WO2006020323A2

WO2006020323A2 - Strain detection for automated nano-manipulation

Info

Publication number: WO2006020323A2
Application number: PCT/US2005/025743
Authority: WO
Inventors: Thomas M. Moore
Original assignee: Moore Thomas M
Priority date: 2004-07-28
Filing date: 2005-07-21
Publication date: 2006-02-23
Also published as: US20070089528A1; EP1782037A2; US7395727B2; WO2006020323A3

Abstract

We disclose a strain detector for in-situ lift-out, comprising a nano-manipulator probe shaft (100); a strain gauge (120) mounted on the probe shaft; and a first cut-out on the probe shaft. The first cut-out has a rectangular cross-section (130 or 160). There is a second cut-out on the probe shaft; the second cut-out having a semiconductor cross-section. The second cut-out is positioned on the shaft opposite from the first cut-out; the first and second cut-out thus defining a thinned region in the probe. The strain gauge is mounted on the probe shaft at the location of the thinned region. There is detecting circuitry for detecting amplifying and conditioning the out put strain gauge; and wires electrically connecting the strain gauge to the detection circuitry. The wires are preferably located in the trench (140) in the probe shaft. Other embodiments are discloses With multiple strain gauge and detectors, as well as method of use.

Description

Strain Detection for Automated Nano-Manipulation

Patent Application of Thomas M. Moore

Claim for Priority This application claims the priority of United States provisional application serial no. 60/592,3322, filed July 28, 2004 and having the title of "Strain detection for automated nano-manipulation." Technical Field This disclosure relates to the removal of specimens inside focused ion-beam (FIB) microscopes and the preparation of specimens for later analysis in the transmission electron microscope (TEM), and apparatus to facilitate these activities. This disclosure also relates to the mechanical testing of materials and tiny structures outside a FIB. Background The use of In-Situ Lift-Out (INLO) for TEM sample preparation in the FIB has become a popular and widely accepted technique. INLO enables the preparation of multiple site-specific TEM samples, at different angles of inspection, and with the imaging resolution of a Scanning Electron Microscope (SEM), without the need for an expensive wet lab for conventional sawing, polishing and grinding, and without the need to sacrifice the wafer being inspected. The ability to perform process control on 300 mm diameter wafers without sacrificing wafers for the inspection is very important because of the value of these wafers. However, accurate process control requires high throughput TEM sample preparation. Automation of the sample preparation process will significantly and favorably impact the analytical throughput of this process and its repeatability. A key apparatus for INLO is an in-situ nano-manipulator that enables full wafer analysis, such as the AutoProbe 200TM manufactured by Omniprobe, Inc. This nano- manipulator can be used to lift-out a tiny wedge-shaped portion (typically 5 x 5 x 10 μm) of the sample and to transfer it to a TEM sample holder that is also present in the FIB vacuum chamber. Ion or electron-beam assisted deposition of metal or other materials from appropriate source gases injected near the surface in the FIB can be used to attach the nano-manipulator probe tip to the excised lift-out sample. The same beam-assisted gas chemistry can be used to attach the lift-out sample to the TEM sample holder. Later, the ion beam in the FIB can be used to detach the probe tip from the lift-out sample, completing the in-situ transfer of the lift-out sample to the TEM sample holder. This lift-out sample can then be thinned to an appropriate thickness for TEM inspection (<100 nm). Surface contact detection is a critical element of the automation of such a nano- manipulator-based operation. One of the methods that can be used to determine that the contact between the nano-manipulator probe tip and the sample surface has been made is electrical continuity detection. This method is impractical for automation due to several reasons. If the sample surface is non-conductive, the detection of the steady- state electrical continuity between the probe tip and the sample surface will not be successful. Even if the sample surface is electrically conductive, it may not be electrically connected to the sample holder, or there may be a tough native oxide on the conductive surface making continuity detection difficult. Without an electrical connection to the sample holder, continuity detection between the probe tip and sample surface will be difficult in the FIB environment. Detection of a transient electrical response due to the connection of the charged sample surface with the probe tip is also impractical for repetitive automated procedures because this effect is time and material dependent and also depends on the behavior of the charged particle beams impinging the surface. A metal layer that covers the surface of the sample and electrically connects the surface and the sample stage may be deposited using an appropriate gas source and electron or ion beam assisted deposition in the FIB. Such a deposition operation is time consuming in the FIB, however, and may render the wafer useless for further processing. In addition, the ion beam may locally remove the metal layer at the place where the probe tip makes contact with a sample surface and hence defeat the purpose of the inspection. What is needed is a safe and reliable method of detecting contact between the sample and the probe of the nano-manipulator, whether inside or outside of a FIB. Summary We disclose a strain detector for in-situ lift-out, comprising a nano-manipulator probe shaft; a strain gauge mounted on the probe shaft; and a first cut-out on the probe shaft. The first cut-out has a rectangular cross-section. There is a second cut-out on the probe shaft; the second cut-out having a semicircular cross-section. The second cut-out is positioned on the shaft opposite from the first cut-out; the first and second cut-outs thus defining a thinned region in the probe. The strain gauge is mounted on the probe shaft at the location of the thinned region. There is detecting circuitry for detecting, amplifying and conditioning the output of the strain gauge; and, wires electrically connecting the strain gauge to the detection circuitry. The wires are preferably located in a trench in the probe shaft. Drawings Figure 1 shows a perspective view of the preferred embodiment, depicting a modified probe shaft with a strain gauge attached to it. Figure 2 shows another embodiment, depicting multiple strain gauges. Description A sensitive strain gauge mounted in the probe shaft of the nano-manipulator can function as an efficient surface contact detector in the FIB. Such a detection method based on mechanical strain in the probe shaft is independent of electrical continuity effects and will function efficiently on any type of sample surface. The sensitivity of such a method depends on the type of strain gauge used, the detection circuitry, the position of the strain gauge on the shaft, and the mechanical design of the probe shaft. In the preferred embodiment, a tiny (<1 mm2) electrical resistance-based silicon strain gauge is effectively used to measure the level of strain necessary for reliable automation of surface contact detection. Other types of strain gauges may also be used, such as resistive foil gauges, or semiconductor strain gauges manufactured by using - A - photolithography masking and solid-state diffusion, instead of adhesive bonding. In the latter type of strain gauge, the electrical leads are attached directly to the strain-gauge pattern. Figure 1 shows a three-dimensional view of a modified probe shaft (100) with a strain gauge (120) attached to it. There are two cut-outs on a probe shaft surface, one is of rectangular cross-section (160), and another one is of triangular or semi-circular (arched) cross-section (130), and they are located on the opposite sides of the probe shaft (100) directly opposite each other creating a very thin section (135) of the probe shaft. There is also a trench (140) in the probe shaft, which continues along the length of the probe shaft (100) from the border of the rectangular cut-out (160) to the external end of the probe shaft (100). In the preferred embodiment, the strain gauge (120) is located at the median of the rectangular probe shaft cut-out (160), exactly on the very thin section of the probe shaft (100), created by the intersection of two cut-outs (130 and 160). The triangular or semi-circular cut-out (130), which serves as the "sensitivity cut-out", reduces the absolute stiffness of the probe shaft (100) and concentrates the strain at the strain gauge (120) location. The strain gauge (120) can be attached to a probe shaft surface with a high elastic modulus adhesive, such as epoxy. Electrical connection between the strain gauge (120) and the detection circuitry (170) can be made using wires (150) that follow the trench (140) running along the axis of the probe shaft (100). The wires (150) are connected to detection circuitry (170) for detecting, amplifying and conditioning the output of the strain gauge (120). For a resistance-based strain gauge, a conventional Wheatstone bridge can be used to detect subtle changes in the strain gauge resistance which can be fed back to the computer control system to indicate load on the probe tip (110). In the figures, a conventional Wheatstone bridge represents the detector circuitry (170), but the reader should understand this as an example. In practice, the detector circuitry (170) would include amplification and signal conditioning elements, as is known in the art. The modified probe shaft (100) can be manufactured using several methods, such as machining, which is difficult with such a small object. Preferable alternatives are laser machining and electrical discharge machining methods. The single strain-gauge system described above can detect strain in one dimension of deflection of the probe tip. In another embodiment, an additional strain gauge (125) can be mounted at the same or different location along the probe shaft and perpendicular to the first strain(120) gauge. This additional strain gauge (125) requires a similar mechanical design of the probe shaft (100), including a local reduction in the probe shaft diameter (sensitivity cut-out). In general, the apparatus just described may be used as follows: First, the target location for the touch-down of the probe (100) is defined by moving the nano- manipulator to a position above the target location. The output of the detector (170) is monitored while the nano-manipulator is moving towards the target location. When the output of the detector (170) is a touch-down signal, that is, strain signifying contact, the nano-manipulator is stopped. I claim:

Claims

1. A strain detector for in-situ lift-out, comprising: a probe shaft; a strain gauge; a first cut-out on the probe shaft; a second cut-out on the probe shaft, the second cut-out opposite from the first cut-out; the first and second cut-outs defining a thinned region in the probe shaft; and, the strain gauge mounted on the probe shaft at the location of the thinned region.

2. The strain detector of claim 1, where the strain gauge is a resistance-based strain gauge.

3. The strain detector of claim 1, where the strain gauge is a silicon strain gauge.

4. The strain detector of claim 1 where the strain gauge is a semiconductor strain gauge.

5. The strain detector of claim 1, further comprising: the probe shaft having a trench; the trench connecting to the first cut-out.

6. The strain detector of claim 1, further comprising: detecting circuitry for detecting, amplifying and conditioning the output of the strain gauge; wires electrically connecting the strain gauge to the detection circuitry.

7. The strain detector of claim 6 where the detection circuitry comprises a Wheatstone bridge.

8. The strain detector of claim 2 where the electrical resistance-based strain gauge is smaller in cross-sectional area than one square millimeter.

9. The strain detector of claim 1 , 1 where the surface of the first cut-out comprises an adhesive for mounting the strain

2 gauge to the probe shaft. 3

4 10. The strain detector of claim 9, where the adhesive is epoxy.

5

6 11. The strain detector of claim 1 , where the first cut-out has a rectangular cross-

7 section. 8

9 12. The strain detector of claim 1, where the second cut-out has a triangular cross-

10 section. 1 1

12 13. The strain detector of claim 1, where the second cut-out has a semi-circular

13 cross-section. 14

15 14. A strain detector for in-situ lift-out, comprising:

16 a probe shaft;

17 a first cut-out on the probe shaft;

18 a second cut-out on the probe shaft, the second cut-out opposite from the first

19 cut-out; the first and second cut-outs defining a first thinned region in the probe

20 shaft;

21 a first strain gauge mounted on the probe shaft at the location of the first thinned

22 region;

23 a third cut-out on the probe shaft;

24 a fourth cut-out on the probe shaft, the fourth cut-out opposite from the third cut-

25 out; the third and fourth cut-outs defining a second thinned region in the probe

26 shaft;

27 a second strain gauge mounted on the probe shaft at the location of the second

28 thinned region;

29 where the second strain gauge is located substantially perpendicular to the first

30 strain gauge. 31

32 15. The strain detector of claim 14, where the first and second strain gauges are

33 resistance-based strain gauges. 1

2 16. The strain detector of claim 15, where the first and second strain gauges are

3 silicon strain gauges. 4

5 17. The strain detector of claim 14, further comprising:

6 the probe shaft having a trench; the trench connecting to the first and third cut-

7 outs. 8

9 18. The strain detector of claim 16, further comprising:

10 detecting circuitry for detecting, amplifying and conditioning the output of the

11 strain gauge;

12 wires electrically connecting the strain gauge to the detection circuitry; the wires

13 located in the trench. 14

15 19. The strain detector of claim 18 where the detection circuitry comprises at least

16 one Wheatstone bridge. 17

18 20. The strain detector of claim 15 where the resistance-based strain gauges are each

19 smaller in cross-sectional area than one square millimeter. 20

21 21. The strain detector of claim 15 ,

22 where the surface of the first cut-out and the third cut-out comprise an adhesive

23 for mounting the first and second strain gauges respectively to the probe shaft.

24

25 22. The strain detector of claim 21, where the adhesive is epoxy. 26

27 23. The strain detector of claim 14, where the first and third cut-outs have a

28 rectangular cross-section. 29

30 24. The strain detector of claim 14, where the second and fourth cut-outs have a

31 triangular cross-section. 32 1 25. The strain detector of claim 14, where the second and fourth cut-outs have a

2 semi-circular cross-section. 3

4 26. A strain detector for in-situ lift-out, comprising:

5 a probe shaft;

6 a strain gauge;

7 a first cut-out on the probe shaft; the first cut-out having a rectangular cross-

8 section;

9 a second cut-out on the probe shaft; the second cut-out having a semicircular

10 cross-section; the second cut-out opposite from the first cut-out; the first and

11 second cut-outs defining a thinned region in the probe;

12 the strain gauge mounted on the probe shaft at the location of the thinned region;

13 a trench connecting to the first cut-out;

14 detecting circuitry for detecting, amplifying and conditioning the output of the

15 strain gauge; and,

16 wires electrically connecting the strain gauge to the detection circuitry; the wires

17 located in the trench. 18

19 27. A method of using an apparatus for detecting contact of a nano-manipulator 0 probe; the probe comprising a probe shaft; at least one strain gauge; at least a first cut-

21 out on the probe shaft; at least a second cut-out on the probe shaft, the second cut-out

22 opposite from the first cut-out; the first and second cut-outs defining a thinned region in

23 the probe shaft; the number of strain gauges corresponding to the number of thinned 4 regions; the strain gauge mounted on the probe shaft at the location of the thinned 5 region; and, the strain gauge connected to a detector; the detector capable of emitting a 6 touch-down signal; the method comprising: 7 moving the nano-manipulator probe to a position above the target location;

28 monitoring the output of the detector while the nano-manipulator is moving

29 towards the target location; and,

30 stopping movement of the nano-manipulator when the output of the detector

31 shows a touch-down signal.