WO2005083253A1 - Engine component part and method for producing the same - Google Patents
Engine component part and method for producing the same Download PDFInfo
- Publication number
- WO2005083253A1 WO2005083253A1 PCT/JP2005/003442 JP2005003442W WO2005083253A1 WO 2005083253 A1 WO2005083253 A1 WO 2005083253A1 JP 2005003442 W JP2005003442 W JP 2005003442W WO 2005083253 A1 WO2005083253 A1 WO 2005083253A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- less
- silicon
- grains
- slide surface
- grain size
- Prior art date
Links
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F02—COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
- F02F—CYLINDERS, PISTONS OR CASINGS, FOR COMBUSTION ENGINES; ARRANGEMENTS OF SEALINGS IN COMBUSTION ENGINES
- F02F1/00—Cylinders; Cylinder heads
- F02F1/18—Other cylinders
- F02F1/20—Other cylinders characterised by constructional features providing for lubrication
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D30/00—Cooling castings, not restricted to casting processes covered by a single main group
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C21/00—Alloys based on aluminium
- C22C21/02—Alloys based on aluminium with silicon as the next major constituent
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/04—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon
- C22F1/043—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon of alloys with silicon as the next major constituent
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F02—COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
- F02F—CYLINDERS, PISTONS OR CASINGS, FOR COMBUSTION ENGINES; ARRANGEMENTS OF SEALINGS IN COMBUSTION ENGINES
- F02F1/00—Cylinders; Cylinder heads
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F02—COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
- F02F—CYLINDERS, PISTONS OR CASINGS, FOR COMBUSTION ENGINES; ARRANGEMENTS OF SEALINGS IN COMBUSTION ENGINES
- F02F3/00—Pistons
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F05—INDEXING SCHEMES RELATING TO ENGINES OR PUMPS IN VARIOUS SUBCLASSES OF CLASSES F01-F04
- F05C—INDEXING SCHEME RELATING TO MATERIALS, MATERIAL PROPERTIES OR MATERIAL CHARACTERISTICS FOR MACHINES, ENGINES OR PUMPS OTHER THAN NON-POSITIVE-DISPLACEMENT MACHINES OR ENGINES
- F05C2201/00—Metals
- F05C2201/90—Alloys not otherwise provided for
- F05C2201/903—Aluminium alloy, e.g. AlCuMgPb F34,37
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T29/00—Metal working
- Y10T29/49—Method of mechanical manufacture
- Y10T29/49229—Prime mover or fluid pump making
- Y10T29/49231—I.C. [internal combustion] engine making
Definitions
- the present invention relates to an engine component
- a cylinder block or a piston e.g., a cylinder block or a piston, and a method for
- the present invention also relates to an engine and an
- a cylinder block may meet with even higher abrasion
- crystal grain size of no less than about 12 11 m and no more
- the engine component further comprises
- average crystal grain size of no more than about 7.5 li ra .
- the engine component having
- the aforementioned structure is a cylinder block, wherein the
- an aluminum alloy containing silicon including a plurality of
- the plurality of silicon crystal grains have a grain size
- peaks include a first peak existing in a crystal grain size
- 0.1 m or more is equal to or less than five.
- the aluminum alloy contains :
- the aluminum alloy contains :
- the slide surface has a
- present invention includes the engine component having the
- the present invention is a cylinder block composed of an aluminum alloy containing: no less than abou ⁇ t 73.4wt% and no
- the plurality of primary-crystal silicon grains have
- silicon grains have an average crystal grain size of no more
- the aluminum alloy contains: no less than
- HRB Rockwell hardness
- the present invention is a cylinder block composed of an aluminum alloy containing: no less than
- the cylinder block including a plurality of
- crystal grains have a grain size distribution having at least
- the at least two peaks include a first peak
- aluminum alloy contains: no less than about 50 wtppm and no
- the slide surface has a Rockwell hardness (HRB) of no less than about 60 and no more
- step (b) of forming the molding is performed so that an area
- molding includes step (b-1) of allowing a plurality of
- the slide surface so as to have an average crystal grain size of no less than about 12 m and no more than about 50 m
- FIG. 1 is a perspective view schematically showing a
- FIG. 2 is a schematic enlarged view of a slide surface of the cylinder block 100;
- FIGS. 3A, 3B, and 3C are diagrams for explaining the
- FIG. 4 is a flowchart illustrating a method for
- FIG. 5 is a schematic, diagram showing a high-pressure
- FIGS. 6A and 6B are metallurgical microscope photographs
- FIGS. 7A and 7B are metallurgical microscope photographs
- FIG. 8 is a graph showing a grain size distribution of
- FIG. 9 is a graph showing a grain size distribution of
- FIG. 10 is an enlarged photograph of the slide surface
- FIG. 11 is an enlarged photograph of the slide surface
- FIG. 12 is a photograph showing a silicon crystal grain
- FIG. 13 is a cross-sectional view schematically showing
- FIGS. 14A to 14E are metallurgical microscope
- FIG. 15 is a graph showing a relationship between
- FIG. 16 is a cross-sectional view schematically showing an engine 150 having the cylinder block 100.
- FIG. 17 is a side view schematically showing a
- silicon crystal grains have a specific grain size
- the present invention has been developed based on
- the present invention is not
- component being a component (e.g., a cylinder block or a
- FIG. 1 shows a cylinder block 100 according to the
- the cylinder block 100 is
- the cylinder block 100 preferably is formed of an aluminum alloy which contains silicon. As shown in FIG. 1, the cylinder block 100 preferably is formed of aluminum alloy which contains silicon. As shown in FIG. 1, the cylinder block 100 preferably is formed of aluminum alloy which contains silicon. As shown in FIG. 1, the cylinder block 100 preferably is formed of aluminum alloy which contains silicon. As shown in FIG. 1, the cylinder block 100 preferably is formed of aluminum alloy which contains silicon. As shown in FIG. 1, the cylinder block 100 preferably
- cylinder bore includes a wall portion (referred to as a "cylinder bore
- jacket 105 for retaining a coolant is provided.
- cylinder bore 102 defines a slide surface which comes into
- FIG. 2 is enlarged in FIG. 2.
- the cylinder block 100 includes a
- silicon crystal grains 1011 and 1012 are dispersed in a
- hypereutectic composition containing a large amount of
- primary-crystal silicon grains are referred to as "primary-crystal silicon grains" .
- the relatively small silicon crystal grains 1012 formed between the primary-crystal silicon grains are
- the eutectic silicon grains 1012 are typically needle ⁇
- silicon crystal grain 1012 is a needle-like crystal.
- grains 1011 are mainly composed of granular crystals, whereas
- the eutectic silicon grains 1012 are mainly composed of
- crystal grain size will be described with reference to FIGS. 3A to 3C .
- silicon grains 1011 exceeds about 50 m, as shown at the
- primary-crystal silicon grains 1011 may possibly be destroyed.
- silicon grains 1011 is less than about 12 Mm, as shown at
- each primary-crystal silicon crystal grain 1011 is buried in the
- the primary-crystal silicon grains 1011 may easily be easily
- crystal silicon grains 1011 will act as abrasive grains due
- the primary-crystal silicon grains 1011 is no less than 12 M
- silicon grains 1011 exist per unit area of the slide surface
- crystal grain size range of no less than about 1 Mm and no
- crystal grain size range of no less than about 12 Mm and no
- abrasion layer also improves the strength of the cylinder bore wall 103.
- an anti-abrasion 100 of the present preferred embodiment, an anti-abrasion
- block 100 allows for an increase in the amount of gas mixture
- FIG. 4 is a flowchart illustrating
- step SI In order to ensure a sufficient abrasion
- an aluminum alloy which contains: no less
- the aluminum alloy may be any aluminum alloy having more than about 3.0wt% of copper.
- the aluminum alloy may be any aluminum alloy having more than about 3.0wt% of copper.
- the prepared aluminum alloy is heated and melted
- step S2 a melt is formed (step S2).
- the melt is heated to a predetermined
- phosphorus be added to the ingot or melt, at
- step S3 the melt is cooled within a
- This step of molding formation is
- T5 treatment is a T5 treatment
- a T6 treatment is a
- a T7 treatment is a treatment for
- step S5 Specifically, a surface abutting with a cylinder head, a surface abutting with a
- crankcase and the inner surface of the cylinder bore wall
- the inner surface i.e., a surface defining
- step S6 the cylinder
- a honing process can be performed,
- the slide surface is cooled at a cooling rate of no less than
- a cylinder block 100 which has
- the first heat treatment step allows any compound of aluminum and copper which exists within the alloy to be
- step allows these copper atoms to cohere within the matrix
- This cohesion state is also referred to as a coherent
- FIG. 5 shows a high-
- the high-pressure die cast apparatus shown in FIG. 5 includes
- the die 1 is composed of a stationary die 2 which
- the movable die 3 includes a base die 4 and a slide die 5.
- These dies are formed of a material which is selected with
- an iron alloy e.g., JIS-SKD61
- JIS-SKD61 JIS-SKD61
- silicon and vanadium have been added each at about 1% .
- split portion has a cylinder 6 (only two such cylinders 6 are
- split portion of the slide die 5 slides along a direction
- forming portion 7a for forming a cylinder bore is provided.
- the cylinder bore forming portion 7a is formed so as to be
- the core 7 ⁇ is formed
- the base die 4 is provided with an extrusion pin 8.
- stationary die 2 is provided with an injection sleeve 9.
- feeding inlet 12 is formed in the injection sleeve 9.
- the plunger tip 11 is in an original position (i.e., "behind"
- melt-feeding inlet 12 Ahead of the melt-feeding inlet 12 is provided a tip sensor 13.
- the tip sensor 13 detects passage
- the cover 14 includes a first cover element 14a for protecting the melt .
- a sealing member 15 such as an O ring is also
- leak valve 16 may be provided on the first cover element 14a.
- suction is performed in the die 1 at casting (i.e., in the
- ventilation passage 17 are closed or opened as the ON/OFF
- valve 18 moves in the upper or lower direction in FIG. 5.
- the ON/OFF valve 18 is energized with a spring so that the
- passage 17 may be formed on the movable die 3.
- the ON/OFF valve 18 is a valve of a metal-touch type
- the melt touches the ON/OFF valve 18 so as to push up the
- a valve may be used instead of such a metal-touch type valve, a valve may
- chill-vent structure may be used to
- element 14a in this example one or more (i.e., two in this example).
- vacuum ducts 20 which communicate with a vacuum tank
- the vacuum tank 19 is connected.
- the vacuum tank 19 is maintained at a
- solenoid valve 20a which is installed in each vacuum duct 20
- control device 22 is controlled by a control device 22 so as to be opened or
- control device 22 controls the opening/closing in accordance with the start/end timing of
- an outer periphery of the die 1 may be covered in an
- cover the cylinder 6 for driving the slide die 5 may be
- a cooling water flow amount adjustment unit 60 controls
- a valve (not shown) is
- time (e.g., a period of time until the die is opened and the molding is taken out ) .
- water- passage 60a extends into the interior of the cylinder
- the controlling of the cooling rate may be performed, as
- the cooling is preferably performed in such a
- the slide die 5 is placed in a
- the cover 14 is sealed upon abutment of the first cover
- the cast cycle time can be
- the cavity 7, and thereafter the die 1 may be covered with
- inlet 12 is open. The interior of the die 1 is exposed to
- one shot worth of aluminum alloy melt is injected into the
- the tip sensor 13 detects the plunger tip 11.
- This evacuation is performed so that evacuation of a
- release agent is prevented from flowing into the cavity 7 and
- pinholes can be prevented with an increased certainty
- the melt surface is prevented from being locally cooled by
- Time t2 The progression speed of the plunger tip 11 is
- Time t4 The vacuum pump 21 is stopped, and the
- Time t5 The leak valve 16 is opened to expose the
- Time t6 The air pressure inside the cover 14 completely returns to the atmospheric pressure. At this point, the die 1 is opened, and the molding (cast article) is taken out.
- the cylinder block 100 shown in FIG. 2 was actually prototyped, and its abrasion resistance and strength were evaluated. Portions of the results are shown below.
- the aluminum alloy an aluminum alloy of a composition shown in Table 1 was used. Table 1
- the calcium content in the aluminum alloy was equal to or less than about
- composition casting was performed by the high-pressure die
- forming portion 7a was performed by allowing cooling water to
- cooling rate was no less than about 25°C/sec and no more than
- FIGS. 6A and 6B show the slide
- FIGS. 7A and 7B show the slide surface 101 of
- silicon grains 2012 (most of which are of a needle-like
- the slide surface 201 of the comparative example had a
- the slide surface 101 of the prototype had a
- grain size of about 0.1 M m or more was counted by visual
- FIG. 8 is a graph for the
- crystal grain sizes fall within the range of no less than
- crystal grain sizes fall within the range of no less than
- FIG. 10 shows an enlarged photograph of the slide
- FIG. 11 shows an enlarged photograph of the slide
- the calcium in the aluminum is to or less than about 0.01wt%.
- silicon crystal grains 1010 protrude from the
- the slide surface was no less than about 12 Mm and no more
- the Rockwell hardness (HRB) of the slide surface was in the range of no less than about 60 and no more than about 80.
- FIGS. 14A to 14E show changes in the average crystal
- FIG. 14A when the cooling rate was equal to or less than
- the average crystal grain size was as large as
- cooling rate was no less than about 4°C/sec and no more than
- the primary-crystal silicon grains had an average crystal grain size of about 10 M m or less.
- FIG. 15 shows a
- the size of the primary-crystal silicon grains is determined as (T1-T2 ) / ( t2-tl) , based on a solidification start temperature TI, a eutectic temperature T2, a solidification start time tl, and a time t2 at which the eutectic temperature is reached.
- the size of the eutectic silicon grains is determined as t2"-t2, based on a time t2' at which the crystallization of the eutectic silicon grains ends.
- the size of the primary- crystal silicon grains increases, the size of the eutectic silicon grains also increases; as the size of the primary- crystal silicon grains decreases, the size of the eutectic silicon grains also decreases.
- invention is suitably used for an engine which is operated at
- a high revolution e.g., an engine of a motorcycle, and can
- FIG. 16 shows an exemplary engine 150 incorporating the
- the engine 150 includes a crankcase 110, the
- crankshaft 111 is accommodated in the crankcase 110.
- the crankshaft 111 includes a crankpin 112 and a crankweb 113.
- crankcase 110 is provided the cylinder block
- a piston 122 is inserted in the cylinder bore of the
- the slide surface of the piston 122 is
- slide surface 101 of the cylinder block 100 that of the slide surface 101 of the cylinder block 100.
- slide surface of the piston 122 may be coated
- the piston 122 may have a surface hardness lower than that of
- slide surface 101 of the cylinder block 100 should have a
- abrasion resistance is to be made based on various
- the cylinder head 130 forms a combustion chamber
- the cylinder head 130 includes an intake port 132 and an
- an exhaust valve 135 In the exhaust port, an exhaust valve 135
- the piston 122 and the crankshaft 111 are connected via
- connection rod 140 Specifically, a piston pin 123 of the
- piston 122 is inserted in a throughhole in a small end 142 of
- crankshaft 111 is inserted in a throughhole in a big end 144
- connection rod 140 whereby the piston 122 and the connection rod 140
- crankshaft 111 are connected together. Between the inner
- crankpin 112 is provided a roller bearing 114.
- the engine 150 has excellent durability. Since the cylinder block 100 of various
- FIG. 17 shows a motorcycle incorporating the engine 150
- a head pipe 302 is
- a front fork 303 is attached so as to be
- a front fork 303 At a lower end of the front fork 303, a front
- wheel 304 is supported so as to be capable of rotating.
- a seat rail 306 is attached to the main-body frame 301 .
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Combustion & Propulsion (AREA)
- General Engineering & Computer Science (AREA)
- Metallurgy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Cylinder Crankcases Of Internal Combustion Engines (AREA)
- Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
- Powder Metallurgy (AREA)
Abstract
Description
Claims
Priority Applications (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP05719757.6A EP1723332B2 (en) | 2004-02-27 | 2005-02-23 | Engine component part and method for producing the same |
US10/552,172 US7412955B2 (en) | 2004-02-27 | 2005-02-23 | Engine component part and method for producing the same |
DE602005009149T DE602005009149D1 (en) | 2004-02-27 | 2005-02-23 | ENGINE COMPONENT AND MANUFACTURING METHOD THEREFOR |
ES05719757.6T ES2310341T5 (en) | 2004-02-27 | 2005-02-23 | Engine component and method to produce it |
US12/045,947 US7765977B2 (en) | 2004-02-27 | 2008-03-11 | Engine component part and method for producing the same |
US12/789,618 US20100229822A1 (en) | 2004-02-27 | 2010-05-28 | Engine component part and method for producing the same |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2004054582 | 2004-02-27 | ||
JP2004-054582 | 2004-02-27 |
Related Child Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US10/552,172 A-371-Of-International US7412955B2 (en) | 2004-02-27 | 2005-02-23 | Engine component part and method for producing the same |
US12/045,947 Continuation US7765977B2 (en) | 2004-02-27 | 2008-03-11 | Engine component part and method for producing the same |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2005083253A1 true WO2005083253A1 (en) | 2005-09-09 |
Family
ID=34908797
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/JP2005/003442 WO2005083253A1 (en) | 2004-02-27 | 2005-02-23 | Engine component part and method for producing the same |
Country Status (11)
Country | Link |
---|---|
US (3) | US7412955B2 (en) |
EP (3) | EP1723332B2 (en) |
JP (1) | JP2010151139A (en) |
CN (2) | CN100585153C (en) |
AT (1) | ATE405740T1 (en) |
DE (1) | DE602005009149D1 (en) |
ES (1) | ES2310341T5 (en) |
MY (1) | MY144677A (en) |
PT (1) | PT1723332E (en) |
TW (1) | TWI321591B (en) |
WO (1) | WO2005083253A1 (en) |
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WO2008081964A1 (en) * | 2006-12-28 | 2008-07-10 | Yamaha Hatsudoki Kabushiki Kaisha | Internal combustion engine component and method for producing the same |
EP2138695A3 (en) * | 2008-06-27 | 2010-02-17 | Yamaha Hatsudoki Kabushiki Kaisha | Cylinder block, internal combustion engine, transportation apparatus, and method for producing cylinder block |
DE102006040362B4 (en) * | 2005-09-01 | 2011-03-03 | GM Global Technology Operations, Inc., Detroit | Abrasion resistant combination of aluminum piston and aluminum cylinder bore and method of making same |
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US20070227475A1 (en) * | 2006-03-28 | 2007-10-04 | Yamaha Hatsudoki Kabushiki Kaisha | Internal combustion engine and transporation apparatus incorporating the same |
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US9133739B2 (en) * | 2012-05-30 | 2015-09-15 | GM Global Technology Operations LLC | Method for in-situ forming of low friction coatings on engine cylinder bores |
TWI447299B (en) * | 2012-06-08 | 2014-08-01 | Colis Ind Co Ltd | Process for manufacture of water-cooled motorcycle cylinder |
CN103522004B (en) * | 2012-07-04 | 2015-09-02 | 可立新实业有限公司 | Water-cooled locomotive cylinder method for making |
EP2905351B1 (en) * | 2012-09-25 | 2017-11-01 | Josho Gakuen Educational Foundation | Hypereutectic aluminum/silicon alloy die-cast member and process for producing same |
DE102013210469A1 (en) * | 2013-06-05 | 2014-12-11 | Bayerische Motoren Werke Aktiengesellschaft | Trough element for a motor vehicle and arrangement of a battery on such a trough element |
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- 2005-02-23 EP EP10003783A patent/EP2241741A1/en not_active Withdrawn
- 2005-02-23 ES ES05719757.6T patent/ES2310341T5/en active Active
- 2005-02-23 CN CN200580000432.1A patent/CN100585153C/en active Active
- 2005-02-23 EP EP08007881A patent/EP1944495A1/en not_active Ceased
- 2005-02-23 AT AT05719757T patent/ATE405740T1/en not_active IP Right Cessation
- 2005-02-23 CN CN200910252842.5A patent/CN101694187A/en active Pending
- 2005-02-23 US US10/552,172 patent/US7412955B2/en active Active
- 2005-02-23 DE DE602005009149T patent/DE602005009149D1/en active Active
- 2005-02-23 PT PT05719757T patent/PT1723332E/en unknown
- 2005-02-25 TW TW094105822A patent/TWI321591B/en active
- 2005-02-25 MY MYPI20050774A patent/MY144677A/en unknown
-
2008
- 2008-03-11 US US12/045,947 patent/US7765977B2/en active Active
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2010
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Cited By (4)
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DE102006040362B4 (en) * | 2005-09-01 | 2011-03-03 | GM Global Technology Operations, Inc., Detroit | Abrasion resistant combination of aluminum piston and aluminum cylinder bore and method of making same |
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US8047174B2 (en) | 2006-12-28 | 2011-11-01 | Yamaha Hatsudoki Kabushiki Kaisha | Internal combustion engine component and method for producing the same |
EP2138695A3 (en) * | 2008-06-27 | 2010-02-17 | Yamaha Hatsudoki Kabushiki Kaisha | Cylinder block, internal combustion engine, transportation apparatus, and method for producing cylinder block |
Also Published As
Publication number | Publication date |
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US20070012173A1 (en) | 2007-01-18 |
ES2310341T3 (en) | 2009-01-01 |
TW200533762A (en) | 2005-10-16 |
EP1723332A1 (en) | 2006-11-22 |
MY144677A (en) | 2011-10-31 |
CN1788149A (en) | 2006-06-14 |
ES2310341T5 (en) | 2015-07-07 |
US7412955B2 (en) | 2008-08-19 |
DE602005009149D1 (en) | 2008-10-02 |
TWI321591B (en) | 2010-03-11 |
EP1944495A1 (en) | 2008-07-16 |
EP1723332B2 (en) | 2015-06-17 |
CN100585153C (en) | 2010-01-27 |
US20100229822A1 (en) | 2010-09-16 |
EP1723332B1 (en) | 2008-08-20 |
US20080163846A1 (en) | 2008-07-10 |
CN101694187A (en) | 2010-04-14 |
ATE405740T1 (en) | 2008-09-15 |
EP2241741A1 (en) | 2010-10-20 |
US7765977B2 (en) | 2010-08-03 |
JP2010151139A (en) | 2010-07-08 |
PT1723332E (en) | 2008-09-16 |
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