WO2003029748A1 - Frequency diversity remote controlled initiation system - Google Patents

Frequency diversity remote controlled initiation system Download PDF

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Publication number
WO2003029748A1
WO2003029748A1 PCT/ZA2002/000151 ZA0200151W WO03029748A1 WO 2003029748 A1 WO2003029748 A1 WO 2003029748A1 ZA 0200151 W ZA0200151 W ZA 0200151W WO 03029748 A1 WO03029748 A1 WO 03029748A1
Authority
WO
WIPO (PCT)
Prior art keywords
signal
frequency
detonators
detonator
high frequency
Prior art date
Application number
PCT/ZA2002/000151
Other languages
French (fr)
Inventor
Erich Nicol Meyer
Charles Michael Lownds
Original Assignee
Smi Technology (Pty) Limited
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Smi Technology (Pty) Limited filed Critical Smi Technology (Pty) Limited
Priority to US10/489,772 priority Critical patent/US7327550B2/en
Priority to CA2460966A priority patent/CA2460966C/en
Priority to EP02773980A priority patent/EP1432959B1/en
Priority to BRPI0213031A priority patent/BRPI0213031B1/en
Priority to DE60216784T priority patent/DE60216784T2/en
Priority to AU2002336727A priority patent/AU2002336727B2/en
Publication of WO2003029748A1 publication Critical patent/WO2003029748A1/en
Priority to ZA2004/02051A priority patent/ZA200402051B/en

Links

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F42AMMUNITION; BLASTING
    • F42DBLASTING
    • F42D1/00Blasting methods or apparatus, e.g. loading or tamping
    • F42D1/04Arrangements for ignition
    • F42D1/045Arrangements for electric ignition
    • F42D1/05Electric circuits for blasting
    • F42D1/055Electric circuits for blasting specially adapted for firing multiple charges with a time delay

Definitions

  • THIS invention relates to electric and electronic blasting systems for
  • detonators a first signal comprising a first frequency and wherein each
  • detonator comprises logic circuitry driven by a second signal having a
  • the second signal may be a clock signal which may be derived from the
  • the first signal may comprise a carrier signal having the first frequency.
  • the first frequency may fall in the range 200 MHz to 100 GHz.
  • modulation technique such as amplitude modulation, frequency
  • Each detonator may comprise a charge storage device which is charged
  • the storage device may comprise a capacitor. In other embodiments the
  • charge storage devices may be charged via a physical conductive link
  • a common source of charge such as a battery.
  • the clock signal may be derived by dividing the frequency of the first
  • the clock frequency may be between 1
  • kHz and 15kHz typically between 4 kHz to 5 kHz.
  • the divider means may be common to at least some of the detonators
  • divider means may be connected to a receiver forming part of
  • Each detonator may comprise an electric or electronic initiator
  • the low frequency part may comprise a phase-locked loop and local
  • An input of the logic circuitry may be connected via a data line to an
  • circuitry may be programmable by delay time data in the data signal to
  • the divider means may divide the first frequency by about five
  • the high and low frequency parts may be integrated on a single chip. In other embodiments, the high frequency and low frequency parts may
  • the first or high frequency part may
  • the detonator is located, and the second part may be located towards a
  • the wireless link may be provided between a remote blast controller
  • the antenna may be a line source, for example the
  • antenna may comprise a cable running the length of a long relatively
  • the RF transmitter may be connected to the blast controller by a
  • a second wireless link may be
  • each detonator forming part of each detonator.
  • the second signal is preferably derived from the first signal by dividing
  • the initiator for a detonator, the initiator comprising:-
  • a high frequency part comprising a radio frequency receiver stage
  • figure 1 is a basic block diagram of a first embodiment of an
  • figure 2 is a block diagram of an electronic initiator according to
  • figure 3 is a basic block diagram of a second embodiment of the
  • figure 4 is a basic block diagram of a third embodiment of the
  • figure 5 is a basic block diagram of a fourth embodiment of the
  • figure 6 is a basic block diagram of a fifth embodiment of the
  • the system comprises a blast controller 12 comprising a radio frequency
  • transmitter 14 connected to an antenna 16.
  • the transmitter in use,
  • the digital data is generated by a data generator 20 and intended for communications with and more
  • the system further comprises a plurality of similar electronic detonators
  • detonator 22.1 comprises an electronic initiator 24 and an explosive
  • the detonator 22.1 is located in one hole 28.1 of a plurality
  • the initiator 24 is connected via a
  • Antenna 32 is connected via lead conductor 30 to a radio
  • the rectifier 34 is connected to a charge storage device in the form of a
  • the output is also connected to level detection circuit 38.
  • level detection circuit is connected to a divider circuit 40 for dividing
  • the signal with lower frequency f 2 is used to drive
  • a resulting low frequency output signal s 2 (f 2 ) of the local oscillator is used as clock
  • the logic circuitry 44 drives a switch
  • circuit 46 to connect a fuse 48 to the capacitor 36 via power line 50
  • delay time is typically programmed into the logic circuitry 44 by delay
  • circuits 34 to 46 may be integrated on a single chip.
  • circuits derive electrical power from capacitor 36, via power line 52.
  • An output of level detection circuit 38 is connected via data line 54 to a
  • the digital data is data relating to the aforementioned delay time
  • the frequency of the carrier may be between 200 MHz and 100 GHz,
  • a divisor of the divider 40 is typically equal to 10 5 .
  • the frequency f 2 may be in the order of 4 kHz.
  • the data may be modulated on the
  • the high frequency f, of the carrier is used to charge
  • FIG 3 there is shown a second embodiment of the system.
  • controller 12 broadcasts the signal having carrier frequency f to a high
  • the high frequency part 60 of a split initiator 61 .
  • initiator including at least the logic circuitry 44, switch and fuse.
  • high frequency part may in use be located in a mouth or collar region of
  • controller 12 is of split configuration.
  • the data generator is housed in a
  • first part 12.1 and the transmitter 14 forms part of a separate second
  • the first and second parts are spaced a distance d, of typically between
  • the second part 12.2 is spaced a
  • FIG 5 there is shown a blast controller 12 transmitting via a
  • central divider 80 connected via a receiver to directional antenna 82
  • the signal s 2 is transmitted via physical conductive link 84 to detonators
  • each detonator comprises an initiator
  • the blast controller 12 is of split configuration comprising a first or master part 12.1 and a second slave
  • the slave part 12.2 comprises a single
  • antenna 92 for communications with the master part via wireless link 93
  • the slave part 12.2 hence
  • transceiver 94 comprises a transceiver 94 and single antenna 92 is connectable by an
  • the first signal 18 may not be utilized to energize
  • the detonators and may comprise a carrier having the first high
  • the data signal is
  • the data signal may hence comprise address data for
  • the detonators may be any suitable detonators hereinbefore described.
  • the detonators may be any suitable detonators
  • detonators may be charged via a physical link such as link 84 shown in
  • Each detonator may still comprise an RF receiver stage for receiving the
  • the RF link and processing by the detonators of the delay time data may
  • the first signal 18 may be utilized both to

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  • Engineering & Computer Science (AREA)
  • General Engineering & Computer Science (AREA)
  • Selective Calling Equipment (AREA)
  • Radio Transmission System (AREA)

Abstract

A blasting system (10) comprises a wireless link (18) between a blast controller (12) and a plurality of electronic detonators (22.1 to 22.n). Each detonator comprises a respective electronic initiator (24) and an explosive charge (26). Charge storage devices of the initiators are chargeable by a carrier of a first signal having a first frequency (f1) in the order of 400 MHz - 500 MHz and which is broadcasted by the blast controller. Each initiator further comprises logic circuitry driven by a clock signal which is derived from the first signal and having a clock frequency of about 4 kHz, which is substantially less than the first frequency.

Description

FREQUENCY DIVERSITY REMOTE CONTROLLED INITIATION SYSTEM
TECHNICAL FIELD
THIS invention relates to electric and electronic blasting systems for
mining applications, detonators and initiators therefor.
SUMMARY OF THE INVENTION
According to the invention there is provided a blasting system
comprising a wireless link for broadcasting towards a plurality of
detonators a first signal comprising a first frequency and wherein each
detonator comprises logic circuitry driven by a second signal having a
second frequency which is substantially lower than the first frequency.
The second signal may be a clock signal which may be derived from the
first signal.
The first signal may comprise a carrier signal having the first frequency.
The first frequency may fall in the range 200 MHz to 100 GHz. The first
frequency is preferably about 400 MHz to 500 MHz. The first signal
may further comprise a data signal modulated on the carrier signal. Any
suitable modulation technique such as amplitude modulation, frequency
modulation, pulse-width modulation, pulse-code modulation etc may be
utilized. Each detonator may comprise a charge storage device which is charged
while the detonators are energized utilizing the first signal. The charge
storage device may comprise a capacitor. In other embodiments the
charge storage devices may be charged via a physical conductive link
from a common source of charge, such as a battery.
The clock signal may be derived by dividing the frequency of the first
signal down by divider means. The clock frequency may be between 1
kHz and 15kHz, typically between 4 kHz to 5 kHz.
The divider means may be common to at least some of the detonators
and the divider means may be connected to a receiver forming part of
the wireless link as well as to said at least some of the detonators by a
physical conductive link.
In other embodiments the divider means may comprise a respective
divider circuit for each detonator.
Each detonator may comprise an electric or electronic initiator
comprising a high frequency part and a low frequency part, the high
frequency part comprising an RF receiver stage, said charge storage device connected to the RF receiver stage and said respective divider
circuit.
The low frequency part may comprise a phase-locked loop and local
oscillator connected to an output of said respective divider circuit and
providing the clock signal to the logic circuitry forming part of the low
frequency part.
An input of the logic circuitry may be connected via a data line to an
output of a level detection circuit in the high frequency part. The logic
circuitry may be programmable by delay time data in the data signal to
operate a switch of the initiator to cause charge on the charge storage
device to be dumped into a fuse of the detonator, a delay time, which is
associated with the delay time data, after a fire signal.
The divider means may divide the first frequency by about five
orders, so that the frequency of the clock signal is in the order of 1
kHz - 1 5 kHz.
The high and low frequency parts may be integrated on a single chip. In other embodiments, the high frequency and low frequency parts may
be split into separate first and second parts respectively and the output
of the divider circuit in the first part may be connected by a physical
conductive link to the second part. The first or high frequency part may
be located towards a mouth or collar of a blast hole wherein the
detonator is located, and the second part may be located towards a
bottom region of the hole.
The wireless link may be provided between a remote blast controller
comprising an RF transmitter and an antenna located in close proximity
to the blast controller on the one hand and the plurality of detonators on
the other hand.
In other embodiments the wireless link may be provided between said
plurality of detonators and an RF transmitter located in closer proximity
to the detonators. The antenna may be a line source, for example the
antenna may comprise a cable running the length of a long relatively
narrow blast site.
The RF transmitter may be connected to the blast controller by a
physical conductive link. Alternatively, a second wireless link may be
provided between the RF transmitter and the remote blast controller. Also included within the scope of the present invention is a method of
operating a blasting system comprising the steps of:
broadcasting a first high frequency RF signal to each of a plurality
of detonators; and
- utilizing a second low frequency signal for driving logic circuitry
forming part of each detonator.
The second signal is preferably derived from the first signal by dividing
down the frequency of the first signal.
Yet further included within the scope of the present invention is an
initiator for a detonator, the initiator comprising:-
a high frequency part comprising a radio frequency receiver stage
for receiving a first high frequency signal; and
- a low frequency part comprising logic circuitry which is driven by
a second signal having a frequency which is lower than the
frequency of the first signal.
BRIEF DESCRIPTION OF THE ACCOMPANYING DIAGRAMS
The invention will now further be described, by way of example
only, with reference to the accompanying diagrams wherein: figure 1 is a basic block diagram of a first embodiment of an
electronic blasting system according to the invention;
figure 2 is a block diagram of an electronic initiator according to
the invention and forming part of a detonator of the
system in figure 1 ;
figure 3 is a basic block diagram of a second embodiment of the
system according to the invention;
figure 4 is a basic block diagram of a third embodiment of the
system according to the invention;
figure 5 is a basic block diagram of a fourth embodiment of the
system according to the invention; and
figure 6 is a basic block diagram of a fifth embodiment of the
system according to the invention.
DESCRIPTION OF PREFERRED EMBODIMENTS OF THE INVENTION
A first embodiment of a blasting system according to the invention is
generally designated by the reference numeral 10 in figure 1.
The system comprises a blast controller 12 comprising a radio frequency
transmitter 14 connected to an antenna 16. The transmitter, in use,
broadcasts a first signal comprising digital data modulated on a carrier
18 having a first high frequency f,. The digital data is generated by a data generator 20 and intended for communications with and more
particularly to program a plurality of electronic detonators forming part
of the system.
The system further comprises a plurality of similar electronic detonators
22.1 to 22. n. Since the detonators are similar in configuration, only
detonator 22.1 will be described in more detail hereinafter. The
detonator 22.1 comprises an electronic initiator 24 and an explosive
charge 26. The detonator 22.1 is located in one hole 28.1 of a plurality
of spaced blast holes 28.1 to 28. n. The initiator 24 is connected via a
lead conductor 30 to an antenna 32.
In figure 2, there is shown a more detailed block diagram of the initiator
24. Antenna 32 is connected via lead conductor 30 to a radio
frequency (RF) receiver stage comprising a rectifier 34. An output of
the rectifier 34 is connected to a charge storage device in the form of a
capacitor 36, to energize or charge the capacitor with energy in the first
signal. The output is also connected to level detection circuit 38. The
level detection circuit is connected to a divider circuit 40 for dividing
down the high frequency carrier 18 of frequency f ., to a signal having a
lower frequency f2. The signal with lower frequency f2 is used to drive
a phase-locked loop circuit and local oscillator 42. A resulting low frequency output signal s2 (f2) of the local oscillator is used as clock
signal to drive logic circuitry 44. The logic circuitry 44 drives a switch
circuit 46 to connect a fuse 48 to the capacitor 36 via power line 50,
after a pre-programmed delay time associated with the detonator. The
delay time is typically programmed into the logic circuitry 44 by delay
time data modulated at a suitable rate on the aforementioned carrier
signal and utilizing a unique pre-programmed address of the device. The
various circuits 34 to 46 may be integrated on a single chip. These
circuits derive electrical power from capacitor 36, via power line 52. In
some embodiments the carrier and data may be divided down and in
other embodiments only the carrier is divided down.
An output of level detection circuit 38 is connected via data line 54 to a
data input 56 of logic circuitry 44. A comparator in logic circuitry 44
recovers the digital data modulated on the carrier 18 and received via
the antenna in known manner. As stated hereinbefore, an example of
the digital data is data relating to the aforementioned delay time and
which data is utilized in known manner by the logic circuitry to cause
the switch to connect the capacitor 36 to the fuse 48 at the end of the
relevant delay time, following a common "fire" signal, for example. The frequency of the carrier may be between 200 MHz and 100 GHz,
typically 400 MHz. A divisor of the divider 40 is typically equal to 105,
so that the frequency f2 is in the order of 4 kHz. The frequency f2 may
fall in the range 1 kHz to 15 kHz. The data may be modulated on the
carrier at a rate in the order of 100 MHz.
Hence, in use, the high frequency f, of the carrier is used to charge
capacitor 36, while the signal s2 having a low frequency f2 is used as
clock signal for the logic circuitry 44. The logic circuitry when
operating on a lower frequency f2 is more power efficient than with a
higher frequency f
In figure 3, there is shown a second embodiment of the system. The
controller 12 broadcasts the signal having carrier frequency f to a high
frequency part 60 of a split initiator 61 . The high frequency part 60
comprises a divider as hereinbefore described and a low frequency
output which is connected via a conductive physical link in the form of
normal, low cost wires 62 to an input of a low frequency part 64 of the
initiator including at least the logic circuitry 44, switch and fuse. The
high frequency part may in use be located in a mouth or collar region of
the blast hole and the low frequency part adjacent the charge 26
towards a bottom region of the hole. In the third embodiment 300 of the system shown in figure 4, the blast
controller 12 is of split configuration. The data generator is housed in a
first part 12.1 and the transmitter 14 forms part of a separate second
part 12.2 which is connected via an extension cable 70 to the first part.
The first and second parts are spaced a distance d, of typically between
200m and 3000m from one another. The second part 12.2 is spaced a
distance d2 of typically in the order of 50m from each of the detonators
22.1 to 22. n in respective blast holes 28.1 to 28. n.
In figure 5, there is shown a blast controller 12 transmitting via a
directional antenna a communication signal comprising digital data
modulated on a high frequency carrier 18 of frequency f A common
and central divider 80 connected via a receiver to directional antenna 82
divides the carrier frequency down to a low frequency f2 of a signal s2 .
The signal s2 is transmitted via physical conductive link 84 to detonators
22.1 to 22. n in blast holes 28.1 to 28. n. This signal is utilized to
energize the detonators and each detonator comprises an initiator
comprising a charge storage device, the required logic circuitry, switch
and fuse as hereinbefore described.
In figure 6, there is shown a fifth embodiment 90 of the system
according to the invention. The blast controller 12 is of split configuration comprising a first or master part 12.1 and a second slave
part or repeater part 12.2. The slave part 12.2 comprises a single
antenna 92 for communications with the master part via wireless link 93
and for communications with respective detonators 22.1 to 22. n also
via a respective wireless link 95.1 to 95. n. The slave part 12.2 hence
comprises a transceiver 94 and single antenna 92 is connectable by an
electronically controllable switch 96 to either a receiver of transceiver
94 cooperating with link 93 or a transmitter of the transceiver for
broadcasting a first high frequency signal to detonators 28.1 to 28. n, as
hereinbefore described.
In other embodiments the first signal 18 may not be utilized to energize
the detonators and may comprise a carrier having the first high
frequency and a data signal modulated on the carrier. The data signal is
used to communicate with the detonators via the wireless link from a
remote site 12. The data signal may hence comprise address data for
an addressed detonator and delay time data for that detonator as
hereinbefore described. In these embodiments the detonators may
comprise respective on-board power supplies or batteries.
Alternatively, charge storage devices in the form of capacitors on these
detonators may be charged via a physical link such as link 84 shown in
figure 5 from a common source of charge such as a battery. Each detonator may still comprise an RF receiver stage for receiving the
programming data via the wireless link. Accordingly the data integrity
required on the physical link would be reduced, since the physical link is
utilized for energizing the detonators and not for data communications.
The steps of charging the detonators, programming the detonators via
the RF link and processing by the detonators of the delay time data may
be performed sequentially.
In yet other embodiments the first signal 18 may be utilized both to
energize the detonators as hereinbefore described and to communicate
with the detonators as hereinbefore described. In these embodiments,
the steps of charging the detonators and of programming the detonators
may be performed substantially concurrently, or sequentially.

Claims

CLAIMS:
1 . A blasting system comprising a wireless link for broadcasting
towards a plurality of detonators a first signal comprising a
first frequency; and wherein each detonator comprises logic
circuitry driven by a second signal having a second frequency
which is substantially lower than the first frequency.
2. A system as claimed in claim 1 wherein the second signal is a
clock signal which is derived from the first signal.
3. A system as claimed in claim 1 or claim 2 wherein the first signal
comprises a carrier having the first frequency and a data signal
modulated on the carrier for communicating with the detonators.
4. A system as claimed in any one of the preceding claims wherein
each detonator comprises a respective charge storage device
which is charged by energy in the first signal.
5. A system as claimed in any one of claims 1 to 3 wherein each
detonator comprises a respective charge storage device which is
charged from a source of charge connected to the respective
charge storage device by a physical conductive link.
6. A system as claimed in claim 4 or claim 5 wherein the respective
charge storage device comprises a capacitor.
7. A system as claimed in any one of the preceding claims wherein
the first frequency falls in a range between 200 MHz and 100
GHz.
8. A system as claimed in claim 7 wherein the first frequency is
about 400 MHz.
9. A system as claimed in any one of claims 2 to 8 wherein the
clock signal is derived by dividing the first frequency down by
divider means.
10. A system as claimed in claim 9 wherein the first frequency is
divided down five orders of magnitude.
1 1. A system as claimed in any one of claims 9 and 10 wherein the
divider means is common to at least some of the detonators and
wherein the divider means is connected to a receiver forming part
of the wireless link and to said at least some of the detonators by
a physical conductive link.
12. A system as claimed in any one of claims 9 to 10 wherein the
divider means comprises a respective divider circuit for each of
said plurality of detonators.
13. A system as claimed in claim 12 wherein each detonator
comprises an electronic initiator comprising a high frequency part
and a low frequency part, the high frequency part comprising a
radio frequency receiver stage, a charge storage device connected
to the receiver stage and said respective divider circuit.
14. A system as claimed in claim 13 wherein the low frequency part
comprises a phase-locked loop and local oscillator connected to
an output of said respective divider circuit and providing the clock
signal to the logic circuitry.
15. A system as claimed in claim 14 wherein an input of the logic
circuitry is connected via a data line to an output of a level
detection circuit in the high frequency part.
16. A system as claimed in claim 15 wherein the logic circuitry is
programmable by a data modulating signal of the first signal, to operate a switch of the initiator to cause charge on the charge
storage device to be dumped into a fuse of the detonator.
17. A system as claimed in any one of claims 13 to 16 wherein the
low frequency and high frequency parts of the initiator are
integrated on a single chip.
18. A system as claimed in any one of claims 13 to 16 wherein the
high frequency part and low frequency part are split and wherein
an output of the high frequency part is connected by a physical
conductive link to an input of the low frequency part.
19. A system as claimed in any one of claims 1 to 18 wherein the
wireless link is provided between a remote blast controller
comprising an RF transmitter and an antenna located in close
proximity to the blast controller on the one hand and the plurality
of detonators on the other hand.
20. A system as claimed in any one of claims 1 to 18 wherein the
wireless link is provided between said plurality of detonators and
an RF transmitter located in close proximity to the detonators.
21. A system as claimed in claim 20 wherein the RF transmitter is
connected to a blast controller by a physical conductive link.
22. A system as claimed in claim 20 wherein a second wireless link is
provided between the RF transmitter and a remote blast
controller.
23. A method of operating a blasting system comprising the steps of:
broadcasting a first high frequency RF signal towards each
of a plurality of detonators; and
utilizing a second low frequency signal for driving logic
circuitry forming part of each detonator.
24. A method as claimed in claim 23 wherein the second signal is
derived from the first signal by dividing down the frequency of the
first signal.
25. An initiator for a detonator, the initiator comprising:-
a high frequency part comprising a radio frequency receiver
stage for receiving a first high frequency signal; and a low frequency part comprising logic circuitry which is
driven by a second signal having a frequency which is
lower than the frequency of the first signal.
PCT/ZA2002/000151 2001-10-02 2002-10-01 Frequency diversity remote controlled initiation system WO2003029748A1 (en)

Priority Applications (7)

Application Number Priority Date Filing Date Title
US10/489,772 US7327550B2 (en) 2001-10-02 2002-10-01 Frequency diversity remote controlled initiation system
CA2460966A CA2460966C (en) 2001-10-02 2002-10-01 Frequency diversity remote controlled initiation system
EP02773980A EP1432959B1 (en) 2001-10-02 2002-10-01 Frequency diversity remote controlled initiation system
BRPI0213031A BRPI0213031B1 (en) 2001-10-02 2002-10-01 detonation system, method of operating a detonation system and initiator for a detonator
DE60216784T DE60216784T2 (en) 2001-10-02 2002-10-01 REMOTE-CONTROLLED IGNITION SYSTEM WITH FREQUENCY DIVERSITY
AU2002336727A AU2002336727B2 (en) 2001-10-02 2002-10-01 Frequency diversity remote controlled initiation system
ZA2004/02051A ZA200402051B (en) 2001-10-02 2004-03-15 Frequency diversity remote controlled initiation system

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
ZA01/8080 2001-10-02
ZA200108080 2001-10-02

Publications (1)

Publication Number Publication Date
WO2003029748A1 true WO2003029748A1 (en) 2003-04-10

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Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/ZA2002/000151 WO2003029748A1 (en) 2001-10-02 2002-10-01 Frequency diversity remote controlled initiation system

Country Status (11)

Country Link
US (1) US7327550B2 (en)
EP (1) EP1432959B1 (en)
AT (1) ATE348313T1 (en)
AU (1) AU2002336727B2 (en)
BR (1) BRPI0213031B1 (en)
CA (1) CA2460966C (en)
DE (1) DE60216784T2 (en)
ES (1) ES2278967T3 (en)
PE (1) PE20030480A1 (en)
WO (1) WO2003029748A1 (en)
ZA (1) ZA200402051B (en)

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US7327550B2 (en) 2008-02-05
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