USRE4747E - Improvement in fabrxcs dyed with aniline black - Google Patents
Improvement in fabrxcs dyed with aniline black Download PDFInfo
- Publication number
- USRE4747E USRE4747E US RE4747 E USRE4747 E US RE4747E
- Authority
- US
- United States
- Prior art keywords
- dyed
- fabrxcs
- improvement
- aniline black
- aniline
- Prior art date
Links
- 229920000767 polyaniline Polymers 0.000 title description 6
- 239000004744 fabric Substances 0.000 description 20
- 150000003839 salts Chemical class 0.000 description 16
- 239000011780 sodium chloride Substances 0.000 description 16
- 229910052802 copper Inorganic materials 0.000 description 14
- 239000010949 copper Substances 0.000 description 14
- RYGMFSIKBFXOCR-UHFFFAOYSA-N copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 14
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-M chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 12
- 239000000243 solution Substances 0.000 description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 8
- XTEGARKTQYYJKE-UHFFFAOYSA-M chlorate Chemical compound [O-]Cl(=O)=O XTEGARKTQYYJKE-UHFFFAOYSA-M 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- QTBSBXVTEAMEQO-UHFFFAOYSA-N acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- 239000003513 alkali Substances 0.000 description 6
- 238000004043 dyeing Methods 0.000 description 6
- KWYUFKZDYYNOTN-UHFFFAOYSA-M potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 6
- 239000004753 textile Substances 0.000 description 6
- 239000003518 caustics Substances 0.000 description 4
- 239000003086 colorant Substances 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Chemical class [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000000344 soap Substances 0.000 description 4
- 235000002723 Dioscorea alata Nutrition 0.000 description 2
- 235000007056 Dioscorea composita Nutrition 0.000 description 2
- 235000009723 Dioscorea convolvulacea Nutrition 0.000 description 2
- 235000005362 Dioscorea floribunda Nutrition 0.000 description 2
- 235000004868 Dioscorea macrostachya Nutrition 0.000 description 2
- 235000005361 Dioscorea nummularia Nutrition 0.000 description 2
- 235000005360 Dioscorea spiculiflora Nutrition 0.000 description 2
- 240000005760 Dioscorea villosa Species 0.000 description 2
- 240000007594 Oryza sativa Species 0.000 description 2
- 235000007164 Oryza sativa Nutrition 0.000 description 2
- 101700046291 PACK Proteins 0.000 description 2
- VKJKEPKFPUWCAS-UHFFFAOYSA-M Potassium chlorate Chemical compound [K+].[O-]Cl(=O)=O VKJKEPKFPUWCAS-UHFFFAOYSA-M 0.000 description 2
- 241000490025 Schefflera digitata Species 0.000 description 2
- 235000015076 Shorea robusta Nutrition 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- 210000003932 Urinary Bladder Anatomy 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 235000006350 apichu Nutrition 0.000 description 2
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 2
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium monoxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 150000001805 chlorine compounds Chemical class 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- 235000004879 dioscorea Nutrition 0.000 description 2
- 230000035620 dolor Effects 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 159000000011 group IA salts Chemical class 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 235000015250 liver sausages Nutrition 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 235000011118 potassium hydroxide Nutrition 0.000 description 2
- 235000009566 rice Nutrition 0.000 description 2
- 235000015175 salami Nutrition 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- 239000008107 starch Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
- 235000013311 vegetables Nutrition 0.000 description 2
Definitions
- aniline is made available forthe production or development of a black color, dye, or stain in textile fabrics and yarns,
- the fabric or yarn is steeped in this solu tion, wrung out, and dried, and then exposed in a room at from GO to 70 Fahrenheit for two or three days; after which, for the purpose of raising the black then developed, the goods are passed through water alone, or water containing in solution an alkaline salt, or an alkali, or alkaline earth, such as caustic so da, caustic potash, caustic ammonia, or caustic lime.
- ainnioniacal gas which is pre this dolor lIllXtJlll'G for producing with steam colgoods; and is printed along with Bladder or garancine colors they are agedor exposed in a room at from .60 to 70 Fahrenheit for three days, then put through the aunnoniacal gas and dunged, dyed, washed, and passedthrough a solution of soap, whereby an intense black is produced.
- Thernetallic salt is not confined to perchloride of copper, as sulphate of copper and many other salts of copper will produce the saine re sult; and-the use of alkaline chlorides can he dispensed with when such a metallic salt as chloride of copper is employed.
- the soluble salts of iron may also be substituted, for those of copper in preparing the dyeing or printing inaterial'for producing-the black. i In some cases the cloth.
- the oxide of the metal or metals used is precipita-ted into the cloth by passing it through a solution of alkali suitable for that purpose; after Washed, dried, and printed,
Description
.UNITED STATE ric or yam,
of chlorate of potash s PATE OFFICE.
JOHN ronrroor,
or BURNLEY, ENGLAND, Assrenon T0 3. J..MULLER K v Lronfrroor, forof Lower House,
tion is herein set forth. Prior to the date of this invention a variety of colors, other than black, derived from aniline, had been utilized in dyeing or printing textile fabrics or yarns.
By this invention aniline is made available forthe production or development of a black color, dye, or stain in textile fabrics and yarns,
more especially those composed of vegetable fibers.
. v v I For dyeing fabrics or yarns so as to develop therein an aniline black there is taken one gallon of water, and in it are dissolved. four ounces of chlorate To this are added eight ounces of aniline previousl y combined of hydrochloric acid at 32 1 stirring well there are add ed one pint of acetic acid and eight ounces I measure of perchloride of copper at 88 Twad- I dell. hen-are added four ounces of sal ami maniac or an equivalent quantity of other suit able alkaline chloride.
The fabric or yarn is steeped in this solu tion, wrung out, and dried, and then exposed in a room at from GO to 70 Fahrenheit for two or three days; after which, for the purpose of raising the black then developed, the goods are passed through water alone, or water containing in solution an alkaline salt, or an alkali, or alkaline earth, such as caustic so da, caustic potash, caustic ammonia, or caustic lime.
For printing fabrics or yarns so as to dcvelop therein an aniline blael c, there is taken one gallon of suitable tilifilifllllll--illlfill starch pound weight ot'st-arch are dissolved four ounces eight ounces of anipaste containing one per gallon-and in it and the metallic salts named which the cloth is line previously combined with eight ounces of hydrochloric acid. There arethen added four ounces measure of perchloride of copper at 88 Twaddell and two ounces of sal ainlnoniac, or an equivalent quantity of other suitableah kaline chloride. f
After printing this color mixture it is aged for three nights, and the black resulting therefrom is then raised, in Water alone or in a weak solution of alkali or soap, as before mentioned; or'the goods may be passed, after printing and aging, through a supplied with. ainnioniacal gas, which is pre this dolor lIllXtJlll'G for producing with steam colgoods; and is printed along with Bladder or garancine colors they are agedor exposed in a room at from .60 to 70 Fahrenheit for three days, then put through the aunnoniacal gas and dunged, dyed, washed, and passedthrough a solution of soap, whereby an intense black is produced.
Thernetallic salt is not confined to perchloride of copper, as sulphate of copper and many other salts of copper will produce the saine re sult; and-the use of alkaline chlorides can he dispensed with when such a metallic salt as chloride of copper is employed. The soluble salts of iron may also be substituted, for those of copper in preparing the dyeing or printing inaterial'for producing-the black. i In some cases the cloth. is padded in a solution of any of the metallic salts named, either separately or mixed together, dried andprinted, or padded with a thickened salt of aniline mixed with aged three to four nights, and finished as previously stated or the cloth is padded in a-solntion of any 01" as betbre, then the oxide of the metal or metals used is precipita-ted into the cloth by passing it through a solution of alkali suitable for that purpose; after Washed, dried, and printed,
or padded with a thickened acid salt of anibox containing rollers, and .o
2 line mixed with chlorate of 'ta-sh,eged three The new artiele of manufzwture,to wit, a texto four nights, and finis as before specitile fabric or yarn in which has been produced fled. p I or developed an aniline black, substantially as v The aniline bleeli thus developed possesses described. peculiar properties which distinguish it from J. J. MULLER PACK.
all other blanks before produced in textile fab- Witnesses:
rice or yarns, and it is especially character-i2 by its power of resisting chemical reagents. H. SALATB'IE,
' V. SPBENGEE.
What is claimed is-
Family
ID=
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