WO2001061312A1 - Method of determining viscosity - Google Patents

Method of determining viscosity Download PDF

Info

Publication number
WO2001061312A1
WO2001061312A1 PCT/GB2001/000599 GB0100599W WO0161312A1 WO 2001061312 A1 WO2001061312 A1 WO 2001061312A1 GB 0100599 W GB0100599 W GB 0100599W WO 0161312 A1 WO0161312 A1 WO 0161312A1
Authority
WO
WIPO (PCT)
Prior art keywords
viscosity
fluid
determining
voltage
measuring
Prior art date
Application number
PCT/GB2001/000599
Other languages
English (en)
French (fr)
Inventor
Stephen William Mahon
Original Assignee
Qinetiq Limited
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Qinetiq Limited filed Critical Qinetiq Limited
Priority to AU2001232104A priority Critical patent/AU2001232104A1/en
Publication of WO2001061312A1 publication Critical patent/WO2001061312A1/en

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N11/00Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
    • G01N11/10Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material
    • G01N11/16Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties by moving a body within the material by measuring damping effect upon oscillatory body

Definitions

  • the invention relates to a simple and effective method of determining the viscosity of a fluid and in particular to a such a method using piezoelectric elements.
  • GB 2342445 describes the use of a piezoelectric bimorph to measure viscosity.
  • the temperature of the fluid is also measured and used, in conjunction with the output from the bimorph, to calculate the viscosity of the fluid.
  • the problem with this method is that two parameters have to be measured to a certain degree of accuracy in order to obtain the viscosity measurement.
  • the inventor has overcome these problems by formulating an effective method to determine viscosity by mean of a simple relationship.
  • This simple and inexpensive device allows the use of such a fluid condition monitoring sensor in large volume applications and in harsh environments, neither of which are possible with existing systems.
  • the relationship also has the advantage that the measurements are not dependent on temperature up to around 150°C.
  • the invention comprises a method of determining the viscosity of the fluid by the steps of: a) determining a linear relationship between viscosity and a constant ⁇ , b) inserting a piezoelectric element into said fluid and exciting said element to cause it to deflect; c) releasing the piezoelectric element and measuring the voltage produced, d) determining the constant ⁇ from the exponential decay of said voltage where
  • V V 0 e- n P'
  • V being voltage produced after n oscillations after a point in time when the voltage is V 0 from ⁇ and step a) determining viscosity of said fluid.
  • Figure 1 shows a piezoelectric element suitable for use in the method of measuring viscosity according to the invention.
  • Figure 2 shows the damped oscillation of a released excited piezoelectric viscometer.
  • Figure 3 shows how energy dissipation is linearly related to viscosity.
  • Figure 1 shows a representation of a bimorph piezoelectric viscometer, cantilevered onto support 2.
  • the bimorph comprises two individual piezoelectric elements 3 and 4 sandwiched together. This ceramics are chemically bonded by sintering them together with a metal-loaded ink. This allows them to be used at high temperatures where adhesives would be non-linear or fail..
  • the elements are electrically polarised in opposite directions. As is clear to the skilled person electric excitation will cause the bimorph to bend. Such a configuration allows large bending amplitudes and has low resonant frequencies.
  • a pulse signal is used to deflect the bimorph and using a charge or voltage amplifier in series with the bimorph, a signal from the bimorph as it decays.
  • a strained piezoelectric element such as that of figure 1
  • it will undergo damped harmonic motion as shown in figure 2.
  • the damping motion can be described by the intrinsic damping associated with the bimorph and the external force of the fluid in which it is immersed. In most situations the extrinsic contribution will dominate and allow the determination of the viscoelastic properties of the fluid to be determined from an analysis of oscillatory decay of the bimorph. The more viscous the fluid, the more damping and the quicker the decay curve flattens out. By measuring the decay constant the viscosity of the fluid can be determined.
  • V is the voltage at n cycles thereafter, and ⁇ is linearly related to viscosity of the fluid as shown in figure 3.
  • V may be suitably measured by measuring the voltage peaks.
  • V 0 e ⁇ ' describes the envelope 5 of the signal (fig 2).
  • is linearly related to viscosity of a fluid and the viscometer may be calibrated by measuring ⁇ at two points, e.g. in air, water or with a standard oil of known viscosity.
  • Figure 3 shows how energy dissipation is linearly related to viscosity.
PCT/GB2001/000599 2000-02-19 2001-02-15 Method of determining viscosity WO2001061312A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AU2001232104A AU2001232104A1 (en) 2000-02-19 2001-02-15 Method of determining viscosity

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB0003804A GB2359368A (en) 2000-02-19 2000-02-19 Determining the viscosity of a fluid from the exponential decay of an excited piezo-electric element
GB0003804.2 2000-02-19

Publications (1)

Publication Number Publication Date
WO2001061312A1 true WO2001061312A1 (en) 2001-08-23

Family

ID=9885906

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/GB2001/000599 WO2001061312A1 (en) 2000-02-19 2001-02-15 Method of determining viscosity

Country Status (3)

Country Link
AU (1) AU2001232104A1 (ar)
GB (1) GB2359368A (ar)
WO (1) WO2001061312A1 (ar)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007043811A1 (de) * 2007-09-13 2009-03-19 Endress + Hauser Gmbh + Co. Kg Verfahren zur Bestimmung und/oder Überwachung der Viskosität und entsprechende Vorrichtung
EP2128596A2 (en) 2008-05-26 2009-12-02 Latvijas Valsts Koksnes Kimijas Instituts (Latvian State Institute of Wood Chemistry) Device for measuring viscosity

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB0328054D0 (en) 2003-12-04 2004-01-07 Council Cent Lab Res Councils Fluid probe
GB0605273D0 (en) 2006-03-16 2006-04-26 Council Cent Lab Res Councils Fluid robe
GB0716202D0 (en) 2007-08-11 2007-09-26 Microvisk Ltd Improved fluid probe

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5999332A (ja) * 1982-11-30 1984-06-08 Nippon Soken Inc 流体の特性測定装置
SU1210077A1 (ru) * 1984-07-24 1986-02-07 Ташкентский Ордена Дружбы Народов Политехнический Институт Им.А.Р.Бируни Пьезоэлектрический преобразователь
WO1998009139A1 (en) * 1996-08-28 1998-03-05 Videojet Systems International, Inc. Resonator sensors employing piezoelectric benders for fluid property sensing
US6006589A (en) * 1995-05-04 1999-12-28 O-Sense Ab Piezoelectric crystal microbalance device

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3306406A1 (de) * 1983-02-24 1984-08-30 Ernst 2000 Hamburg Thöne Verfahren und vorrichtung zum messen der viskositaet einer fluessigkeit
US5710374A (en) * 1995-04-06 1998-01-20 University Of Virginia Patent Foundation Electronic viscometer
GB2342445A (en) * 1998-09-17 2000-04-12 Nigel Alexander Buchanan Viscosity measurement utilising piezo-electric bars

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5999332A (ja) * 1982-11-30 1984-06-08 Nippon Soken Inc 流体の特性測定装置
SU1210077A1 (ru) * 1984-07-24 1986-02-07 Ташкентский Ордена Дружбы Народов Политехнический Институт Им.А.Р.Бируни Пьезоэлектрический преобразователь
US6006589A (en) * 1995-05-04 1999-12-28 O-Sense Ab Piezoelectric crystal microbalance device
WO1998009139A1 (en) * 1996-08-28 1998-03-05 Videojet Systems International, Inc. Resonator sensors employing piezoelectric benders for fluid property sensing

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
DATABASE WPI Section EI Week 198636, Derwent World Patents Index; Class S02, AN 1986-237939, XP002166066 *
PATENT ABSTRACTS OF JAPAN vol. 008, no. 215 (P - 305) 2 October 1984 (1984-10-02) *
RODAHL M ET AL: "Quartz crystal microbalance setup for frequency and Q-factor measurements in gaseous and liquid environments", REVIEW OF SCIENTIFIC INSTRUMENTS, vol. 66, no. 7, 1 July 1995 (1995-07-01), ISSN 0034-6748, pages 3924 - 3930, XP000524297 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007043811A1 (de) * 2007-09-13 2009-03-19 Endress + Hauser Gmbh + Co. Kg Verfahren zur Bestimmung und/oder Überwachung der Viskosität und entsprechende Vorrichtung
US8756980B2 (en) 2007-09-13 2014-06-24 Endress + Hauser Gmbh + Co. Kg Method for determining and/or monitoring viscosity and corresponding apparatus
US9709475B2 (en) 2007-09-13 2017-07-18 Endress + Hauser Gmbh + Co. Kg Method for determining and/or monitoring viscosity and corresponding apparatus
EP2128596A2 (en) 2008-05-26 2009-12-02 Latvijas Valsts Koksnes Kimijas Instituts (Latvian State Institute of Wood Chemistry) Device for measuring viscosity

Also Published As

Publication number Publication date
AU2001232104A1 (en) 2001-08-27
GB0003804D0 (en) 2000-04-05
GB2359368A (en) 2001-08-22

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