WO1997046309A1 - Procede et dispositif pour melanger un second milieu a un premier milieu - Google Patents

Procede et dispositif pour melanger un second milieu a un premier milieu Download PDF

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Publication number
WO1997046309A1
WO1997046309A1 PCT/FI1997/000325 FI9700325W WO9746309A1 WO 1997046309 A1 WO1997046309 A1 WO 1997046309A1 FI 9700325 W FI9700325 W FI 9700325W WO 9746309 A1 WO9746309 A1 WO 9746309A1
Authority
WO
WIPO (PCT)
Prior art keywords
casing
recited
mixer
medium
flow
Prior art date
Application number
PCT/FI1997/000325
Other languages
English (en)
Inventor
Kari Peltonen
Reijo Vesala
Original Assignee
A. Ahlström Osakeyhtiö
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from PCT/FI1996/000330 external-priority patent/WO1997001074A1/fr
Application filed by A. Ahlström Osakeyhtiö filed Critical A. Ahlström Osakeyhtiö
Priority to DE69709102T priority Critical patent/DE69709102T2/de
Priority to EP97924040A priority patent/EP0907409B1/fr
Priority to CA002256594A priority patent/CA2256594C/fr
Priority to AT97924040T priority patent/ATE210492T1/de
Priority to US09/194,358 priority patent/US6193406B1/en
Publication of WO1997046309A1 publication Critical patent/WO1997046309A1/fr
Priority to US09/757,479 priority patent/US20010006484A1/en

Links

Classifications

    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C9/00—After-treatment of cellulose pulp, e.g. of wood pulp, or cotton linters ; Treatment of dilute or dewatered pulp or process improvement taking place after obtaining the raw cellulosic material and not provided for elsewhere
    • D21C9/10—Bleaching ; Apparatus therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/50—Pipe mixers, i.e. mixers wherein the materials to be mixed flow continuously through pipes, e.g. column mixers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/96—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with openwork frames or cages
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21B—FIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
    • D21B1/00—Fibrous raw materials or their mechanical treatment
    • D21B1/04—Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
    • D21B1/12—Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres by wet methods, by the use of steam
    • D21B1/30—Defibrating by other means
    • D21B1/34—Kneading or mixing; Pulpers
    • D21B1/342—Mixing apparatus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/30—Driving arrangements; Transmissions; Couplings; Brakes
    • B01F35/32—Driving arrangements
    • B01F35/32005—Type of drive
    • B01F35/32015—Flow driven

Definitions

  • the present invention relates to a method and apparatus for mixing a second medium with a first medium.
  • the method and apparatus of the invention are especially suitable for mixing different chemicals, both fluid and gaseous ones, or steam with a so-called first medium, which is composed of both solid and fluid matter, like for example, cellulose fibre suspensions of the wood- processing industry or mixtures of, e.g., different beet chips (such as potato and sugar beet) and water.
  • Prior art mixers used for this purpose are disclosed, e.g., in US patents 5,279,709 and 5,575,559 and in patent applications EP-A-92921912, EP-A-9100973, WO-A-96/32186, and WO-A-96/33007. It is a characteristic feature of all mixers of the art that they employ a rotatable rotor in order to provide a sufficient mixing efficiency.
  • the rotatable rotor specifically refers to a member which is connected to the drive through a shaft and most usually receives its power from the electricity supply of the mill.
  • the mixer construction is usually such that a certain pressure loss occurs in the mixer.
  • the method and apparatus in accordance with the invention eliminate one of the power-losing factors mentioned above.
  • the rotor of the mixer is arranged to rotate freely in the flow, whereby the mixer naturally causes a certain pressure loss.
  • the pressure loss has not increased, at least not essentially, when compared with a motor-driven rotor.
  • no change in the mixing result can be found, at least not for the worse.
  • So-called static mixers are known in the art, but they are mostly of the type disclosed in, e.g., US patents 4,030,969, 5,492,409, and 5,556,200, in which a throttl- ing effect of some degree is arranged in the flow chan ⁇ nel, whereby the flow rate increases and the pressure is reduced.
  • the chemical or equivalent to be mixed is then conveyed to this lower-pressure zone, and the turbulence effect, also developed by throttling, then mixes the chemical or equivalent with the actual flow material.
  • Another alternative is disclosed in, for example, US patents 4,936,689 and 5,564,827, where the flow channel is provided with obstacles to flow so as to create turbu ⁇ lence. It is a characteristic feature of both types of mixers that the turbulence created is of local nature only and short in duration.
  • the kinetic energy originating from the pressure losses caused by the throttling device may be forwarded to the mixing zone in a more controlled manner and to a wider area, which will substantially grow the efficient mixing volume and substantially lengthen the mixing time.
  • Fig. 1 is an axial section view of an apparatus in accordance with a preferred embodiment of the invention
  • Fig. 2 is an axial section view of an apparatus in accordance with a second preferred embodiment of the invention.
  • Fig. 3 is an axial section view of an apparatus in accordance with a third preferred embodiment of the in ⁇ vention.
  • Fig. 1 shows an apparatus in accordance with a preferred embodiment, comprising a casing 10, which in its simplest form is cylindrical in the direction of flow of the medium, but it may also be cylindrical in the direction of the rotor shaft.
  • the casing 10 of the mixer may also be of some other, more complicated shape, if such is considered reasonable.
  • the casing 10 is provided with an inlet 12 and an outlet 16, with flanges 14 and 18, res ⁇ pectively, the outlet being preferably tangential to the direction of rotation of the rotor, and with a rotor 20 arranged rotatably within the casing 10.
  • the mixer is attached through its flange 14 to a so-called inlet pip- ing, i.e., the flow channel of the incoming fiber suspen ⁇ sion, and through its flange 18 to a so-called outlet piping, i.e. the flow channel of the fiber suspension being discharged from the mixer.
  • the rotor 20 is formed of a shaft 22 mounted on bearings to a wall of the casing 10, the shaft being preferably perpendicular to the axis X of the casing 10.
  • the shaft 22 is con ⁇ gruent or at least parallel with the inlet axis.
  • the rotor blades should be helical in order for the rotor to rotate.
  • At least two blades 24 are attached to that end of the shaft 22 which extends to the inside of the casing 10, so that an open space remains in the cen ⁇ ter of the rotor 20 when the blades 24 rotate.
  • the em ⁇ bodiment shown in Fig. 1 is provided with five blades 24, and they are substantially rectangular in cross section while the main shaft is radial. The most essential thing, with regard to the shape of the blades is, however, that it makes the rotor rotate and also brings about the desired mixing effect.
  • the blades 24 extend preferably about 10 to 80 mm from the wall of the casing 10.
  • the rotor 20 may be disposed in the casing 10 either central- ly so that the distance of the circle of rotation C of the blades 24 from the wall of the casing 10 is equal on both sides of " the rotor 20 or eccentrically so that the clearance between the circle of rotation C and the wall of the casing 10 is smaller on one side of the rotor 20 than on the other side.
  • the rotor 20 or, more specifi ⁇ cally, the rotor blades may be, e.g., such in shape that the shape of the surface of revolution is substantially spherical or cylindrical. Also other shapes of the sur ⁇ face of revolution are feasible as long as they are fitted together with the cross-sectional shape of the casing.
  • the casing may also be provided with ribs 26 and 28 which, together with the rotor 20, cause a turbulence which brings about an adequate mixing effect in the sus ⁇ pension flow.
  • the rib 26 is so arranged in connection with the inlet 12 that it directs the axial flow from the inlet 12 to the casing 10 of the mixer unevenly to the casing 10, thereby ensuring rotation of the rotor 20.
  • rib 26 may also be, e.g., a plate disposed perpendicu ⁇ larly to the axis of the flow path, covering part of the flow path. The most essential thing is that the member deviates the mass center of the flow from the axis of the flow channel.
  • the freely rotatable mixer shown in Fig. 1 is as such applicable for use with the heat exchanger illustrated in Fig. 6 of PCT/FI96/00330, in which two heat exchangers are connected in series so that the tube between the heat exchangers is provided with a mixing member.
  • the mixer by no means needs to fluidize pulp; "stirring" is sufficient for thorough mixing of pulp particles with each other, no matter of what size they are at this stage.
  • the mixer may be, e.g., an apparatus similar to the one shown in Fig. 1 or an apparatus where the mixing member is a circular or elliptic ring, which rotates freely in the flow under the effect of the flow.
  • Fig. 1 further illustrates how the casing of the mixer may be provided with an auxiliary, i.e., a control valve 30, either as an integral part of the mixer or, alternatively, attached to the mixer flange 14.
  • the con ⁇ trol valve 30 shown in Fig. 1 is a conventional gate valve, but also other forms of valves are applicable.
  • One task of the valve 30 is naturally to control the flow, whereby locating the rotor 20 near the valve 30 also con- tributes to the operation of the valve 30, ensuring that fibers cannot adhere to the gate or other valve member and thereby gradually cause the valve opening 32 to become clogged.
  • Another task of the valve 30 is essential to the mixer, namely, it directs the flow in an eccentric form into the mixer casing 10. By ensuring that the flow entering the casing 10 is eccentric, especially respect ⁇ ive of the rotor shaft, one may be sure that the rotor 20 rotates in all circumstances in the direction of arrow A.
  • Fig. 1 also illustrates how either the mixer casing 10 or the inlet piping may be provided with a conduit 38, 38' for adding a chemical, dilution liquid, steam, or other material to the flow.
  • the valve potentially attached to the flange 14 of the casing 10 can be considered part of said inlet piping.
  • Location of a chemical feed conduit is chosen optimally in accordance with both the mixer oper ⁇ ation and the medium to be mixed. For example, when liquid is fed, it is advantageous to direct the incoming liquid jet in the direction of rotation of the rotor in order not to decelerate rotation.
  • the inlet conduit for gas is preferably disposed in the lower section of the casing and the outlet in the upper section thereof in order for the gas flow from the inlet to the outlet to proceed reliably.
  • a conduit is nat ⁇ urally unnecessary.
  • the mixing conduit 38 has to be located far enough from the outlet 16 of the casing 10 of the mixer so that the chemical or equivalent has an adequate time to mix well enough with the pulp prior to being discharged from the mixer. It could be a guideline that the mixing conduit 38 should be disposed against the direction of rotation of the rotor at the distance of at least 90 degrees, prefer ⁇ ably 180 degrees, from outlet 16.
  • the medium to be mixed also sets its own limits to the location of the mixing conduit.
  • Fig. 2 illustrates a mixing apparatus in accordance with a second preferred embodiment.
  • the same reference numerals as in Fig. 1 have been used where applicable, except that all reference numerals of Fig. 2 start with number 1.
  • a valve 130 is illustrated as a member which is clearly separate from the casing 10 of the mixer, which member is attached to a flange 114 of the casing.
  • Another difference is to locate the outlet 116 of the casing 10 at an angle of 90 degrees, or if a widening of the outlet is taken into account, at an angle of approximately 100 degrees with respect to the inlet piping.
  • the outlet 116 is provided with an outlet pipe 140 which widens preferably in the direction of flow just like a diffuser pipe.
  • the purpose of the widening of the outlet duct 140 is to recover dynamic pressure from the flow being discharged from the casing 10 of the mixer.
  • Fig. 3 shows a mixing apparatus in accordance with a third preferred embodiment.
  • the same reference numerals as in Fig. 1 have been used where applicable, except that all reference numerals of Fig. 3 start with number 2.
  • the outlet 216 of the mixer is disposed opposite to the inlet 212 of the mixer. Further, the outlet 216 is provided with an outlet pipe 240, as in
  • Fig. 2 Unlike the outlet pipe 140 of Fig. 2, which is an integral part of the mixer casing 10, the outlet pipe 240 of Fig. 3 is attached to the flange 218 of the outlet 216 of the casing 10. Naturally, the location and way of attachment of the outlet pipe are not dependent on each other, but a detachable outlet pipe may be disposed also in a mixer discharged from its side as in Fig. 2, and a stationary outlet pipe also in an arrangement as shown in Fig. 3.
  • the apparatus functions so that throttl ⁇ ing, effected by either a valve or a rib, on the inlet side of the mixer controls the velocity of the fiber suspension jet entering the mixer, to be preferably in the range of 5 to 30 m/s, more preferably in the range of 10 to 20 m/s.
  • the combination of the flow being deviated from the central flow direction and said flow velocity makes the rotor 20 arranged in the casing 10 rotate.
  • the mixer causes a pressure loss of the order of 0.5 to 3.5 bar, preferably 0.5 to 2.5 bar, most of the pressure loss being caused by throttling arranged at the inlet of the mixer by means of a valve or a rib 26.
  • the pressure loss is controllable, by adjusting the inlet side throttling.
  • the total pressure loss caused by the mixer may be reduced by shaping the outlet pipe of the outlet side of the mixer optimal, i.e., such that it will recover part of the dynamic pressure.

Landscapes

  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mechanical Engineering (AREA)
  • Paper (AREA)
  • Silicon Compounds (AREA)
  • Preparation Of Clay, And Manufacture Of Mixtures Containing Clay Or Cement (AREA)

Abstract

L'invention concerne un procédé et un dispositif permettant de mélanger un second milieu à un premier milieu. Ce procédé et ce dispositif sont particulièrement avantageux quand ils sont utilisés pour mélanger différents produits chimiques, aussi bien liquides que gazeux, ou pour mélanger de la vapeur à une suspension de pâte dans l'industrie de transformation du bois. Selon l'invention, on amène le premier milieu dans le châssis (10) du mélangeur, on le mélange et on le sort dudit châssis (10), le flux du milieu qui entre dans le châssis (10) faisant tourner un rotor (20) à rotation libre placé à l'intérieur.
PCT/FI1997/000325 1996-06-03 1997-05-29 Procede et dispositif pour melanger un second milieu a un premier milieu WO1997046309A1 (fr)

Priority Applications (6)

Application Number Priority Date Filing Date Title
DE69709102T DE69709102T2 (de) 1996-06-03 1997-05-29 Verfahren und vorrichtung zum mischen von einem zweiten medium mit einer pulpe
EP97924040A EP0907409B1 (fr) 1996-06-03 1997-05-29 Procede et dispositif pour melanger un second milieu a une pulpe
CA002256594A CA2256594C (fr) 1996-06-03 1997-05-29 Procede et dispositif pour melanger un second milieu a un premier milieu
AT97924040T ATE210492T1 (de) 1996-06-03 1997-05-29 Verfahren und vorrichtung zum mischen von einem zweiten medium mit einer pulpe
US09/194,358 US6193406B1 (en) 1996-12-20 1997-05-29 Method and apparatus for mixing pulp a suspension with a fluid medium with a freely rotatable mixing rotor
US09/757,479 US20010006484A1 (en) 1996-12-20 2001-01-11 Method and apparatus for mixing a second medium with a first medium

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
PCT/FI1996/000330 WO1997001074A1 (fr) 1995-06-20 1996-06-03 Procede et dispositif de traitement d'un materiau faiblement thermoconducteur
USPCT/FI96/00330 1996-06-03
FI965137A FI104621B (fi) 1996-06-03 1996-12-20 Menetelmä ja laite toisen väliaineen sekoittamiseksi ensimmäiseen väliaineeseen
FI965137 1996-12-20

Publications (1)

Publication Number Publication Date
WO1997046309A1 true WO1997046309A1 (fr) 1997-12-11

Family

ID=26160283

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/FI1997/000325 WO1997046309A1 (fr) 1996-06-03 1997-05-29 Procede et dispositif pour melanger un second milieu a un premier milieu

Country Status (6)

Country Link
EP (1) EP0907409B1 (fr)
AT (1) ATE210492T1 (fr)
CA (1) CA2256594C (fr)
DE (1) DE69709102T2 (fr)
FI (1) FI104621B (fr)
WO (1) WO1997046309A1 (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1347092A1 (fr) * 2002-03-21 2003-09-24 Andritz AG Procédé et dispositif de mélange de substances fluides dans des matériaux fluides

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US735530A (en) * 1902-10-22 1903-08-04 Paul Kuehne Apparatus for mixing concrete.
GB811186A (en) * 1956-10-04 1959-04-02 Elliots Newark Ltd Improvements in gas filters
GB1255638A (en) * 1967-12-01 1971-12-01 Du Pont Improvements in mixing apparatus
US4030969A (en) * 1972-06-13 1977-06-21 Defibrator Ab Method of dispersing a bleaching agent into a stream of fibrous cellulosic pulp material in a throttling nozzle
US5258100A (en) * 1992-02-28 1993-11-02 Kamyr, Inc. Minimizing gas separation in a mixer outlet
EP0664150A1 (fr) * 1994-01-25 1995-07-26 A. Ahlstrom Corporation Procédé et appareil pour mélanger des produits chimiques gazeuses dans des suspensions de fibres
US5466334A (en) * 1991-09-05 1995-11-14 Sunds Defibrator Industries Aktiebolag Method and apparatus for mixing a treatment agent with a pulp suspension

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US735530A (en) * 1902-10-22 1903-08-04 Paul Kuehne Apparatus for mixing concrete.
GB811186A (en) * 1956-10-04 1959-04-02 Elliots Newark Ltd Improvements in gas filters
GB1255638A (en) * 1967-12-01 1971-12-01 Du Pont Improvements in mixing apparatus
US4030969A (en) * 1972-06-13 1977-06-21 Defibrator Ab Method of dispersing a bleaching agent into a stream of fibrous cellulosic pulp material in a throttling nozzle
US5466334A (en) * 1991-09-05 1995-11-14 Sunds Defibrator Industries Aktiebolag Method and apparatus for mixing a treatment agent with a pulp suspension
US5258100A (en) * 1992-02-28 1993-11-02 Kamyr, Inc. Minimizing gas separation in a mixer outlet
EP0664150A1 (fr) * 1994-01-25 1995-07-26 A. Ahlstrom Corporation Procédé et appareil pour mélanger des produits chimiques gazeuses dans des suspensions de fibres

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1347092A1 (fr) * 2002-03-21 2003-09-24 Andritz AG Procédé et dispositif de mélange de substances fluides dans des matériaux fluides

Also Published As

Publication number Publication date
DE69709102D1 (de) 2002-01-24
EP0907409B1 (fr) 2001-12-12
ATE210492T1 (de) 2001-12-15
CA2256594C (fr) 2006-09-26
FI965137A0 (fi) 1996-12-20
DE69709102T2 (de) 2002-07-18
CA2256594A1 (fr) 1997-12-11
EP0907409A1 (fr) 1999-04-14
FI104621B (fi) 2000-03-15
FI965137A (fi) 1997-12-04

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