WO1997011358A1 - Measurement of moisture content of timber - Google Patents
Measurement of moisture content of timber Download PDFInfo
- Publication number
- WO1997011358A1 WO1997011358A1 PCT/NO1996/000222 NO9600222W WO9711358A1 WO 1997011358 A1 WO1997011358 A1 WO 1997011358A1 NO 9600222 W NO9600222 W NO 9600222W WO 9711358 A1 WO9711358 A1 WO 9711358A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- timber
- drying
- moisture content
- measuring
- measuring device
- Prior art date
Links
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B25/00—Details of general application not covered by group F26B21/00 or F26B23/00
- F26B25/22—Controlling the drying process in dependence on liquid content of solid materials or objects
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/02—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material
- G01N23/025—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by transmitting the radiation through the material using neutrons
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/46—Wood
Definitions
- the invention relates to the measurement of moisture content of timber by thermalizing fast neutrons which are attenuated by the hydrogen content of the timber. Then, by means of calibration data, the moisture content of the timber can be calculated from the number of thermalized neutrons measured per unit time, and be used for adjusting the parameters of drying during the drying process.
- the parameters of drying must be controlled such that the water transport from the interior of the timber towards the surface is balanced against the proper tension in the timber, such tension occuring as a result of the water transport. This can be achieved by knowing at all times the moisture content of the timber and adapting the parameters of the drying process correspondingly. In other words, the parameters of drying may be synchronized with the moisture content of the timber, with the desired drying rate and the intended final moisture content.
- Continuous measurement of the moisture content of the timber during the drying process gives the possibility of improving the control of the drying climate such that damages due to the drying are reduced. Then it is also possible to terminate the drying process when the timber has obtained the desired final moisture content, and thus predetermined specifications regarding the amount of moisture content can easily and reproducibly be met. In addition, there is no need to monitor the material, thereby saving both time and energy to dry. Other application areas also exist, in which it is usefull to measure the moisture content, such as by rough grading of materials and quality control.
- the moisture level may be measured by means of electrodes which are pierced into the wood to measure electrical resistance.
- this measurement method is not suitable for measuring moisture contents above 25 - 30 %, and therefore, by using measuring equipment of this kind, it is not possible to control the course of the drying above the fiber saturation point.
- most moisture meters which are commercially available exhibit a highly limited accuracy due to the lack of proper temperature compensation, and/or because they are not able to measure the moisture content continuously in the timber kiln. In this kind of measurements, the measurement accuracy is very uncertain due to the complex interaction between resistance, tempera ⁇ ture and moisture (see publications 2, 3 and 4 of the bibliography).
- an object of the invention is to provide a measuring device to measure the moisture content of timber, and a method of calibrating such a device in such a manner that the moisture content can be measured with a satisfactory accuracy independently of the density of the timber.
- Another object of the invention is to specify a method of adjusted the drying of timber controlled by such a calibrated measuring device. Disclosure of Invention
- the invention relates to a method of calibrating a device for the measurement of moisture content of timber with respect of varying dry density of the different types of timber to be measured, whereby the timber is irradiated by fast neutrons from a neutron source and the number of resulting thermal neutrons which per unit time has been attenuated by hydrogen atoms of the moisture content of the timber is recorded by at least one detector as an expression of the moisture content of the timber and indicated on a measuring instrument, the method being characterized by the following step: a) for the timber to be measured recording graphs of the readings of the measuring instrument as a function of a known moisture content at maximum and minimum dry density, respectively, and determining a mean value graph between the maximum graph and the minimum graph, b) determining a first alteration in the instrument reading between the mean value graph and the graphs of maximum and minimum dry density, respectively, at a given constant moisture value for which the greatest difference in dry density exists between the graphs, c) determining a second alteration as the change in instrument reading per moisture
- the invention also relates to a device for measuring the moisture content of timber, comprising a neutron source for irradiating the timber by fast neutrons and at least one detector to count the number of resulting thermal neutrons which per unit time has been attenuated by hydrogen atoms of the water content of the timber, and a measuring instrument to indicate a metered value as a function of the counted number of neutrons as a measure of the moisture content of the timber.
- the device of the invention is characterized in that the neutron source and the detector are arranged side by side in a wall, floor or ceiling adjacent the timber, and that the device comprises a data register for the storage of parameters of drying and calibrated processing of neutron measure ⁇ ment data from the detector to be displayed on the measuring instrument.
- the measuring instrument comprises a computer screen for the display of the moisture content of the timber as a function of time.
- the invention relates to a method of drying wet timber by means of a controlled forced air current and adjusted wet bulb and dry bulb temperatures of the air current by making use of the measuring device and calibration specified above.
- the characterizing features of the method lie the steps of: a) reading into a drying control module, the wood species and dimensions of the timber to be measured, as well as a recorded outside temperature, the initial mean moisture content of the timber and the desired final moisture content thereof, b) for the complete desired course of drying, by use of the control module, calculating empirically proper parameters of drying (that is, wet and dry bulb temperatures, and fan operating program) on the basis of the data stored in step a), c) under control of the control module, tracing the course of drying on a computer screen of the measuring device in the form of a graph having moisture contents indicated along the ordinate axis and drying period along the abscissa axis, and d) during the course of drying, measuring the moisture content of the timber by means of the measuring device and, by altering the parameters of drying, correcting a possible difference between a measured value of drying and the intended and traced course of drying.
- the moisture content of the timber is measured continuously by means of the measuring device and the average moisture content during a selected time period, such as the last three hours, is calculated and displayed on a computer screen as an actual control value, and if this actual value, at the time of display, differs from a corresponding nominal value on the graph of the drying course, a quick correction of the drying climate is made by altering the parameters of drying. Then the calculated moisture content can be displayed on the computer screen at fixed intervals, such as once every hour.
- the metering principle being the basis of the invention is founded on the ability of the hydrogen to modify fast neutrons to slow, socalled thermalized neutrons. Therefore, this thermalization of neutrons can be utilized to measure the moisture content of a mixture of water and dry matter to record the relationship between the number of fast neutrons being transmitted into the medium to be measured and the number of thermal neutrons being reflected.
- the number of neutrons being thermalized and detectable is deter ⁇ mined by, inter alia, the composition of materials, the dry density, water content, and the dimensions of the object being measured (measurement geometry).
- the dry matter of the object to be measured mainly consists of molecules having "heavy" atoms
- the hydrogen in the water contributes to the thermaliza ⁇ tion, and the number of thermal neutrons detected is then a measure of the moisture content of that measurement object. This allows the instrument to be calibrated on the basis of moisture samples taken from the medium to be measured.
- the dry matter of the object to be measured is an organic material, such as wood
- the dry matter also contributes to some extent to the thermalization.
- the number of thermal neutrons which are detectable is a function not only of water density and geometry but also of the dry density.
- the dry matter of wood contains about 6,2 % of hydrogen (H), 50 % of carbon (C) and about 43 % of oxygen (O), and the contents vary from one wood species to another. Additionally the wood species exhibit large differences in dry density.
- the mass of a hydrogen atom and that of a neutron are approximately the same (1 amu). Hydrogen atoms and neutrons collide at a varying degree, all the way from sideslips with nearly no neutron energy loss, to head-on collisions whereby the neutron looses neariy all of its energy. On average, about 18 collisions with hydrogen atoms are required to slow down a fast neutron from a source to thermal energy, which means that it becomes thermally balanced with the medium being measured. In comparison, on average, 114 collisions are necessary to thermalize a neutron by carbon atoms, and correspondingly 150 collisions, if it is to be thermalized by oxygen atoms. Therefore, the sensitivity of the neutrons to hydrogen atoms is substantially higher than for other atoms in wood.
- Figure 1 is a schematic view of a drying chamber
- figure 2 schematically shows a measuring device according to the invention for measuring moisture contents during the drying of timber in a chamber
- figure 3 is a diagram showing graphs of instrument readings on a moisture meter for completely dry wood having varying dry density, and wood having constant dry density and varying moisture content, respectively, as a function of the density
- figure 4 is a diagram indicating graphs for comparison of two different drying courses of one and the same wooden material but having different initial moisture content
- figure 5 shows a calibration graph indicating instrument readings as a function of moisture content of 50 mm spruce
- figure 6 is a diagram of a system arrangement utilizing nuclear moisture meters for the control of a timber kiln
- figure 7 is a graphic diagram indicating instrument readings as a function of moisture content of timber having varying dry density, and which can be used to calculate the measurement accuracy
- a container including a source 7, detector 4, reflector 3 and an elevation mechanism 5, 8, 10 for the neutron source, collectively denoted as a probe and shown in figure 2,
- the neutron source 7 employed in the measuring probe consists of an americium- beryllium source. Americium emits ⁇ -particles reacting with beryllium cores which then emit neutrons.
- the detector 4 consists of two 3 He proportionality counters.
- the reflector is a water container 3 covered by a cadmium plate 18.
- the measurement probe was placed in a hole in the floor underneath a cluster of boards.
- IFE Institutt for Energiteknikk
- the measuring device was developed further to include, inter alia, a counter circuit to be installed in a computer unit (PC) as a replacement of the calculation unit. Then the device was installed in a chamber dryer at Frognerseteren Bruk, Oslo. Here the purpose of the tests was to produce reference values of sufficient quality to be able to translate with a sufficient degree of certainty, a pulse rate being read into a moisture percentage by means of an experimentally determined calibration curve. Furthermore, experiments were carried out, inter alia, to judge the reproducibility of the measured values and to check whether deviations were present in the measuring device.
- PC computer unit
- the operation of the device was controlled by placing an aluminium container of a known volume of water above the measuring instrument. Initially it was found that the deviations of the apparatus were too large but this was repaired by changing the amplifier and high voltage source. Then no instrument deviation could be detected for the measuring device.
- the measuring device was installed in a kiln at Ormstad Sag og H ⁇ vleri, and some further improvements were made. At Ormstad the measuring device has exhibited very good reproducibility of the measurement results. Most clearly this can be seen by comparing the fiber saturation point of different courses of drying.
- FIG 4 the moisture, dry bulb temperature and the temperature difference between the dry bulb and wet bulb temperatures are shown for two courses of drying A and B. Roughly, the temperature difference is the same in the two drying courses, and the difference in dry bulb temperature is relatively small.
- drying courses A and B the initial moisture content was 63 %, and 46 %, respectively. In the beginning the moisture content increased (heating phase) and the timber started to dry as the moisture content was reduced.
- the measuring device does not disturb the process and does not involve additional labour when loading the timber in and out of the kiln.
- the design and location of the measuring device render it physically protected. It is very important that a well defined measurement geometry is measured, and usually this is achieved by locating the measuring probe underneath the innermost cluster of boards.
- the measuring device comprises a detector unit which, during the drying process, reads the moisture content in one or two of said clusters of boards, a computer assembly (control module) having input means for loading data concerning wood species, wood dimensions, outside temperature and desired moisture content, and a PC for processing and displaying data, see figure 6.
- a plurality of detector units may be connected to the same PC, such as shown in the figure.
- the operator of the drying process gives a message to the control module through his computer keyboard concerning type of wood, board dimensioning and desired final moisture content. Simultaneously the mean moisture content of the timber and the outside temperature are measured. When this data is acquired and stored, the correct parameters of drying based on experience are calculated for the complete course of drying (that is, wet and dry bulb temperatures as well as a program of the operation of fans). Then the process of drying can be started.
- the intended progress of drying is traced on the screen of the PC as a graph with moisture contents along the y-axis and drying period along the x-axis. This curve then defines the nominal value of the course of drying.
- the moisture content of the timber is measured continuously, and the average moisture content during the last three hours is displayed on the screen once an hour as the actual value. If it appears that there is a difference between the actual and nominal values one can quickly make corrections to the drying climate by changing the parameters of drying such that the intended optimum course of drying is maximally followed. This may be accomplished automatically or manually.
- the measuring device comprises two detectors 4, one neutron source 7, one pulse amplifier, and a high voltage unit (not shown).
- the device is installed in a 100 x 120 mm acid-proof channel underneath the inner column of boards transversely to the direction of the boards.
- the same channel is to serve as one or more supports of the column.
- a power supply and registers "R" which are updated with measurement data, are located in a box outside the drying chamber.
- the data is acquired by the PC unit every 60 seconds and stored in a data base. Once every hour the average of the recordings during the last three hours is calculated expressed in moisture percentage.
- the result is displayed on the computer screen and stored in a data base.
- the reason for such a long period of integration is that the neutron recording pulses from the detector which represents the moisture content, are statistically distributed. Therefore, a large number of pulses is required to obtain accurate measurements. In stead of having high source power, time is used. This is advantageous both for economical and technical radiation reasons.
- the detector unit may also be located between two clusters of boards. This may especially be the case in relation with experimental work and research.
- the number of thermal neutrons is recorded as a function of the total hydrogen density, using hydrogen density in water p H . wa er and hydrogen density in wood PH- WOO d as variables. Since the neutron cross-sections ⁇ tota
- the dry density of timber varies naturally between p d (max) and p dry (min).
- an average dry density ⁇ d (min) is deduced.
- the change in the number of thermal neutrons as a function of the maximum difference from p d (mean) for a given moisture content (change 1) must be compared with the change in the number of thermalized neutrons per percentage change in moisture content by a given value of ⁇ dry (mean), i.e. change 2.
- the measuring accuracy of the apparatus is then found as the difference, + or -, from the true moisture content, by dividing change 1 by change 2. Consequently the measuring accuracy can be determined by comparing the alterations in the number of thermal neutrons as a function of:
- X1 the number of thermalized neutrons when the wood has maximum or minimum dry density at moisture value A (as indicated in figure 7)
- X2 the number of thermalized neutrons when the wood has average density and moisture A
- X3 the number of thermalized neutrons when the wood has moisture value B (as indicated in figure 7) and mean density
- X4 the number of thermalized neutrons when the wood has moisture B +/- 1 % and mean density .
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- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- General Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Wood Science & Technology (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Analysing Materials By The Use Of Radiation (AREA)
Abstract
Description
Claims
Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AU72302/96A AU7230296A (en) | 1995-09-20 | 1996-09-19 | Measurement of moisture content of timber |
DE19680932T DE19680932T1 (en) | 1995-09-20 | 1996-09-19 | Measurement of the moisture content of timber |
FI972106A FI116583B (en) | 1995-09-20 | 1997-05-16 | Method of calibrating an apparatus for measuring moisture content in wood |
SE9701830A SE515755C2 (en) | 1995-09-20 | 1997-05-16 | Measurement of moisture content in timber |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
NO953706A NO303091B1 (en) | 1995-09-20 | 1995-09-20 | Method for calibrating a measuring device for measuring moisture in wood, and a device for measuring it and using it |
NO953706 | 1995-09-20 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO1997011358A1 true WO1997011358A1 (en) | 1997-03-27 |
Family
ID=19898583
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/NO1996/000222 WO1997011358A1 (en) | 1995-09-20 | 1996-09-19 | Measurement of moisture content of timber |
Country Status (6)
Country | Link |
---|---|
AU (1) | AU7230296A (en) |
DE (1) | DE19680932T1 (en) |
FI (1) | FI116583B (en) |
NO (1) | NO303091B1 (en) |
SE (1) | SE515755C2 (en) |
WO (1) | WO1997011358A1 (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108413763A (en) * | 2018-04-03 | 2018-08-17 | 安徽唯嵩光电科技有限公司 | A kind of drying system and its control system of automatic adjustment hot wind |
CN111693552A (en) * | 2020-08-06 | 2020-09-22 | 承德鼎信自动化工程股份有限公司 | MZ-1 neutron on-line coal quality analyzer and relative measurement method |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
IT202100007163A1 (en) * | 2021-04-06 | 2022-10-06 | Incotech S R L | IMPROVED WOOD HEAT TREATMENT PROCESS USING REMOTE TEMPERATURE CONTROL SYSTEMS |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1921681A1 (en) * | 1969-04-28 | 1970-11-05 | Foth Dipl Ing Joachim | Measurement and control of water content - in concrete mix |
US4243886A (en) * | 1978-06-19 | 1981-01-06 | National Nuclear Corp. | Apparatus and method for the measurement of neutron moderating or absorbing properties of objects |
EP0498116A1 (en) * | 1991-02-04 | 1992-08-12 | Halliburton Company | Measuring water content of slurry |
EP0644300A2 (en) * | 1993-08-18 | 1995-03-22 | Kurt Heim | Floor drying method |
-
1995
- 1995-09-20 NO NO953706A patent/NO303091B1/en not_active IP Right Cessation
-
1996
- 1996-09-19 DE DE19680932T patent/DE19680932T1/en not_active Ceased
- 1996-09-19 AU AU72302/96A patent/AU7230296A/en not_active Abandoned
- 1996-09-19 WO PCT/NO1996/000222 patent/WO1997011358A1/en active IP Right Grant
-
1997
- 1997-05-16 FI FI972106A patent/FI116583B/en active IP Right Grant
- 1997-05-16 SE SE9701830A patent/SE515755C2/en not_active IP Right Cessation
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1921681A1 (en) * | 1969-04-28 | 1970-11-05 | Foth Dipl Ing Joachim | Measurement and control of water content - in concrete mix |
US4243886A (en) * | 1978-06-19 | 1981-01-06 | National Nuclear Corp. | Apparatus and method for the measurement of neutron moderating or absorbing properties of objects |
EP0498116A1 (en) * | 1991-02-04 | 1992-08-12 | Halliburton Company | Measuring water content of slurry |
EP0644300A2 (en) * | 1993-08-18 | 1995-03-22 | Kurt Heim | Floor drying method |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108413763A (en) * | 2018-04-03 | 2018-08-17 | 安徽唯嵩光电科技有限公司 | A kind of drying system and its control system of automatic adjustment hot wind |
CN108413763B (en) * | 2018-04-03 | 2024-01-12 | 安徽唯嵩光电科技有限公司 | Automatic adjust hot-blast drying system and control system thereof |
CN111693552A (en) * | 2020-08-06 | 2020-09-22 | 承德鼎信自动化工程股份有限公司 | MZ-1 neutron on-line coal quality analyzer and relative measurement method |
Also Published As
Publication number | Publication date |
---|---|
DE19680932T1 (en) | 1997-11-27 |
FI972106A (en) | 1997-07-14 |
NO303091B1 (en) | 1998-05-25 |
NO953706L (en) | 1997-03-21 |
AU7230296A (en) | 1997-04-09 |
SE515755C2 (en) | 2001-10-08 |
SE9701830L (en) | 1997-06-18 |
FI972106A0 (en) | 1997-05-16 |
SE9701830D0 (en) | 1997-05-16 |
FI116583B (en) | 2005-12-30 |
NO953706D0 (en) | 1995-09-20 |
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