WO2006117938A1 - Optical fiber preform including a non-axisymmetric cross section - Google Patents

Optical fiber preform including a non-axisymmetric cross section Download PDF

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Publication number
WO2006117938A1
WO2006117938A1 PCT/JP2006/305483 JP2006305483W WO2006117938A1 WO 2006117938 A1 WO2006117938 A1 WO 2006117938A1 JP 2006305483 W JP2006305483 W JP 2006305483W WO 2006117938 A1 WO2006117938 A1 WO 2006117938A1
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WO
WIPO (PCT)
Prior art keywords
glass
optical fiber
softening temperature
preform
degrees
Prior art date
Application number
PCT/JP2006/305483
Other languages
French (fr)
Inventor
Ryuichi Sugizaki
Akifumi Sako
Takeshi Yagi
Original Assignee
The Furukawa Electric Co., Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from JP2005127905A external-priority patent/JP2005350340A/en
Application filed by The Furukawa Electric Co., Ltd filed Critical The Furukawa Electric Co., Ltd
Publication of WO2006117938A1 publication Critical patent/WO2006117938A1/en

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Classifications

    • GPHYSICS
    • G02OPTICS
    • G02BOPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B6/00Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
    • G02B6/02Optical fibres with cladding with or without a coating
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01Manufacture of glass fibres or filaments
    • C03B37/012Manufacture of preforms for drawing fibres or filaments
    • C03B37/01205Manufacture of preforms for drawing fibres or filaments starting from tubes, rods, fibres or filaments
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01Manufacture of glass fibres or filaments
    • C03B37/012Manufacture of preforms for drawing fibres or filaments
    • C03B37/01205Manufacture of preforms for drawing fibres or filaments starting from tubes, rods, fibres or filaments
    • C03B37/01211Manufacture of preforms for drawing fibres or filaments starting from tubes, rods, fibres or filaments by inserting one or more rods or tubes into a tube
    • C03B37/01217Manufacture of preforms for drawing fibres or filaments starting from tubes, rods, fibres or filaments by inserting one or more rods or tubes into a tube for making preforms of polarisation-maintaining optical fibres
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2203/00Fibre product details, e.g. structure, shape
    • C03B2203/30Polarisation maintaining [PM], i.e. birefringent products, e.g. with elliptical core, by use of stress rods, "PANDA" type fibres
    • C03B2203/31Polarisation maintaining [PM], i.e. birefringent products, e.g. with elliptical core, by use of stress rods, "PANDA" type fibres by use of stress-imparting rods, e.g. by insertion
    • GPHYSICS
    • G02OPTICS
    • G02BOPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B6/00Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
    • G02B6/02Optical fibres with cladding with or without a coating
    • G02B6/036Optical fibres with cladding with or without a coating core or cladding comprising multiple layers
    • G02B6/03616Optical fibres characterised both by the number of different refractive index layers around the central core segment, i.e. around the innermost high index core layer, and their relative refractive index difference
    • G02B6/03622Optical fibres characterised both by the number of different refractive index layers around the central core segment, i.e. around the innermost high index core layer, and their relative refractive index difference having 2 layers only
    • GPHYSICS
    • G02OPTICS
    • G02BOPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B6/00Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
    • G02B6/02Optical fibres with cladding with or without a coating
    • G02B6/036Optical fibres with cladding with or without a coating core or cladding comprising multiple layers
    • G02B6/03616Optical fibres characterised both by the number of different refractive index layers around the central core segment, i.e. around the innermost high index core layer, and their relative refractive index difference
    • G02B6/03638Optical fibres characterised both by the number of different refractive index layers around the central core segment, i.e. around the innermost high index core layer, and their relative refractive index difference having 3 layers only

Definitions

  • the present invention relates to an optical fiber preform and a method for
  • optical fiber preform manufacturing the optical fiber preform, and more particularly, to an optical fiber
  • optical fiber through which the light passes is totally synthesized so as to have less
  • OH radicals examples include vapour-phase axial
  • VAD outside vapour deposition
  • OTD modified chemical vapour
  • MCVD deposition
  • the optical fiber is
  • the axisymmetric structure is the most desirable structure to manufacture the optical fiber. Accordingly, although
  • some optical fiber such as a polarization-maintaining optical fiber, may have a non-
  • Techniques for manufacturing the optical fiber preform include a rot-in-tube
  • RIT technique in addition to the total synthesis technique.
  • the RIT technique is
  • RIC rot-in-cylinder
  • the glass rod by heating is conducted concurrently with the drawing step.
  • optical fibers proposed heretofore include a non-axisymmetric
  • optical fiber and a photonic-crystal optical fiber having a plurality of air
  • 34203 IA describes a preform for the photonic-crystal optical fiber and a method for
  • preform is manufactured by assembling and fusing a plurality of non-axisymmetric
  • optical fiber is now being used as an interconnection in an optical
  • This technique can utilize the high-speed characteristic of the optical signal.
  • the up-to-date optical circuit now uses a vertical-cavity surface-emitting
  • VCSEL VCSEL
  • optical fiber If the optical fiber includes a core having a specific shape
  • the arbitrary shape of the core is generally obtained by
  • the polarization-maintaining optical fiber is known as such
  • optical fiber having a non-axisymmetric structure, which is suited for use in direct
  • the present invention provides, in a first aspect thereof, a method for
  • manufacturing a preform including the steps of: covering an outer periphery of a
  • first glass having a single first softening temperature by a second glass having a
  • the present invention provides, in a second aspect thereof, a method for
  • manufacturing an optical fiber including the steps of: covering an outer periphery of
  • the present invention provides, in a third aspect thereof, an optical fiber
  • preform including a plurality of glasses including first and second glasses, wherein
  • the first glass configures a central core section and has a non-axisymmetric structure
  • the second glass configures a cladding section covering an outer periphery of the
  • the first glass has a softening temperature higher than a softening
  • the present invention provides, in a fourth aspect thereof, an optical fiber
  • the method of the present invention has an advantage over the prior art that
  • an optical fiber having a desired shape can be manufactured from the preform
  • optical fiber preform of the present invention an optical fiber preform of the present invention
  • Fig. 1 is a cross-sectional view of a preform according to an embodiment of
  • Fig. 2 is a cross-sectional view of a core of an optical fiber obtained by
  • Fig. 3 is a cross-sectional view of a preform manufactured in a second
  • Fig. 4 is a cross-sectional view of a preform manufactured in a third
  • invention includes a core having a polygonal shape, for example, in the cross-
  • optical fiber thus manufactured may preferably be used
  • a second glass such as a cladding section
  • periphery of the first glass provides an optical fiber having an arbitrary shape with a
  • applying section having the arbitrary shape is doped with a dopant, such as
  • germanium, boron and fluorine and has a softening temperature lower than the
  • the periphery of the first glass having a polygonal shape, for example, with the second glass having a softening temperature lower the softening temperature of the first
  • the second glass fuses and adheres onto the first glass by heating.
  • the heating temperature at which the second glass is fused is set below the
  • a glass tube may be used as an outer member for the second glass member.
  • the first and second glasses are arranged or assembled within the glass
  • the glass tube is configured as a part of the cladding
  • the tube is preferably higher than the softening temperature of the second glass
  • the softening temperature of the first glass may be preferably equal to the softening temperature of the first glass.
  • Fig. 1 shows a cross-sectional view of a preform according to a first
  • Glass members 11, 12 and 13 having the shape as
  • Fig. 1 shown in Fig. 1 were obtained by grinding glass materials, and were assembled and
  • the glass member 11 had a shape
  • a pair of glass members 12 each had a substantially half-
  • the glass member 11 being sandwiched therebetween, and the glass members 12
  • the resultant preform had a shape of a
  • the glass member 11 was made of a material having a softening
  • the glass member 11 was made of
  • the glass members 12 and 13 were made of quartz doped with fluorine. In general, the glass material is easily deformed at a temperature
  • the glass member 11 had a softening
  • a burner providing a flame may be used for this
  • the softening temperature 1650 degrees
  • the preform as described above is drawn to an optical fiber in a drawing
  • the resultant optical fiber had no
  • a core having a square cross-section such as shown in Fig. 1, as well as another core having a polygonal cross-section
  • the cladding in the resultant optical fiber was as low as about 1.0%, without
  • the glass member 11 was made of quartz doped with
  • germanium and the glass members 12 and 13 were made of pure quartz. In this case
  • the first glass member 11 had a softening temperature of 1600 degrees C
  • the glass members 12 and 13 had a softening temperature of 1800 degrees
  • preform was drawn to an optical fiber at a temperature of 1900 degrees C, which
  • Fig. 2 shows the cross-section of the core of the optical fiber obtained in the first comparative example.
  • first comparative example had a significant deformation.
  • the deformation was
  • optical fiber obtained from this comparative example is used for direct transmission
  • the transmitted image will have a significant deformation
  • optical fiber does not achieve the object of the present invention.
  • optical fiber obtained in the first comparative example had a non-circularity of 0.9%
  • Fig. 3 shows a preform according to a second example of the present
  • Glass members 31 to 33 were similar to the glass members 11 to 13
  • Another glass member 34 is a glass tube made of a material
  • the glass members 31 to 33 are similar to the material of the glass member 31 (11).
  • the glass members 31 to 33 are similar to the material of the glass member 31 (11).
  • the glass members of the present example had a dimensional ratio different from the
  • optical fiber had a deformation in the core comparable to the deformation in the first
  • optical fiber optical fiber
  • the core used in the above examples had a square cross-section; however,
  • the core may have any contour such as polygon or star shape for achieving a similar
  • Fig. 4 shows a preform according to a third example.
  • member 41a is of a cylinder inserted in the glass member 41b having a square
  • the glass member 41a has a softening temperature lower than the softening temperature of the glass member 41b, which is higher than
  • the glass member is similar to the relationship in the normal optical fiber. That is, the glass member
  • heating temperature of 1760 degrees C or higher resulted in deformation of the core.
  • the viscosity of the core glass should be lowered to some
  • Table 2 shows heating temperatures dependency of the deformation of core
  • a softening temperature of the glass members 11 is
  • glass members 12 and 13 and also 50 degrees C or above lower than the softening

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Optics & Photonics (AREA)
  • Manufacture, Treatment Of Glass Fibers (AREA)

Abstract

A method for manufacturing an optical fiber includes the steps of covering an outer periphery of a first glass (11) having a first softening temperature and a non-axisymmetric structure by a second glass (12, 13) having a second softening temperature which is lower than the first softening temperature, heating the first and second glasses (11, 12, 13) for fusion together to thereby obtain an optical fiber preform; and drawing the preform to the optical fiber.

Description

DESCRIPTION
OPTICAL FIBER PREFORM INCLUDING
A NON-AXISYMMETRIC CROSS SECΗON
TECHNICAL FIELD
[0001]
The present invention relates to an optical fiber preform and a method for
manufacturing the optical fiber preform, and more particularly, to an optical fiber
preform used for manufacturing an optical fiber for use in a relatively short distance
transmission.
BACKGROUND ART
[0002]
It is known that an optical fiber including OH radicals has a large absorption
peak in the vicinity wavelength of 1380nm. To prevent the occurring of such an
absorption peak, a technique is generally employed wherein the portion of the
optical fiber through which the light passes is totally synthesized so as to have less
OH radicals. Examples of the total synthesis technique include vapour-phase axial
deposition (VAD), outside vapour deposition (OVD) and modified chemical vapour
deposition (MCVD).
In general, since the light transmits in an axial symmetry, the optical fiber is
manufactured to have an axisymmetric structure by paying the full attention on the
circularity of a core of the optical fiber. In addition, the axisymmetric structure is the most desirable structure to manufacture the optical fiber. Accordingly, although
some optical fiber, such as a polarization-maintaining optical fiber, may have a non-
axisymmetric structure of a stress-applying part other than the core, even the stress-
applying part of the most of the polarization-maintaining optical fibers is generally
formed to have the axisymmetric structure.
[0003]
Techniques for manufacturing the optical fiber preform include a rot-in-tube
(RIT) technique in addition to the total synthesis technique. The RIT technique is
such that the glass rod including the core and manufactured by the total synthesis
technique is inserted into a glass tube, and the glass tube and the glass rod are
collapsed by heating to form an optical fiber preform. The techniques further
include a rot-in-cylinder (RIC) technique wherein the collapsing the glass tube and
the glass rod by heating is conducted concurrently with the drawing step.
[0004]
Since the required characteristics of the optical fiber are being complicated
in these days, a variety of optical fibers corresponding to these requirements are
proposed. The optical fibers proposed heretofore include a non-axisymmetric
optical fiber and a photonic-crystal optical fiber, the latter having a plurality of air
holes in the cladding section of the optical fiber. Patent Publication JP-2003-
34203 IA describes a preform for the photonic-crystal optical fiber and a method for
manufacturing the same. It is recited in the publication that the optical fiber
preform is manufactured by assembling and fusing a plurality of non-axisymmetric
glass rods. DISCLOSURE OF THE INVENTION
Problems to be solved by the Invention
[0005]
The optical fiber is now being used as an interconnection in an optical
circuit. This technique can utilize the high-speed characteristic of the optical signal.
In addition, the up-to-date optical circuit now uses a vertical-cavity surface-emitting
laser (VCSEL) device, which has not been used heretofore in a long-distance
optical communication system. Suppose a case wherein the light emitted from a
luminous object such as the VCSEL device is directly transmitted through an
optical fiber. If the optical fiber includes a core having a specific shape
corresponding to the light-intensity distribution of the luminous object such as a
star-shaped or polygonal distribution, for example, an extremely efficient light
transmission can be achieved.
[0006]
In order for manufacturing a preform including a core, or stress-applying
section, having an arbitrary shape, such as a star or polygonal shape, it is generally
necessary to prevent deformation of the core shape and thereby maintain the precise
shape of the core during the heat treating. In the total synthesis technique as
described above, however, it is difficult to form a preform having such an arbitrary
shape of the core. Thus, the arbitrary shape of the core is generally obtained by
assembling and fusing together a plurality of glass members each having a specific
shape corresponding to a portion of the arbitrary shape. [0007]
For example, the polarization-maintaining optical fiber is known as such
obtained by assembling and fusing together a plurality of glass members. The
technique is such that a plurality of holes each having a specific shape are formed in
a preform, and respective glass members, or cylindrical glass rods, which are
shaped beforehand to have a small diameter, are inserted in the holes. In this
technique, it is generally difficult to obtain a desired shape with a precise
dimensional accuracy, particularly in a process for forming an axisymmetric shape
which is liable to deformation during the fusing step.
[0008]
In view of the above, it is an object of the present invention to provide an
optical fiber having a non-axisymmetric structure, which is suited for use in direct
transmission of a video image or photographic image, for example.
It is another object of the present invention to provide a method for
manufacturing an optical fiber having an arbitrary shape with a precise dimensional
accuracy, and to provide a preform used in the method.
Means for solving the Problems
[0009]
The present invention provides, in a first aspect thereof, a method for
manufacturing a preform including the steps of: covering an outer periphery of a
first glass having a single first softening temperature by a second glass having a
single second softening temperature which is lower than the first softening temperature; and heating the first and second glasses up to a heating temperature for
fusion, thereby forming an integral body of the first and second glasses.
[0010]
The present invention provides, in a second aspect thereof, a method for
manufacturing an optical fiber including the steps of: covering an outer periphery of
a first glass having a single first softening temperature by a second glass having a
single second softening temperature which is lower than the first softening
temperature; inserting an assembly of the first and second glasses in a glass tube;
and collapsing said glass tube and said assembly of said first and second glasses by
heating at the same time of drawing the optical fiber.
[0011]
The present invention provides, in a third aspect thereof, an optical fiber
preform including a plurality of glasses including first and second glasses, wherein
the first glass configures a central core section and has a non-axisymmetric structure,
the second glass configures a cladding section covering an outer periphery of the
first glass, and the first glass has a softening temperature higher than a softening
temperature of the second glass.
[0012]
The present invention provides, in a fourth aspect thereof, an optical fiber
manufactured by drawing the optical fiber preform of the present invention.
Effects of the Invention
[0013] The method of the present invention has an advantage over the prior art that
an optical fiber having a desired shape can be manufactured from the preform
wherein the outer periphery of the first glass having the first softening temperature
is covered with the second glass having the second softening temperature lower
than the first softening temperature.
[0014]
According to the optical fiber preform of the present invention, an optical
fiber including a core having a non-axisymmetric structure with a higher
dimensional accuracy can be obtained from the optical fiber preform because the
second glass configuring the cladding section has the second softening temperature
lower than the first softening temperature of the first glass configuring the core.
BRIEF DESCRIPTION OF HE DRAWINGS
Fig. 1 is a cross-sectional view of a preform according to an embodiment of
the present invention.
Fig. 2 is a cross-sectional view of a core of an optical fiber obtained by
drawing a preform in a first comparative example.
Fig. 3 is a cross-sectional view of a preform manufactured in a second
example of the present invention.
Fig. 4 is a cross-sectional view of a preform manufactured in a third
example of the present invention.
BEST MODES FOR CARRYING OUT THE INVENTION [0015]
An optical fiber preform according to a preferred embodiment of the present
invention includes a core having a polygonal shape, for example, in the cross-
section thereof, and is thus different from a conventional preform including an
axisymmetric core. An optical fiber manufactured from the optical fiber preform of
the preferred embodiment includes a core having a polygonal shape as well in the
cross-section thereof. The optical fiber thus manufactured may preferably be used
for direct transmission of a photographic image having a polygonal shape, for
example.
Moreover, the configuration wherein the softening temperature of a first
glass, such as a core section, having an arbitrary shape is higher than the softening
temperature of a second glass, such as a cladding section, covering the outer
periphery of the first glass provides an optical fiber having an arbitrary shape with a
higher accuracy.
[0016]
In an optical fiber having an arbitrary shape, the core section or stress-
applying section having the arbitrary shape is doped with a dopant, such as
germanium, boron and fluorine, and has a softening temperature lower than the
softening temperature of the glass member covering the core section or stress-
applying section.
A method for manufacturing an optical fiber according to a preferred
embodiment of the present invention includes the step of covering the outer
periphery of the first glass having a polygonal shape, for example, with the second glass having a softening temperature lower the softening temperature of the first
glass, heating first and second glasses up to a heating temperature for fusion,
thereby forming a preform of an integral body of first and second glasses, and
drawing the preform to the optical fiber.
First, the second glass fuses and adheres onto the first glass by heating.
The heating temperature at which the second glass is fused is set below the
softening temperature of the first glass, whereby the first glass maintains the
original polygonal shape in the cross-section thereof. This achieves a higher
accuracy of the polygonal shape of the first glass, thereby providing an optical fiber
having a desired polygonal shape with a higher accuracy.
[0017]
A glass tube may be used as an outer member for the second glass member.
In this case, the first and second glasses are arranged or assembled within the glass
tube, and are heated. This prevents deformation from the polygonal shape to obtain
a preform having a desired shape. In case the glass tube attached outside the second
glass configuring a cladding, the glass tube is configured as a part of the cladding
after drawing the preform to an optical fiber. Use of the glass tube allows the
cladding shape to be maintained with ease. The softening temperature of the glass
tube is preferably higher than the softening temperature of the second glass, and
may be preferably equal to the softening temperature of the first glass.
EXAMPLES
[First Example] [0018]
Fig. 1 shows a cross-sectional view of a preform according to a first
example of the present invention. Glass members 11, 12 and 13 having the shape as
shown in Fig. 1 were obtained by grinding glass materials, and were assembled and
fused together to form an optical fiber preform. The glass member 11 had a shape
of a pole having a square cross-section, and a pair of glass members 13 each had a
shape of a pole having a rectangular cross-section, wherein one of the shorter sides
of the rectangle configured a circular arc, which formed a part of the cylindrical
surface of the cladding. A pair of glass members 12 each had a substantially half-
cylindrical surface, which was assembled with the circular arc of the glass members
13 so that a substantially complete cylindrical surface was formed from the glass
members 12 and 13. These glass members 11, 12 and 13 were assembled together
such that the glass members 13 were disposed first so as to oppose each other, with
the glass member 11 being sandwiched therebetween, and the glass members 12
were then disposed, with the flat surface of the glass members 12 abutting to the flat
surface of the glass members 11 and 13. The resultant preform had a shape of a
cylinder.
[0019]
The glass member 11 was made of a material having a softening
temperature higher than the softening temperature of the glass members 12 and 13,
and thus was not liable to deformation at a heating temperature lower the softening
temperature thereof. As a concrete example, the glass member 11 was made of
pure quartz, whereas the glass members 12 and 13 were made of quartz doped with fluorine. In general, the glass material is easily deformed at a temperature
exceeding the softening temperature thereof. The glass member 11 had a softening
temperature of 1800 degrees C, whereas the glass members 12 and 13 had a
softening temperature of 1600 degrees C due to doping the quartz with 2wt.-percent
fluorine. Those glass members 11, 12 and 13 were assembled together, as shown in
Fig. 1, and fused together by heating in an electric furnace. A specific case of
fusing together these members at a temperature of 1650 degrees C provided an
optimum cross-sectional shape having a least deformation.
[0020]
In the process of the present embodiment, an electric furnace was used for
fusing, but not limited thereto. A burner providing a flame may be used for this
purpose so long as the burner provides a uniform temperature distribution during
the fusion coupling of the glass members. The softening temperature, 1650 degrees
C, is only an example, and a softening temperature in a range between the softening
temperatures of both the glass materials may be used instead. An excessively lower
temperature dose not provide a suitable fusion and a peeling-off may occur. On the
other hand, an excessively higher temperature involves a larger deformation. Thus,
it is preferable that a temperature about 50 degrees C higher than the lower
softening temperature be used for the fusing.
[0021]
The preform as described above is drawn to an optical fiber in a drawing
furnace at a temperature of 1820 degrees C. The resultant optical fiber had no
substantial deformation in the core. In general, a core having a square cross-section, such as shown in Fig. 1, as well as another core having a polygonal cross-section
may be evaluated for the degree of deformation thereof by expressing the vertex
angle at each corner or apex of the cross-section. In the resultant optical fiber, the
corner of the cross section of the core was maintained at a substantially right angle
without incurring a problem in the deformation. In addition, the non-circularity of
the cladding in the resultant optical fiber was as low as about 1.0%, without
incurring a substantial problem in the circularity of the optical fiber.
[0022]
[First Comparative Example]
In a first comparative example of the preform having a structure similar to
the structure shown in Fig. 1, the glass member 11 was made of quartz doped with
germanium and the glass members 12 and 13 were made of pure quartz. In this
structure, the first glass member 11 had a softening temperature of 1600 degrees C
whereas the glass members 12 and 13 had a softening temperature of 1800 degrees
C. Fusing of these glass members 11, 12 and 13 was conducted at a temperature of
1650 degrees, which is 50 degrees C higher than the softening temperature of the
glass member 11. This provided a preform having a least deformation among other
fusing processes for the same structure at different temperatures. The resultant
preform was drawn to an optical fiber at a temperature of 1900 degrees C, which
was about 80 degrees C higher than the drawing temperature used in the first
example.
[0023]
Fig. 2 shows the cross-section of the core of the optical fiber obtained in the first comparative example. The core HA obtained from the glass member 11 of the
first comparative example had a significant deformation. The deformation was
such that each of the corners of the core 11 in the preform was melted, flowed out
into the gap between the glass member 12 and the glass member 13 configuring a
part of the cladding, and solidified in the as-melted state within the gap . If the
optical fiber obtained from this comparative example is used for direct transmission
of a photographic image, the transmitted image will have a significant deformation
whereby the optical fiber does not achieve the object of the present invention. The
optical fiber obtained in the first comparative example had a non-circularity of 0.9%
which was comparable to the non-circularity obtained in the first example of the
present invention.
[0024]
[Second Example]
Fig. 3 shows a preform according to a second example of the present
invention. Glass members 31 to 33 were similar to the glass members 11 to 13
shown in Fig. 1. Another glass member 34 is a glass tube made of a material
similar to the material of the glass member 31 (11). The glass members 31 to 33
were assembled together and inserted into the glass member 34. More precisely,
the glass members of the present example had a dimensional ratio different from the
dimensional ratio of the glass members 11 to 13 in the first example, for achieving
the final diameter of the core that is comparable to the final diameter of the core in
the first example. This was achieved by the configuration wherein the dimensions
of the glass member 31 were equal to the dimensions of the glass member 11, and the outer diameter of the glass member 34 was equal to the outer diameter of the
preform shown in Fig. 1.
[0025]
After assembling the glass members 31 to 34 in the structure as shown in
Fig. 3, the assembly of glass members 31 to 34 was drawn to an optical fiber at a
temperature similar to the temperature used in the first example. The resultant
optical fiber had a deformation in the core comparable to the deformation in the first
example; however, the non-circularity of the cladding was 0.2% which was superior
to that of the first example. Comparison of the structure obtained by inserting the
glass members 31 to 33 assembled and fused beforehand into the glass tube 34
against the structure obtained by inserting the as-assembled glass members 31 to 33
into the glass tube 34 did not provide a significant difference after drawing to the
optical fiber.
[0026]
The core used in the above examples had a square cross-section; however,
the core may have any contour such as polygon or star shape for achieving a similar
result, which was confirmed in other experiments.
[0027]
[Third Example]
Fig. 4 shows a preform according to a third example. The glass members
42 to 44 in Fig. 4 are similar to glass members 32 to 34 shown in Fig. 3. The glass
member 41a is of a cylinder inserted in the glass member 41b having a square
cross-section in the outline. The glass member 41a has a softening temperature lower than the softening temperature of the glass member 41b, which is higher than
the softening temperature of the other glass members 42 to 44. This configuration
achieves a drawing process incurring substantially no deformation.
[0028]
After assembling the glass members 41 to 44 in the structure as shown in
Fig. 4, the assembly of glass members 41 to 44 was drawn to an optical fiber at a
temperature similar to the temperature used in the first example. The relationship in
the softening temperature between the glass member 41a and the glass member 41b
is similar to the relationship in the normal optical fiber. That is, the glass member
41a has a softening temperature lower than the softening temperature of the glass
member 41b. In this structure, the axial symmetry of the glass member 41a
provided substantially no deformation in the glass members 41a and 41b after
drawing to an optical fiber.
[0029]
Samples having a structure of the first example and a softening temperature
of 1700 degrees C in the glass members 12 and 13 were prepared, and subjected to
a fusing process at temperatures between 1700 degrees C and 1800 degrees C. A
softening temperature of the glass members 11 is 1800 degrees C. Results of the
structure with respect to the core deformation and degree of fusion of the glass
members after the fusing process are shown in the following table 1. Table 1
Figure imgf000016_0001
[0030]
In the table 1, "G" indicates Good, "NG" indicates No Good, and "--"
indicates not measurable. In the above results, the fusion itself was achieved
without a problem so long as the heating temperature was higher than the softening
temperature of the glass members 12 and 13 by 50 degrees C or higher. However, a
heating temperature of 1760 degrees C or higher resulted in deformation of the core.
For the purpose of fusing, the viscosity of the core glass should be lowered to some
extent. That is, a temperature 50 degrees C lower than the softening temperature of
the glass member 11, at which the glass member is on the verge of melting, is most
suitable in the view point of prevention of deformation.
[0031]
Table 2 shows heating temperatures dependency of the deformation of core
for the glass members 12 and 13 having softening temperatures between 1600 degrees C and 1720 degrees C. A softening temperature of the glass members 11 is
1800 degrees C.
Table 2
Figure imgf000017_0001
[0032]
In the table 2, "G" indicates Good, "NG" indicates No Good, and "--" indicates not measurable. A heating temperature less than 50 degrees C higher than
the softening temperature of the glass members 12 and 13 achieved insufficient
fusion whereby a suitable preform was not formed. On the other hand, a
temperature 50 degrees or above higher than the softening temperature of the glass
members 12 and 13 achieved a suitable fusion without a problem. In these
experiments, since the heating temperature was set at 1750 degrees C or lower,
which is 50 degrees C lower than the softening temperature of the glass members
11, in consideration of the results shown in Fig. 1, all the samples that achieved a
suitable fusion exhibited no significant deformation.
In addition, although not shown in Table 2, a lower heating temperature
provides a lower degree of deformation of the core, and thus should be employed so
long as fusion itself is achieved. This means a heating temperature 50 degrees C
higher than the softening temperature of the glass members 12 and 13 is optimum.
Drawing of all the preforms manufactured in these experiments provided optical
fibers having a degree of deformation of the core and non-circularity of the cladding
comparable to those achieved in the first example.
[0033]
From the above results, the heating temperature for fusion coupling should
be preferably 50 degrees C or above higher than the softening temperature of the
glass members 12 and 13, and also 50 degrees C or above lower than the softening
temperature of the glass member 11. Thus, the softening temperature of the glass
members 12 and 13 should preferably be 100 degrees C or above lower than the
softening temperature of the glass member 11. [0034]
Since the above embodiment and examples are described only for
exemplification purposes, the present invention is not limited to the above
embodiment or examples and various modifications or alterations can be easily
made therefrom by those skilled in the art without departing from the scope of the
present invention.

Claims

1. A method for manufacturing a preform comprising the steps of:
covering an outer periphery of a first glass (11) having a single first
softening temperature by a second glass (12, 13) having a single second softening
temperature which is lower than said first softening temperature; and
heating said first and second glasses (11, 12, 13) up to a heating temperature
for fusion, thereby forming an integral body of said first and second glasses.
2. The method according to claim 1, wherein said second glass includes at
least two glass members (12, 13) assembled.
3. The method according to claim 1, wherein said second softening
temperature is 100 degrees C or above lower than said first softening temperature.
4. The method according to claim 1, wherein said heating temperature is 50
degrees C or above higher than said second softening temperature, and 50 degrees
C or above lower than said first softening temperature.
5. The method according to any one of claims 1 to 4, wherein said first glass
has a non-axisymmetric structure.
6. The method according to any one of claims 1 to 5, wherein said first glass
(11) configures a core section.
7. A method for manufacturing an optical fiber comprising the steps of:
covering an outer periphery of a first glass (31) having a single first
softening temperature by a second glass (32, 33) having a single second softening
temperature which is lower than said first softening temperature;
inserting an assembly of said first and second glasses (31, 32, 33) in a glass
tube (34); and
collapsing said glass tube (34) and said assembly of said first and second
glasses (31, 32, 33) by heating at the same time of drawing the optical fiber.
8. The method according to claim 7, wherein said first glass (31) has a non-
axisymmetric structure.
9. The method according to claim 7 or 8, wherein said first glass (31)
configures a core section.
10. An optical fiber preform comprising a plurality of glasses including first and
second glasses (11, 12, 13), wherein said first glass (11) configures a central core
section and has a non-axisymmetric structure, said second glass (12, 13) configures
a cladding section covering an outer periphery of said first glass (11), and said first
glass (11) has a softening temperature higher than a softening temperature of said
second glass (12, 13).
11. The optical fiber preform according to claim 10, wherein said first glass
(11) has a polygonal cross-section.
12. An optical fiber manufactured by drawing the optical fiber preform
according to claim 10 or 11.
PCT/JP2006/305483 2005-04-26 2006-03-14 Optical fiber preform including a non-axisymmetric cross section WO2006117938A1 (en)

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JP2005-127905 2005-04-26

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2322489A1 (en) * 2009-11-16 2011-05-18 IXFiber Method for manufacturing a preform to be fibred and constant polarisation or polarising optical fibre obtained by fibreing said preform
EP2460036A2 (en) * 2009-05-27 2012-06-06 CeramOptec GmbH Precisely-shaped core fibers and method of manufacture

Citations (4)

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Publication number Priority date Publication date Assignee Title
JPS5120834A (en) * 1974-08-12 1976-02-19 Olympus Optical Co
JP2002277667A (en) * 2001-03-14 2002-09-25 Sumitomo Electric Ind Ltd Optical fiber
JP2003342031A (en) * 2002-05-23 2003-12-03 Masataka Nakazawa Preform for photonic crystal optical fiber and its manufacturing method
WO2004034094A2 (en) * 2002-06-12 2004-04-22 Corning Incorporated Microstructured optical fibers preforms and methods of fabricating microstructured optical fibers

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5120834A (en) * 1974-08-12 1976-02-19 Olympus Optical Co
JP2002277667A (en) * 2001-03-14 2002-09-25 Sumitomo Electric Ind Ltd Optical fiber
JP2003342031A (en) * 2002-05-23 2003-12-03 Masataka Nakazawa Preform for photonic crystal optical fiber and its manufacturing method
WO2004034094A2 (en) * 2002-06-12 2004-04-22 Corning Incorporated Microstructured optical fibers preforms and methods of fabricating microstructured optical fibers

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2460036A2 (en) * 2009-05-27 2012-06-06 CeramOptec GmbH Precisely-shaped core fibers and method of manufacture
EP2460036A4 (en) * 2009-05-27 2015-04-01 Biolitec Pharma Ip & Invest Ltd Precisely-shaped core fibers and method of manufacture
EP2322489A1 (en) * 2009-11-16 2011-05-18 IXFiber Method for manufacturing a preform to be fibred and constant polarisation or polarising optical fibre obtained by fibreing said preform
FR2952726A1 (en) * 2009-11-16 2011-05-20 Ixfiber METHOD FOR MANUFACTURING A FIBER PREFER AND OPTICAL FIBER HAVING POLARIZATION OR POLARIZATION OBTAINED BY FIBRING THE SAID PREFORM

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