WO2003089692A3 - Methods for controlling crystal growth, crystallization, structures and phases in materials and systems - Google Patents

Methods for controlling crystal growth, crystallization, structures and phases in materials and systems Download PDF

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Publication number
WO2003089692A3
WO2003089692A3 PCT/US2003/008904 US0308904W WO03089692A3 WO 2003089692 A3 WO2003089692 A3 WO 2003089692A3 US 0308904 W US0308904 W US 0308904W WO 03089692 A3 WO03089692 A3 WO 03089692A3
Authority
WO
WIPO (PCT)
Prior art keywords
crystallization
systems
spectral energy
reaction vessel
conditioning
Prior art date
Application number
PCT/US2003/008904
Other languages
French (fr)
Other versions
WO2003089692A2 (en
Inventor
Bentley J Blum
Juliana H J Brooks
Mark G Mortenson
Original Assignee
Berkshire Lab Inc
Bentley J Blum
Juliana H J Brooks
Mark G Mortenson
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Berkshire Lab Inc, Bentley J Blum, Juliana H J Brooks, Mark G Mortenson filed Critical Berkshire Lab Inc
Priority to CA002480003A priority Critical patent/CA2480003A1/en
Priority to US10/508,462 priority patent/US7972390B2/en
Priority to EP03746926A priority patent/EP1492603A4/en
Priority to JP2003586399A priority patent/JP2005524595A/en
Priority to AU2003251288A priority patent/AU2003251288A1/en
Publication of WO2003089692A2 publication Critical patent/WO2003089692A2/en
Publication of WO2003089692A3 publication Critical patent/WO2003089692A3/en
Priority to US13/110,456 priority patent/US8734535B2/en

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Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/0005Reversible uptake of hydrogen by an appropriate medium, i.e. based on physical or chemical sorption phenomena or on reversible chemical reactions, e.g. for hydrogen storage purposes ; Reversible gettering of hydrogen; Reversible uptake of hydrogen by electrodes
    • C01B3/001Reversible uptake of hydrogen by an appropriate medium, i.e. based on physical or chemical sorption phenomena or on reversible chemical reactions, e.g. for hydrogen storage purposes ; Reversible gettering of hydrogen; Reversible uptake of hydrogen by electrodes characterised by the uptaking medium; Treatment thereof
    • C01B3/0031Intermetallic compounds; Metal alloys; Treatment thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/005Selection of auxiliary, e.g. for control of crystallisation nuclei, of crystal growth, of adherence to walls; Arrangements for introduction thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0063Control or regulation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/12Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
    • B01J19/121Coherent waves, e.g. laser beams
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/12Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
    • B01J19/122Incoherent waves
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/12Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
    • B01J19/122Incoherent waves
    • B01J19/127Sunlight; Visible light
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/02Preparation of oxygen
    • C01B13/0203Preparation of oxygen from inorganic compounds
    • C01B13/0211Peroxy compounds
    • C01B13/0214Hydrogen peroxide
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/0005Reversible uptake of hydrogen by an appropriate medium, i.e. based on physical or chemical sorption phenomena or on reversible chemical reactions, e.g. for hydrogen storage purposes ; Reversible gettering of hydrogen; Reversible uptake of hydrogen by electrodes
    • C01B3/001Reversible uptake of hydrogen by an appropriate medium, i.e. based on physical or chemical sorption phenomena or on reversible chemical reactions, e.g. for hydrogen storage purposes ; Reversible gettering of hydrogen; Reversible uptake of hydrogen by electrodes characterised by the uptaking medium; Treatment thereof
    • C01B3/0026Reversible uptake of hydrogen by an appropriate medium, i.e. based on physical or chemical sorption phenomena or on reversible chemical reactions, e.g. for hydrogen storage purposes ; Reversible gettering of hydrogen; Reversible uptake of hydrogen by electrodes characterised by the uptaking medium; Treatment thereof of one single metal or a rare earth metal; Treatment thereof
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B5/00Water
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D3/00Halides of sodium, potassium or alkali metals in general
    • C01D3/04Chlorides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D3/00Halides of sodium, potassium or alkali metals in general
    • C01D3/10Bromides
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12NMICROORGANISMS OR ENZYMES; COMPOSITIONS THEREOF; PROPAGATING, PRESERVING, OR MAINTAINING MICROORGANISMS; MUTATION OR GENETIC ENGINEERING; CULTURE MEDIA
    • C12N13/00Treatment of microorganisms or enzymes with electrical or wave energy, e.g. magnetism, sonic waves
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30Hydrogen technology
    • Y02E60/32Hydrogen storage

Abstract

This invention relates to novel methods for affecting, controlling and/or directing various crystal formation, structure formation or phase formation/phase change reaction pathways or systems by exposing one or more components in a holoreaction system to at least one spectral energy pattern. In a first aspect of the invention, at least one spectral energy pattern can be applied to a crystallization reaction system. In a second aspect of the invention, at lest one spectral energy conditioning pattern can be applied to a conditioning reaction system. The spectral energy conditioning pattern can, for example, be applied at a separate location from the reaction vessel (e.g., in a conditioning reaction vessel) or can be applied in (or to) the reaction vessel, but prior to other (or all) crystallization reaction system participants being introduced into the reaction vessel.
PCT/US2003/008904 2002-03-21 2003-03-21 Methods for controlling crystal growth, crystallization, structures and phases in materials and systems WO2003089692A2 (en)

Priority Applications (6)

Application Number Priority Date Filing Date Title
CA002480003A CA2480003A1 (en) 2002-03-21 2003-03-21 Methods for controlling crystal growth, crystallization, structures and phases in materials and systems
US10/508,462 US7972390B2 (en) 2002-03-21 2003-03-21 Methods for controlling crystal growth, crystallization, structures and phases in materials and systems
EP03746926A EP1492603A4 (en) 2002-03-21 2003-03-21 Methods for controlling crystal growth, crystallization, structures and phases in materials and systems
JP2003586399A JP2005524595A (en) 2002-03-21 2003-03-21 Method for controlling crystal growth, crystallization, structure and phase in materials and systems
AU2003251288A AU2003251288A1 (en) 2002-03-21 2003-03-21 Methods for controlling crystal growth, crystallization, structures and phases in materials and systems
US13/110,456 US8734535B2 (en) 2002-03-21 2011-05-18 Methods for controlling crystal growth, crystallization, structures and phases in materials and systems

Applications Claiming Priority (8)

Application Number Priority Date Filing Date Title
US36675502P 2002-03-21 2002-03-21
US60/366,755 2002-03-21
US40325102P 2002-08-13 2002-08-13
US40322502P 2002-08-13 2002-08-13
US60/403,251 2002-08-13
US60/403,225 2002-08-13
US43922303P 2003-01-10 2003-01-10
US60/439,223 2003-01-10

Related Child Applications (2)

Application Number Title Priority Date Filing Date
US10508462 A-371-Of-International 2003-03-21
US13/110,456 Division US8734535B2 (en) 2002-03-21 2011-05-18 Methods for controlling crystal growth, crystallization, structures and phases in materials and systems

Publications (2)

Publication Number Publication Date
WO2003089692A2 WO2003089692A2 (en) 2003-10-30
WO2003089692A3 true WO2003089692A3 (en) 2004-07-08

Family

ID=29255570

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2003/008904 WO2003089692A2 (en) 2002-03-21 2003-03-21 Methods for controlling crystal growth, crystallization, structures and phases in materials and systems

Country Status (5)

Country Link
EP (1) EP1492603A4 (en)
JP (2) JP2005524595A (en)
AU (1) AU2003251288A1 (en)
CA (1) CA2480003A1 (en)
WO (1) WO2003089692A2 (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
HUE053226T2 (en) 2007-07-11 2021-06-28 Clene Nanomedicine Inc Continuous method for treating liquids and manufacturing certain constituents
CA2749805C (en) 2009-01-15 2017-05-09 Gr Intellectual Reserve, Llc Continuous, semicontinuous and batch methods for treating liquids and manufacturing certain constituents (e.g., nanoparticles) in liquids, apparatuses and nanoparticles and nanoparticle/liquid solution(s) and colloids resulting therefrom
EP4180105A1 (en) * 2020-07-13 2023-05-17 NGK Insulators, Ltd. Refining method
CN116443896B (en) * 2023-03-28 2023-11-14 天津大学 Large-particle spherical non-hydrated inorganic salt and preparation method and application thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3933573A (en) * 1973-11-27 1976-01-20 The United States Of America As Represented By The Secretary Of The Air Force Aluminum nitride single crystal growth from a molten mixture with calcium nitride
US5062862A (en) * 1986-11-29 1991-11-05 Grasso's Koninklijke Machinefabrieken N.V. Process and apparatus for recovering a pure substance from a liquid mixture by crystallization

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5360329A (en) * 1957-10-22 1994-11-01 Lemelson Jerome H Molding/extrusion apparatus with temperature and flow control
JPH0717477B2 (en) * 1989-03-15 1995-03-01 シャープ株式会社 Epitaxial growth method of compound semiconductor
FI901415A0 (en) * 1989-10-26 1990-03-21 Nippon Kokan Kk ANORDINATION FOR FRAMING A KISELENKRISTALLER.
JPH08293495A (en) * 1995-04-21 1996-11-05 Hitachi Ltd Inorganic material manufacturing solution and method of manufacturing inorganic film
JP2958448B2 (en) * 1997-05-20 1999-10-06 名古屋工業大学長 Method and apparatus for manufacturing compound semiconductor
JP2002504023A (en) * 1997-06-18 2002-02-05 バークシャー・ラボラトリーズ・インコーポレーテッド Spectrum catalyst
JP3502905B2 (en) * 2000-08-28 2004-03-02 大阪大学長 Method of forming organic single crystal
JP4139888B2 (en) * 2002-02-12 2008-08-27 国立大学法人群馬大学 Manufacturing method of macromolecular crystal and manufacturing apparatus used therefor

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3933573A (en) * 1973-11-27 1976-01-20 The United States Of America As Represented By The Secretary Of The Air Force Aluminum nitride single crystal growth from a molten mixture with calcium nitride
US5062862A (en) * 1986-11-29 1991-11-05 Grasso's Koninklijke Machinefabrieken N.V. Process and apparatus for recovering a pure substance from a liquid mixture by crystallization

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See also references of EP1492603A4 *

Also Published As

Publication number Publication date
AU2003251288A1 (en) 2003-11-03
JP2012136424A (en) 2012-07-19
JP2005524595A (en) 2005-08-18
WO2003089692A2 (en) 2003-10-30
CA2480003A1 (en) 2003-10-30
AU2003251288A8 (en) 2003-11-03
EP1492603A4 (en) 2005-07-06
JP5632400B2 (en) 2014-11-26
EP1492603A2 (en) 2005-01-05

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