USRE17682E - of corning - Google Patents
of corning Download PDFInfo
- Publication number
- USRE17682E USRE17682E US17682DE USRE17682E US RE17682 E USRE17682 E US RE17682E US 17682D E US17682D E US 17682DE US RE17682 E USRE17682 E US RE17682E
- Authority
- US
- United States
- Prior art keywords
- frosting
- batch
- pounds
- soda ash
- sodium fluoride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 description 48
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 45
- 239000000243 solution Substances 0.000 description 34
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 28
- 235000013024 sodium fluoride Nutrition 0.000 description 24
- 239000011775 sodium fluoride Substances 0.000 description 24
- 229910000029 sodium carbonate Inorganic materials 0.000 description 22
- 235000017550 sodium carbonate Nutrition 0.000 description 22
- 238000002156 mixing Methods 0.000 description 17
- 229960002050 hydrofluoric acid Drugs 0.000 description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- MIMUSZHMZBJBPO-UHFFFAOYSA-N 6-methoxy-8-nitroquinoline Chemical compound N1=CC=CC2=CC(OC)=CC([N+]([O-])=O)=C21 MIMUSZHMZBJBPO-UHFFFAOYSA-N 0.000 description 9
- 238000000227 grinding Methods 0.000 description 9
- 239000000463 material Substances 0.000 description 9
- 238000000034 method Methods 0.000 description 9
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 description 6
- 239000001099 ammonium carbonate Substances 0.000 description 6
- 235000012501 ammonium carbonate Nutrition 0.000 description 6
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 5
- 239000000203 mixture Substances 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 239000002253 acid Substances 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 239000002002 slurry Substances 0.000 description 3
- DDFHBQSCUXNBSA-UHFFFAOYSA-N 5-(5-carboxythiophen-2-yl)thiophene-2-carboxylic acid Chemical compound S1C(C(=O)O)=CC=C1C1=CC=C(C(O)=O)S1 DDFHBQSCUXNBSA-UHFFFAOYSA-N 0.000 description 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 229910052783 alkali metal Inorganic materials 0.000 description 2
- 150000001340 alkali metals Chemical class 0.000 description 2
- 230000000737 periodic effect Effects 0.000 description 2
- NROKBHXJSPEDAR-UHFFFAOYSA-M potassium fluoride Chemical compound [F-].[K+] NROKBHXJSPEDAR-UHFFFAOYSA-M 0.000 description 2
- 239000011698 potassium fluoride Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 159000000000 sodium salts Chemical class 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000002939 deleterious effect Effects 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 150000002222 fluorine compounds Chemical class 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 235000003270 potassium fluoride Nutrition 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C15/00—Surface treatment of glass, not in the form of fibres or filaments, by etching
Definitions
- This invention relates to the art of frosting glass articles, and more particularly to an improvement in the frosting solutions.
- the batch for the frosting solution contains Pounds Soda aslnNa CO 15 so Ammonium carbonate, (NH,) CO Sodium fluoride, NaF 11 Hydrofluorie acid, HF (60%) 135 Ammonium bifluoride, NILFIIF 168 Wate'r 109 Ammonium fluoride, NH,F
- pounds of sodium fluoride is mixed with 72 pounds of water, pounds of 60% hydrofluoric acid and 99 pounds of ammonium bifluoride, preferably in a rubber lined ball mill, to form a second part of the batch, and
- part of the soda ash is fused and ground to the desired ,degree of fineness This is then ground together with the balance of the soda ash and the ammonium carbona-te to form one part of the batch.
- the water, hydrofluoric acid, and ammonium bifluoride are stirred together to form a second part of the batch, the ground carbonates are added to this with stirring, and then the potassium fluoride is stirred in. While various mixtures of fused and unfused soda ash may beused, a suitable mixture consists of 10 A parts'of fused soda ash and 8 parts of I claim:
- the method of preparing a frosting solution which consists infusing a salt of an alkali metal of the first periodic group having an atomic weight between 22 and 4,0,. grinding the fused material to the desired degree of fineness and then mixing it with proper batch materials to form a frosting solution.
- the method of preparing a frosting solution which consists in fusing a sodium salt, grinding the fused material to the desired degree of fineness and then mixing it with proper batch materials to form the frosting solution.
- the method of preparing a frosting solution which consists in fusing sodium fluoride andsoda ash separately, grinding these separately to the desired degree of fineness, then mixing the soda ash with ammonium carbonate and part of the. water, hydrofluoric acid'fand ammonium bifiuoride to form one part of the batch, mixing the sodium fluoride with the balance of the water, hydrofluoric acid and ammonium bifluoride, to form a second part of-the batch, and blending these two portions to form the frosting solution.
- a batch for a frosting solution containing a fused sodium salt 10.
- a batch for a frosting solution containing fused sodium fluoride and fused soda ash 11.
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Surface Treatment Of Glass (AREA)
- Dental Preparations (AREA)
- Re-Forming, After-Treatment, Cutting And Transporting Of Glass Products (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US312054XA | 1928-05-19 | 1928-05-19 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| USRE17682E true USRE17682E (en) | 1930-05-27 |
Family
ID=21858165
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US17682D Expired USRE17682E (en) | 1928-05-19 | of corning |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | USRE17682E (enrdf_load_stackoverflow) |
| DE (1) | DE545866C (enrdf_load_stackoverflow) |
| FR (1) | FR673113A (enrdf_load_stackoverflow) |
| GB (1) | GB312054A (enrdf_load_stackoverflow) |
| NL (1) | NL25299C (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3171768A (en) * | 1961-04-25 | 1965-03-02 | Ball Brothers Co Inc | Method of detecting flaws in glass surfaces and solution used therefor |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3262767A (en) * | 1960-08-22 | 1966-07-26 | H I Thompson Fiber Glass Compa | Method for preparing vitreous silica fibers |
| FR2702765A1 (fr) * | 1993-03-16 | 1994-09-23 | Solman Jean | Procédé pour conférer à un article en verre une variation d'indice de réfraction suffisante pour modifier la quantité de lumière transmise et articles obtenus par ce procédé. |
-
0
- US US17682D patent/USRE17682E/en not_active Expired
- NL NL25299D patent/NL25299C/xx active
-
1929
- 1929-04-15 FR FR673113D patent/FR673113A/fr not_active Expired
- 1929-04-17 GB GB11946/29A patent/GB312054A/en not_active Expired
- 1929-05-01 DE DEC43030D patent/DE545866C/de not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3171768A (en) * | 1961-04-25 | 1965-03-02 | Ball Brothers Co Inc | Method of detecting flaws in glass surfaces and solution used therefor |
Also Published As
| Publication number | Publication date |
|---|---|
| NL25299C (enrdf_load_stackoverflow) | |
| FR673113A (fr) | 1930-01-10 |
| GB312054A (en) | 1930-07-17 |
| DE545866C (de) | 1932-03-07 |
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