WO2003002981A1 - Method and apparatus for measuring a property of air - Google Patents

Method and apparatus for measuring a property of air Download PDF

Info

Publication number
WO2003002981A1
WO2003002981A1 PCT/AU2002/000855 AU0200855W WO03002981A1 WO 2003002981 A1 WO2003002981 A1 WO 2003002981A1 AU 0200855 W AU0200855 W AU 0200855W WO 03002981 A1 WO03002981 A1 WO 03002981A1
Authority
WO
WIPO (PCT)
Prior art keywords
air
size
property
air flow
sample
Prior art date
Application number
PCT/AU2002/000855
Other languages
French (fr)
Inventor
Greg Ayers
Original Assignee
Commonwealth Scientific And Industrial Research Organisation
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Commonwealth Scientific And Industrial Research Organisation filed Critical Commonwealth Scientific And Industrial Research Organisation
Publication of WO2003002981A1 publication Critical patent/WO2003002981A1/en

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume, or surface-area of porous materials
    • G01N15/02Investigating particle size or size distribution
    • G01N15/0255Investigating particle size or size distribution with mechanical, e.g. inertial, classification, and investigation of sorted collections
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/2202Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/26Devices for withdrawing samples in the gaseous state with provision for intake from several spaces
    • G01N15/075
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/2202Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling
    • G01N2001/222Other features
    • G01N2001/2223Other features aerosol sampling devices
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume, or surface-area of porous materials
    • G01N15/02Investigating particle size or size distribution
    • G01N2015/0288Sorting the particles
    • G01N2015/1024
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N5/00Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
    • G01N5/02Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by absorbing or adsorbing components of a material and determining change of weight of the adsorbent, e.g. determining moisture content

Definitions

  • the present invention relates to a method of calculating a measure of a property of air and apparatus for measuring a property of air.
  • the invention is particularly suited to measuring the concentration of particles of different sizes in air.
  • SSI selective size inlet
  • the particle measurement system has an air pump to cause air to flow through the SSI to a icrobalance (such as the Tapered Element Oscillating Microbalance available from Rupprecht and Patashnick Inc.) which measures the mass of particle material collected from the air flow in real time. The measured mass is then used to produce a measure of the concentration of particles in the air.
  • Measurements of more than a single particle size are made by co-location of separate particle measurement systems for each particle size being measured.
  • the capital cost of the overall particle measurement system is dominated by the cost of the microbalance, pump, supporting electronics and data logger, with the selective size inlet being a minor cost component.
  • the inventor has realised that because levels of particles in the atmosphere such as air pollutants, change slowly, if data is gathered over a plurality of sample periods spaced throughout the measurement period, it is possible to obtain valid data over the measurement period without measuring constantly.
  • the invention provides apparatus for measuring a property of air for two different particle sizes over a measurement period, said apparatus including: a first size selective inlet; a second size selective inlet with a cut-off size different to said first size selective inlet; a shared measurement device for measuring said property of air; and air flow directing means for directing air through one of said first and said second size selective inlets at a time to said shared measurement device, the air flow directing means being configured to repeatedly switch air flow during said measurement period so that the air flow is directed through each of said first and second size selective inlets for a plurality of sample periods to thereby obtain a plurality of sample measures for each of said first and second size selective inlets which can be used to calculate a measure of the property for each of said particle sizes, wherein the air flow directing means is configured to switch said air flow such that any change in the property of air between consecutive sample periods for each particle size will not significantly affect calculated measures of the property of air for the measurement period.
  • said shared measurement device is used to obtain sample measures of the concentration of particles in air.
  • said air flow directing means includes a controllable valve located between both the size selective inlets and said shared measurement device for controlling which of the size selective inlets air is directed through.
  • said airflow directing means includes an air pump for directing air through said size selective inlets .
  • said particle sizes are chosen from the group of: particles less than lO ⁇ m in size; particles less than 2.5 ⁇ m in size; and particles less than l.O ⁇ m in size, where size is defined as aerodynamic diameter.
  • said sample period is in the range of 2-15 minutes.
  • said sample period is about five _. minutes.
  • said sample period is about ten minutes .
  • said measurement period is between 1 and 48 hours.
  • said measurement period is about 24 hours .
  • said measurement period is about one hour .
  • consecutive sample periods may be spaced by switching periods.
  • the invention also provides a method of calculating a measure of a property of air for a plurality of different particle sizes over a measurement period, said method involving: measuring said property of air for each different size during a plurality of spaced apart sample periods by measuring the property of air for each of said different sizes in turn so that the sample periods of respective ones of said particles sizes are spaced apart by sample periods of the other particle size or sizes; and calculating said measure of the property of air for each of said particle sizes from the measurements obtained during said sample periods, wherein the duration and spacing of consecutive sample periods for each different particle size are chosen such that any change in the property of air between consecutive sample periods does not significantly affect the calculated measure of the property of air over the measurement period.
  • FIG. 1 is a block diagram showing the apparatus of the present invention
  • Figure 2 is a graph showing calculated and measured data.
  • the present invention arises from the realisation that levels of particles in the atmosphere, and in particular air pollutants, change slowly through a diurnal pattern. This relatively slow variation in the diurnal pollutant patterns is the reason why regulatory authorities typically publish data at hourly-average or longer averaging times. Indeed, statutory authorities world-wide mandate PM10 (particles of less than lO ⁇ m) and PM2.5 (particles less than 2.5 ⁇ m standards only as 24 -hour averages. Thus, accuracy at these long averaging times is ultimately what is required of measuring systems.
  • the invention described in the preferred embodiment was made by the realisation that against these long averaging times, and the slowly-varying nature of PM levels valid PM data at the hourly or mandated daily- average level should be obtainable using only sample periods across the measurement period. For example, in the preferred embodiment every second or third five-minute period in each hourly or daily measurement period is used as a sample period during which the concentrations of particles in air is measured for particles of a particular size.
  • Figure 1 is a block diagram of the apparatus of a preferred embodiment of the present invention.
  • a pump (not illustrated) is operable to cause air to flow through three size selective inlets which are provided by a first size selective inlet (SSI) 1 which only allows particles of size PM10 or less to pass (i.e lO ⁇ m or less) .
  • a second SSI 2 only allows particles of size PM2.5 or less to pass (i.e.2.5 ⁇ m or less), and a third SSI 3 only allows particles of size PM1 or less to pass (i.e. l ⁇ m or less).
  • size refers to the aerodynamic diameter of the particles.
  • each of the SSIs are in fluid communication with a low particle-loss valve 4 which is controlled to direct each of the air flows from the respective SSIs in turn to a Tapered Element Oscillating Microbalance (TEOM) 5 (available from Rupprecht and Patashnick Inc.).
  • TEOM Tapered Element Oscillating Microbalance
  • the valve 4 is programmed so as to direct the air flows of the respective SSI's in turn for a sample period of 5 minutes.
  • the microbalance weighs the particles in the air flow during this sample period to produce a real-time measure of the concentration of particles in the air.
  • the concentration measure for the sample periods are then communicated to the data logger 6 which stores the concentrations for future or real-time processing.
  • the logged data can then be processed to provide measures of the concentrations of particles of each of the three sizes during the measurement period.
  • the measurement period is typically one hour or 24 hours depending on the application as these are the periods used by statutory authorities. It will be apparent to persons skilled in the art that other measurement periods can be used.
  • Performance potential for this system was tested via two numerical simulations based on eight days of raw PM10 data obtained using a tapered element oscillating microbalance (TEOM) and sample periods of 5 minutes .
  • TEOM is a registered trade mark of Rupprecht and Patashnick, Inc
  • the data was recorded at an urban site in the city of Melbourne, Australia.
  • every alternate data point was deemed to be from a PM2.5 SSI, with its value assumed to be a factor of 0.7 times the original PM10 value.
  • each data series consisted of one 5-minute data point taken (alternatively) every ten minutes.
  • the second simulation was analogous, but was based on time-sharing the measurements across three SS s, PM10, PM2.5 and PM1, each measurement being allocated to very third 5-minute data point.
  • PM2.5 was assumed to equal PM10 scaled by 0.7.
  • PM1 was assumed to equal PM10 scaled by 0.4.
  • Performance of the concept was tested for each simulation by computing and comparing hourly and daily averages from the original complete data series and the reconstructed data series derived from the time-shared series.
  • Figure 2 shows the comparison for hourly data points .
  • Table 1 contains regression results from the hourly data comparison.
  • Table 2 shows the errors in daily average results that result from the simulations.
  • the apparatus of the preferred embodiment can be modified so as to incorporate two SSIs or alternatively that only two SSIs need to be used at any one time. Further, additional SSIs may be provided if it is desired to measure particles of other sizes. For example, it will be apparent that there may be a switching period between consecutive sample periods during which the valve 4 is switched from one SSI to another and this can be accounted for in the calculation of the measure of particle concentrations.
  • sample period of five minutes is chosen for convenience as this is a standard measurement period of the TEOM. It will be apparent to persons skilled in the art that other sample periods can be used.

Abstract

The invention provides apparatus for measuring a property of air for two different particle sizes over a measurement period. The apparatus includes a first size selective inlet, a second size selective inlet with a cut-off size different to said first size selective inlet, a shared measurement device for measuring said property of air and air flow directing means for directing air through one of said first and said second size selective inlets at a time to said shared measurement device, the air flow directing means being configured to repeatedly switch air flow during said measurement period so that the air flow is directed through each of said first and second size selective inlets for a plurality of sample periods to thereby obtain a plurality of sample measures for each of said first and second size selective inlets which can be used to calculate a measure of the property for each of said particle sizes, wherein the air flow directing means is configured to switch said air flow such that any change in the property of air between consecutive sample periods for each particle size will not significantly affect calculated measures of the property of air for the measurement period.

Description

METHOD AND APPARATUS FOR MEASURING A PROPERTY OF AIR
Field of the Invention
The present invention relates to a method of calculating a measure of a property of air and apparatus for measuring a property of air. The invention is particularly suited to measuring the concentration of particles of different sizes in air.
Background to the Invention
Current techniques for measuring concentrations of particles in air for air quality assessment involve the use of particle measurement systems. Such particle measurement systems have a selective size inlet (SSI) which selectively allows particles smaller than the cutoff size to pass the inlet so that properties of that particle size fraction can be measured. Typically, a SSI allows particles of less than one of the sizes lOμm, 2.5μm or lμm to pass. The particle measurement system has an air pump to cause air to flow through the SSI to a icrobalance (such as the Tapered Element Oscillating Microbalance available from Rupprecht and Patashnick Inc.) which measures the mass of particle material collected from the air flow in real time. The measured mass is then used to produce a measure of the concentration of particles in the air. These measurements are sent to a data logger which stores the information for further processing.
Measurements of more than a single particle size are made by co-location of separate particle measurement systems for each particle size being measured. The capital cost of the overall particle measurement system is dominated by the cost of the microbalance, pump, supporting electronics and data logger, with the selective size inlet being a minor cost component.
The inventor has realised that because levels of particles in the atmosphere such as air pollutants, change slowly, if data is gathered over a plurality of sample periods spaced throughout the measurement period, it is possible to obtain valid data over the measurement period without measuring constantly.
Summary of the Invention
Accordingly, the invention provides apparatus for measuring a property of air for two different particle sizes over a measurement period, said apparatus including: a first size selective inlet; a second size selective inlet with a cut-off size different to said first size selective inlet; a shared measurement device for measuring said property of air; and air flow directing means for directing air through one of said first and said second size selective inlets at a time to said shared measurement device, the air flow directing means being configured to repeatedly switch air flow during said measurement period so that the air flow is directed through each of said first and second size selective inlets for a plurality of sample periods to thereby obtain a plurality of sample measures for each of said first and second size selective inlets which can be used to calculate a measure of the property for each of said particle sizes, wherein the air flow directing means is configured to switch said air flow such that any change in the property of air between consecutive sample periods for each particle size will not significantly affect calculated measures of the property of air for the measurement period.
Preferably, said shared measurement device is used to obtain sample measures of the concentration of particles in air.
Preferably, said air flow directing means includes a controllable valve located between both the size selective inlets and said shared measurement device for controlling which of the size selective inlets air is directed through.
Preferably, said airflow directing means includes an air pump for directing air through said size selective inlets .
Preferably, said particle sizes are chosen from the group of: particles less than lOμm in size; particles less than 2.5μm in size; and particles less than l.Oμm in size, where size is defined as aerodynamic diameter.
Preferably, said sample period is in the range of 2-15 minutes.
Preferably, said sample period is about five _. minutes.
Thus, when two particle sizes are being measured, their respective sample periods will typically be spaced apart by five minutes .
Alternatively, said sample period is about ten minutes .
Preferably, said measurement period is between 1 and 48 hours.
Preferably, said measurement period is about 24 hours .
Alternatively, said measurement period is about one hour .
In some embodiments, consecutive sample periods may be spaced by switching periods.
The invention also provides a method of calculating a measure of a property of air for a plurality of different particle sizes over a measurement period, said method involving: measuring said property of air for each different size during a plurality of spaced apart sample periods by measuring the property of air for each of said different sizes in turn so that the sample periods of respective ones of said particles sizes are spaced apart by sample periods of the other particle size or sizes; and calculating said measure of the property of air for each of said particle sizes from the measurements obtained during said sample periods, wherein the duration and spacing of consecutive sample periods for each different particle size are chosen such that any change in the property of air between consecutive sample periods does not significantly affect the calculated measure of the property of air over the measurement period.
Brief Description of the Drawings
A preferred embodiment will now be described with reference to the accompanying drawings in which:
Figure 1 is a block diagram showing the apparatus of the present invention;
Figure 2 is a graph showing calculated and measured data.
Description of the Preferred Embodiment
The present invention arises from the realisation that levels of particles in the atmosphere, and in particular air pollutants, change slowly through a diurnal pattern. This relatively slow variation in the diurnal pollutant patterns is the reason why regulatory authorities typically publish data at hourly-average or longer averaging times. Indeed, statutory authorities world-wide mandate PM10 (particles of less than lOμm) and PM2.5 (particles less than 2.5μm standards only as 24 -hour averages. Thus, accuracy at these long averaging times is ultimately what is required of measuring systems.
The invention described in the preferred embodiment was made by the realisation that against these long averaging times, and the slowly-varying nature of PM levels valid PM data at the hourly or mandated daily- average level should be obtainable using only sample periods across the measurement period. For example, in the preferred embodiment every second or third five-minute period in each hourly or daily measurement period is used as a sample period during which the concentrations of particles in air is measured for particles of a particular size.
This allows, in the apparatus of the preferred embodiment, a single microbalance to measure air which has been directed through two or more size selective inlets while still allowing the estimation of valid hourly and daily-average data from the data collected during the sample periods for each of the particle sizes.
Figure 1 is a block diagram of the apparatus of a preferred embodiment of the present invention.
A pump (not illustrated) is operable to cause air to flow through three size selective inlets which are provided by a first size selective inlet (SSI) 1 which only allows particles of size PM10 or less to pass (i.e lOμm or less) . A second SSI 2 only allows particles of size PM2.5 or less to pass (i.e.2.5μm or less), and a third SSI 3 only allows particles of size PM1 or less to pass (i.e. lμm or less). Herein the term "size" refers to the aerodynamic diameter of the particles.
The outlets of each of the SSIs are in fluid communication with a low particle-loss valve 4 which is controlled to direct each of the air flows from the respective SSIs in turn to a Tapered Element Oscillating Microbalance (TEOM) 5 (available from Rupprecht and Patashnick Inc.). Thus, in combination the pump and the valve provide means for directing air flow through each of the size selective inlets to a shared microbalance.
In the preferred embodiment, the valve 4 is programmed so as to direct the air flows of the respective SSI's in turn for a sample period of 5 minutes. The microbalance weighs the particles in the air flow during this sample period to produce a real-time measure of the concentration of particles in the air. The concentration measure for the sample periods are then communicated to the data logger 6 which stores the concentrations for future or real-time processing. The logged data can then be processed to provide measures of the concentrations of particles of each of the three sizes during the measurement period. The measurement period is typically one hour or 24 hours depending on the application as these are the periods used by statutory authorities. It will be apparent to persons skilled in the art that other measurement periods can be used.
Thus, the capital costs of such a particle measurement system is greatly reduced relative to the current situation where it is necessary to co-locate multiple particle measurement systems to measure concentrations of particles of different sizes because it is possible to sample PM10, PM2.5 and PMl data using a single microbalance which is the major cost of such measurement systems .
Further, it is possible to improve data quality by use of a single particle measurement system rather than multiple co-located systems as this eliminates calibration differences. Performance potential for this system was tested via two numerical simulations based on eight days of raw PM10 data obtained using a tapered element oscillating microbalance (TEOM) and sample periods of 5 minutes . (TEOM is a registered trade mark of Rupprecht and Patashnick, Inc) . The data was recorded at an urban site in the city of Melbourne, Australia. In the first simulation every alternate data point was deemed to be from a PM2.5 SSI, with its value assumed to be a factor of 0.7 times the original PM10 value. This generated two data series, one PM10 series consisting of half the original 5-minute values (i.e. every second data point), and a fictitious PM2.5 series consisting of the other half of the original PM10 series, scaled by a factor of 0.7. Thus each data series consisted of one 5-minute data point taken (alternatively) every ten minutes.
Complete data serdes were reconstructed from these two series by using cubic spline interpolation to provide an interpolated PM10 or PM2.5 value for each of the, alternate, missing 5-minute data points. A comparison between these reconstructed data series and the original, complete PM10 data series, and fictitious PM2.5 data series (the measured PM10 series scaled by 0.7) provides a test of the concept.
The second simulation was analogous, but was based on time-sharing the measurements across three SS s, PM10, PM2.5 and PM1, each measurement being allocated to very third 5-minute data point. As in the previous simulation PM2.5 was assumed to equal PM10 scaled by 0.7. PM1 was assumed to equal PM10 scaled by 0.4.
Performance of the concept was tested for each simulation by computing and comparing hourly and daily averages from the original complete data series and the reconstructed data series derived from the time-shared series. Figure 2 shows the comparison for hourly data points . Table 1 contains regression results from the hourly data comparison. Table 2 shows the errors in daily average results that result from the simulations.
Figure imgf000009_0001
Table 1. Results of regression of hourly-average data from reconstructed data series versus complete original data series (192 data pairs) .
Figure imgf000009_0002
Table 2. Errors in 24-hour average PM10 (μgm~3) calculated from reconstructed PM10 data series yielded by numerical simulations with the EROM time-shared between two or three separate inlets .
The result of the simulations suggest a negligible difference in hourly and daily-averaged data derived from the time-shared series, in comparison with the original complete series . It will apparent from the foregoing, that the apparatus of the preferred embodiment can be modified so as to incorporate two SSIs or alternatively that only two SSIs need to be used at any one time. Further, additional SSIs may be provided if it is desired to measure particles of other sizes. For example, it will be apparent that there may be a switching period between consecutive sample periods during which the valve 4 is switched from one SSI to another and this can be accounted for in the calculation of the measure of particle concentrations.
The sample period of five minutes is chosen for convenience as this is a standard measurement period of the TEOM. It will be apparent to persons skilled in the art that other sample periods can be used.
It will be apparent to persons skilled in the art, that while the present technique is particularly suited to measurement of particle concentrations, it may also be used to measure other properties of air which vary over time. For example, measurement of the optical property Bsp (aerosol scattering coefficient) for particles in selected size ranges rather than particle mass concentration could be achieved by replacing the microbalance (TEOM) in the embodiment with an appropriate optical measurement system (a nephelometer) .
Various other modifications will be apparent to persons skilled in the art and should be understood as falling within the scope of the invention described herein

Claims

CLAIMS :
1. Apparatus for measuring a property of air for two different particle sizes over a measurement period, said apparatus including: a first size selective inlet; a second size selective inlet of a size different to said first size selective inlet; a shared measurement device for measuring said property of air; and air flow directing means for directing air through one of said first and said second size selective inlets at a time to said shared measurement device, the air flow directing means being configured to repeatedly switch air flow during said measurement period so that the air flow is directed through each of said first and second size selective inlets for a plurality of sample periods to thereby obtain a plurality of sample measures for each of said first and second size selective inlets which can be used to calculate a measure of the property for each of said particle sizes, wherein the air flow directing means is configured to switch said air flow such that any change in the property of air between consecutive sample periods for each particle size will not significantly affect calculated measures of the property of air for the measurement period.
2. Apparatus as claimed in claim 1, wherein said shared measurement device is used to obtain sample measures of the concentration of particles in air.
3. Apparatus as claimed in claim 2 , wherein said shared measurement device is a microbalance.
4. Apparatus as claimed in claim 3, wherein said microbalance is a tapered element oscillating microbalance .
5. Apparatus as claimed in any one of claims 1 to 4, wherein said air flow directing means includes a controllable valve located between both the size selective inlets and said shared measurement device for controlling which of the size selective inlets air is directed through.
6. Apparatus as claimed in any one of claims 1 to 5, wherein said airflow directing means includes an air pump for directing air through said size selective inlets.
7. Apparatus as claimed in any one of claims 1 to 6, including at least one further size selective inlet of different size to the other size selective inlets, and wherein said air flow directing means is configured to direct air flow through each of the size selective inlets in turn in order to obtain a plurality of sample measures "*" for each size selective inlet.
8. Apparatus as claimed claim 1, wherein the size of each size selective inlet is selected from the sizes: less than or equal to lOμm; less than or equal to 2.5μm; and less than or equal to lμm.
9. Apparatus as claimed in any one of claims 1 to 8, wherein the air flow directing means is configured to direct air flow through each size selective inlet for sample periods in the range of 2 to 15 minutes.
10. Apparatus as claimed in any one of claims 1 to 8, wherein the air flow directing means is configured to direct air flow through each size selective inlet for sample periods of about five minutes.
11. Apparatus as claimed in any one of claims 1 to 8, wherein the air flow directing means is configured to direct air flow through each size selective inlet for sample periods of about 10 minutes.
12. Apparatus as claimed in any one of claims 1 to 11, wherein said measurement period is between 1 and 48 hours .
13. Apparatus as claimed in any one of claims 1 to 11, wherein said measurement period is 24 hours.
14 Apparatus as claimed in any one of claims 1 to 13, including a data logger for recording the sample measures .
15. A method of calculating a measure of a property of air for a plurality of different particle sizes over a measurement period, said method involving: measuring said property of air for each different size during a plurality of spaced apart sample periods by measuring the property of air for each of said different sizes in turn so that the sample periods of respective ones of said particles sizes are spaced apart by sample periods of the other particle size or sizes; and calculating said measure of the property of air for each of said particle sizes from the measurements obtained during said sample periods, wherein the duration and spacing of consecutive sample periods for each different particle size are chosen such that any change in the property of air between consecutive sample periods does not significantly affect the calculated measure of the property of air over the measurement period.
16. A method as claimed in claim 15, wherein said property of air is the concentration of particles in air.
17. A method as claimed in claim 15 or claim 16, wherein said method measures concentrations of two different particle sizes.
18. A method as claimed in claim 15 or claim 16, wherein said method measures concentrations of three different particles size.
19. A method as claimed in claim 17, wherein said particle sizes are chosen from the group of: particles less than lOμm in size; particles less than 2.5μm in size; and particles less than l.Oμm in size, where size is defined as aerodynamic diameter.
20. A method as claimed in any one of claims 15 to 19, wherein said sample period is in the range of 2-15 minutes .
21. A method as claimed in any^one of claims 15 to 19, wherein said sample period is about five minutes.
22. A method as claimed in any one of claims 15 to 19, wherein said sample period is about ten minutes.
23. A method as claimed in any one of claims 15 to 22, wherein said measurement period is between 1 and 48 hours .
24. A method as claimed in any one of claims 15 to 22, wherein said measurement period is about 24 hours.
25. A method as claimed in any one of claims 15 to 24, wherein consecutive sample periods are spaced by switching periods.
PCT/AU2002/000855 2001-06-28 2002-06-28 Method and apparatus for measuring a property of air WO2003002981A1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
AUPR6007A AUPR600701A0 (en) 2001-06-28 2001-06-28 Method and apparatus for measuring a property of air
AUPR6007 2001-06-28

Publications (1)

Publication Number Publication Date
WO2003002981A1 true WO2003002981A1 (en) 2003-01-09

Family

ID=3829973

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/AU2002/000855 WO2003002981A1 (en) 2001-06-28 2002-06-28 Method and apparatus for measuring a property of air

Country Status (2)

Country Link
AU (1) AUPR600701A0 (en)
WO (1) WO2003002981A1 (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7631568B2 (en) 2007-08-28 2009-12-15 Quest Technologies Particulate monitor
EP2335714A1 (en) 2005-06-16 2011-06-22 Hadasit Medical Research Services And Development Ltd. A complex comprising IL-6 and soluble IL-6 receptor for use in the treatment of renal failure
GB2506991A (en) * 2012-09-21 2014-04-16 Msp Corp Measuring the mass of particulate matter in a gas
EP2992898A1 (en) 2014-09-04 2016-03-09 Klinikum rechts der Isar der Technischen Universität München T-cell adjuvant and its use for therapeutic or prophylactic vaccination
US9541488B2 (en) 2012-09-21 2017-01-10 Msp Corporation Particle sampling and measurement in the ambient air
US11085861B1 (en) 2014-03-03 2021-08-10 Msp Corporation Apparatus for real-time size-distributed measurement of aerosol mass concentration

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5072626A (en) * 1989-07-14 1991-12-17 Research Triangle Institute Measurement of ultrafine particle size distributions
GB2265847A (en) * 1992-03-31 1993-10-13 Ind Tech Res Inst Particle content monitoring device
US5553507A (en) * 1993-06-10 1996-09-10 Rupprecht & Patashnick Company, Inc. Airborne particulate
US5717147A (en) * 1996-08-22 1998-02-10 Rupprecht & Patashnick Company, Inc. Air sampler filter cassette carrier
US5932795A (en) * 1997-01-22 1999-08-03 President And Fellows Of Harvard College Methods and apparatus for continuous ambient particulate mass monitoring
US6023982A (en) * 1998-05-01 2000-02-15 Rupprecht & Patashnick Company, Inc. Sequential air sampler with automatic sample collector changer
US6134942A (en) * 1998-06-26 2000-10-24 Institut Francais Du Petrole System for sampling specific pollutants contained in diluted exhaust gases from thermal engines
US6205842B1 (en) * 1999-02-02 2001-03-27 Rupprecht & Patashnick Company, Inc. Differential particulate mass monitor with intrinsic correction for volatilization losses

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5072626A (en) * 1989-07-14 1991-12-17 Research Triangle Institute Measurement of ultrafine particle size distributions
GB2265847A (en) * 1992-03-31 1993-10-13 Ind Tech Res Inst Particle content monitoring device
US5553507A (en) * 1993-06-10 1996-09-10 Rupprecht & Patashnick Company, Inc. Airborne particulate
US5717147A (en) * 1996-08-22 1998-02-10 Rupprecht & Patashnick Company, Inc. Air sampler filter cassette carrier
US5898114A (en) * 1996-08-22 1999-04-27 Rupprecht & Patashnick Co., Inc. Air sampler filter cassette carrier
US5932795A (en) * 1997-01-22 1999-08-03 President And Fellows Of Harvard College Methods and apparatus for continuous ambient particulate mass monitoring
US6023982A (en) * 1998-05-01 2000-02-15 Rupprecht & Patashnick Company, Inc. Sequential air sampler with automatic sample collector changer
US6138521A (en) * 1998-05-01 2000-10-31 Rupprecht & Patashnick Company, Inc. Sequential air sampler with automatic sample collector changer
US6134942A (en) * 1998-06-26 2000-10-24 Institut Francais Du Petrole System for sampling specific pollutants contained in diluted exhaust gases from thermal engines
US6205842B1 (en) * 1999-02-02 2001-03-27 Rupprecht & Patashnick Company, Inc. Differential particulate mass monitor with intrinsic correction for volatilization losses

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2335714A1 (en) 2005-06-16 2011-06-22 Hadasit Medical Research Services And Development Ltd. A complex comprising IL-6 and soluble IL-6 receptor for use in the treatment of renal failure
US7631568B2 (en) 2007-08-28 2009-12-15 Quest Technologies Particulate monitor
US7987695B2 (en) 2007-08-28 2011-08-02 3M Innovative Properties Company Particulate monitor
US8813583B2 (en) 2007-08-28 2014-08-26 3M Innovative Properties Company Particulate monitor
GB2506991A (en) * 2012-09-21 2014-04-16 Msp Corp Measuring the mass of particulate matter in a gas
US9541488B2 (en) 2012-09-21 2017-01-10 Msp Corporation Particle sampling and measurement in the ambient air
US11085861B1 (en) 2014-03-03 2021-08-10 Msp Corporation Apparatus for real-time size-distributed measurement of aerosol mass concentration
EP2992898A1 (en) 2014-09-04 2016-03-09 Klinikum rechts der Isar der Technischen Universität München T-cell adjuvant and its use for therapeutic or prophylactic vaccination

Also Published As

Publication number Publication date
AUPR600701A0 (en) 2001-07-26

Similar Documents

Publication Publication Date Title
Papapostolou et al. Development of an environmental chamber for evaluating the performance of low-cost air quality sensors under controlled conditions
Cross et al. Use of electrochemical sensors for measurement of air pollution: correcting interference response and validating measurements
Babich et al. Method comparisons for particulate nitrate, elemental carbon, and PM2. 5 mass in seven US cities
Adams et al. Determinants of fine particle (PM2. 5) personal exposure levels in transport microenvironments, London, UK
US6829919B2 (en) High-quality continuous particulate matter monitor
AU702058B2 (en) A method and apparatus for performing modal mass analysis of exhaust gas from motor vehicle
EP1785702A3 (en) Method and device for measuring gas meter and volume corrector accuracy
Aggarwal et al. Traceability issue in PM 2.5 and PM 10 measurements
WO2003002981A1 (en) Method and apparatus for measuring a property of air
CN107063955B (en) Air particulate matter detector calibration method and management system
Chen et al. Calibration of low-cost particle sensors by using machine-learning method
Green et al. Evaluation of TEOMTM ‘correction factors’ for assessing the EU Stage 1 limit values for PM10
Lee Jr et al. National air surveillance cascade impactor network. I. Size distribution measurements of suspended particulate matter in air
US20040118223A1 (en) Exhaust gas particulate measuring system
Babich et al. Development and evaluation of a continuous ambient PM2. 5 mass monitor
Xue et al. Very low particle matter mass measurements from light-duty vehicles
Yanosky et al. A comparison of four gravimetric fine particle sampling methods
Tierney et al. Hygroscopic effects on weight determinations of particulates collected on glass-fiber filters
Chen et al. Field evaluation of portable and central site PM samplers emphasizing additive and differential mass concentration estimates
CN110736691B (en) Concentration correction method of particulate matter sensor by laser scattering method
Delfino et al. Estimation of unmeasured particulate air pollution data for an epidemiological study of daily respiratory morbidity
Chen et al. Coarse particulate matter concentrations from residential outdoor sites associated with the North Carolina Asthma and Children's Environment Studies (NC-ACES)
EP0936467A3 (en) Exhaust gas analyzer and modal mass analysis method by gas trace process using the analyzer thereof
Stevens et al. Sources of mutagenic activity in urban fine particles
Luoma et al. Autocorrelation and variability of indoor air quality measurements

Legal Events

Date Code Title Description
AK Designated states

Kind code of ref document: A1

Designated state(s): AE AG AL AM AT AU AZ BA BB BG BR BY BZ CA CH CN CO CR CU CZ DE DK DM DZ EC EE ES FI GB GD GE GH GM HR HU ID IL IN IS JP KE KG KP KR KZ LC LK LR LS LT LU LV MA MD MG MK MN MW MX MZ NO NZ OM PH PL PT RO RU SD SE SG SI SK SL TJ TM TN TR TT TZ UA UG US UZ VN YU ZA ZM ZW

AL Designated countries for regional patents

Kind code of ref document: A1

Designated state(s): GH GM KE LS MW MZ SD SL SZ TZ UG ZM ZW AM AZ BY KG KZ MD RU TJ TM AT BE CH CY DE DK ES FI FR GB GR IE IT LU MC NL PT SE TR BF BJ CF CG CI CM GA GN GQ GW ML MR NE SN TD TG

121 Ep: the epo has been informed by wipo that ep was designated in this application
DFPE Request for preliminary examination filed prior to expiration of 19th month from priority date (pct application filed before 20040101)
REG Reference to national code

Ref country code: DE

Ref legal event code: 8642

122 Ep: pct application non-entry in european phase
NENP Non-entry into the national phase

Ref country code: JP

WWW Wipo information: withdrawn in national office

Country of ref document: JP