WO2003060044A1 - Procede d'extraction d'huiles vegetales et dispositif de mise en oeuvre de ce procede - Google Patents

Procede d'extraction d'huiles vegetales et dispositif de mise en oeuvre de ce procede Download PDF

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Publication number
WO2003060044A1
WO2003060044A1 PCT/RU2002/000553 RU0200553W WO03060044A1 WO 2003060044 A1 WO2003060044 A1 WO 2003060044A1 RU 0200553 W RU0200553 W RU 0200553W WO 03060044 A1 WO03060044 A1 WO 03060044A1
Authority
WO
WIPO (PCT)
Prior art keywords
ρasτvορiτelya
solvent
eκsτρaκτορa
fact
unit
Prior art date
Application number
PCT/RU2002/000553
Other languages
English (en)
Russian (ru)
Inventor
Vitaly Nikolaevich Kuznetsov
Elvina Ivanovna Ivanova
Vladimir Vasilevich Ivantsov
Original Assignee
Vitaly Nikolaevich Kuznetsov
Elvina Ivanovna Ivanova
Vladimir Vasilevich Ivantsov
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Vitaly Nikolaevich Kuznetsov, Elvina Ivanovna Ivanova, Vladimir Vasilevich Ivantsov filed Critical Vitaly Nikolaevich Kuznetsov
Priority to AU2002362213A priority Critical patent/AU2002362213A1/en
Publication of WO2003060044A1 publication Critical patent/WO2003060044A1/fr

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/10—Production of fats or fatty oils from raw materials by extracting
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0215—Solid material in other stationary receptacles
    • B01D11/0223—Moving bed of solid material
    • B01D11/0226—Moving bed of solid material with the general transport direction of the solids parallel to the rotation axis of the conveyor, e.g. worm
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0215—Solid material in other stationary receptacles
    • B01D11/0223—Moving bed of solid material
    • B01D11/023—Moving bed of solid material using moving bands, trays fixed on moving transport chains
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0215—Solid material in other stationary receptacles
    • B01D11/0223—Moving bed of solid material
    • B01D11/0242—Moving bed of solid material in towers, e.g. comprising contacting elements
    • B01D11/0246—Moving bed of solid material in towers, e.g. comprising contacting elements comprising rotating means

Definitions

  • the invention is subject to oil industry, in particular to the production of vegetable oils by means of the extraction of organic products.
  • the method of extracting oils from vegetable raw materials is known, according to a quick-growing, raw raw material that processes the product.
  • the processing is carried out with the use of a weak concentrated concentrate from the factory, which was obtained at the second stage of the process.
  • the processing is carried out using a pure manufacturer.
  • the processing at the second stage is carried out in the loading mode with the cyclic discharge of the distributor and the discharge after each delivery (see, on the contrary, on the other hand, ⁇ ned ⁇ s ⁇ a ⁇ am izves ⁇ n ⁇ g ⁇ s ⁇ s ⁇ ba m ⁇ zhn ⁇ ⁇ nes ⁇ i vys ⁇ uyu ⁇ ntsen ⁇ atsiyu ⁇ as ⁇ v ⁇ i ⁇ elya in ⁇ e ⁇ s ⁇ agi ⁇ vann ⁇ m ma ⁇ e ⁇ iale, ch ⁇ d ⁇ lni ⁇ eln ⁇ ⁇ ebue ⁇ ⁇ imeneniya s ⁇ etsialny ⁇ a ⁇ a ⁇ a ⁇ v for ⁇ g ⁇ n ⁇ i and ⁇ e ⁇ u ⁇ e ⁇ atsii ⁇ as ⁇ v ⁇ i ⁇ elya.
  • the invention is directed to the creation of such a method of extracting vegetable oils and devices for its use, which would increase the loss of volume.
  • the processed material is cooled by the supply of the oil and the medium is supplied
  • the posed problem is solved due to the fact that by heating the hood out of it, it sucks away the vapor from the solvent, which makes it non-corrosive and refuses to
  • the oil is extracted in a pre-charge mode and the miscella is drained.
  • the extracted material is supplied to a direct extract of oil for an oil.
  • you place an electrically absorbable material on the bottom of the product first turn on the product with a fluffy discharge agent. Then, the removable internal area of the direct exhaust media is used to increase the volume of the inlet to the inlet of the inlet to the
  • the distributor is in the form of a fog.
  • the industrial component is heated and the product is supplied by the manufacturer from a non-integrated vehicle
  • the dispensers of the food processor are generated by the direct dispenser of the liquid in the zone of heating of the mains.
  • an agitated gas inlet is produced by the agitated material. After the export of the product from the consumer, they carry out the unloading of the product from the consumer.
  • the material that is being processed can be cooled by the reflux of the product. When this is done, they arrange the appropriate transfer of saturated vapor to the cooling zone of the processed material.
  • the steams of the distributor which are then compensated, may be disconnected. After compensating the distributor, the condenser will return to the portable compressor.
  • the flow rate of the miscella into the discharge can be increased. Then, in the flow of miscella, they produce local perturbations.
  • Example of implementation of a method The material being consumed in the form of a soybean product is fed into the unloading crate, which is moved downward when it is in transit and is saturated with it. Upon further placement, the material being exported is launched into an empty type, where the operation is carried out at a temperature of 45%.
  • the type of product is partially degreased with a 30-35% concentration of the product, and the product is in the process P ⁇ sle e ⁇ s ⁇ a ⁇ tsii oil in ⁇ iv ⁇ chn ⁇ m e ⁇ s ⁇ a ⁇ e on eg ⁇ vy ⁇ de ⁇ luchayu ⁇ g ⁇ vy sh ⁇ , maslichn ⁇ s ⁇ ⁇ g ⁇ s ⁇ s ⁇ avlyae ⁇ 1,2- 1,8% s ⁇ de ⁇ zhanie therein ⁇ as ⁇ v ⁇ i ⁇ elya not ⁇ evyshae ⁇ 0,09-0,15% and ⁇ em ⁇ e ⁇ a ⁇ u ⁇ a ⁇ g ⁇ s ⁇ s ⁇ avlyae ⁇ 78-85 ° C.
  • FIG. 1 device for extracting vegetable oils fig. 2 One of the variants of the operational execution of the transfer unit and the FIG. 3 - One of the variants of the operational design of the transfer unit.
  • the lower part of the unit is equipped with an unloading unit 3, it is connected to a fully-equipped unit, it is supplied with a free-load unit
  • the extractor 5 was loaded with a built-in internal version of the drive, which could not be worn out.
  • the extract 5 of the loading type contains the application 7 for the recycling of the miscella, which may be performed, for example, as a pump.
  • 11 may be used, for example, a screw barrel with displaced blades.
  • a simple product 10 is provided with a free download area, and there are 11
  • a simple extract of 10 is used for loading 12 for downloading 13, but, for example, it may be, for example.
  • Liquid dispenser 16 which may be completed, for example, in the form of a nozzle.
  • the appliance 17 is used for heating the heater, there is a large amount of blackout ⁇ aib ⁇ lee ⁇ ed ⁇ ch ⁇ i ⁇ elnym yavlyae ⁇ sya • ⁇ a ⁇ y va ⁇ ian ⁇ ⁇ ns ⁇ u ⁇ ivn ⁇ g ⁇ vy ⁇ lneniya ⁇ is ⁇ s ⁇ bleniya 17 nag ⁇ eva ⁇ as ⁇ v ⁇ i ⁇ elya, ⁇ i ⁇ m ⁇ n vy ⁇ lnen as ⁇ ubash ⁇ i with ⁇ a ⁇ ub ⁇ ami s ⁇ ve ⁇ s ⁇ venn ⁇ for ⁇ dv ⁇ da and ⁇ v ⁇ da ⁇ e ⁇ l ⁇ n ⁇ si ⁇ elya ( ⁇ a ⁇ a).
  • Devices for the extraction of vegetable oils can be carried out with the device for processing and the compensation of the consumer and the resulting condensate
  • a load node (extractor 5 of the load type)
  • any known mechanism is used ⁇ aib ⁇ lee ⁇ ed ⁇ ch ⁇ i ⁇ elnym yavlyae ⁇ sya ⁇ a ⁇ y va ⁇ ian ⁇ ⁇ ns ⁇ u ⁇ ivn ⁇ g ⁇ vy ⁇ lneniya ⁇ ans ⁇ i ⁇ uyuscheg ⁇ me ⁇ anizma b, ⁇ i ⁇ m ⁇ n vy ⁇ lnen as shne ⁇ v ⁇ g ⁇ ⁇ ans ⁇ e ⁇ a ( ⁇ ig. 1) l ⁇ as ⁇ i ⁇ g ⁇ m ⁇ gu ⁇ by ⁇ ⁇ e ⁇ i ⁇ vany.
  • the transport mechanism of the 6 transfer unit can be made in the form of a screed (Fig. 2).
  • the expanding mechanism of the 6th transfer unit can be made in the form of a ribbon screw conveyor (Fig. 3).
  • Dispenser 7 for recycling miscella may include a splitter 25, designed to separate the waste from the process of excluding the body from the process. One is empty in capacity 26 for discharging the miscella, and the other is returned with the use of inlet 7 for recycling the miscella in the extract 5.
  • the operating mechanism 6 displaces the process material in the direct part of the machine 10, where the machine is in the process of operating P ⁇ i ⁇ e ⁇ emeschenii e ⁇ s ⁇ agi ⁇ uem ⁇ g ⁇ ma ⁇ e ⁇ iala ⁇ ⁇ l ⁇ s ⁇ i ⁇ iv ⁇ chn ⁇ g ⁇ e ⁇ s ⁇ a ⁇ a 10 ma ⁇ e ⁇ ial first ⁇ shae ⁇ sya s ⁇ e ⁇ ayuschim sve ⁇ u ⁇ as ⁇ v ⁇ i ⁇ elem and za ⁇ em ⁇ s ⁇ u ⁇ ae ⁇ in z ⁇ nu where ⁇ ve ⁇ n ⁇ s ⁇ chas ⁇ its e ⁇ s ⁇ agi ⁇ uem ⁇ g ⁇ ma ⁇ e ⁇ iala ⁇ shayu ⁇ ⁇ u ⁇ em
  • Spraying a fuel dispenser in the form of a mist In case of a solution, the distributor is equally distributed between all particles of the absorbable material. In the last stage, the main process wastewater is processed in a 10-hour process, 15 If a liquid is spilled into the appliance, it will experience 17 heating and generating power to the vaporizer.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Fats And Perfumes (AREA)
  • Exposure And Positioning Against Photoresist Photosensitive Materials (AREA)

Abstract

Cette invention concerne un procédé d'extraction d'huiles végétales consistant à extraire l'huile au moyen d'un solvant dans un extracteur à écoulement, à distiller le solvant, à chauffer le tourteau d'extraction, à asperger le matériau extrait avec le solvant et à créer une vanne de gaz au niveau de la sortie de l'extracteur à contre-courant au moyen du matériau extrait. Il convient d'effectuer une extraction préalable dans un extracteur à immersion avant de procéder à l'extraction de l'huile dans l'extracteur à contre-courant. Lors de l'extraction principale, on asperge à nouveau le matériau avec du solvant vaporisé de manière à former un brouillard. Des vapeurs de solvant surchauffées sont générées dans l'extracteur à contre-courant. Le matériau est imprégné de vapeurs saturées de solvant avant d'être soumis à une extraction supplémentaire. Le dispositif d'extraction d'huiles végétales de la présente invention comprend une colonne de chargement, une unité de transfert composée d'un extracteur à immersion et d'un extracteur à contre-courant. Cet extracteur à contre-courant est équipé d'un élément de chauffage, d'une unité principale ainsi que d'unités supplémentaires d'acheminement du solvant. La colonne de chargement est équipée d'un accessoire d'évacuation servant à évacuer les vapeurs de solvant. Le mécanisme de transport de l'unité de surcharge et son boîtier constituent un canal permettant le passage des vapeurs de solvant.
PCT/RU2002/000553 2001-12-26 2002-12-25 Procede d'extraction d'huiles vegetales et dispositif de mise en oeuvre de ce procede WO2003060044A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AU2002362213A AU2002362213A1 (en) 2001-12-26 2002-12-25 Method for extracting vegetable oils and device for carrying out said method

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
RU2001135097/13A RU2210589C1 (ru) 2001-12-26 2001-12-26 Способ экстракции растительных масел и устройство для его осуществления
RU2001135097 2001-12-26

Publications (1)

Publication Number Publication Date
WO2003060044A1 true WO2003060044A1 (fr) 2003-07-24

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PCT/RU2002/000553 WO2003060044A1 (fr) 2001-12-26 2002-12-25 Procede d'extraction d'huiles vegetales et dispositif de mise en oeuvre de ce procede

Country Status (3)

Country Link
AU (1) AU2002362213A1 (fr)
RU (1) RU2210589C1 (fr)
WO (1) WO2003060044A1 (fr)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2005100518A1 (fr) * 2004-04-14 2005-10-27 Stavrulov, Igor Anatolievich Procede d'extraction d'huile vegetale et extracteur submersible de type a contre-courant pour mettre en oeuvre ce procede
CN103691148A (zh) * 2013-12-20 2014-04-02 济宁金百特生物机械有限公司 一种连续逆流提取生产线

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10557104B2 (en) * 2017-12-19 2020-02-11 Botanex Intelletual Property LLC Modular, mobile, and automated solvent extraction and distillation systems, and methods of using the same
CN110387289A (zh) * 2018-04-16 2019-10-29 广西壮族自治区林业科学研究院 一种提取植物芳香油的装置及其工艺方法
CN111659156B (zh) * 2020-06-18 2022-03-25 徐州生物工程职业技术学院 一种中药连续逆流提取方法和设备

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB665857A (en) * 1948-12-08 1952-01-30 Sugar Extraction Inc Method and apparatus for the elution of sugar and/or juices from sliced beets and other extractable materials
RU2051171C1 (ru) * 1993-03-17 1995-12-27 Андрей Иванович Соболев Линия для получения масла из кофейного шлама и отходов производства кофе
RU2091455C1 (ru) * 1994-09-27 1997-09-27 Всероссийский научно-исследовательский институт консервной и овощесушильной промышленности Противоточный экстрактор для виноградных выжимок
RU2166533C2 (ru) * 1999-06-23 2001-05-10 Иванова Эльвина Ивановна Способ экстракции растительных масел и устройство для его осуществления

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB665857A (en) * 1948-12-08 1952-01-30 Sugar Extraction Inc Method and apparatus for the elution of sugar and/or juices from sliced beets and other extractable materials
RU2051171C1 (ru) * 1993-03-17 1995-12-27 Андрей Иванович Соболев Линия для получения масла из кофейного шлама и отходов производства кофе
RU2091455C1 (ru) * 1994-09-27 1997-09-27 Всероссийский научно-исследовательский институт консервной и овощесушильной промышленности Противоточный экстрактор для виноградных выжимок
RU2166533C2 (ru) * 1999-06-23 2001-05-10 Иванова Эльвина Ивановна Способ экстракции растительных масел и устройство для его осуществления

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
SERGEEV A.G.: "Rukovodstvo po tekhnologii polucheniya i pererabotki rastitelnykh masel i zhirov", VNIIZH, vol. 1, no. 2, 1974, LENINGRAD, pages 70 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2005100518A1 (fr) * 2004-04-14 2005-10-27 Stavrulov, Igor Anatolievich Procede d'extraction d'huile vegetale et extracteur submersible de type a contre-courant pour mettre en oeuvre ce procede
CN103691148A (zh) * 2013-12-20 2014-04-02 济宁金百特生物机械有限公司 一种连续逆流提取生产线
CN103691148B (zh) * 2013-12-20 2015-12-16 济宁金百特生物机械有限公司 一种连续逆流提取生产线

Also Published As

Publication number Publication date
AU2002362213A1 (en) 2003-07-30
RU2001135097A (ru) 2004-03-27
RU2210589C1 (ru) 2003-08-20

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