WO2006065819A3 - Metal components with silicon-containing protective coatings and methods of forming such protective coatings - Google Patents

Metal components with silicon-containing protective coatings and methods of forming such protective coatings Download PDF

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Publication number
WO2006065819A3
WO2006065819A3 PCT/US2005/045078 US2005045078W WO2006065819A3 WO 2006065819 A3 WO2006065819 A3 WO 2006065819A3 US 2005045078 W US2005045078 W US 2005045078W WO 2006065819 A3 WO2006065819 A3 WO 2006065819A3
Authority
WO
WIPO (PCT)
Prior art keywords
protective coatings
silicon
forming
methods
metal components
Prior art date
Application number
PCT/US2005/045078
Other languages
French (fr)
Other versions
WO2006065819A2 (en
Inventor
David C Fairbourn
Original Assignee
Aeromet Technologies Inc
David C Fairbourn
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from PCT/US2004/041896 external-priority patent/WO2006036171A1/en
Application filed by Aeromet Technologies Inc, David C Fairbourn filed Critical Aeromet Technologies Inc
Priority to EP16171410.0A priority Critical patent/EP3095895B1/en
Priority to EP05853894.3A priority patent/EP1834009B1/en
Priority to PL16171410T priority patent/PL3095895T3/en
Priority to US11/721,564 priority patent/US8623461B2/en
Publication of WO2006065819A2 publication Critical patent/WO2006065819A2/en
Publication of WO2006065819A3 publication Critical patent/WO2006065819A3/en
Priority to US14/147,818 priority patent/US9157140B2/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/125—Process of deposition of the inorganic material
    • C23C18/1279—Process of deposition of the inorganic material performed under reactive atmosphere, e.g. oxidising or reducing atmospheres
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/06—Coating on selected surface areas, e.g. using masks
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1204—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material inorganic material, e.g. non-oxide and non-metallic such as sulfides, nitrides based compounds
    • C23C18/1208—Oxides, e.g. ceramics
    • C23C18/1212—Zeolites, glasses
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1229—Composition of the substrate
    • C23C18/1241—Metallic substrates
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/125—Process of deposition of the inorganic material
    • C23C18/1275—Process of deposition of the inorganic material performed under inert atmosphere
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/48—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 not containing phosphates, hexavalent chromium compounds, fluorides or complex fluorides, molybdates, tungstates, vanadates or oxalates
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/73—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals characterised by the process
    • C23C22/74—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals characterised by the process for obtaining burned-in conversion coatings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Ceramic Engineering (AREA)
  • Other Surface Treatments For Metallic Materials (AREA)
  • Turbine Rotor Nozzle Sealing (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Chemically Coating (AREA)

Abstract

A metal component (10) with a protective coating (16) containing silicon and a process for forming such protective coatings (14). The protective coating (16) is formed by applying a silicon-containing fluid composition to the metal component (10) as a silicon-containing layer (12) and heating the silicon-containing layer (12) to a temperature exceeding 400°F.
PCT/US2005/045078 2004-09-16 2005-12-12 Metal components with silicon-containing protective coatings and methods of forming such protective coatings WO2006065819A2 (en)

Priority Applications (5)

Application Number Priority Date Filing Date Title
EP16171410.0A EP3095895B1 (en) 2004-12-13 2005-12-12 Method of forming silicon-containing protective coatings on metal components
EP05853894.3A EP1834009B1 (en) 2004-12-13 2005-12-12 Metal components with silicon-containing protective coatings and methods of forming such protective coatings
PL16171410T PL3095895T3 (en) 2004-12-13 2005-12-12 Method of forming silicon-containing protective coatings on metal components
US11/721,564 US8623461B2 (en) 2004-09-16 2005-12-12 Metal components with silicon-containing protective coatings substantially free of chromium and methods of forming such protective coatings
US14/147,818 US9157140B2 (en) 2004-09-16 2014-01-06 Metal components with silicon-containing protective coatings substantially free of chromium and methods of forming such protective coatings

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
USPCT/US2004/041896 2004-12-13
PCT/US2004/041896 WO2006036171A1 (en) 2004-09-16 2004-12-13 Superalloy jet engine components with protective coatings and method of forming such protective coatings on superalloy jet engine components

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2004/041896 Continuation-In-Part WO2006036171A1 (en) 2004-09-16 2004-12-13 Superalloy jet engine components with protective coatings and method of forming such protective coatings on superalloy jet engine components

Related Child Applications (2)

Application Number Title Priority Date Filing Date
US11/721,564 A-371-Of-International US8623461B2 (en) 2004-09-16 2005-12-12 Metal components with silicon-containing protective coatings substantially free of chromium and methods of forming such protective coatings
US14/147,818 Continuation US9157140B2 (en) 2004-09-16 2014-01-06 Metal components with silicon-containing protective coatings substantially free of chromium and methods of forming such protective coatings

Publications (2)

Publication Number Publication Date
WO2006065819A2 WO2006065819A2 (en) 2006-06-22
WO2006065819A3 true WO2006065819A3 (en) 2006-11-30

Family

ID=36405882

Family Applications (2)

Application Number Title Priority Date Filing Date
PCT/US2005/044843 WO2007067185A2 (en) 2004-09-16 2005-12-12 Turbine engine components with non-aluminide silicon-containing and chromium-containing protective coatings and methods of forming such non-aluminide protective coatings
PCT/US2005/045078 WO2006065819A2 (en) 2004-09-16 2005-12-12 Metal components with silicon-containing protective coatings and methods of forming such protective coatings

Family Applications Before (1)

Application Number Title Priority Date Filing Date
PCT/US2005/044843 WO2007067185A2 (en) 2004-09-16 2005-12-12 Turbine engine components with non-aluminide silicon-containing and chromium-containing protective coatings and methods of forming such non-aluminide protective coatings

Country Status (4)

Country Link
EP (3) EP1831428B1 (en)
ES (1) ES2368436T3 (en)
PL (2) PL1831428T3 (en)
WO (2) WO2007067185A2 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2103713A1 (en) * 2008-03-20 2009-09-23 Münch Chemie International GmbH Anti-corrosion primer

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4500364A (en) * 1982-04-23 1985-02-19 Exxon Research & Engineering Co. Method of forming a protective aluminum-silicon coating composition for metal substrates
EP0327311A2 (en) * 1988-02-02 1989-08-09 Hitachi Chemical Co., Ltd. A coating fluid for forming an oxide coating
WO1998030735A2 (en) * 1997-01-09 1998-07-16 University Of Cincinnati Method of preventing corrosion of metals using silanes
WO2002099153A2 (en) * 2001-06-05 2002-12-12 Aeromet Technologies, Inc. Inoculants for intermetallic layer
WO2003035942A2 (en) * 2001-08-03 2003-05-01 Elisha Holding Llc An electrolytic and electroless process for treating metallic surfaces and products formed thereby
US20030185990A1 (en) * 2000-09-25 2003-10-02 Klaus Bittner Method for pretreating and coating metal surfaces prior to forming, with a paint-like coating and use of substrates so coated
WO2006036171A1 (en) * 2004-09-16 2006-04-06 Aeromet Technologies, Inc. Superalloy jet engine components with protective coatings and method of forming such protective coatings on superalloy jet engine components

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB893397A (en) * 1959-07-29 1962-04-11 Dow Corning Improvements in or relating to coating metals
CA1004964A (en) * 1972-05-30 1977-02-08 Union Carbide Corporation Corrosion resistant coatings and process for making the same
CH597364A5 (en) * 1974-04-11 1978-03-31 Bbc Sulzer Turbomaschinen
GB1529441A (en) * 1976-01-05 1978-10-18 Bp Chem Int Ltd Protective surface films of oxide or silicide
JPS5754282A (en) * 1980-09-17 1982-03-31 Mitsubishi Heavy Ind Ltd Surface treatment of heat resistant alloy
US4774149A (en) * 1987-03-17 1988-09-27 General Electric Company Oxidation-and hot corrosion-resistant nickel-base alloy coatings and claddings for industrial and marine gas turbine hot section components and resulting composite articles
US6503347B1 (en) * 1996-04-30 2003-01-07 Surface Engineered Products Corporation Surface alloyed high temperature alloys
US5721061A (en) * 1996-11-15 1998-02-24 General Electric Company Oxidation-resistant coating for niobium-base alloys
GB9821748D0 (en) * 1998-10-07 1998-12-02 Rolls Royce Plc A titanium article having a protective coating and a method of applying a protective coating to a titanium article
EP1111192B1 (en) * 1999-12-20 2005-08-31 United Technologies Corporation Articles provided with corrosion resistant coatings
US6521356B2 (en) * 2001-02-02 2003-02-18 General Electric Company Oxidation resistant coatings for niobium-based silicide composites

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4500364A (en) * 1982-04-23 1985-02-19 Exxon Research & Engineering Co. Method of forming a protective aluminum-silicon coating composition for metal substrates
EP0327311A2 (en) * 1988-02-02 1989-08-09 Hitachi Chemical Co., Ltd. A coating fluid for forming an oxide coating
WO1998030735A2 (en) * 1997-01-09 1998-07-16 University Of Cincinnati Method of preventing corrosion of metals using silanes
US20030185990A1 (en) * 2000-09-25 2003-10-02 Klaus Bittner Method for pretreating and coating metal surfaces prior to forming, with a paint-like coating and use of substrates so coated
WO2002099153A2 (en) * 2001-06-05 2002-12-12 Aeromet Technologies, Inc. Inoculants for intermetallic layer
WO2003035942A2 (en) * 2001-08-03 2003-05-01 Elisha Holding Llc An electrolytic and electroless process for treating metallic surfaces and products formed thereby
WO2006036171A1 (en) * 2004-09-16 2006-04-06 Aeromet Technologies, Inc. Superalloy jet engine components with protective coatings and method of forming such protective coatings on superalloy jet engine components

Also Published As

Publication number Publication date
ES2368436T3 (en) 2011-11-17
EP3095895A1 (en) 2016-11-23
EP1834009A2 (en) 2007-09-19
EP1831428A2 (en) 2007-09-12
PL3095895T3 (en) 2019-10-31
EP3095895B1 (en) 2019-05-01
WO2007067185A3 (en) 2007-08-02
WO2007067185A2 (en) 2007-06-14
PL1831428T3 (en) 2012-03-30
WO2006065819A2 (en) 2006-06-22
EP1834009B1 (en) 2016-07-20
EP1831428B1 (en) 2011-06-22

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