, 4 is used regeneratively, pressure indicators 5-10 must already be in position in compliance with the legislation of certain countries.
  • shut-off valves 11, 12, 13 are also required.
  • a pump 14 which normally pumps product into the heat exchanger 1 is also used in the method.
  • the pump 14 which normally consists of a circulation pump must be frequency controlled.
  • In the first section 2 there is, on production, hot water on one side which enters into the heat exchanger 1 through the conduit 15. The water pressure in this conduit 15 is monitored using the pressure indicator 5.
  • the upstream side has a part 17 of the product conduit which is monitored using the pressure indicator 7.
  • the downstream side has another part 18 of the product conduit which is monitored using the pressure indicator 8.
  • the third section 4 there is, on production, on the one side ice water which enters into the heat exchanger 1 through the conduit 19. The water pressure in this conduit 19 is monitored using the pressure indicator 9.
  • the first step is to close the shut-off valve 12. Thereafter, the pump 14 is accelerated in order to give a pressure increase in the conduit system.
  • the pressure indicator 10 shows approx 6 bar
  • the valve 12 closes so that an excess pressure of approx. 6 bar is enclosed on the downstream side in the third section 4.
  • the pump 14 is decelerated somewhat and when the pressure indicator 8 shows approx. 5.5 bar, the shut-off valve 13 closes so that an excess pressure of approx. 5.5 bar is enclosed on the downstream side in the second section 3 of the heat exchanger 1.
  • the pump 14 is decelerated slightly further and when the pressure indicator 6 shows approx. 5 bar, the pump 14 is completely decelerated. An excess pressure of approx. 5 bar has now been enclosed on the upstream side in the first heat exchanger section 2.
  • the downstream side in the first section 2 and the upstream sides in the second and third sections 3, 4 have a normal pressure of approx. 2 bar, which can be read off with the aid of the pressure indicators 5, 7 and 9, respectively.
  • The. values, of the_pressure_ indicators. 5J-Q are registered in the. master or control unit of the plant during a given, predetermined period of time, for example
  • the entire read-off period may suitably be printed out so that there will by such means be obtained different graphs of the pressurised sides of each respective section 2, 3, 4.
  • Steps between the different sections may be larger or smaller than 0.5 bar. However, the difference must be distinguishable on a graph.
  • the excess pressure is preferably laid on the downstream side of the heat exchanger 1 and preferably on the main conduit through the heat exchanger 1, i.e. on that side where the product is led.
  • the shut-off valves 11, 12, 13 are opened, the water is empted from the conduits and heat exchanger 1 and, if no leakage is present, the heat exchanger 1 is now ready for production.
  • the present invention realises a method for discovering leakage which is rapid and reliable. Since the method is carried out on an intact heat exchanger, the method may be put into effect routinely, preferably in conjunction with washing of the plant. Given that the leakage monitoring may be carried out often and regularly, this contributes to increased product safety and reliability which is of vital importance above all in the food industry.

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  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Examining Or Testing Airtightness (AREA)

Abstract

The present invention relates to a method of discovering leakage in a heat exchanger (1). The method is carried into effect on an intact heat exchanger (1) which, together with surrounding conduits, is filled with water. The heat exchanger (1) is to have requisite pressure indicators (5-10) mounted between each section (2, 3, 4), as well as requisite shut-off valves (11, 12, 13). The method comprises the steps that, in each section (2, 3, 4) of the heat exchanger (1) an excess pressure is applied on one side and is enclosed there, while the other side is at normal pressure. The pressure is enclosed during a period of time and is monitored during this period of time.

Description

A METHOD OF DISCOVERING LEAKAGE IN A HEAT EXCHANGER
TECHNICAL FIELD
The present invention relates to a methocLof diseoyeringJeakage in a heat exchanger, the heat exchanger being, together with surrounding conduits, filled with water, and the method comprising the steps that, in each section of the heat exchanger, an excess pressure is applied on the one side and is closed in across the section during a period of time, while the other side in the section is at normal pressure, and that the pressure difference is monitored during the period of time.
BACKGROUND ART
In order to heat treat liquid products use is made of various types of heat exchangers in indirect heating. The commonest types of heat exchangers are plate heat exchangers and tube heat exchangers. The method according to the present invention is applicable to both types, but is preferably intended for plate heat exchangers. Heat exchangers are also used to a considerable extent within the food industry, such as in dairies and in juice factories. Depending upon the temperature to which the product is heated, a pasteurised or a sterile product will be obtained.
A heat exchanger normally consists of different sections which all have two sides - one side for product and one side for a heating medium, such as water or other liquid at different temperature, or steam. Alternatively, the sections may be disposed regeneratively, so that a cold product is heated up by an already heated product.
It is naturally always desirable that both of the sides in each respective section are kept separate and discrete, but within the food industry this is extremely important. Otherwise, a ready-treated product may be reinfected by a heating medium or by untreated product.
Various methods of discovering leakage in a heat exchanger have been used with the passage of time, such as saline solutions and coloured water on the one side in a section and normal water on the other side, whereafter, by conductivity measurements of alternatively ocular observations, it has been possible to discover any possible leakage. These methods take up considerable time and another of their drawbacks is that it is difficult to discover minor leakage.
A further method is described in international Patent Specification
Figure imgf000003_0001
external unit with the aid of which different pressures are applied on the different sides in a section in a heat exchanger. The unit makes for the simultaneous testing of several sections. This method is effective as regards discovering minor leakage, but it is also time-consuming and involves external service costs, for example, for a dairy.
OBJECTS OF THE INVENTION
One object of the present invention is to realise a method which is rapid and reliable.
A further object of the present invention is to realise a method which may be carried out routinely, for example in connection with washing of the plant.
SOLUTION
These and other objects have been attained according to the present invention in that the method of the type described by way of introduction has been given the characterising feature that the method is carried out on an intact heat exchanger with requisite pressure indicator mounted between each section, as well as requisite shut- off valves.
Preferred embodiments of the present invention have further been given the characterising features as set forth in the appended subclaims.
BRIEF DESCRIPTION OF THE ACCOMPANYING DRAWING
One preferred embodiment of the present invention will now be described in greater detail hereinbelow, with reference to the accompanying Drawing. In the accompanying Drawing:
Fig. 1 shows a part of a flow diagram with a heat exchanger. The drawing shows only those details and parts essential to an understanding of the present invention, and the remaining part of the plant in which the heat exchanger is included has been omitted. DESCRIPTION OF PREFERRED EMBODIMENT
The method according to the present invention is intended to be employed to detect leakage in a heat exchanger. The method is primarily intended for a plate heat exchanger,, as shown in Fig. l^but the method may also be used for other types of heat exchangers, such as tube heat exchangers, which process liquid foods.
The method may be employed in connection with an existing heat exchanger without it needing to be dismounted or without the need to dismount connecting conduits. Preferably, the method may be used directly in conjunction with washing of the plant in which the heat exchanger is included. Directly in conjunction with the washing, the heat exchanger and connecting conduits are filled with rinsing water from the washing operation. Naturally, the method may be carried into effect on other occasions, for example before start up of production, but then conduits and the heat exchanger must first be filled with water.
Given that the method may be carried on an intact heat exchanger, this implies that it is rapid, approx. 30 minutes. This implies that the method may be employed routinely at, for example, a dairy, which contributes in increased product safety. Previous methods have involved the separate planning of service inputs which have taken up to half a day to complete.
The heat exchanger 1 in Fig. 1 has three sections 2, 3, 4, but the method may naturally also be employed for both more and fewer sections 2, 3, 4. Each section
2, 3, 4 is provided with a pressure indicator 5-10. The pressure indicator 5-10 is preferably electric, but also other types of pressure indicators 5-10 may occur. The pressure indicators 5-10 emit signals to the master or control unit of the plant.
Conventional heat exchangers 1 may perhaps need to be retrofitted with pressure indicators 5-10, but in those cases where one or more of the sections 2, 3, 4 is used regeneratively, pressure indicators 5-10 must already be in position in compliance with the legislation of certain countries.
For carrying the method into effect, a number of shut-off valves 11, 12, 13 are also required. A pump 14 which normally pumps product into the heat exchanger 1 is also used in the method. The pump 14 which normally consists of a circulation pump must be frequency controlled. In the first section 2 there is, on production, hot water on one side which enters into the heat exchanger 1 through the conduit 15. The water pressure in this conduit 15 is monitored using the pressure indicator 5. On the other side in the first section 2r there is a part 16 of the product conduit which is monitored using the pressure indicator 6.
In the second section 3, there are product conduits on both sides. The upstream side has a part 17 of the product conduit which is monitored using the pressure indicator 7. The downstream side has another part 18 of the product conduit which is monitored using the pressure indicator 8. In the third section 4 there is, on production, on the one side ice water which enters into the heat exchanger 1 through the conduit 19. The water pressure in this conduit 19 is monitored using the pressure indicator 9. On the other side in the third section 4, there is a part 20 of the product conduit which is monitored using the pressure indicator 10. When the method is to be carried into effect, the heat exchanger 1 and connecting conduits are to be filled with water. The pressure of the water through the heat exchanger 1 and the conduits should be approx. 2 bar, which is normal pressure on production and washing.
When the method is to be put into effect, the first step is to close the shut-off valve 12. Thereafter, the pump 14 is accelerated in order to give a pressure increase in the conduit system. When the pressure indicator 10 shows approx 6 bar, the valve 12 closes so that an excess pressure of approx. 6 bar is enclosed on the downstream side in the third section 4.
Thereafter, the pump 14 is decelerated somewhat and when the pressure indicator 8 shows approx. 5.5 bar, the shut-off valve 13 closes so that an excess pressure of approx. 5.5 bar is enclosed on the downstream side in the second section 3 of the heat exchanger 1.
The pump 14 is decelerated slightly further and when the pressure indicator 6 shows approx. 5 bar, the pump 14 is completely decelerated. An excess pressure of approx. 5 bar has now been enclosed on the upstream side in the first heat exchanger section 2. The downstream side in the first section 2 and the upstream sides in the second and third sections 3, 4 have a normal pressure of approx. 2 bar, which can be read off with the aid of the pressure indicators 5, 7 and 9, respectively.
The. values, of the_pressure_ indicators. 5J-Q are registered in the. master or control unit of the plant during a given, predetermined period of time, for example
30 minutes. The entire read-off period may suitably be printed out so that there will by such means be obtained different graphs of the pressurised sides of each respective section 2, 3, 4. By pressurising the different sections 2, 3, 4 in steps, it is simple to distinguish the different sections 2, 3, 4 from one another. Steps between the different sections may be larger or smaller than 0.5 bar. However, the difference must be distinguishable on a graph.
If leakage were to occur in some section 2, 3, 4, the pressure in the pressurised side will fall and begin to approach the pressure in the unpressurised side. Large leakages show a rapid pressure equalisation. For minor leakage it is important to use a relatively long measurement period, since the pressure equalisation in such a case is considerably slower.
The excess pressure is preferably laid on the downstream side of the heat exchanger 1 and preferably on the main conduit through the heat exchanger 1, i.e. on that side where the product is led. After the carrying out of the method, the shut-off valves 11, 12, 13 are opened, the water is empted from the conduits and heat exchanger 1 and, if no leakage is present, the heat exchanger 1 is now ready for production.
In those cases where the heat exchanger 1 has more or fewer sections, more or fewer pressure indicators 5-10 and shut-off valves 11, 12, 13 must naturally be used so that it is possible in a corresponding manner to enclose an excess pressure on one side of each respective section 2, 3, 4 in the heat exchanger 1.
As will have been apparent from the foregoing description, the present invention realises a method for discovering leakage which is rapid and reliable. Since the method is carried out on an intact heat exchanger, the method may be put into effect routinely, preferably in conjunction with washing of the plant. Given that the leakage monitoring may be carried out often and regularly, this contributes to increased product safety and reliability which is of vital importance above all in the food industry.

Claims

WHAT IS CLAIMED IS:
1. A method of discovering leakage in a heat exchanger (1), the heat exchanger (l) being,, together with surrounding conduits, filled with water, and the method comprising the steps that, in each section (2, 3, 4) of the heat exchanger (1) an excess pressure is applied on one side and enclosed over the section (2, 3, 4) during a period of time, while the other side in the section (2, 3, 4) is at normal pressure, and that the pressure difference is monitored during the period of time, characterised in that the method is carried into effect on an intact heat exchanger (1) with requisite pressure indicators (5-10) mounted between each section (2, 3, 4) as well as requisite shut-off valves (11, 12, 13).
2. The method as claimed in Claim I5 characterised in that the excess pressure is approx 6 bar.
3. The method as claimed in Claim 1, characterised in that the excess pressure is applied preferably on the downstream side of the heat exchanger (1) and preferably on that side of the heat exchanger (1) where the product is led.
4. The method as claimed in Claim 1, characterised in that the excess pressure is reduced stepwise for each section (2, 3, 4) which is closed off using each respective shut-off valve (11, 12, 13).
5. The method as claimed in Claim 1, characterised in that the time interval is approx. 30 minutes.
PCT/SE2006/001378 2005-12-02 2006-11-30 A method of discovering leakage in a heat exchanger WO2007064285A1 (en)

Priority Applications (9)

Application Number Priority Date Filing Date Title
US12/083,562 US7975529B2 (en) 2005-12-02 2006-11-30 Method of discovering leakage in a heat exchanger
DK06824508.3T DK1957951T3 (en) 2005-12-02 2006-11-30 METHOD FOR DETECTING LEAK IN A HEAT EXCHANGE
PL06824508T PL1957951T3 (en) 2005-12-02 2006-11-30 A method of discovering leakage in a heat exchanger
AU2006321018A AU2006321018B2 (en) 2005-12-02 2006-11-30 A method of discovering leakage in a heat exchanger
NZ567238A NZ567238A (en) 2005-12-02 2006-11-30 A method of discovering leakage in a heat exchanger
EP06824508.3A EP1957951B1 (en) 2005-12-02 2006-11-30 A method of discovering leakage in a heat exchanger
CN2006800448026A CN101317079B (en) 2005-12-02 2006-11-30 A method of discovering leakage in a heat exchanger
JP2008543236A JP2009517689A (en) 2005-12-02 2006-11-30 How to find leaks in a heat exchanger
CA2630230A CA2630230C (en) 2005-12-02 2006-11-30 A method of discovering leakage in a heat exchanger

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
SE0502642A SE529453C2 (en) 2005-12-02 2005-12-02 Method for detecting leaks in a heat exchanger
SE0502642-2 2005-12-02

Publications (1)

Publication Number Publication Date
WO2007064285A1 true WO2007064285A1 (en) 2007-06-07

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PCT/SE2006/001378 WO2007064285A1 (en) 2005-12-02 2006-11-30 A method of discovering leakage in a heat exchanger

Country Status (11)

Country Link
US (1) US7975529B2 (en)
EP (1) EP1957951B1 (en)
JP (1) JP2009517689A (en)
CN (1) CN101317079B (en)
AU (1) AU2006321018B2 (en)
CA (1) CA2630230C (en)
DK (1) DK1957951T3 (en)
NZ (1) NZ567238A (en)
PL (1) PL1957951T3 (en)
SE (1) SE529453C2 (en)
WO (1) WO2007064285A1 (en)

Cited By (3)

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US7772569B2 (en) 2008-04-01 2010-08-10 The Jackson Laboratory 3D biplane microscopy
WO2010139801A1 (en) 2009-06-05 2010-12-09 Unison Engineering Services Limited Heat exchanger integrity testing
US8217992B2 (en) 2007-01-11 2012-07-10 The Jackson Laboratory Microscopic imaging techniques

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US8261593B1 (en) * 2009-10-02 2012-09-11 Leon Sanders Leak detector for heat exchanger
CN102589912B (en) * 2012-01-18 2014-04-16 广州飞机维修工程有限公司 System and method for repairing and inspecting airplane heat exchanger
JP6470093B2 (en) * 2015-04-15 2019-02-13 株式会社フロンティアエンジニアリング Food and beverage production equipment
JP7084155B2 (en) * 2018-02-20 2022-06-14 三菱重工エンジニアリング株式会社 Tube leak detection device and tube leak detection method

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WO2002086438A1 (en) * 2001-04-23 2002-10-31 Tetra Laval Holdings & Finance S.A. Method and device for detecting a leak in a heat exchanger, especially a plate-type heat exchanger
WO2003016847A2 (en) * 2001-08-16 2003-02-27 Weizman, Michael System and method for detecting flaws in plate-type heat exchanger

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US4138856A (en) * 1977-10-07 1979-02-13 Sun-Econ, Inc. Leak detector device
EP1022552A2 (en) * 1999-01-19 2000-07-26 Carrier Corporation Test for the automated detection of leaks between high and low pressure sides of a refrigeration system
WO2002025238A1 (en) * 2000-09-19 2002-03-28 Apv Limited Method of testing for leakage
WO2002086438A1 (en) * 2001-04-23 2002-10-31 Tetra Laval Holdings & Finance S.A. Method and device for detecting a leak in a heat exchanger, especially a plate-type heat exchanger
WO2003016847A2 (en) * 2001-08-16 2003-02-27 Weizman, Michael System and method for detecting flaws in plate-type heat exchanger

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8217992B2 (en) 2007-01-11 2012-07-10 The Jackson Laboratory Microscopic imaging techniques
US7772569B2 (en) 2008-04-01 2010-08-10 The Jackson Laboratory 3D biplane microscopy
US7880149B2 (en) 2008-04-01 2011-02-01 The Jackson Laboratory 3D biplane microscopy
WO2010139801A1 (en) 2009-06-05 2010-12-09 Unison Engineering Services Limited Heat exchanger integrity testing

Also Published As

Publication number Publication date
CN101317079B (en) 2010-09-01
US20090158818A1 (en) 2009-06-25
EP1957951B1 (en) 2018-11-07
CN101317079A (en) 2008-12-03
EP1957951A1 (en) 2008-08-20
CA2630230A1 (en) 2007-06-07
DK1957951T3 (en) 2019-02-11
JP2009517689A (en) 2009-04-30
EP1957951A4 (en) 2015-11-18
SE529453C2 (en) 2007-08-14
US7975529B2 (en) 2011-07-12
SE0502642L (en) 2007-06-03
CA2630230C (en) 2014-07-29
AU2006321018A1 (en) 2007-06-07
NZ567238A (en) 2010-03-26
AU2006321018B2 (en) 2012-05-17
PL1957951T3 (en) 2019-05-31

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