WO2005009453B1 - Process for the preparation of debitterised and defatted trigonella foenum graecum as well as formulations containing the same - Google Patents

Process for the preparation of debitterised and defatted trigonella foenum graecum as well as formulations containing the same

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Publication number
WO2005009453B1
WO2005009453B1 PCT/IN2003/000253 IN0300253W WO2005009453B1 WO 2005009453 B1 WO2005009453 B1 WO 2005009453B1 IN 0300253 W IN0300253 W IN 0300253W WO 2005009453 B1 WO2005009453 B1 WO 2005009453B1
Authority
WO
WIPO (PCT)
Prior art keywords
preparation
rich
formulation
fibre
powder
Prior art date
Application number
PCT/IN2003/000253
Other languages
French (fr)
Other versions
WO2005009453A1 (en
Inventor
Ramesh Babu Potluri
Venkata Srihari Tadimalla
Subramanian Hariharakr Venkata
Ramesh Nagubandi
Original Assignee
Ramesh Babu Potluri
Venkata Srihari Tadimalla
Subramanian Hariharakr Venkata
Ramesh Nagubandi
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ramesh Babu Potluri, Venkata Srihari Tadimalla, Subramanian Hariharakr Venkata, Ramesh Nagubandi filed Critical Ramesh Babu Potluri
Priority to PCT/IN2003/000253 priority Critical patent/WO2005009453A1/en
Priority to AU2003263576A priority patent/AU2003263576A1/en
Publication of WO2005009453A1 publication Critical patent/WO2005009453A1/en
Publication of WO2005009453B1 publication Critical patent/WO2005009453B1/en

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Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Medical Informatics (AREA)
  • Medicinal Chemistry (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Epidemiology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)

Abstract

A new process has been developed for the preparation of debitterised and defatted fenugreek powder containing 4-hydroxy isoleucine and higher content of soluble fiber. The debitterised and defatted powder has been formulated to yield compositions containing fiber rich dietary supplements.

Claims

22AMENDED CLAIMS [received by the International Bureau on 29 November 2004 (29.11.04); claims 1-22 amended, claims 23-38 cancelled (3 pages)]
1. A process for the preparation of debitterised, defatted and deodorized dietary fenugreek powder containing 4-hydroxy isoleucine and is rich in soluble dietic fiber comprises; a. Treating the pulverized fenugreek powder with an organic solvent, b. Achieving the preparation by drying & grinding, c. Achieving rich in soluble fibre fraction & rich insoluble fibre fraction by drying & sieving. d. Distillation of the solvent at range of 50-100°c under reduced pressure in order to remove the moisture present in binary mixture; e. Preparation of formulation using the same.
2. A process of preparation as claimed in claim 1 , wherein the total debitterised powder contains the soluble dietary fibre in the range of 30- 40% of total weight and insoluble dietary fibre in the range of 30-40% of the total weight & 4-hydroxy isoleucine of 0.4 to 1.0 %
3. A process of preparation as claimed in claim 1 , wherein rich in soluble fibre fraction contains the soluble dietary fibre in the range of 40-50% of total weight and insoluble dietary fibre in the range of 20-30% of the total weight and 4-hydroxy isoleucine of 0.4 to 1.0%
4. A process of preparation as claimed in claim 1 , wherein rich in insoluble fibre fraction contains the soluble dietary fibre in the range of 10-20% of the total weight and insoluble dietary fibre in the range of 40-50% of the total weight & 4-hydroxy isoleucine of 0.4 to 1.0%.
5. A process of preparation as claimed in claim 1 , wherein organic solvents are, methanol, ethanol, 1-propanol and 2-propanol, preferably an alkanol.
6. A process of preparation as claimed in claim 1 , wherein alkanol contains less than 1% moisture by weight.
7. A process of preparation as claimed in claim 1 , wherein moisture content of the powder after distillation of binary mixture is preferably less than 1% by weight.
8. A process of preparation as claimed in claim 1 , wherein the extraction process is repeated until the alkanol extract gives negligible residue on evaporation.
9. A process of preparation as claimed in claim 1 , wherein the debitterised powder is dried at 40° to 100°C.
10. A process of preparation as claimed in claim 1 , wherein the rich in insoluble fibre fraction contains high protein.
11. process of preparation as claimed in claim 2, wherein the contents of the total debitterised powder are;
Figure imgf000003_0001
12. A process of preparation as claimed in claim 3, wherein the content of the rich in soluble fibre fraction are:
Figure imgf000003_0002
13. A process of preparation as claimed in claim 4, wherein the content of the rich in insoluble fibre fraction are;
Figure imgf000003_0003
24
Percentage 10 - 20% 40 - 50% SO - 70% 0.4 to 1.0% 30 - 45%
14. A process of preparation as claimed in claim 1 , wherein formulation containing the total debetterised powder or rich in soluble fibre fraction or rich in insoluble fibre fracton or combination of any, vitamins, minerals, amino acids, permitted food colours and flavours, other ingredients is prepared and is useful as fibre containing food supplement.
15. A formulation as claimed in claim 14, wherein the vitamins used are vitamin B complex, vitamin C, vitamin A, and vitamin E.
16. A formulation as claimed in claim 14, wherein the content of vitamin premix is 1.5% by weight.
17. A formulation as claimed in claim 14, wherein the minerals added are salts of chromium, copper, manganese, selenium and zinc.
18. A formulation as claimed in claim 14, wherein the content of the mineral premix is 0.5% by weight.
19. A formulation as claimed in claim 14, wherein the amino acids is L- Carnitine.
20. A formulation as claimed in claim 14, wherein the other ingredients are methyl cellulose, guargum, cinnamon powder, gymnema sylvestre extract, bitter gourd extract, permitted food colours, approved sweeteners, flavours, effervescents, tastemakers, emulsifiers and stabilizers.
21. A formulation as claimed in claim 14, wherein the content of guargum and methylcellulose together are in the range of 1 to 16 % by weight.
22. A formulation as claimed in claim 14, wherein the effervescents used are citric acid and malic acid and alkali or an alkaline earth carbonates like potassium carbonate, sodium carbonate or calcium carbonate.
PCT/IN2003/000253 2003-07-28 2003-07-28 Process for the preparation of debitterised and defatted trigonella foenum graecum as well as formulations containing the same WO2005009453A1 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
PCT/IN2003/000253 WO2005009453A1 (en) 2003-07-28 2003-07-28 Process for the preparation of debitterised and defatted trigonella foenum graecum as well as formulations containing the same
AU2003263576A AU2003263576A1 (en) 2003-07-28 2003-07-28 Process for the preparation of debitterised and defatted trigonella foenum graecum as well as formulations containing the same

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/IN2003/000253 WO2005009453A1 (en) 2003-07-28 2003-07-28 Process for the preparation of debitterised and defatted trigonella foenum graecum as well as formulations containing the same

Publications (2)

Publication Number Publication Date
WO2005009453A1 WO2005009453A1 (en) 2005-02-03
WO2005009453B1 true WO2005009453B1 (en) 2005-03-24

Family

ID=34090466

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/IN2003/000253 WO2005009453A1 (en) 2003-07-28 2003-07-28 Process for the preparation of debitterised and defatted trigonella foenum graecum as well as formulations containing the same

Country Status (2)

Country Link
AU (1) AU2003263576A1 (en)
WO (1) WO2005009453A1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101677613B (en) * 2007-04-19 2014-05-07 好侍食品株式会社 Fenugreek seed having reduced bitter taste, and method for production thereof

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008130057A1 (en) * 2007-04-19 2008-10-30 House Foods Corporation Fenugreek seed having reduced bitter taste, and method for production thereof
EP2214512A1 (en) * 2007-10-29 2010-08-11 Avesthagen Limited An organoleptically improved dietary fiber composition and a process thereof (teestar)
EP2346351B1 (en) * 2008-09-22 2019-07-03 Rubicon Research Private Limited Compositions exhibiting delayed transit through the gastrointestinal tract
EP2346353A2 (en) * 2008-10-03 2011-07-27 Rubicon Research Private Limited Compositions comprising fenugreek hydrocolloids
EP2640203B1 (en) 2010-04-06 2016-12-07 Rubicon Research Private Limited Excipient from trigonella foenum-graecum seeds and process for preparation thereof
ITPD20110179A1 (en) * 2011-05-27 2012-11-28 Sanypet Spa EDIBLE COMPOSITION FOR THE CONTROL OF DISGLICEMIA IN ANIMALS AND PRODUCT FOR THE FEEDING OF ANIMALS CONTAINING SUCH COMPOSITION

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5658571A (en) * 1994-11-24 1997-08-19 Vitamed Remedies Private Limited Process for extraction and use of fenugreek (Trigonella foenumgraecum)
CA2206157C (en) * 1997-05-26 2000-06-13 Cheng, Peter Method of extraction of commercially valuable fractions of fenugreek
IN192689B (en) * 2000-02-14 2004-05-15 Rao Gariimella Bhaskar Dr

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101677613B (en) * 2007-04-19 2014-05-07 好侍食品株式会社 Fenugreek seed having reduced bitter taste, and method for production thereof

Also Published As

Publication number Publication date
WO2005009453A1 (en) 2005-02-03
AU2003263576A1 (en) 2005-02-14

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