WO2001002084A1 - Detachable separation module - Google Patents

Detachable separation module Download PDF

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Publication number
WO2001002084A1
WO2001002084A1 PCT/JP2000/004467 JP0004467W WO0102084A1 WO 2001002084 A1 WO2001002084 A1 WO 2001002084A1 JP 0004467 W JP0004467 W JP 0004467W WO 0102084 A1 WO0102084 A1 WO 0102084A1
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WO
WIPO (PCT)
Prior art keywords
housing element
separation module
head
module according
port
Prior art date
Application number
PCT/JP2000/004467
Other languages
French (fr)
Japanese (ja)
Inventor
Ryohichi Sugita
Original Assignee
Pall Corporation
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Pall Corporation filed Critical Pall Corporation
Priority to AU58482/00A priority Critical patent/AU5848200A/en
Priority to JP2001507569A priority patent/JP4698105B2/en
Publication of WO2001002084A1 publication Critical patent/WO2001002084A1/en

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D65/00Accessories or auxiliary operations, in general, for separation processes or apparatus using semi-permeable membranes

Definitions

  • the present invention relates to a detachable separation module.
  • a separation module can be suitably used as a membrane filtration module, and in particular, can be suitably used for filtering an ultraclean fluid such as a fluid used in a semiconductor manufacturing process.
  • killer defects can typically be caused by particles as small as 110, the smallest feature size of a semiconductor chip. Therefore, at all stages of the semiconductor manufacturing process, a membrane filter for cleaning both liquid and gas is used. In a semiconductor manufacturing process device, if the membrane filtration module is designed to be sandwiched between a pair of connecting portions, it becomes difficult to connect the membrane filtration module to the process device.
  • the design shape of the membrane filtration module requires that all the connecting parts be provided on one end side of the membrane filtration module. Many.
  • the feed and permeate ports are typically placed in a horizontal orientation on top of the membrane filtration module or on the end called the "head”. Is done.
  • This membrane filtration module is referred to as "T" shaped because of its shape. This T-shaped membrane filtration module simplifies coupling to the rest of the fluid processing system.
  • Japanese Patent Application Laid-Open No. H10-66684 describes a power cartridge type filter installed inside a vending machine or the like for filtering tap water or the like.
  • This filter Has a cap and a filter main body, and the filter main body has a double structure including a metal outer cylinder and a synthetic resin inner cylinder that can be detachably mounted in the outer cylinder. Then, the engagement piece attached to the inside of the cap and the projection provided on the outer cylinder can engage with each other.
  • the membrane filtration module In the conventional membrane filtration module, it was not always easy to attach and detach the head part provided with the port and the housing element in which the separation element was incorporated. For example, you may want to replace a housing element while the head port remains connected to the process piping. Then, depending on the position where the membrane filtration module is arranged, the engaging portion between the housing element and the head cannot always be visually confirmed. For example, when the membrane filtration module is placed near the floor due to design reasons, it is cumbersome for workers to squat down or lie down on the floor to see the engagement. It is hoped that they can be replaced without relying on the eyes to see and feel.
  • the work may need to be done by the participant.Therefore, the head and the housing element must be connected with the same level of strength, regardless of who removes and attaches the housing element. Is desired. Furthermore, not all workers are muscular, some are delicate and not strong. It is desired that even a worker having limited strength can easily replace the housing element.
  • an object of the present invention is to provide a filtration module that can be easily attached and detached.
  • a head having an inflow port and an outflow port, a housing having a separation element incorporated therein,
  • a connection member for detachably connecting the head part and the housing element, a separation module comprising:
  • a separation module wherein positioning means for determining a relative positional relationship between the head part and the housing element is formed on at least one of the head part and the housing element. Is provided.
  • the positioning means includes the housing element and the head portion. At least one fitting portion formed on one of the housing element and the other of the housing element and the head portion so as to be detachably fitted to the fitting portion. It is preferable that the connecting member includes a fitting portion.
  • the housing element has a contact surface that comes into contact with the head portion, and the head portion comes into contact with the housing element.
  • a contact surface wherein the positioning means comprises: at least one protrusion formed on one of the contact surface of the housing element and the contact surface of the head portion; It preferably comprises at least one recess formed in the other of the contact surface of the housing element and the contact surface of the head portion so as to be detachably fitted to the housing element.
  • the convex portion or the concave portion extends substantially parallel to a radial direction of the housing element or the head portion. Furthermore, it is preferable that a taper is formed in the convex portion or the concave portion. Further, it is preferable that a step is formed in the convex portion or the concave portion.
  • the housing element or the head portion has a locking portion
  • the connecting member has a locked portion that is removably locked to the locking portion
  • the locking portion is formed at a radial end of the positioning means.
  • the locking portion is a radially projecting portion, and the locked portion corresponds to the projecting portion, an insertion portion extending in the axial direction, and a continuous with the insertion portion, and a circumferential direction orthogonal to the insertion portion.
  • the groove extends. More preferably, the groove is tapered.
  • the separating element includes a filter element or a plurality of hollow fiber membranes.
  • the separation element comprises a microporous membrane, an ultrafiltration membrane, a reverse osmosis membrane.
  • the connecting member has a ring shape.
  • a step of permeating a feed solution through the separation module to obtain a permeate solution in another aspect of the present invention, a step of permeating a feed solution through the separation module to obtain a permeate solution
  • a step of manufacturing a semiconductor device using the permeate; A method for manufacturing a semiconductor device is provided.
  • a packaging element having a separation element incorporated therein, which can be used in the separation module.
  • FIG. 1 is a sectional view of a preferred embodiment of the separation module of the present invention.
  • FIG. 2 is an exploded perspective view of the separation module shown in FIG.
  • FIG. 3 is a side view of the separation module shown in FIG.
  • FIG. 4 is a top view of the separation module shown in FIG.
  • FIG. 5 is a sectional view of a port that can be used in one embodiment of the separation module of the present invention.
  • FIG. 6 shows another embodiment of the positioning means of the present invention.
  • FIG. 6 (a) is a top view of a housing element
  • FIG. 6 (b) is a side view of a housing element.
  • FIG. 7 shows another embodiment of the positioning means of the present invention.
  • FIG. 7 (a) is a top view of a housing element
  • FIG. 7 (b) is a side view of a housing element.
  • FIG. 8 shows another embodiment of the positioning means of the present invention.
  • FIG. 8 (a) is a top view of a housing element
  • FIG. 8 (b) is a side view of a housing element.
  • FIG. 9 shows another embodiment of the positioning means of the present invention.
  • FIG. 9 (a) is a top view of a housing element
  • FIG. 9 (b) is a side view of a housing element.
  • FIG. 10 shows another embodiment of the positioning means of the present invention.
  • FIG. 10 (a) is a top view of a housing element
  • FIG. 10 (b) is a side view of a housing element.
  • FIG. 11 shows another embodiment of the positioning means of the present invention.
  • FIG. 11 (a) is a top view of a housing element
  • FIG. 11 (b) is a side view of a housing element.
  • FIG. 12 shows another embodiment of the positioning means of the present invention.
  • FIG. 12 (a) is a top view of a housing element
  • FIG. 12 (b) is a side view of a housing element.
  • the separation module 1 of the present embodiment includes a head part 10, a housing element 20 in which a separation element 40 is incorporated, the head part and the housing part. And a connecting member 30 for detachably connecting the housing element to the housing element.
  • positioning means 18, 22 for determining a relative positional relationship between the head portion 10 and the housing element 20 include the head portion 10 and the housing element 2. It is formed on at least one of zero.
  • the positioning means includes at least one fitting portion, for example, a convex portion 22 formed on one of the housing element and the head portion, and It is preferable that the housing element and the head portion include at least one fitted portion, for example, a concave portion 18 formed on the other of the housing portion so as to be detachably fitted.
  • the positioning between the head part and the housing element can be facilitated, and it is possible to confirm with the touch from the hand at the time of work without visually confirming the engagement part of both. it can. Therefore, the housing part can be easily fixed to the head part.
  • the positioning means when a force is applied to the connecting member 30 so as to connect the head portion 10 and the housing element 20, when the force is applied to the connecting member 30, the positioning means is connected to the ports lla, llb, 1 1 of the head portion 10. 1c can be prevented from being applied with force.
  • the positioning means 18, 22 resist the rotational force. This prevents the ports lla, llb, and 11c from being stressed.
  • the housing element or the head portion has a locking portion 23, and the locked member 35 is provided so that the connecting member 30 is removably locked to the locking portion. It is preferred to have.
  • the connecting member having the locked portion the housing element can be always fixed to the head with a constant strength.
  • the locking portion and locked portion are only used herein to clarify that they are paired with each other, and the locking portion 35 is attached to the connecting member 30. It may be said that it is provided.
  • the head section 10 is preferably located at the top of the membrane filtration module. It can be positioned at the bottom or bottom without leaving the essence. From now on, the terms “top” and “head” refer to the end of the membrane filtration module where the connection port is located, and the terms “bottom” and “bottom” refer to the opposite end. Is used to indicate The membrane filtration module is not always used in the vertical direction, that is, in the axial direction of the module, but may be used in the horizontal direction.
  • the head portion 10 is, for example, disc-shaped and has a first port 11a, a second port 11b, and a third port 11c.
  • the first port 11a acts as an inflow port
  • the second port 11b acts as an outflow port
  • the third port 11c acts as a vent port. Is also good.
  • the first port 11a may act as an outflow port
  • the second port 11b may act as an inflow port.
  • the first port 11a, the second port lib, and the third port 11c are preferably arranged linearly in parallel with the radial direction of the head portion 10.
  • the head portion 10 has a contact surface 10b that contacts the housing element
  • the housing element 20 has a contact surface 21a that contacts the head portion 10.
  • the positioning means includes a convex portion 22 formed on the contact surface 21 a of the housing element 20 and a head portion 10 so as to be detachably fitted to the convex portion 22. And a concave portion 18 formed in the contact surface 10b of the contact hole 10b. It is preferable that the convex portions 22 and the concave portions 18 extend in parallel with the radial direction.
  • the convex portion 22 of the housing element 20 has a first opening 24 a and a second opening 2 corresponding to the first port 11 a, the second port 11 b and the third port 11 c, respectively. 4b and a third opening 24c are preferably provided.
  • a locking portion is formed at a radial end of the convex portion 22 of the housing element 20 so as to be removably locked to the locked portion of the connecting member. 3 is formed. That is, it is preferable that the side surface of the housing element 20 on the side of the contact surface 21 a has a protruding portion 23 protruding in the radial direction.
  • the upper surface of the protrusion 22 and the upper surface of the protrusion 23 may be on the same plane. Of course, there may be a step between the upper surface of the protrusion 22 and the upper surface of the protrusion 23, or a taper may be formed continuously.
  • the housing element 20 is composed of a hollow cylindrical body 2 1 and a separating element disposed therein. 40.
  • the separating element is preferably a filter element, and as shown in FIG. 1, may be a cylindrical filter element which can be housed inside the housing element 20. Good.
  • the filter element preferably comprises a microporous membrane, an ultrafiltration,] reverse osmosis membrane.
  • the fill element may be a pleat.
  • the separation element is a hollow fiber membrane arranged in a cylindrical shape, and each hollow fiber membrane is a microporous membrane. Ultrafiltration, reverse osmosis membranes may also be used.
  • Microporous, ultrafiltration, and reverse osmosis membranes can be used in semiconductor manufacturing processes to remove particulates or gases from liquids.
  • the present invention can remove particulate matter or gas in a liquid other than the semiconductor manufacturing process. Furthermore, it does not prevent the removal of particulate matter in the gas.
  • pure water from which ions have been removed can be obtained by using a granular ion exchange resin as a separation element, for example, a mixture of a cation exchange resin and an anion exchange resin.
  • the filter element 40 includes, for example, a core member 41, a filter main body 42 fixed to the core member, and a coating layer 43 fixed to the filter main body in this order in the radial direction. May be arranged.
  • the core member 41, the filter body 42, and the coat layer 43 may be sandwiched between the end members 44 and 45.
  • the end member 44 may have an opening communicating with the port 11b, while the end member 45 may be closed.
  • the connecting member 30 includes a cylindrical main body 31 and a pressing portion 32 extending inward of the upper edge of the main body 31.
  • the main body 31 includes an insertion portion 33 formed from the lower edge in the axial direction of the main body 31, and a groove 34 continuous with the insertion portion 33 and extending in a circumferential direction orthogonal to the insertion portion 33. It is preferable that the locked portion 35 is formed. ⁇ The projection 23 of the housing element 20 is inserted into the insertion portion 33 of the connecting member 30, and then the housing element 20 is By rotating the connecting member 30, the protruding portion 23 rotates along the groove 34, and the head portion 10 and the housing element 20 can be pressed against each other and fixed.
  • the groove 34 is preferably provided with a taper 34a.
  • the groove 34 has a slight play in the axial direction, and as the protrusion 23 rotates, the play in the axial direction decreases. It can be shaped to be tight and progressively tighter.
  • the protrusion 23 has a rectangular shape, and is formed so as to extend outward from the peripheral edge of the cylindrical body 21. Further, two protruding portions 23 are provided so as to form a straight line with the ports 11a to 11c.
  • the locked portion 35 is provided at two places so as to correspond to the pair of projecting portions 23, and the insertion portion 33 is formed in a rectangular shape.
  • the numbers of the protruding portions and the locked portions are not limited, and may be one or three or more.
  • the inside and the outside of the housing element 20 are communicated with each other via pipes 12a, 12b, and 12c. That is, the first to third openings 24a, 24b, and 24c are through holes that pass through the upper portion of the housing element 20, respectively, and the first opening 24a and the second opening 25 are respectively formed in the filter main body 42.
  • the third opening 26 is located directly above the hollow portion surrounded by the core member 41.
  • 27a, 27b and 27c are formed.
  • Seal member installation part 27a, 271, 27. Is formed such that the end of the first to third openings 24a, 24b, 24c on the contact surface 2la side is wider than the inner diameter of each of the openings 24a, 24b, 24c and is circularly concave.
  • Sealing member mounting portions 27a, 27b, 27c are provided with sealing members, for example, 0-rings 28a, 28b, 28c, respectively, and are liquid-tight by the sealing members 28a, 28b, 28c.
  • the structure is made.
  • the seal members 28a, 28b, 28c are not limited as long as the head portion and the housing element can be formed in a liquid-tight structure.
  • the depth of the seal member installation portion 27 is slightly smaller than the thickness of the seal members 28a, 28b, and 28c, and the outer diameter of the seal member installation portion 27 is slightly larger than the outside diameter of a, 28b, 28c.
  • the inner diameter surfaces of the pressed and crushed seal members 28a, 28b, 28c are connected to the respective pipes 12a. , 12b, 12c.
  • one sealing member 28a, 28b, 28c allows the contact portion between the sealing member 28a, 28b, 28c and each pipe 12a, 12b, 12c and the sealing member 28a, 28c.
  • the seal can be made at two places of contact between the b and 28 heads and the contact surface 10b of the head portion 10, and a higher liquid-tight structure can be achieved as compared with the conventional one.
  • One embodiment of the first port 11a is shown in FIG.
  • the shape and structure of the port are not limited to this embodiment, and there is no limitation as long as fluid can pass through.
  • the first port 11a, the second port 11b, and the third port 11c may all have the same shape, structure, material, or the like, or may have any or all of different shapes, structures, and materials. May be.
  • the first port 11a, the second port lib, and the third port 11c are respectively the first pipe 12a, the second pipe 12b, and the third pipe 12b. c.
  • the first pipe 12a, the second pipe 12b, and the third pipe 12c respectively extend in the axial direction of the separation module 1, penetrate the head part 10, and face the surface 10a and abut.
  • Surface 10b extends from the side.
  • the first port lla, the second port lib, and the third port 1lc respectively have removable sealing members 50a, 50b in order to maintain the internal cleanliness. , 50 c. Sealing members are reused They may be disposable or disposable.
  • a sealing member 50 is attached to each open end of the first port lla, the second port 11b, and the third port 11c.
  • Adhesive tapes are affixed as a, 50b, and 50c.
  • the sealing members 50a, 50b, and 50c are removed, and the first port 11a, the second port 11b, and the third port 11c are respectively processed by a process not shown.
  • an open nut member is provided at the end of the port 11a.
  • a cap member having a U-shaped cross section may be arranged as a sealing member instead of the nut member that is open.
  • the first port 11a and the second port 11b of the head portion 10 are connected to the process piping. Then, the housing element 20 can be replaced. Thereby, when exchanging the housing element 20, the work of connecting and disconnecting the first port 11a and the second port 11b can be omitted.
  • the positioning means of the present invention is not limited to the above embodiment, but can be variously modified. 6 to 12 show another embodiment of the positioning means of the present invention.
  • reference numeral 20 indicates a housing element
  • reference numeral 22 indicates a projection
  • Reference numbers 23a to 23n and 23p indicate protrusions. 6 to 12, the opening communicating with the inside of the housing element 20 is omitted for convenience of explanation.
  • the projections 22 and the projections 23 a to 23 n and 23 p continuous with the projections 22 are provided on the housing element 20.
  • a concave portion or a corresponding shape is formed in the head portion 10. This facilitates the positioning of the housing element 20 and the head.
  • the projection 22, in particular the center line of the projection 22 extends substantially parallel to the radial direction of the housing element 20.
  • the center line of each of the protrusions 22 extending in three directions extends substantially parallel to the radial direction of the housing element 20.
  • the projection 22 has a step 22 a parallel to the axial direction.
  • the side surfaces of the convex portions 22 are tapered.
  • the upper surface of the projection 22 is tapered.
  • a step 22b parallel to the horizontal direction is provided.
  • protrusions 23 i and 23 j are formed, which also function as positioning means.
  • a recess 22c is formed between the pair of protrusions 23k and 231, based on the protrusions 23k and 231.
  • the recess 22 protrudes upward with reference to the surface 20 a of the housing element 20.
  • FIG. 12 it can be said that a step is formed in the convex portion 22.
  • the projection 22 is continuous with the three projections 23 m, 23 n, and 23 p.
  • the head 10 is oriented in a specific direction with respect to the housing element 20, i.e. from the projections 23 a, 23 c, 23 e and 23 g, respectively.
  • the head portion 10 can be easily fitted to the housing element by sliding in a direction parallel to the radial direction in the protruding portions 23 b, 23 d, 23 mm, and 23 h.
  • the head portion 10 is difficult to slide in the reverse direction in parallel with the radial direction with respect to the housing element 20, which is preferable in certain applications.
  • the housing element may have a concave portion and the head portion may have a convex portion.
  • a protruding portion that acts as a locking portion in the radial direction may be further provided continuously to the protruding portion of the head portion. That is, in the embodiment of FIG. 2 and FIGS. 6 to 12, the housing element 20 is formed with the protrusion 22, but instead of the protrusion 22, a recess may be formed. .
  • the protrusion 22 and the protrusions 23a to 23n, 23p in the embodiment of FIGS. 2 and 6 to 12 may be formed on the head.
  • the upper surface and the side surfaces of the projection 22 need not be flat, but may be curved.
  • the concave portion corresponding to the convex portion 22 may be similarly formed with a curved surface.
  • At least one convex portion and at least one concave portion are formed on the contact surface of the housing element, and the contact surface of the head portion is detachably fitted to the convex portion of the housing element.
  • each protrusion and recess may be smaller than the protrusion 22 of the embodiment of FIGS. 2 and 6 to 12.
  • the cross-sectional shape of each of the concave portions and the convex portions may be circular, polygonal, or the like, and the depth of one concave portion does not need to be uniform. You may.
  • the positioning means is not limited to the convex portion and the concave portion, and includes, for example, a shape, a structure, and a mechanism that can be fitted to each other.
  • a fluororesin such as tetrafluoroethylene, a thermoplastic resin such as polyethylene, polypropylene, or polyamide; a metal material such as stainless steel is used.
  • a fluororesin such as tetrafluoroethylene, a thermoplastic resin such as polyethylene, polypropylene, or polyamide; a metal material such as stainless steel is used.
  • a fluorine resin such as tetrafluoroethylene
  • a thermoplastic resin such as polyethylene, polypropylene, or polyamide
  • a fluororesin such as tetrafluoroethylene, a thermoplastic resin such as polyethylene or polypropylene; and a metal material such as stainless steel are used.
  • thermoplastic resin such as fluororesin, polyethylene, polypropylene, or polyamide
  • metal material such as stainless steel
  • sealing members 28a, 28b, 28c for example, a rubber material such as perfluoro rubber, fluoro rubber, ethylene propylene rubber, and silicone rubber is used.
  • sealing member 50 include a fluororesin such as tetrafluoroethylene, a thermoplastic resin such as polyethylene, polypropylene, and polyamide; a rubber material such as polyfluoro rubber, fluoro rubber, ethylene propylene rubber, and silicone rubber. Is used.
  • Examples of the connecting member 40 include a metal material such as stainless steel; a thermoplastic resin, Plastic materials such as thermosetting resins and engineering plastics are used.
  • the plastic material includes a plastic material containing a reinforcing material such as glass fiber.
  • the connecting member 40 may be made of a plastic material containing a reinforcing material.
  • the first port 11a is connected to a supply liquid discharge pipe (not shown) for various manufacturing processes
  • the second boat 11b is connected to a permeate supply pipe (not shown).
  • the separation module 1 of the present embodiment is provided with the positioning means, the positioning is facilitated, and the housing element can be easily replaced.
  • the aspect of membrane separation has been mainly described.
  • the present invention is not limited to membrane separation, but can be applied to ion removal using an ion exchange resin.
  • the separation module of the present invention can be suitably used in a semiconductor manufacturing process.
  • the property that the housing element can be easily replaced is not limited to the semiconductor manufacturing process, but is applied to, for example, nuclear power, pharmaceuticals, food, wastewater (domestic wastewater, industrial wastewater) treatment, water supply, purification of reagents, etc. be able to.
  • the present invention is not limited to the above embodiment, and can be variously modified.
  • the pipes 12a, 12b, and 12c protrude from the contact surface 10b of the head 10 in the direction of the filter element 40.
  • the pipes 12a, 12b, and 12c do not need to protrude from the contact surface 10b of the head 10 in the direction of the fill element 40.
  • the pipes 12a, 12b, 12 are made by injection molding or the like.
  • a liquid separator module described in Japanese Patent Application Laid-Open No. H10-666836 may be used as the housing element.
  • the ring-shaped connecting member 30 will be described as an example. did.
  • the connecting member 30 may be another embodiment.
  • an outer cylinder described in JP-A-10-66804 may be used for the connecting member.
  • the housing element and the head portion are formed in a rectangular cross-sectional shape, and a flange is provided on each of the housing element and the head portion. Head parts may be connected.
  • the connecting member does not need to be separate from the housing element or the head part, and may be previously connected to the housing element or the head part in some form.
  • the “circumferential direction” does not need to be strictly along the circumferential direction, and may have a slight angle instead of a direction perpendicular to the axial direction.
  • the “radial direction” does not need to be strictly along the diametrical direction, but may be a direction substantially perpendicular to the axial direction, and may have a slight angle.

Abstract

A detachable separation module allowing housing elements to be replaced easily, comprising a head part (10) and a connection member (30) for connecting the head part (10) detachably to the housing elements (20), wherein positioning means (18, 22) determining the relative positional relation between the head part (10) and the housing elements (20) are formed in the head part or housing elements, whereby the separation module can be used as a membrane filtration module, particularly used to filtrate super clean fluid, for example, a fluid used in a semiconductor production process.

Description

明 細 書 着脱可能な分離モジュール 技術分野  Description Detachable detachable module Technical field
本発明は、 着脱可能な分離モジュールに関する。 かかる分離モジュールは、 膜 ろ過モジュールとして好適に用いることができ、 特に、 超清浄流体、 例えば、 半 導体製造プロセスで使用するような流体をろ過するのに好適に用いることができ る。  The present invention relates to a detachable separation module. Such a separation module can be suitably used as a membrane filtration module, and in particular, can be suitably used for filtering an ultraclean fluid such as a fluid used in a semiconductor manufacturing process.
背景技術  Background art
半導体製造プロセスにおける粒状物汚染を制御するためには、 サブミクロン微 粒子を除去する膜を持つ超清浄フィルター (即ち膜フィルター) を使用する必要 がある。 半導体ウェハ一上に付着した粒子は、 それが十分に大きい場合には半導 体ウェハ一に欠陥をもたらすものであることは良く知られている。  Controlling particulate contamination in semiconductor manufacturing processes requires the use of ultra-clean filters (ie, membrane filters) with membranes that remove submicron particulates. It is well known that particles deposited on a semiconductor wafer, if large enough, cause defects in the semiconductor wafer.
半導体工業ではキラー欠陥は代表的には、 半導体チップの最小特徴寸法の 1 1 0もの小ささの粒子によりもたらされ得る。 従って、 半導体製造プロセスの全 ての段階で、 液体とガスとを共に清浄化するための膜フィルタ一が使用される。 半導体製造プロセス装置にて、 膜ろ過モジュールを一対の連結部の間に挟まれ るように設計した場合には、 膜ろ過モジュールをプロセス装置へ接続するのが難 しくなる。  In the semiconductor industry, killer defects can typically be caused by particles as small as 110, the smallest feature size of a semiconductor chip. Therefore, at all stages of the semiconductor manufacturing process, a membrane filter for cleaning both liquid and gas is used. In a semiconductor manufacturing process device, if the membrane filtration module is designed to be sandwiched between a pair of connecting portions, it becomes difficult to connect the membrane filtration module to the process device.
そこで、 プロセス装置への組付けを簡易化し且つ膜フィルタ一の交換を容易化 するために、 膜ろ過モジュールの設計形状では、 全ての連結部が膜ろ過モジユー ルの一端部側に設けられることが多い。 この形式の膜ろ過モジュールでは、 送給 物ポ一卜と透過物ポートとは、 代表的には、 膜ろ過モジュールの上部或は "へッ ド" といわれる端部側に水平配向状態で配設される。 この膜ろ過モジュールはそ の形状から、 "T " 字型として参照される。 この T字型の膜ろ過モジュールは、 流体プロセスシステムの残余部分への結合を簡易化するものである。  Therefore, in order to simplify the assembly to the process equipment and facilitate replacement of the membrane filter, the design shape of the membrane filtration module requires that all the connecting parts be provided on one end side of the membrane filtration module. Many. In this type of membrane filtration module, the feed and permeate ports are typically placed in a horizontal orientation on top of the membrane filtration module or on the end called the "head". Is done. This membrane filtration module is referred to as "T" shaped because of its shape. This T-shaped membrane filtration module simplifies coupling to the rest of the fluid processing system.
一方、 特開平 1 0— 6 6 8 0 4号公報には、 自動販売機などの内部に付設し、 水道水等をろ過するための力一トリッジ式濾過器が記載されている。 この濾過器 はキャップと濾過器本体とを有し、 濾過器本体は、 金属製の外筒とこの外筒内に 着脱自在に装着し得る合成樹脂製の内筒とからなる二重構造になっている。 そし て、 キャップの内部に取り付けられた係合片と、 外筒に設けられた突出部とが互 いに係合することができる。 On the other hand, Japanese Patent Application Laid-Open No. H10-66684 describes a power cartridge type filter installed inside a vending machine or the like for filtering tap water or the like. This filter Has a cap and a filter main body, and the filter main body has a double structure including a metal outer cylinder and a synthetic resin inner cylinder that can be detachably mounted in the outer cylinder. Then, the engagement piece attached to the inside of the cap and the projection provided on the outer cylinder can engage with each other.
発明の開示  Disclosure of the invention
従来の膜ろ過モジュールでは、 ポートが設けられているヘッド部と、 分離要素 を内部に組み込んだハウジング要素との着脱が必ずしも容易ではなかった。 例え ば、 ヘッド部のポートが、 プロセス配管に連結されているまま、 ハウジング要素 を交換したい場合がある。 すると、 膜ろ過モジュールが配置されている位置によ つては、 必ずしも、 ハウジング要素とヘッド部との係合部分を目で見て確認でき ない。 例えば、 膜ろ過モジュールが設計の都合により、 床近くに配置されている ときには、 作業員がしゃがんで又は床に寝そべって係合部分を見るのは煩雑であ る。 目で見ることなく、 手からの感触に頼って、 交換することができることが望 まれる。  In the conventional membrane filtration module, it was not always easy to attach and detach the head part provided with the port and the housing element in which the separation element was incorporated. For example, you may want to replace a housing element while the head port remains connected to the process piping. Then, depending on the position where the membrane filtration module is arranged, the engaging portion between the housing element and the head cannot always be visually confirmed. For example, when the membrane filtration module is placed near the floor due to design reasons, it is cumbersome for workers to squat down or lie down on the floor to see the engagement. It is hoped that they can be replaced without relying on the eyes to see and feel.
また、 ハウジング要素を交換する際には、 アルバイ卜が作業する場合もあるの で、 誰がハウジング要素の着脱を行っても、 ヘッド部とハウジング要素とが同じ 程度の強さで連結していることが望まれる。 更に、 全ての作業員が筋骨隆々とい うわけではなく、 華奢であり、 力持ちではないものもいる。 そして、 腕力が限ら れている作業員であっても、 簡易にハウジング要素を交換することができること が所望される。  Also, when replacing the housing element, the work may need to be done by the participant.Therefore, the head and the housing element must be connected with the same level of strength, regardless of who removes and attaches the housing element. Is desired. Furthermore, not all workers are muscular, some are delicate and not strong. It is desired that even a worker having limited strength can easily replace the housing element.
従って、本発明の目的は、着脱が容易なろ過モジュールを提供することにある。 本発明の一側面では、 流入ポートと流出ポートとを有するへッド部と、 分離要素を内部に組み込んだハゥジング要素と、  Therefore, an object of the present invention is to provide a filtration module that can be easily attached and detached. In one aspect of the present invention, a head having an inflow port and an outflow port, a housing having a separation element incorporated therein,
前記へッド部と前記ハウジング要素とを着脱可能に連結するための連結部材と を具備する分離モジュールであって、  A connection member for detachably connecting the head part and the housing element, a separation module comprising:
前記へッド部と前記ハウジング要素との間の相対的な位置関係を定める位置決 め手段が、 前記へッド部及び前記ハウジング要素の少なくとも一方に形成されて いることを特徴とする分離モジュールが提供される。  A separation module, wherein positioning means for determining a relative positional relationship between the head part and the housing element is formed on at least one of the head part and the housing element. Is provided.
本発明において、 前記位置決め手段は、 前記ハウジング要素及び前記ヘッド部 の何れか一方に形成された少なくとも 1の嵌合部と、 前記嵌合部に着脱可能に嵌 合するように、 前記ハウジング要素及び前記へッド部の他方に形成した少なくと も 1の被嵌合部とからなることが好ましい。 In the present invention, the positioning means includes the housing element and the head portion. At least one fitting portion formed on one of the housing element and the other of the housing element and the head portion so as to be detachably fitted to the fitting portion. It is preferable that the connecting member includes a fitting portion.
このような嵌合部及び被嵌合部の一実施形態として、 前記ハゥジング要素は前 記へッド部に当接する当接面を有し、 前記へッド部は前記ハウジング要素に当接 する当接面を有し、 前記位置決め手段は、 前記ハウジング要素の前記当接面及び 前記へッド部の前記当接面の何れか一方に形成された少なくとも 1の凸部と、 前 記凸部に着脱可能に嵌合するように、 前記ハウジング要素の前記当接面及び前記 へッド部の前記当接面の他方に形成した少なくとも 1の凹部とからなることが好 ましい。  As one embodiment of such a fitting portion and a fitted portion, the housing element has a contact surface that comes into contact with the head portion, and the head portion comes into contact with the housing element. A contact surface, wherein the positioning means comprises: at least one protrusion formed on one of the contact surface of the housing element and the contact surface of the head portion; It preferably comprises at least one recess formed in the other of the contact surface of the housing element and the contact surface of the head portion so as to be detachably fitted to the housing element.
更に、 前記凸部又は前記凹部が前記ハウジング要素又は前記へッド部の径方向 とほぼ平行に伸びていることが好ましい。 更にまた、 前記凸部又は前記凹部にテ —パが形成されていることが好ましい。 更に、 前記凸部又は前記凹部に段差が形 成されていることが好ましい。  Further, it is preferable that the convex portion or the concave portion extends substantially parallel to a radial direction of the housing element or the head portion. Furthermore, it is preferable that a taper is formed in the convex portion or the concave portion. Further, it is preferable that a step is formed in the convex portion or the concave portion.
また、 前記ハウジング要素又は前記ヘッド部が係止部を有し、 前記連結部材が 前記係止部に係脱可能に係止する被係止部を有することが好ましい。  Further, it is preferable that the housing element or the head portion has a locking portion, and the connecting member has a locked portion that is removably locked to the locking portion.
更に、 前記位置決め手段の径方向の端部に、 前記係止部が形成されていること が好ましい。  Further, it is preferable that the locking portion is formed at a radial end of the positioning means.
また、 前記係止部が径方向への突出部であり、 前記被係止部が前記突出部に対 応し、 軸方向に延びる挿入部及び前記挿入部に連続し、 かつ、 直交する周方向に 延びる溝であることが好ましい。 この溝にテーパーが形成されていることが更に 好ましい。  Further, the locking portion is a radially projecting portion, and the locked portion corresponds to the projecting portion, an insertion portion extending in the axial direction, and a continuous with the insertion portion, and a circumferential direction orthogonal to the insertion portion. Preferably, the groove extends. More preferably, the groove is tapered.
前記分離要素が、 フィル夕要素又は複数の中空糸膜を含むことが好ましい。 前記分離要素が、 微多孔質 (microporous)膜、 限外ろ過 (ultrafiltration)膜、 逆 浸透圧 (reverse osmosis) 膜を含むことが好ましい。  Preferably, the separating element includes a filter element or a plurality of hollow fiber membranes. Preferably, the separation element comprises a microporous membrane, an ultrafiltration membrane, a reverse osmosis membrane.
更に、 前記連結部材が、 リング形状を有することが好ましい。  Further, it is preferable that the connecting member has a ring shape.
本発明の他の側面では、 供給液を上記の分離モジュールを透過させて透過液を 得る工程と、  In another aspect of the present invention, a step of permeating a feed solution through the separation module to obtain a permeate solution;
前記透過液を用いて、 半導体デバイスを製造する工程と、 を含む半導体デバイスの製造方法が提供される。 A step of manufacturing a semiconductor device using the permeate; A method for manufacturing a semiconductor device is provided.
本発明の他の側面では、 上記分離モジュールに用いることができる、 分離要素 を内部に組み込んだハゥジング要素が提供される。  According to another aspect of the present invention, there is provided a packaging element having a separation element incorporated therein, which can be used in the separation module.
図面の簡単な説明  BRIEF DESCRIPTION OF THE FIGURES
図 1は、 本発明の分離モジュールの好ましい一実施形態の断面図である。  FIG. 1 is a sectional view of a preferred embodiment of the separation module of the present invention.
図 2は、 図 1に示す分離モジュールの分解斜視図である。  FIG. 2 is an exploded perspective view of the separation module shown in FIG.
図 3は、 図 1に示す分離モジュールの側面図である。  FIG. 3 is a side view of the separation module shown in FIG.
図 4は、 図 1に示す分離モジュールの上面図である。  FIG. 4 is a top view of the separation module shown in FIG.
図 5は、 本発明の分離モジュールの一実施形態に用いることができる、 ポート の断面図である。  FIG. 5 is a sectional view of a port that can be used in one embodiment of the separation module of the present invention.
図 6は、 本発明の位置決め手段の他の実施形態を示し、 図 6 (a) は、 ハウジ ング要素の上面図であり、 図 6 (b) は、 ハウジング要素の側面図である。  FIG. 6 shows another embodiment of the positioning means of the present invention. FIG. 6 (a) is a top view of a housing element, and FIG. 6 (b) is a side view of a housing element.
図 7は、 本発明の位置決め手段の他の実施形態を示し、 図 7 (a) は、 ハウジ ング要素の上面図であり、 図 7 (b) は、 ハウジング要素の側面図である。  FIG. 7 shows another embodiment of the positioning means of the present invention. FIG. 7 (a) is a top view of a housing element, and FIG. 7 (b) is a side view of a housing element.
図 8は、 本発明の位置決め手段の他の実施形態を示し、 図 8 (a) は、 ハウジ ング要素の上面図であり、 図 8 (b) は、 ハウジング要素の側面図である。  FIG. 8 shows another embodiment of the positioning means of the present invention. FIG. 8 (a) is a top view of a housing element, and FIG. 8 (b) is a side view of a housing element.
図 9は、 本発明の位置決め手段の他の実施形態を示し、 図 9 (a) は、 ハウジ ング要素の上面図であり、 図 9 (b) は、 ハウジング要素の側面図である。  FIG. 9 shows another embodiment of the positioning means of the present invention. FIG. 9 (a) is a top view of a housing element, and FIG. 9 (b) is a side view of a housing element.
図 10は、 本発明の位置決め手段の他の実施形態を示し、 図 10 (a) は、 ハ ウジング要素の上面図であり、 図 10 (b) は、 ハウジング要素の側面図である。 図 1 1は、 本発明の位置決め手段の他の実施形態を示し、 図 1 1 (a) は、 ハ ウジング要素の上面図であり、 図 1 1 (b) は、 ハウジング要素の側面図である。 図 12は、 本発明の位置決め手段の他の実施形態を示し、 図 12 (a) は、 ハ ウジング要素の上面図であり、 図 12 (b) は、 ハウジング要素の側面図である。  FIG. 10 shows another embodiment of the positioning means of the present invention. FIG. 10 (a) is a top view of a housing element, and FIG. 10 (b) is a side view of a housing element. FIG. 11 shows another embodiment of the positioning means of the present invention. FIG. 11 (a) is a top view of a housing element, and FIG. 11 (b) is a side view of a housing element. . FIG. 12 shows another embodiment of the positioning means of the present invention. FIG. 12 (a) is a top view of a housing element, and FIG. 12 (b) is a side view of a housing element.
発明を卖施するための ft良の形餱  Ft good form to apply the invention
以下、 本発明の分離モジュールの好ましい一実施形態について、 図面を参照し て説明する。 ただし、 本発明は、 本実施形態により制限されるものではない。 本実施形態の分離モジュール 1は、図 1乃至 4に示すように、へッド部 10と、 分離要素 40を内部に組み込んだハウジング要素 20と、 前記へッド部と前記ハ ウジング要素とを着脱可能に連結するための連結部材 3 0とを具備する。 Hereinafter, a preferred embodiment of the separation module of the present invention will be described with reference to the drawings. However, the present invention is not limited by the present embodiment. As shown in FIGS. 1 to 4, the separation module 1 of the present embodiment includes a head part 10, a housing element 20 in which a separation element 40 is incorporated, the head part and the housing part. And a connecting member 30 for detachably connecting the housing element to the housing element.
本発明の一側面では、 へッド部 1 0とハウジング要素 2 0との間の相対的な位 置関係を定める位置決め手段 1 8、 2 2が、 前記ヘッド部 1 0及び前記ハウジン グ要素 2 0の少なくとも一方に形成されている。  According to one aspect of the present invention, positioning means 18, 22 for determining a relative positional relationship between the head portion 10 and the housing element 20 include the head portion 10 and the housing element 2. It is formed on at least one of zero.
本発明の一実施形態では、 前記位置決め手段は、 前記ハウジング要素及び前記 へッド部の何れか一方に形成された少なくとも 1の嵌合部、例えば、凸部 2 2と、 前記嵌合部に着脱可能に嵌合するように、 前記ハウジング要素及び前記へッド部 の他方に形成した少なくとも 1の被嵌合部、 例えば、 凹部 1 8とからなることが 好ましい。  In one embodiment of the present invention, the positioning means includes at least one fitting portion, for example, a convex portion 22 formed on one of the housing element and the head portion, and It is preferable that the housing element and the head portion include at least one fitted portion, for example, a concave portion 18 formed on the other of the housing portion so as to be detachably fitted.
従って、 へッド部及びハウジング要素との間で位置決めが容易にすることがで き、 両者の係合部分を目で確認しなくても、 作業時の手からの感触で確認するこ とができる。 よって、 前記ハウジング部を前記ヘッド部に容易に固定することが できる。  Therefore, the positioning between the head part and the housing element can be facilitated, and it is possible to confirm with the touch from the hand at the time of work without visually confirming the engagement part of both. it can. Therefore, the housing part can be easily fixed to the head part.
更に、 一実施形態では、 ヘッド部 1 0及びハウジング要素 2 0を連結すべく、 連結部材 3 0に力を付与したときに、 位置決め手段は、 このヘッド部 1 0のポー ト l l a、 l l b、 1 1 cに力がかかることを防止することができる。 例えば、 へッド部 1 0及びハウジング要素 2 0に対して連結部材 3 0を回転させるように 力を付与したときに、 位置決め手段 1 8、 2 2がこの回転力に対して抵抗するこ とができ、 ポート l l a、 l l b、 1 1 cに力がかかることを防止することがで きる。  Further, in one embodiment, when a force is applied to the connecting member 30 so as to connect the head portion 10 and the housing element 20, when the force is applied to the connecting member 30, the positioning means is connected to the ports lla, llb, 1 1 of the head portion 10. 1c can be prevented from being applied with force. For example, when a force is applied to the head part 10 and the housing element 20 so as to rotate the connecting member 30, the positioning means 18, 22 resist the rotational force. This prevents the ports lla, llb, and 11c from being stressed.
また、本発明では、前記ハウジング要素又は前記へッド部が係止部 2 3を有し、 前記連結部材 3 0が前記係止部に係脱可能に係止する被係止部 3 5を有すること が好ましい。 このように、 被係止部を備えた連結部材を用いることにより、 常に 一定の強さで、 ハウジング要素がヘッド部に固定することができる。 これに対し て、 例えば、 ボルト及びナットで固定したときには、 強く締めつけられる場合も あれば、 弱く締め付けられる場合もある。 なお、 係止部、 被係止部という用語は、 本明細書にて、互いに対をなすことを明確にするために用いられているに過ぎず、 連結部材 3 0に係止部 3 5が設けられているといってもよい。  Further, in the present invention, the housing element or the head portion has a locking portion 23, and the locked member 35 is provided so that the connecting member 30 is removably locked to the locking portion. It is preferred to have. As described above, by using the connecting member having the locked portion, the housing element can be always fixed to the head with a constant strength. On the other hand, for example, when fixed with bolts and nuts, there are cases where it is tightened strongly and cases where it is loosely tightened. The terms “locking portion” and “locked portion” are only used herein to clarify that they are paired with each other, and the locking portion 35 is attached to the connecting member 30. It may be said that it is provided.
ヘッド部 1 0は膜ろ過モジュールの上部に位置するのが好ましいが、 本発明の 本質から離れることなく、 下部或は底部に位置付けることもできる。 今後、 "上 部" 及び "ヘッド" なる用語は、 膜ろ過モジュールの、 連結用ポートが設けられ た端部を示すものとして、 また "下部" 及び "底部" なる用語はその反対側の端 部を示すものとして使用される。 なお、 膜ろ過モジュールは、 縦方向、 即ち、 モ ジュールの軸方向が鉛直方向となるように用いられるとは限らず、 横方向に用い られることもある。 The head section 10 is preferably located at the top of the membrane filtration module. It can be positioned at the bottom or bottom without leaving the essence. From now on, the terms "top" and "head" refer to the end of the membrane filtration module where the connection port is located, and the terms "bottom" and "bottom" refer to the opposite end. Is used to indicate The membrane filtration module is not always used in the vertical direction, that is, in the axial direction of the module, but may be used in the horizontal direction.
へッド部 1 0は、 例えば、 円盤状であり、 第 1ポート 1 1 a、 第 2ポート 1 1 b、 第 3ポー卜 1 1 cを有する。 一実施形態では、 例えば、 第 1ポート 1 1 aが 流入ポートとして作用し、 第 2ポート 1 1 bが流出ポ一トとして作用し、 第 3ポ ート 1 1 cがベントポートとして作用してもよい。あるいは、他の実施形態では、 第 1ポート 1 1 aが流出ポートとして作用し、 第 2ポ一ト 1 1 bが流入ポートと して作用してもよい。 第 1ポート 1 1 a、 第 2ポート l i b、 第 3ポート 1 1 c は、 ヘッド部 1 0の径方向と平行に直線状に配置されていることが好ましい。 へッド部 1 0はハウジング要素に当接する当接面 1 0 bを有し、 ハウジング要 素 2 0はヘッド部 1 0に当接する当接面 2 1 aを有する。 図 2で、 位置決め手段 は、 ハウジング要素 2 0の当接面 2 1 aに形成された凸部 2 2と、 凸部 2 2に着 脱可能に嵌合するように、 へッド部 1 0の当接面 1 0 bに形成した凹部 1 8とか らなる。 凸部 2 2及び凹部 1 8は、 径方向と平行に伸びていることが好ましい。 ハウジング要素 2 0の凸部 2 2には、 第 1ポート 1 1 a、 第 2ポート 1 1 b及 び第 3ポート 1 1 cそれぞれに対応して、 第 1開口 2 4 a、 第 2開口 2 4 b及び 第 3開口 2 4 cが設けられていることが好ましい。  The head portion 10 is, for example, disc-shaped and has a first port 11a, a second port 11b, and a third port 11c. In one embodiment, for example, the first port 11a acts as an inflow port, the second port 11b acts as an outflow port, and the third port 11c acts as a vent port. Is also good. Alternatively, in other embodiments, the first port 11a may act as an outflow port and the second port 11b may act as an inflow port. The first port 11a, the second port lib, and the third port 11c are preferably arranged linearly in parallel with the radial direction of the head portion 10. The head portion 10 has a contact surface 10b that contacts the housing element, and the housing element 20 has a contact surface 21a that contacts the head portion 10. In FIG. 2, the positioning means includes a convex portion 22 formed on the contact surface 21 a of the housing element 20 and a head portion 10 so as to be detachably fitted to the convex portion 22. And a concave portion 18 formed in the contact surface 10b of the contact hole 10b. It is preferable that the convex portions 22 and the concave portions 18 extend in parallel with the radial direction. The convex portion 22 of the housing element 20 has a first opening 24 a and a second opening 2 corresponding to the first port 11 a, the second port 11 b and the third port 11 c, respectively. 4b and a third opening 24c are preferably provided.
ハウジング要素 2 0の凸部 2 2の径方向の端部には、 連結部材の被係止部に係 脱可能に係止する係止部が形成されていることが好ましく、 例えば、 突出部 2 3 が形成されている。 即ち、 ハウジング要素 2 0の当接面 2 1 a側の側面には、 径 方向に突出している突出部 2 3を有していることが好ましい。 凸部 2 2の上面と 突出部 2 3の上面とは同一平面であってもよい。 もっとも、 凸部 2 2の上面と突 出部 2 3の上面との間には段差があってもよいし、 あるいは、 連続的にテ一パが 形成されていてもよい。  It is preferable that a locking portion is formed at a radial end of the convex portion 22 of the housing element 20 so as to be removably locked to the locked portion of the connecting member. 3 is formed. That is, it is preferable that the side surface of the housing element 20 on the side of the contact surface 21 a has a protruding portion 23 protruding in the radial direction. The upper surface of the protrusion 22 and the upper surface of the protrusion 23 may be on the same plane. Of course, there may be a step between the upper surface of the protrusion 22 and the upper surface of the protrusion 23, or a taper may be formed continuously.
ハウジング要素 2 0は、 中空の円柱体 2 1と、 その内部に配置された分離要素 4 0とを有する。 分離要素は、 フィル夕一要素であることが好ましく、 図 1に記 載されているように、 ハウジング要素 2 0の内部に収納することができるような 筒形状のフィル夕一要素であってもよい。 フィル夕一要素は、 微多孔質 (microporous)膜、 限外ろ過 (ultrafiltration), 〕 浸透圧 (reverse osmosis) 膜 を含むことが好ましい。 フィル夕一要素は、 ひだ付き (pleat)であってもよい。 あるいは、 特開平 1 0— 6 6 8 3 6号に記載されているように、 分離要素は、 筒 形状に配置された中空糸膜であり、各々の中空糸膜が微多孔質 (microporous)膜、 限外ろ過 (u rafiltration)、 逆浸透圧 (reverse osmosis) 膜であってもよい。 微多孔質 (microporous)膜、 限外ろ過 (ultrafiltration)、 逆浸透圧 (reverse osmosis) 膜は、 半導体製造プロセスにおいて、 液体中の粒状物又は気体の除去 に用いることができる。 もっとも、 本発明は半導体製造プロセス以外において、 液体中の粒状物又は気体の除去をすることもできる。 更に、 気体中の粒状物を除 去することを妨げるものではない。 更にまた、 分離要素として粒状等のイオン交 換樹脂、 例えば、 陽イオン交換樹脂及び陰イオン交換樹脂の混合物を用いて、 ィ オンを除去した純水を得ることもできる。 The housing element 20 is composed of a hollow cylindrical body 2 1 and a separating element disposed therein. 40. The separating element is preferably a filter element, and as shown in FIG. 1, may be a cylindrical filter element which can be housed inside the housing element 20. Good. The filter element preferably comprises a microporous membrane, an ultrafiltration,] reverse osmosis membrane. The fill element may be a pleat. Alternatively, as described in Japanese Patent Application Laid-Open No. H10-66883, the separation element is a hollow fiber membrane arranged in a cylindrical shape, and each hollow fiber membrane is a microporous membrane. Ultrafiltration, reverse osmosis membranes may also be used. Microporous, ultrafiltration, and reverse osmosis membranes can be used in semiconductor manufacturing processes to remove particulates or gases from liquids. However, the present invention can remove particulate matter or gas in a liquid other than the semiconductor manufacturing process. Furthermore, it does not prevent the removal of particulate matter in the gas. Furthermore, pure water from which ions have been removed can be obtained by using a granular ion exchange resin as a separation element, for example, a mixture of a cation exchange resin and an anion exchange resin.
フィルタ一要素 4 0は、 例えば、 コア部材 4 1、 コア部材に固定されているフ ィル夕一本体 4 2、 フィルタ一本体に固定されているコート層 4 3がこの順序で 径方向に外側に配置されていてもよい。 例えば、 コア部材 4 1、 フィルター本体 4 2及びコート層 4 3は、 端部部材 4 4と端部部材 4 5との間に挟まれていても よい。 端部部材 4 4には、 ポート 1 1 bに連通する開口部が形成されていてもよ く、 一方、 端部部材 4 5は閉じていてもよい。  The filter element 40 includes, for example, a core member 41, a filter main body 42 fixed to the core member, and a coating layer 43 fixed to the filter main body in this order in the radial direction. May be arranged. For example, the core member 41, the filter body 42, and the coat layer 43 may be sandwiched between the end members 44 and 45. The end member 44 may have an opening communicating with the port 11b, while the end member 45 may be closed.
一実施形態では、 連結部材 3 0は、 円筒状の本体 3 1と、 本体 3 1の上縁内方 に延設された押さえ部 3 2とを備えている。 本体 3 1には、 下縁から本体 3 1の 軸方向に向けて形成された挿入部 3 3と、 揷入部 3 3に連続し、 かつ、 直交する 周方向に延びる溝 3 4と、 からなる被係止部 3 5が形成されていることが好まし レ^ 連結部材 3 0の挿入部 3 3にハウジング要素 2 0の突出部 2 3を挿入し、 次 いで、 ハウジング要素 2 0に対して連結部材 3 0を回転させることにより、 突出 部 2 3が溝 3 4に沿って回転し、 へッド部 1 0とハウジング要素 2 0とを圧接さ せて固定することができる。 このときに、 凸部 2 2及び凹部 1 8が、 回転力に対 して抵抗することができ、 ボート 11 a、 l l b、 11 cに力がかからない。 溝 34には、 テーパ一34 aが設けられていることが好ましい。 これにより、 突出部 23が挿入された時点及び連結部材を少し回転させたときには、 溝 34に は軸方向に若干の遊びがあり、 突出部 23が回転するにつれて、 軸方向の遊びが 減少していき、 次第にきつく締まるように形成することができる。 In one embodiment, the connecting member 30 includes a cylindrical main body 31 and a pressing portion 32 extending inward of the upper edge of the main body 31. The main body 31 includes an insertion portion 33 formed from the lower edge in the axial direction of the main body 31, and a groove 34 continuous with the insertion portion 33 and extending in a circumferential direction orthogonal to the insertion portion 33. It is preferable that the locked portion 35 is formed. ^ The projection 23 of the housing element 20 is inserted into the insertion portion 33 of the connecting member 30, and then the housing element 20 is By rotating the connecting member 30, the protruding portion 23 rotates along the groove 34, and the head portion 10 and the housing element 20 can be pressed against each other and fixed. At this time, the convex portion 22 and the concave portion 18 are not capable of rotating torque. You can resist the boat 11a, llb, 11c with no force. The groove 34 is preferably provided with a taper 34a. Thus, when the protrusion 23 is inserted and when the connecting member is slightly rotated, the groove 34 has a slight play in the axial direction, and as the protrusion 23 rotates, the play in the axial direction decreases. It can be shaped to be tight and progressively tighter.
更に詳述すると、 本実施形態では、 突出部 23は、 長方体形状であり、 円柱体 21の周縁から外方に延出するように形成されている。 また、 突出部 23は、 ポ ート 11 a乃至 11 cと直線を形成するように 2っ配設されている。 被係止部 3 5は、 一対の突出部 23と対応するように、 2力所に設けられており、 挿入部 3 3は、 長方形状に形成されている。 もっとも、 突出部及び被係止部の数に制限は なく、 1つであってもよいし、 3以上であってもよい。  More specifically, in the present embodiment, the protrusion 23 has a rectangular shape, and is formed so as to extend outward from the peripheral edge of the cylindrical body 21. Further, two protruding portions 23 are provided so as to form a straight line with the ports 11a to 11c. The locked portion 35 is provided at two places so as to correspond to the pair of projecting portions 23, and the insertion portion 33 is formed in a rectangular shape. However, the numbers of the protruding portions and the locked portions are not limited, and may be one or three or more.
また、 ハウジング要素 20の内部と外部とが配管 12 a、 12 b, 12 cを介 して連通されている。 即ち、 第 1乃至 3開口 24 a, 24b, 24 cは、 それぞ れハウジング要素 20の上部を貫通する貫通孔であり、 第 1開口 24 a及び第 2 開口 25は、 それぞれフィルタ一本体 42の直上に位置し、 第 3開口 26は、 コ ァ部材 41で囲まれた中空部上に位置している。  The inside and the outside of the housing element 20 are communicated with each other via pipes 12a, 12b, and 12c. That is, the first to third openings 24a, 24b, and 24c are through holes that pass through the upper portion of the housing element 20, respectively, and the first opening 24a and the second opening 25 are respectively formed in the filter main body 42. The third opening 26 is located directly above the hollow portion surrounded by the core member 41.
第 1開口 24 a、 第 2開口 24 b及び第 3開口 24 cにおける当接面 21 a側 の端部には、 それぞれ、 シール部材 28 a, 28b、 28 cを載置するシール部 材設置部 27 a、 27 b, 27 cが形成されている。 シール部材設置部 27 a、 271、 27。は、 第 1乃至第 3開口 24 a、 24 b, 24 cの当接面 2 l a側 端部を各開口 24a、 24b、 24cの内径よりも広く、 円形に凹欠させて形成 されている。  At the end of the first opening 24a, the second opening 24b, and the third opening 24c on the side of the contact surface 21a, a sealing member mounting portion for placing the sealing members 28a, 28b, 28c respectively. 27a, 27b and 27c are formed. Seal member installation part 27a, 271, 27. Is formed such that the end of the first to third openings 24a, 24b, 24c on the contact surface 2la side is wider than the inner diameter of each of the openings 24a, 24b, 24c and is circularly concave.
シール部材設置部 27 a、 27b、 27 cには、 それぞれ、 シール部材、 例え ば、 0—リング 28 a、 28b、 28 cが設けられ、 シール部材 28 a、 28 b, 28 cにより、 液密構造となされている。 もっとも、 シ一ル部材 28 a、 28 b, 28 cは、 ヘッド部とハウジング要素とを液密構造にすることができる限り、 制 限されない。  Sealing member mounting portions 27a, 27b, 27c are provided with sealing members, for example, 0-rings 28a, 28b, 28c, respectively, and are liquid-tight by the sealing members 28a, 28b, 28c. The structure is made. However, the seal members 28a, 28b, 28c are not limited as long as the head portion and the housing element can be formed in a liquid-tight structure.
また、 シール部材設置部 27の深さは、 シール部材 28 a、 28b、 28 cの 厚みよりも若干、 薄く、 また、 シール部材設置部 27の外径は、 シール部材 28 a、 28 b、 28 cの外径よりも若干大きい。 これにより、 ハウジング要素 20 とヘッド部材 10とを連結したときには、 シ一ル部材 28 a、 28 b、 28 cが 上下方向に押し潰されて、 水平方向に変形することができる。 なお、 シール部材 28 a、 28 b, 28 cの内径は、 第 1乃至 3配管 12 a、 12 b、 12 cの外 形とほぼ同じである。 In addition, the depth of the seal member installation portion 27 is slightly smaller than the thickness of the seal members 28a, 28b, and 28c, and the outer diameter of the seal member installation portion 27 is slightly larger than the outside diameter of a, 28b, 28c. Thus, when the housing element 20 and the head member 10 are connected, the seal members 28a, 28b, 28c are crushed in the vertical direction and can be deformed in the horizontal direction. The inner diameters of the seal members 28a, 28b, 28c are substantially the same as the outer shapes of the first to third pipes 12a, 12b, 12c.
この実施形態では、 ヘッド部 10とシール部材 28 a、 28 b, 28 cとが圧 接されると、 圧接されて潰れたシール部材 28 a、 28 b, 28 cの内径面が各 配管 12 a、 12 b, 12 cの外周面に圧接される。 このため、 一つのシール部 材 28 a、 28 b、 28 cにより、 シール部材 28 a、 28 b, 28 cと各配管 12 a、 12 b、 12 cとの接触部分及びシール部材 28 a、 28 b, 28じと へッド部 10の当接面 10 bとの接触部分の 2力所でシールをすることができ、 従来のものに比してより高い液密構造とすることができる。  In this embodiment, when the head portion 10 and the seal members 28a, 28b, 28c are pressed against each other, the inner diameter surfaces of the pressed and crushed seal members 28a, 28b, 28c are connected to the respective pipes 12a. , 12b, 12c. For this reason, one sealing member 28a, 28b, 28c allows the contact portion between the sealing member 28a, 28b, 28c and each pipe 12a, 12b, 12c and the sealing member 28a, 28c. The seal can be made at two places of contact between the b and 28 heads and the contact surface 10b of the head portion 10, and a higher liquid-tight structure can be achieved as compared with the conventional one.
第 1ポート 1 1 aの一実施形態について、 図 5に示す。 もっとも、 ポートの形 状、 構造は、 この実施形態に限られず、 流体を通過させることができる限り、 制 限はない。  One embodiment of the first port 11a is shown in FIG. However, the shape and structure of the port are not limited to this embodiment, and there is no limitation as long as fluid can pass through.
第 1ポート 1 1 a、 第 2ポート 1 1 b及び第 3ポート 1 1 cは、 形状、 構造、 材質等全て同一であってもよいし、 形状、 構造、 材質の何れか又は全てが異なつ ていても良い。  The first port 11a, the second port 11b, and the third port 11c may all have the same shape, structure, material, or the like, or may have any or all of different shapes, structures, and materials. May be.
図 1及び図 5の実施形態では、 第 1ポート 1 1 a、 第 2ポート l i b、 第 3ポ —ト 1 1 cは、 それぞれ、 第 1配管 12 a、 第 2配管 12 b及び第 3配管 12 c を有している。 第 1配管 12 a、 第 2配管 12 b及び第 3配管 12 cは、 それぞ れ、 分離モジュール 1の軸方向に延びており、 ヘッド部 10を貫通して、 表面 1 0 a側及び当接面 10 b側から延出されている。  In the embodiments of FIGS. 1 and 5, the first port 11a, the second port lib, and the third port 11c are respectively the first pipe 12a, the second pipe 12b, and the third pipe 12b. c. The first pipe 12a, the second pipe 12b, and the third pipe 12c respectively extend in the axial direction of the separation module 1, penetrate the head part 10, and face the surface 10a and abut. Surface 10b extends from the side.
また、 ヘッド部 10の表面 10 a側に位置する端部には、 L字型で両端部にね じ切りが形成され、 ナツト部材 14が螺合されてなる連結部材 15がナツ卜部材 14を介して連結されて、 プロセス配管 (図示せず) と連結可能にされている。 また、 本実施形態においては、 第 1ポー卜 l l a、 第 2ポート l i b及び第 3 ポート 1 l cには、 それぞれ、 内部の清浄度を保持するために、 取り外し可能な 封止部材 50 a, 50 b, 50 cが設けられている。 封止部材は、 再利用される ものでもよいし、 使い捨てされるものでもよい。 Further, at the end located on the surface 10a side of the head portion 10, an L-shaped thread cut is formed at both ends, and a connecting member 15 formed by screwing a nut member 14 is used to connect the nut member 14. Through a pipe, and can be connected to a process pipe (not shown). In the present embodiment, the first port lla, the second port lib, and the third port 1lc respectively have removable sealing members 50a, 50b in order to maintain the internal cleanliness. , 50 c. Sealing members are reused They may be disposable or disposable.
具体的には、 本実施形態においては、 図 1に示すように、 第 1ポート l l a、 第 2ポ一ト 1 1 b及び第 3ポート 1 1 cのそれぞれの開口端に、封止部材 5 0 a , 5 0 b , 5 0 cとして、 粘着テープが貼付されている。 そして、 封止部材 5 0 a , 5 0 b , 5 0 cを取り外して、 第 1ポー卜 1 1 a、 第 2ポート 1 1 b及び第 3ポ —ト 1 1 cをそれぞれ図示されていないプロセス配管に連結することができる。 図 5では、 ポ一ト 1 1 aの端部には、 開口しているナット部材が設けられてい る。 ここで、 開口しているナット部材の代わりに、 断面コの字状のキャップ材が、 封止部材として配置されていてもよい。  Specifically, in the present embodiment, as shown in FIG. 1, a sealing member 50 is attached to each open end of the first port lla, the second port 11b, and the third port 11c. Adhesive tapes are affixed as a, 50b, and 50c. Then, the sealing members 50a, 50b, and 50c are removed, and the first port 11a, the second port 11b, and the third port 11c are respectively processed by a process not shown. Can be connected to piping. In FIG. 5, an open nut member is provided at the end of the port 11a. Here, a cap member having a U-shaped cross section may be arranged as a sealing member instead of the nut member that is open.
このように、 ヘッド部 1 0とハウジング要素 2 0とを別体にすることにより、 へッド部 1 0の第 1ポート 1 1 a及び第 2ポート 1 1 bをプロセス配管に連結し た状態で、 ハウジング要素 2 0を交換することができる。 これにより、 ハウジン グ要素 2 0を交換するときに、 第 1ポート 1 1 a及び第 2ポート 1 1 bの連結、 取り外しという作業を省略することができる。  Thus, by separating the head portion 10 and the housing element 20 from each other, the first port 11a and the second port 11b of the head portion 10 are connected to the process piping. Then, the housing element 20 can be replaced. Thereby, when exchanging the housing element 20, the work of connecting and disconnecting the first port 11a and the second port 11b can be omitted.
更に、本発明の位置決め手段は、上記実施形態に制限されるものではなく、種々 変形可能である。 図 6乃至図 1 2に、 本発明の位置決め手段の他の実施形態を示 す。  Furthermore, the positioning means of the present invention is not limited to the above embodiment, but can be variously modified. 6 to 12 show another embodiment of the positioning means of the present invention.
図 6乃至図 1 2では、 引用番号 2 0は、 ハウジング要素を示し、 図 6乃至 9及 び 1 2で、 引用番号 2 2は、 凸部を示す。 また、 引用番号 2 3 a乃至 2 3 n及び 2 3 pは、 突出部を示す。 なお、 図 6乃至図 1 2では、 説明の便宜上、 ハウジン グ要素 2 0の内部に連通する開口部が省略されている。  6 to 12, reference numeral 20 indicates a housing element, and in FIGS. 6 to 9 and 12, reference numeral 22 indicates a projection. Reference numbers 23a to 23n and 23p indicate protrusions. 6 to 12, the opening communicating with the inside of the housing element 20 is omitted for convenience of explanation.
図 2及び図 6乃至図 1 2の実施形態では、 位置決め手段として、 ハウジング要 素 2 0に凸部 2 2及び凸部 2 2に連続する突出部 2 3 a乃至 2 3 n、 2 3 pが形 成され、 ヘッド部 1 0に凹部又は対応する形状が形成されている。 これにより、 ハウジング要素 2 0とヘッド部との位置決めが容易にされている。 図 6乃至図 1 1の実施形態でも、 凸部 2 2、 特に、 凸部 2 2の中心線は、 ハウジング要素 2 0 の径方向とほぼ平行に伸びている。 また、 図 1 2の実施形態でも、 3方向に伸び ている凸部 2 2の各々の中心線は、 ハウジング要素 2 0の径方向とほぼ平行に伸 びている。 図 6では、 凸部 2 2に、 軸方向と平行な段差 2 2 aが設けられている。 図 7で は、 凸部 2 2の側面がテ一パされている。 図 8では、 凸部 2 2の上面がテ一パさ れている。 図 9では、 水平方向と平行な段差 2 2 bが設けられている。 図 1 0で は、 位置決め手段としても作用する、 突出部 2 3 i 、 2 3 jが形成されている。 図 1 1では、 一対の突出部 2 3 k、 2 3 1の間に突出部 2 3 k、 2 3 1を基準と しては凹部 2 2 cが形成されている。 この凹部 2 2は、 ハウジング要素 2 0の表 面 2 0 aを基準としては上方に突起している。 なお、 図 1 1では、 凸部 2 2に段 差が形成されているということができる。 図 1 2では、 凸部 2 2が、 3つの突出 部 2 3 m、 2 3 n、 2 3 pに連続している。 In the embodiments of FIGS. 2 and 6 to 12, as the positioning means, the projections 22 and the projections 23 a to 23 n and 23 p continuous with the projections 22 are provided on the housing element 20. A concave portion or a corresponding shape is formed in the head portion 10. This facilitates the positioning of the housing element 20 and the head. In the embodiment of FIGS. 6 to 11 as well, the projection 22, in particular the center line of the projection 22, extends substantially parallel to the radial direction of the housing element 20. Also, in the embodiment of FIG. 12, the center line of each of the protrusions 22 extending in three directions extends substantially parallel to the radial direction of the housing element 20. In FIG. 6, the projection 22 has a step 22 a parallel to the axial direction. In FIG. 7, the side surfaces of the convex portions 22 are tapered. In FIG. 8, the upper surface of the projection 22 is tapered. In FIG. 9, a step 22b parallel to the horizontal direction is provided. In FIG. 10, protrusions 23 i and 23 j are formed, which also function as positioning means. In FIG. 11, a recess 22c is formed between the pair of protrusions 23k and 231, based on the protrusions 23k and 231. The recess 22 protrudes upward with reference to the surface 20 a of the housing element 20. In FIG. 11, it can be said that a step is formed in the convex portion 22. In FIG. 12, the projection 22 is continuous with the three projections 23 m, 23 n, and 23 p.
図 6乃至図 9の実施形態では、 ハウジング要素 2 0に対して、 ヘッド部 1 0を 特定の方向に、 即ち、 それぞれ、 突出部 2 3 a、 2 3 c、 2 3 e、 2 3 gから突 出部 2 3 b、 2 3 d、 2 3 ί、 2 3 hの方向に、 径方向と平行にスライドさせる ことにより、 ヘッド部 1 0をハウジング要素に容易に嵌合することができる。 特 に、 図 7及び図 8の実施形態では、 ハウジング要素 2 0に対して、 ヘッド部 1 0 を逆方向に径方向と平行にスライドし難いので、 ある用途では好ましい。  In the embodiment of FIGS. 6 to 9, the head 10 is oriented in a specific direction with respect to the housing element 20, i.e. from the projections 23 a, 23 c, 23 e and 23 g, respectively. The head portion 10 can be easily fitted to the housing element by sliding in a direction parallel to the radial direction in the protruding portions 23 b, 23 d, 23 mm, and 23 h. In particular, in the embodiment of FIGS. 7 and 8, the head portion 10 is difficult to slide in the reverse direction in parallel with the radial direction with respect to the housing element 20, which is preferable in certain applications.
他の実施形態では、 ハウジング要素に凹部が形成され、 ヘッド部に凸部が形成 されていてもよい。 この実施形態では、 更に、 ヘッド部の凸部に連続して、 径方 向に係止部として作用する突出部が設けられても良い。 即ち、 図 2及び図 6乃至 図 1 2の実施形態では、 ハウジング要素 2 0に凸部 2 2が形成されているが、 こ の凸部 2 2の替わりに、 凹部が形成されていてもよい。 そして、 ヘッド部に、 図 2及び図 6乃至図 1 2の実施形態における、 凸部 2 2及び突出部 2 3 a乃至 2 3 n、 2 3 pが形成されていてもよい。  In another embodiment, the housing element may have a concave portion and the head portion may have a convex portion. In this embodiment, a protruding portion that acts as a locking portion in the radial direction may be further provided continuously to the protruding portion of the head portion. That is, in the embodiment of FIG. 2 and FIGS. 6 to 12, the housing element 20 is formed with the protrusion 22, but instead of the protrusion 22, a recess may be formed. . The protrusion 22 and the protrusions 23a to 23n, 23p in the embodiment of FIGS. 2 and 6 to 12 may be formed on the head.
あるいは、 ある実施形態では、 凸部 2 2の上面、側面は平面である必要はなく、 曲面が形成されていてもよい。 この実施形態では、 凸部 2 2に対応する凹部も同 様に曲面が形成されていてもよい。  Alternatively, in one embodiment, the upper surface and the side surfaces of the projection 22 need not be flat, but may be curved. In this embodiment, the concave portion corresponding to the convex portion 22 may be similarly formed with a curved surface.
あるいは、 ハウジング要素の当接面には、 少なくとも 1の凸部と少なくとも 1 の凹部が形成され、 かつ、 ヘッド部の当接面には、 ハウジング要素の凸部に着脱 可能に嵌合することができる少なくとも一つの凹部と、 前記ハウジング要素の前 記凹部に着脱可能に嵌合することができる少なくとも一つの凸部が形成されてい てもよい。 図 2及び図 6乃至 1 2の実施形態の凸部 2 2と比べて、 この実施形態 では、 各々の凸部及び凹部は小さくても良い。 例えば、 各々の凹部及び凸部の横 断面形状は、 円形、 多角形などであってもよいし、 一つの凹部の深さが均一であ る必要はなく、 一の凹部の底面に段差があってもよい。 位置決め手段は、 凸部及 び凹部に限定されるものではなく、 例えば、 互いに嵌合できる形状、 構造、 機構 が含まれる。 Alternatively, at least one convex portion and at least one concave portion are formed on the contact surface of the housing element, and the contact surface of the head portion is detachably fitted to the convex portion of the housing element. At least one concave portion, and at least one convex portion that can be detachably fitted into the concave portion of the housing element. You may. In this embodiment, each protrusion and recess may be smaller than the protrusion 22 of the embodiment of FIGS. 2 and 6 to 12. For example, the cross-sectional shape of each of the concave portions and the convex portions may be circular, polygonal, or the like, and the depth of one concave portion does not need to be uniform. You may. The positioning means is not limited to the convex portion and the concave portion, and includes, for example, a shape, a structure, and a mechanism that can be fitted to each other.
次いで、 本実施形態の分離モジュール 1の各部材の好ましい形成材料について 説明する。  Next, a preferable material for forming each member of the separation module 1 of the present embodiment will be described.
ヘッド部 1 0としては、 例えば、 テトラフルォロエチレン等のフッ素樹脂、 ポ リエチレン、 ポリプロピレン、 ポリアミド等の熱可塑性樹脂;ステンレス鋼等の 金属材料等が用いられる。  As the head portion 10, for example, a fluororesin such as tetrafluoroethylene, a thermoplastic resin such as polyethylene, polypropylene, or polyamide; a metal material such as stainless steel is used.
ハウジング要素 2 0のハウジングとしては、 例えば、 テトラフルォロエチレン 等のフッ素樹脂、ポリエチレン、ポリプロピレン、ポリアミド等の熱可塑性樹脂; ステンレス鋼等の金属材料等が用いられる。  As the housing of the housing element 20, for example, a fluororesin such as tetrafluoroethylene, a thermoplastic resin such as polyethylene, polypropylene, or polyamide; a metal material such as stainless steel is used.
フィル夕一要素 4 0としては、 例えば、 テトラフルォロエチレン等のフッ素樹 脂、 ポリエチレン、 ポリプロピレン、 ポリアミド等の熱可塑性樹脂等が用いられ る。  As the filter element 40, for example, a fluorine resin such as tetrafluoroethylene, a thermoplastic resin such as polyethylene, polypropylene, or polyamide is used.
配管 1 2 a、 1 2 b、 1 2 cとしては、 例えば、 テトラフルォロエチレン等の フッ素樹脂、 ポリエチレン、 ポリプロピレン等の熱可塑性樹脂;ステンレス鋼等 の金属材料等が用いられる。  As the pipes 12a, 12b, and 12c, for example, a fluororesin such as tetrafluoroethylene, a thermoplastic resin such as polyethylene or polypropylene; and a metal material such as stainless steel are used.
連結部材 1 5としては、 例えば、 フッ素樹脂、 ポリエチレン、 ポリプロピレン、 ポリアミド等の熱可塑性樹脂;ステンレス鋼等の金属材料等が用いられる。  As the connecting member 15, for example, a thermoplastic resin such as fluororesin, polyethylene, polypropylene, or polyamide; a metal material such as stainless steel is used.
シール部材 2 8 a、 2 8 b、 2 8 cとしては、 例えば、 パーフロロゴム、 フッ 素ゴム、 エチレンプロピレンゴム、 シリコンゴム等のゴム材料等が用いられる。 封止部材 5 0としては、 例えば、 テトラフルォロエチレン等のフッ素樹脂、 ポ リエチレン、 ポリプロピレン、 ポリアミド等の熱可塑性樹脂;パ一フロロゴム、 フッ素ゴム、 エチレンプロピレンゴム、 シリコンゴム等のゴム材料等が用いられ る。  As the sealing members 28a, 28b, 28c, for example, a rubber material such as perfluoro rubber, fluoro rubber, ethylene propylene rubber, and silicone rubber is used. Examples of the sealing member 50 include a fluororesin such as tetrafluoroethylene, a thermoplastic resin such as polyethylene, polypropylene, and polyamide; a rubber material such as polyfluoro rubber, fluoro rubber, ethylene propylene rubber, and silicone rubber. Is used.
連結部材 4 0としては、 例えば、 ステンレス鋼等の金属材料;熱可塑性樹脂、 熱硬化性樹脂、 エンジニアリングプラスチック等のプラスチック材料が用いられ る。 Examples of the connecting member 40 include a metal material such as stainless steel; a thermoplastic resin, Plastic materials such as thermosetting resins and engineering plastics are used.
なお、 本明細書には、 プラスチック材料には、 ガラスファイバ一等の強化材を 含むプラスチック材料が含まれる。 例えば、 連結部材 4 0として、 強化材を含む プラスチック材料を用いても良い。  In this specification, the plastic material includes a plastic material containing a reinforcing material such as glass fiber. For example, the connecting member 40 may be made of a plastic material containing a reinforcing material.
本実施形態の分離モジュール 1は、 第 1ポート 1 1 aを各種製造プロセスの供 給液の排出配管(図示せず)に連結し、第 2ボート 1 1 bを透過液の導入配管(図 示せず) に連結し、 第 3ポート 1 1 cを介して気体排出用の配管 (図示せず) に 連結し、第 1ポート 1 1 aに供給液を導入することにより使用することができる。 そして、 本実施形態の分離モジュール 1は、 位置決め手段が設けられているの で、 位置決めが容易になり、 ハウジング要素を容易に交換することができる。 本発明の分離モジュールについては、 膜分離という側面を主に説明した。 しか し、 本発明は、 膜分離に限られることなく、 イオン交換樹脂を用いるイオンの除 去に適用することもできる。  In the separation module 1 of the present embodiment, the first port 11a is connected to a supply liquid discharge pipe (not shown) for various manufacturing processes, and the second boat 11b is connected to a permeate supply pipe (not shown). ) Can be used by connecting to a gas discharge pipe (not shown) via the third port 11c and introducing the supply liquid to the first port 11a. Further, since the separation module 1 of the present embodiment is provided with the positioning means, the positioning is facilitated, and the housing element can be easily replaced. As for the separation module of the present invention, the aspect of membrane separation has been mainly described. However, the present invention is not limited to membrane separation, but can be applied to ion removal using an ion exchange resin.
本発明の分離モジュールは、半導体製造プロセスに好適に用いることができる。 しかし、 ハウジング要素を容易に交換できるという特性は、 半導体製造プロセス に限られることなく、 例えば、 原子力、 医薬品、 食品、 廃水 (生活廃水、 工業廃 水) 処理、 上水道、 試薬の精製等に適用することができる。  The separation module of the present invention can be suitably used in a semiconductor manufacturing process. However, the property that the housing element can be easily replaced is not limited to the semiconductor manufacturing process, but is applied to, for example, nuclear power, pharmaceuticals, food, wastewater (domestic wastewater, industrial wastewater) treatment, water supply, purification of reagents, etc. be able to.
更に、 本発明は、 上記実施形態に制限されるものではなく、 種々変形可能であ る。  Furthermore, the present invention is not limited to the above embodiment, and can be variously modified.
例えば、 図 1では、 配管 1 2 a、 1 2 b、 1 2 cは、 ヘッド部 1 0の当接面 1 0 bからフィルタ一要素 4 0の方向へ突出している。 しかし、 配管 1 2 a、 1 2 b、 1 2 cは、 ヘッド部 1 0の当接面 1 0 bからフィル夕一要素 4 0の方向へ突 出していなくてもよい。 この後者の実施態様では、 射出成形などにより、 配管 1 2 a、 1 2 b , 1 2。又は配管1 2 3、 1 2 b、 1 2 cを含むポート 1 1 a、 1 1 b、 1 1 cをへッド部と一体的に成形することが容易になる。  For example, in FIG. 1, the pipes 12a, 12b, and 12c protrude from the contact surface 10b of the head 10 in the direction of the filter element 40. However, the pipes 12a, 12b, and 12c do not need to protrude from the contact surface 10b of the head 10 in the direction of the fill element 40. In this latter embodiment, the pipes 12a, 12b, 12 are made by injection molding or the like. Alternatively, it becomes easy to integrally mold the ports 11a, 11b, and 11c including the pipes 123, 12b, and 12c with the head portion.
例えば、 ハウジング要素として、 特開平 1 0— 6 6 8 3 6号公報に記載されて いる液体分離器モジュールを用いても良い。  For example, a liquid separator module described in Japanese Patent Application Laid-Open No. H10-666836 may be used as the housing element.
また、 上述の実施形態においては、 リング形状の連結部材 3 0を例示して説明 した。 しかし、 連結部材 3 0は他の実施形態であってもよい。 例えば、 特開平 1 0 - 6 6 8 0 4号公報に記載されている外筒を連結部材に用いても良い。 また、 ハウジング要素及びへッド部の横断面形状を長方形に形成し、 ハウジング要素及 びへッド部にそれぞれフランジを設けて、 連結部材をそのフランジに横方向から スライドさせて、 ハウジング要素及びへッド部を連結させてもよい。 In the above-described embodiment, the ring-shaped connecting member 30 will be described as an example. did. However, the connecting member 30 may be another embodiment. For example, an outer cylinder described in JP-A-10-66804 may be used for the connecting member. Further, the housing element and the head portion are formed in a rectangular cross-sectional shape, and a flange is provided on each of the housing element and the head portion. Head parts may be connected.
更に、 連結部材は、 ハウジング要素又はヘッド部と別体である必要はなく、 ハ ゥジング要素又はへッド部に何らかの形態で予め連結されていてもよい。  Further, the connecting member does not need to be separate from the housing element or the head part, and may be previously connected to the housing element or the head part in some form.
なお、 本明細書において 「周方向」 とは、 厳密に周方向に沿う必要ななく、 軸 方向と直角方向ではなく、 若千角度を有してもよい。  In the present specification, the “circumferential direction” does not need to be strictly along the circumferential direction, and may have a slight angle instead of a direction perpendicular to the axial direction.
本明細書において 「径方向」 とは、 厳密に直径方向に沿う必要ななく、 軸方向 とほぼ直角方向であればよく、 若干角度を有してもよい。  In the present specification, the “radial direction” does not need to be strictly along the diametrical direction, but may be a direction substantially perpendicular to the axial direction, and may have a slight angle.
本発明の分離モジュールは、 へッド部とハウジング要素との位置決めが容易で あり、 ハウジング要素を容易にへッド部に取り付けることができる。  ADVANTAGE OF THE INVENTION In the separation module of this invention, positioning of a head part and a housing element is easy, and a housing element can be easily attached to a head part.

Claims

請求の範囲 The scope of the claims
1 . 流入ポートと流出ポートとを有するへッド部と、 1. a head having an inflow port and an outflow port;
分離要素を内部に組み込んだハウジング要素と、  A housing element with a separating element incorporated therein;
前記へッド部と前記ハウジング要素とを着脱可能に連結するための連結部材と を具備する分離モジュールであって、  A connection member for detachably connecting the head part and the housing element, a separation module comprising:
前記へッド部と前記ハウジング要素との間の相対的な位置関係を定める位置決 め手段が、 前記へッド部及び前記ハウジング要素の少なくとも一方に形成されて いることを特徴とする分離モジュール。  A separation module, wherein positioning means for determining a relative positional relationship between the head part and the housing element is formed on at least one of the head part and the housing element. .
2 . 前記位置決め手段は、 前記ハウジング要素及び前記ヘッド部の何れか一方 に形成された少なくとも 1の嵌合部と、前記嵌合部に着脱可能に嵌合するように、 前記ハウジング要素及び前記へッド部の他方に形成した少なくとも 1の被嵌合部 とからなる請求項 1に記載の分離モジュール。 2. The positioning means comprises: at least one fitting portion formed on one of the housing element and the head portion; The separation module according to claim 1, comprising at least one fitted portion formed on the other of the pad portions.
3 . 前記ハウジング要素は前記へッド部に当接する当接面を有し、  3. The housing element has a contact surface that contacts the head portion,
前記へッド部は前記ハウジング要素に当接する当接面を有し、  The head has an abutment surface that abuts the housing element,
前記位置決め手段は、 前記ハウジング要素の前記当接面及び前記へッド部の前 記当接面の何れか一方に形成された少なくとも 1の凸部と、 前記凸部に着脱可能 に嵌合するように、 前記ハウジング要素の前記当接面及び前記へッド部の前記当 接面の他方に形成した少なくとも 1の凹部とからなる請求項 1又は 2に記載の分 離モシユーリレ。  The positioning means is detachably fitted to at least one projection formed on one of the contact surface of the housing element and the contact surface of the head. The separation module according to claim 1, comprising the contact surface of the housing element and at least one recess formed in the other of the contact surfaces of the head portion.
4. 前記凸部又は前記凹部が前記ハウジング要素又は前記へッド部の径方向と ほぼ平行に伸びている請求項 3に記載の分離モジュール。  4. The separation module according to claim 3, wherein the convex portion or the concave portion extends substantially parallel to a radial direction of the housing element or the head portion.
5 . 前記凸部又は前記凹部にテーパが形成されている請求項 3又は 4に記載の 分離モジュール。  5. The separation module according to claim 3, wherein the convex portion or the concave portion is tapered.
6 . 前記凸部又は前記凹部に段差が形成されている請求項 3、 4又は 5に記載 の分離モジュール。  6. The separation module according to claim 3, 4 or 5, wherein a step is formed in the convex portion or the concave portion.
7 . 前記ハウジング要素又は前記ヘッド部が係止部を有し、 前記連結部材が前 記係止部に係脱可能に係止する被係止部を有する、 上記請求項の何れかに記載の 分離モジュール。 7. The method according to claim 1, wherein the housing element or the head portion has a locking portion, and the connecting member has a locked portion that is removably locked to the locking portion. Separation module.
8 . 前記位置決め手段の径方向の端部に、 前記係止部が形成されている請求項 7に記載の分離モジュール。 8. The separation module according to claim 7, wherein the locking portion is formed at a radial end of the positioning means.
9 . 前記係止部が径方向への突出部であり、 前記被係止部が前記突出部に対応 し、 軸方向に延びる揷入部及び前記挿入部に連続し、 かつ、 直交する周方向に延 びる溝である請求項 7又は 8に記載の分離モジュール。  9. The locking portion is a radially protruding portion, and the locked portion corresponds to the protruding portion, and is continuous with the insertion portion extending in the axial direction and the insertion portion, and in a circumferential direction orthogonal to the insertion portion. 9. The separation module according to claim 7, wherein the separation module is an extending groove.
1 0 . 前記溝にテ一パが形成されている請求項 9に記載の分離モジュール。 10. The separation module according to claim 9, wherein a taper is formed in the groove.
1 1 . 前記分離要素が、 フィルタ要素又は複数の中空糸膜を含む上記請求項の 何れかに記載の分離モジュ一ル。 11. The separation module according to claim 1, wherein the separation element includes a filter element or a plurality of hollow fiber membranes.
1 2 . 前記分離要素が、 微多孔質膜、 限外ろ過膜、 逆浸透圧膜を含む上記請求 項の何れかに記載の分離モジュ一ル。  12. The separation module according to claim 1, wherein the separation element includes a microporous membrane, an ultrafiltration membrane, and a reverse osmosis membrane.
1 3 . 前記連結部材が、 リング形状を有する上記請求項の何れかに記載の分離 モンユール。  13. The separation module according to claim 1, wherein the connecting member has a ring shape.
1 4. 供給液を上記請求項の何れかに記載の分離モジュールを透過させて透過 液を得る工程と、  1 4. a step of permeating the feed liquid through the separation module according to any of the above claims to obtain a permeate;
前記透過液を用いて、 半導体デバイスを製造する工程と、  A step of manufacturing a semiconductor device using the permeate;
を含む半導体デバイスの製造方法。 A method for manufacturing a semiconductor device, comprising:
1 5 . 請求項 1〜1 3に記載の分離モジュールに用いることができる、 分離要 素を内部に組み込んだハウジング要素。  15. A housing element with a separating element incorporated therein, which can be used in the separating module according to claims 1 to 13.
PCT/JP2000/004467 1999-07-05 2000-07-05 Detachable separation module WO2001002084A1 (en)

Priority Applications (2)

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AU58482/00A AU5848200A (en) 1999-07-05 2000-07-05 Detachable separation module
JP2001507569A JP4698105B2 (en) 1999-07-05 2000-07-05 Detachable separation module

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Application Number Priority Date Filing Date Title
JP19079099 1999-07-05
JP11/190790 1999-07-05

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JP2019217437A (en) * 2018-06-18 2019-12-26 三浦工業株式会社 Water treatment device

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Publication number Priority date Publication date Assignee Title
JP2005349283A (en) * 2004-06-09 2005-12-22 Japan Organo Co Ltd Cartridge type filter
JP2019217437A (en) * 2018-06-18 2019-12-26 三浦工業株式会社 Water treatment device
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JP4698105B2 (en) 2011-06-08

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