WO1989012497A1 - A granulating method - Google Patents

A granulating method Download PDF

Info

Publication number
WO1989012497A1
WO1989012497A1 PCT/DK1989/000150 DK8900150W WO8912497A1 WO 1989012497 A1 WO1989012497 A1 WO 1989012497A1 DK 8900150 W DK8900150 W DK 8900150W WO 8912497 A1 WO8912497 A1 WO 8912497A1
Authority
WO
WIPO (PCT)
Prior art keywords
container
working
working bodies
rotation
mixing means
Prior art date
Application number
PCT/DK1989/000150
Other languages
French (fr)
Inventor
Peter Lip
Original Assignee
F.L. Smidth & Co. A/S
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by F.L. Smidth & Co. A/S filed Critical F.L. Smidth & Co. A/S
Publication of WO1989012497A1 publication Critical patent/WO1989012497A1/en

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/10Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic in stationary drums or troughs, provided with kneading or mixing appliances
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/12Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic in rotating drums

Definitions

  • the invention concerns a method of the type defined in the introductory portion of claim 1
  • Known granu ⁇ lating methods using rotary discs or screw conveyors are vitiated by various drawbacks, partly in the form of high costs, partly in the form of defects in the granulate produced, such as a too great size or layered structure which might result in a tendency to breaking or disintegration.
  • the raw material is subjected to moistening in a screw conveyor,"grinding in a moistening edge mill, and typically passes through a vibrating screen or, via a so-called “mincing machine” principle, through a plate with holes adapted for that purpose, whereby the kneaded material is discharged in a number of lengths and is chopped into suitable pieces.
  • This manufacturing process also entails rather heavy costs, and additionally it necessitates extensive pre- and aftertreatment of the raw material in view of the requisite moistening and kneading prior to chop ⁇ ping off.
  • This manufacturing process provides granulates of a non ball-shaped nature, which is inexpedient when exposing the granulates to loads, e.g. by storage or transportation, which easily entails a certain waste of material .
  • a granulating system which uses a rotary mixing machine known per se, which, in combination with a new method, has been found to be advantageous for making granulates.
  • the mixing vessel is here filled with a layer of ball-shaped objects, such as stones or the like. Using such objects in a rotary mixing container is known in connection with so-called ball mills, but the object here, in contrast to the object of the present invention, is to obtain comminution of materials.
  • the present invention is based on the finding that correspondingly good results can be obtained in a work ⁇ ing container having a horizontal axis of rotation, and the characteristic features of the method of the invention are accordingly defined in the characteriz ⁇ ing portion in claim 1.
  • the speed of rotation is preferably kept at a low value, as stated in claim 2, such that the material will substantially be worked by pressure and rubbing.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Glanulating (AREA)
  • Preparation Of Clay, And Manufacture Of Mixtures Containing Clay Or Cement (AREA)
  • Processing Of Solid Wastes (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

A method of granulating material, such as lime powder or the like, wherein the material is subjected to mechanical working in a container. To obtain an improved granulate material, use is made of a working container with a horizontal or inclined axis of rotation about which the container and/or mixing means contained therein are rotatable. The container contains loosely situated working bodies, and the material is added with or is given such a degree of moisture that after treatment for some time in the container it sticks to the working bodies and peels off after a certain additional treatment period and is discharged from the container through a grate.

Description

A granulating method
The invention concerns a method of the type defined in the introductory portion of claim 1 „ Known granu¬ lating methods using rotary discs or screw conveyors are vitiated by various drawbacks, partly in the form of high costs, partly in the form of defects in the granulate produced, such as a too great size or layered structure which might result in a tendency to breaking or disintegration.
Methods of granulating are known in which either rotary discs or a screw conveyor system (an edge mill prin¬ ciple) is used. These known methods have several draw¬ backs. Thus, the rotary disc principle usually entails expensive plants, and furthermore the granulating method is inexpedient as the granulates proper obtain a layered structure causing the granulates to tend to break or disintegrate, when dried at high temperatures.
According to the edge mill principle the raw material is subjected to moistening in a screw conveyor,"grinding in a moistening edge mill, and typically passes through a vibrating screen or, via a so-called "mincing machine" principle, through a plate with holes adapted for that purpose, whereby the kneaded material is discharged in a number of lengths and is chopped into suitable pieces. This manufacturing process also entails rather heavy costs, and additionally it necessitates extensive pre- and aftertreatment of the raw material in view of the requisite moistening and kneading prior to chop¬ ping off. This manufacturing process provides granulates of a non ball-shaped nature, which is inexpedient when exposing the granulates to loads, e.g. by storage or transportation, which easily entails a certain waste of material . Thus, there has been developed a granulating system which uses a rotary mixing machine known per se, which, in combination with a new method, has been found to be advantageous for making granulates. The mixing vessel is here filled with a layer of ball-shaped objects, such as stones or the like. Using such objects in a rotary mixing container is known in connection with so-called ball mills, but the object here, in contrast to the object of the present invention, is to obtain comminution of materials.
The applicants' patent application 1026/87 filed on February 27, 1987 describes a method of the present type, wherein a vessel, which rotates about a vertical axis and is equipped with scraper means, is used as a working container. The bottom of the vessel is covered with a layer of substantially ball-shaped working bodies, and the moisture degree of the added material is regu¬ lated before or after adding, so that, after a certain time of working, the material settles as peels on the working bodies and peels off after additional working for some time and is finally discharged through a grate in the bottom of the vessel.
With this method it has been found possible to manu¬ facture stable granulates at low costs, e.g. with a greatest dimension of the order of 0.5-6 mm.
The present invention is based on the finding that correspondingly good results can be obtained in a work¬ ing container having a horizontal axis of rotation, and the characteristic features of the method of the invention are accordingly defined in the characteriz¬ ing portion in claim 1.
In this embodiment of the method, the speed of rotation is preferably kept at a low value, as stated in claim 2, such that the material will substantially be worked by pressure and rubbing.
Other expedient details are stated in claims 3-6.

Claims

P a t e n t C l a i m s
1. A method of granulating material, such as lime powder or the like, wherein the material is subjected to mechanical working in a container, c h a r a c - t e r i z e d by using a working container having a horizontal or inclined axis of rotation about which the container and/or mixing means contained therein are rotatable, said container containing loosely situated working bodies, said material being added with or being given such a degree of moisture that after treatment for some time in the container it sticks to the working bodies and peels off after a certain additional treat¬ ment period and is discharged from the container through a grate.
2. A method according to claim 1, c h a r a c t e r ¬ i z e d by keeping the speed of rotation of the con¬ tainer and/or the mixing means at such a low value that the working bodies remain in contact with one another.
3. A method according to claim 1, c h a r a c t e r ¬ i z e d in that the working bodies are made of metal, e.g. steel or aluminium, ceramic material, quartzite, densite or stone, e.g. flint nodules, and that their diameter is in the range 10 - 200 mm.
4. A method according to claim 1, 2 or 3, c h a r a c ¬ t e r i z e d by adjusting the moisture content of the added material to between 5 and 50%, preferably between 5 and 15%.
5. A method according any of the preceding claims, c h a r a c t e r i z e d by adding a binder, e.g. bentonite, lime hydrate, burnt clay, cement, carboxy- methyl cellulose, tar substances, glue or peridur, for binding the material in the individual granulates.
6. A method according to any of the preceding claims, c h a r a c t e r i z e d in that the treatment time is 2-60 minutes, preferably 5-10 minutes.
PCT/DK1989/000150 1988-06-20 1989-06-19 A granulating method WO1989012497A1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DK335888A DK159643C (en) 1988-06-20 1988-06-20 granulation
DK3358/88 1988-06-20

Publications (1)

Publication Number Publication Date
WO1989012497A1 true WO1989012497A1 (en) 1989-12-28

Family

ID=8121972

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/DK1989/000150 WO1989012497A1 (en) 1988-06-20 1989-06-19 A granulating method

Country Status (4)

Country Link
DK (1) DK159643C (en)
ES (1) ES2016142A6 (en)
PT (1) PT90917B (en)
WO (1) WO1989012497A1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1849518A2 (en) * 2006-04-28 2007-10-31 Ing. Bonfiglioli S.p.A. Method for manufacturing granular material to be tamped on the ground and relative plant

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB960041A (en) * 1961-01-24 1964-06-10 Kloeckner Humboldt Deutz Ag A method of preparing granulated mixtures of fine-granular materials
DE1939375B2 (en) * 1968-09-27 1974-05-22 Paul Beauvais Thuering (Frankreich) Granulating device
SE390382B (en) * 1975-04-24 1976-12-20 Sala International Ab DEVICE FOR MICROPELLETIZATION OF POWDERED MATERIAL
SE406278B (en) * 1976-09-06 1979-02-05 Graenges Ab WAY TO TREAT SILICODE
WO1988006486A1 (en) * 1987-02-27 1988-09-07 F. L. Smidth & Co. A/S A method of granulating lime powder or the like

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB960041A (en) * 1961-01-24 1964-06-10 Kloeckner Humboldt Deutz Ag A method of preparing granulated mixtures of fine-granular materials
DE1939375B2 (en) * 1968-09-27 1974-05-22 Paul Beauvais Thuering (Frankreich) Granulating device
SE390382B (en) * 1975-04-24 1976-12-20 Sala International Ab DEVICE FOR MICROPELLETIZATION OF POWDERED MATERIAL
SE406278B (en) * 1976-09-06 1979-02-05 Graenges Ab WAY TO TREAT SILICODE
WO1988006486A1 (en) * 1987-02-27 1988-09-07 F. L. Smidth & Co. A/S A method of granulating lime powder or the like

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1849518A2 (en) * 2006-04-28 2007-10-31 Ing. Bonfiglioli S.p.A. Method for manufacturing granular material to be tamped on the ground and relative plant
EP1849518A3 (en) * 2006-04-28 2012-11-21 Ing. Bonfiglioli S.p.A. Method for manufacturing granular material to be tamped on the ground and relative plant

Also Published As

Publication number Publication date
PT90917A (en) 1989-12-29
DK335888D0 (en) 1988-06-20
DK159643C (en) 1991-04-08
ES2016142A6 (en) 1990-10-16
DK335888A (en) 1989-12-21
PT90917B (en) 1994-11-30
DK159643B (en) 1990-11-12

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