WO2006098652A1 - Diamant de joaillerie cultive personnifie et procede de production associe - Google Patents

Diamant de joaillerie cultive personnifie et procede de production associe Download PDF

Info

Publication number
WO2006098652A1
WO2006098652A1 PCT/RU2005/000113 RU2005000113W WO2006098652A1 WO 2006098652 A1 WO2006098652 A1 WO 2006098652A1 RU 2005000113 W RU2005000113 W RU 2005000113W WO 2006098652 A1 WO2006098652 A1 WO 2006098652A1
Authority
WO
WIPO (PCT)
Prior art keywords
diamond
animal
hair
grown
microelements
Prior art date
Application number
PCT/RU2005/000113
Other languages
English (en)
Russian (ru)
Inventor
Sergey Gennadievich Anufriev
Anatoly Ilich Saprykin
Sergey Aleksandrovich Viktorov
Daniel Eduardovich Efremenko
Oleg Borisovich Latypov
Sergey Valentinovich Martynenko
Valery Alekseevich Morozov
Dmitry Aleksandrovich Seleznev
Original Assignee
Obshestvo S Ogranichennoi Otvetstvennostiu 'brilliant Dushi'
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Obshestvo S Ogranichennoi Otvetstvennostiu 'brilliant Dushi' filed Critical Obshestvo S Ogranichennoi Otvetstvennostiu 'brilliant Dushi'
Priority to PCT/RU2005/000113 priority Critical patent/WO2006098652A1/fr
Publication of WO2006098652A1 publication Critical patent/WO2006098652A1/fr

Links

Classifications

    • A—HUMAN NECESSITIES
    • A44—HABERDASHERY; JEWELLERY
    • A44C—PERSONAL ADORNMENTS, e.g. JEWELLERY; COINS
    • A44C17/00—Gems or the like
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/25—Diamond
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/25—Diamond
    • C01B32/26—Preparation

Definitions

  • the invention is intended for use in the jewelry industry and is aimed at obtaining a gemstone, in particular a diamond, which can be personalized (identified) with a specific person or animal.
  • a gemstone is known, in particular, natural diamond, which includes material of human or animal origin and contains internal channels filled with structures formed from the ashes of cremation material of human or animal origin, while this structure is transparent and refracts light like a precious stone (WO2004076058 Al, Galop Vepora, Wispot Moti, 10.09.04).
  • microchannels are created by laser drilling in a natural gemstone, which are filled with glassy structures with a refractive index close to 5 diamond and formed during the crystallization of animal material mixed with lead oxide, sodium chloride and sodium bromide in the process of crystallization from the ashes.
  • the crystal is used only as a capsule for the ashes, as a result of drilling the integrity of the precious stone is disturbed by filling the channels formed with a glassy structure, although visually indistinguishable from the whole.
  • Synthetic gemstones are known, in particular diamonds containing elements, namely carbon extracted from the remains of animal species, and methods for their preparation (US 20030017932 Al Vapdep Wiesepd ets, 01.23.03; US 20040031434 Al, Vapdep Wesepwdetts, 19.02. 04). So, in accordance with the application US 20030017932, in obtaining precious stones, the remains of a person or animal are cremated at temperatures from 1000 to 1800 F (538 - 982 0 C), the carbon obtained is filtered, subjected to high-temperature vacuum cleaning with halogens and used for growing diamonds.
  • the approach to using the remains of a deceased person as a source for extracting carbon used to grow diamonds requires great sensitivity and is unacceptable for a number of crops for ethical reasons.
  • the cremation of the remains requires the inclusion in the technological cycle of additional links (crematoria in different regions, training of cremation operators), which leads to an increase in production time and a significant increase in the cost of the product.
  • the obtained gem can be considered only in the aspect of the memory of the dead, as a memorial item, for the personification of which each gem is laser-labeled with individual figures on it corresponding to the previously assigned remains of animal origin. Since the process of high-temperature vacuum cleaning removes all trace elements, and the residues are considered only as a source of carbon, it is impossible to identify the chemical composition of the grown diamond with
  • SUBSTITUTE SHEET (RULE 26) the remains of a certain person or animal.
  • the objective of this invention is to create a personalized grown diamond jewelery containing elements of a specific person or animal, and proof of the compliance of the chemical composition of the grown diamond with the chemical composition of the material of a certain person or animal.
  • a personalized grown diamond jewelry contains a set of trace elements that make up the hair of a given person or animal and characterize a certain person or animal.
  • the problem is solved by the fact that the set of trace elements that characterize a certain person or animal contains at least heavy metals, such as Sr, Cd, In, Sn, Ba, Pb, Bi.
  • the task is also solved by the fact that in the method of obtaining a personalized jewelery diamond grown, including the processing of a material of a certain person or animal and the growth of diamond crystals, their hair is used as a material of a certain person or animal,
  • SUBSTITUTE SHEET (RULE 26) which are treated with mineralization at a temperature not higher than 550 ° C until complete destruction of protein molecules, spectral determination of a set of trace elements characterizing a certain person or animal is carried out in the hair mineralization product, a carbon source is formed from spectrally pure graphite with the addition of hair mineralization products for diamond growth, then grown diamond determine the set of trace elements and carry out the identification of the grown diamond according to the set of trace elements it contains trace elements hair characterizing a certain person or animal.
  • trace element concentrations of at least heavy metals for example, Sr, Cd, In, Sn, Ba , Pb, Bi, which is an individual characteristic of a certain person or animal relative to the concentration, for example, Pb.
  • concentration of trace elements in diamond is determined taking into account the experimentally established coefficients of their distribution between the melt and the diamond crystal.
  • SUBSTITUTE SHEET (RULE 26) When diamond is grown, some metals and metalloids (Ni, Fe, Co, Mo, Cr, Pt, Mn, Ti, V, W, B, Al, Si) can have a catalytic effect on the graphitization process of carbon-graphite materials, others (Cu, Ag, Mg, Zn, Cd, Ge, Sn, Pb, Sb, Bi, Se, Te, Pd) have no such effect. Also, the chemical composition of the grown diamond is influenced by impurities present in the growth system (Fe-Ni alloy and graphite).
  • the carbon source for diamond growth is formed from the product of hair mineralization and spectrally pure
  • SUBSTITUTE SHEET (RULE 26) graphite the use of the latter does not contaminate the system with impurities of heavy metals and ensures the preservation of a set of chemical elements selected to characterize a certain person or animal, and growing diamond at high temperatures and pressure from the melt in the presence of a metal catalyst, ensures proportional entry of these elements into the diamond while maintaining relative concentrations, taking into account the experimentally established distribution coefficients of the elements in the melt.
  • Quantitative chemical analysis of the hair mineralization product, carbon source and grown diamond is carried out using modern instrumental methods (mass spectrometry, atomic emission, atomic absorption).
  • the relative concentrations of elements are recalculated taking into account the distribution coefficients, the result obtained is compared with the ratio of the concentrations of heavy metals in the hair mineralization product.
  • the coincidence of values taking into account the measurement error allows the identification of the diamond, i.e. prove conformity of a grown diamond to a certain
  • SUBSTITUTE SHEET (RULE 26) human or animal, and certify a diamond based on its chemical composition.
  • a hair sample of a specific person weighing -500 mg was subjected to mineralization at a temperature of 550 ° C.
  • the weight of the resulting mineralization product (ash residue) of the hair was about ⁇ 5 mg.
  • ⁇ 1 mg of the mineralization product was taken, mixed with spectral purity graphite and placed in the growth cell of the known high-pressure apparatus “Discharge Sphere” (BARS) (described, for example, in the work of Chepurov AI and others. “Exclusive modeling of the alma-zine process” 1997, c.8-20). Conducted the cultivation of single crystal diamond from the melt by the method of recrystallization on the seed. As a result, a single-crystal diamond of jewelry purity weighing ⁇ 0.2 carat and having a fancy yellow color was obtained.
  • BARS Charge Sphere
  • C x / ⁇ modifier is the relative concentration of the element X to Pb in the grown diamond
  • K ⁇ / pb is the relative concentration of the element X to Pb in the grown diamond, taking into account the distribution coefficients K ⁇ / pb of the element X and Pb between

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Adornments (AREA)

Abstract

La présente invention est destinée à être utilisée dans l'industrie joaillière, et vise à produire une pierre précieuse, en particulier un diamant, qui peut être personnifiée (identifié) par un être humain ou un animal déterminé. L'invention concerne un diamant de joaillerie cultivé personnifié, qui contient un jeu de micro-éléments caractérisant ledit être humain ou animal donné et figurant dans la composition de la chevelure dudit être humain ou du pelage dudit animal. Le jeu de micro-éléments renferme au moins des métaux lourds tels que Sr, Cd, In, Ba, Pb et Bi. L'invention a également trait à un procédé permettant d'obtenir un diamant de joaillerie cultivé personnifié obtenu à partir de cheveux ou de poils de l'être humain ou de l'animal donnés, qui consiste : à traiter lesdits cheveux ou poils par minéralisation à une température inférieure ou égale à 550 °C ; à effectuer, dans le produit de la minéralisation des cheveux ou des poils, une détermination spectrale du jeu de micro-éléments contenant au moins des métaux lourds tels que Sr, Cd, In, Ba, Pb et Bi et caractérisant l'être humain ou l'animal donné ; à former, pour faire croître le diamant, une source de carbone à partir de graphite pur spectral auquel sont ajoutés les produits de la minéralisation des cheveux ou des poils ; à déterminer ensuite le jeu de micro-éléments dans le diamant cultivé ; et à procéder à l'identification du diamant cultivé, en mettant en correspondance le jeu de micro-éléments avec du jeu de micro-éléments des cheveux ou des poils caractérisant l'être humain ou l'animal donné.
PCT/RU2005/000113 2005-03-14 2005-03-14 Diamant de joaillerie cultive personnifie et procede de production associe WO2006098652A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PCT/RU2005/000113 WO2006098652A1 (fr) 2005-03-14 2005-03-14 Diamant de joaillerie cultive personnifie et procede de production associe

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/RU2005/000113 WO2006098652A1 (fr) 2005-03-14 2005-03-14 Diamant de joaillerie cultive personnifie et procede de production associe

Publications (1)

Publication Number Publication Date
WO2006098652A1 true WO2006098652A1 (fr) 2006-09-21

Family

ID=36991947

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/RU2005/000113 WO2006098652A1 (fr) 2005-03-14 2005-03-14 Diamant de joaillerie cultive personnifie et procede de production associe

Country Status (1)

Country Link
WO (1) WO2006098652A1 (fr)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115253908A (zh) * 2022-08-29 2022-11-01 洛阳美钻钻石培育有限公司 一种人工制备生物钻石的方法
CN115367731A (zh) * 2022-08-29 2022-11-22 洛阳美钻钻石培育有限公司 一种生物碳粉的提取工艺

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU577444A1 (ru) * 1975-07-11 1977-10-25 Предприятие П/Я А-1067 Способ подготовки пробы дл исследовани распределени компонента между жидкой и твердой фазами
EP0322217A1 (fr) * 1987-12-21 1989-06-28 De Beers Industrial Diamond Division (Proprietary) Limited Synthèse de diamant
RU2129426C1 (ru) * 1998-04-09 1999-04-27 Общество с ограниченной ответственностью "Научно-медицинский центр "Силвер" Silver" Способ определения макро- и микроэлементного баланса в организме
RU2180121C1 (ru) * 2001-03-11 2002-02-27 ООО Медико-профилактический центр "Силвер" Способ определения изменений в биологической системе макро- и микроэлементного гомеостаза у человека при различных заболеваниях
US20030017932A1 (en) * 2001-07-17 2003-01-23 Vandenbiesen Russell P. Method for making synthetic gems comprising elements recovered from complete or partial human or animal remains and the product thereof
WO2004105540A1 (fr) * 2003-05-29 2004-12-09 Eiji Fukasawa Gemme artificielle et son procede de production

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU577444A1 (ru) * 1975-07-11 1977-10-25 Предприятие П/Я А-1067 Способ подготовки пробы дл исследовани распределени компонента между жидкой и твердой фазами
EP0322217A1 (fr) * 1987-12-21 1989-06-28 De Beers Industrial Diamond Division (Proprietary) Limited Synthèse de diamant
RU2129426C1 (ru) * 1998-04-09 1999-04-27 Общество с ограниченной ответственностью "Научно-медицинский центр "Силвер" Silver" Способ определения макро- и микроэлементного баланса в организме
RU2180121C1 (ru) * 2001-03-11 2002-02-27 ООО Медико-профилактический центр "Силвер" Способ определения изменений в биологической системе макро- и микроэлементного гомеостаза у человека при различных заболеваниях
US20030017932A1 (en) * 2001-07-17 2003-01-23 Vandenbiesen Russell P. Method for making synthetic gems comprising elements recovered from complete or partial human or animal remains and the product thereof
WO2004105540A1 (fr) * 2003-05-29 2004-12-09 Eiji Fukasawa Gemme artificielle et son procede de production

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
"Chernye almazy mogut imet kosmicheskoe proiskhozdenie", PESTRY MIR., 29 June 2004 (2004-06-29), Retrieved from the Internet <URL:http://www.sines.uz/articles.pl?/12/17815> *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115253908A (zh) * 2022-08-29 2022-11-01 洛阳美钻钻石培育有限公司 一种人工制备生物钻石的方法
CN115367731A (zh) * 2022-08-29 2022-11-22 洛阳美钻钻石培育有限公司 一种生物碳粉的提取工艺
CN115253908B (zh) * 2022-08-29 2023-10-13 洛阳美钻新材料有限公司 一种人工制备生物钻石的方法

Similar Documents

Publication Publication Date Title
Weber et al. Depth related changes in the 13C12C ratio of skeletal carbonate deposited by the Caribbean reef-frame building coral Montastrea annularis: further implications of a model for stable isotope fractionation by scleractinian corals
Huang et al. Early diagnosis and management of nitrogen deficiency in plants utilizing Raman spectroscopy
Douka et al. Improved AMS 14C dating of shell carbonates using high-precision X-ray diffraction and a novel density separation protocol (CarDS)
Tomlinson et al. Trace element compositions of submicroscopic inclusions in coated diamond: A tool for understanding diamond petrogenesis
EP1862433A1 (fr) Diamant synthetique de differentes couleurs, personnalise, obtenu a partir de keratine humaine ou animale (vivante ou morte), et son procede de fabrication
Uchima Gut content analysis of neritic copepods Acartia omorii and Oithona davisae by a new method.
Eaton-Magaña et al. Raman and photoluminescence mapping of gem materials
Wang et al. LATEST-GENERATION CVD-GROWN SYNTHETIC DIAMONDS FROM APOLLO DIAMOND INC.
WO2006098652A1 (fr) Diamant de joaillerie cultive personnifie et procede de production associe
RU2282584C1 (ru) Персонифицированный выращенный ювелирный алмаз и способ его получения
Fridrichová et al. Use of spectroscopic methods for determination of diamond origin and treatment
Jurikova et al. Incorporation of minor and trace elements into cultured brachiopods: Implications for proxy application with new insights from a biomineralisation model
Oppelt et al. Biogeochemical analysis of the calcification patterns of cold-water corals Madrepora oculata and Lophelia pertusa along contact surfaces with calcified tubes of the symbiotic polychaete Eunice norvegica: evaluation of a ‘mucus’ calcification hypothesis
WO2009091285A1 (fr) Diamant de culture personnalisé destiné à la joaillerie
Cartier et al. A Case Study of Ivory Species Identification Using a Combination of Morphological, Gemmological and Genetic Methods.
Sturm Morphology and growth trends of accessory zircons from various granitoids of the South-western Bohemian Massif (Moldanubicum, Austria)
SEVIK et al. Availability of Cedrus atlantica annual rings in monitoring the change in airborne sulfur pollution
JP6333506B2 (ja) 血液由来成分含有物質の製造方法、および血液由来成分含有物質
Bruni et al. An Archaeometric investigation of gems and glass beads decorating the double-arm reliquary cross from Liège, Belgium
Sharifuddin et al. Technique of soil testing and plant analysis and their utilization for crop production in malaysia
Eaton-Magaña CVD-Grown Diamond with Few Diagnostic Features.
Johnson Technological developments in the 1990s: Their impact on gemology
Rydelek Application of scanning electron microscope (SEM) in peat studies
Chapman Argyle Violet Diamonds.
RU2656032C1 (ru) Способ контроля сохранности кристаллов драгоценных камней в процессах технологической переработки

Legal Events

Date Code Title Description
ENP Entry into the national phase

Ref document number: 2005109546

Country of ref document: RU

Kind code of ref document: A

DPE2 Request for preliminary examination filed before expiration of 19th month from priority date (pct application filed from 20040101)
121 Ep: the epo has been informed by wipo that ep was designated in this application
NENP Non-entry into the national phase

Ref country code: DE

122 Ep: pct application non-entry in european phase

Ref document number: 05789930

Country of ref document: EP

Kind code of ref document: A1