US988445A - Still. - Google Patents

Description

J. T. DAVIS. Y

STILLl APPLIOTION FILED 001228, 1808. BENEWED DBO. 27, 1910.

Patented Apr.4,1911.

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I J. T. DAVIS.

i STILL.

A v YPLIUATION FILED 00T. 28, 19GB. RENEWED DBO. 27. IBl.

'l I 988,445, j Patented Apr. 4. V1911.

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JOHN T. Davis, or OAKLAND. camifonitm.

l Specicatian of Letters Patent.

Patented A pr. 4. 1 91 1'.

Application filed October 28. 1908, Serial No. 459.915'. Renewed December 27, 1910. Serial No. 599,532.

lmprovements` in Stills, of which the following is a specification.

M v invention relates to ati apparatus for distillation and its principal object is to provide a device wherebvthe process of distillation will be continuous, eitherfor wh e or partial distillation. I accomplish this by g means that are simple. and b v mechanical arrangements that are economical of construction and operation.

B v in v invention I use super-heated steam in pipes. or tubes. as a heating means. and by a mechanical means cause the material to he distilled to flow in a thin film down over the heated pipes. or tubes. The distillates so produced are carried to a condenser.A or to condensers if fractional distillation is desired. while the residauni ilows from the still through an outlet provided at or near the bottoni of the apparatus.

drawings. which illustrate an apparatus eonstrut-ted iii accordance with ni)v invention. and which form a part of this specification. In the drawings like numerals refer to like parts.

In the said drawings: Figure 1, is a side elevation with the casing b i'oken away showing the internal arrangement, Fig. '2, is an end elevation with the casing broken away showing the internal' arrangement, and Fig. 3, is a sectional detail view of a trough and partition.

I he numeral 1 i'epiesents a casing uttn end pieces 2 ot iron or any such suitable material; will M seen a portion of one of the ends 2 is hinged at 2* so that this part i ithin this casing 1 are may be moved. horizontal tubes. or pipes. 3 arranged one above the other and joined continuously to- .'ether :is shown by thereturn joints 4. The

. uppermost and the lowerinost of these pipes ointsasshown. and through the walls 5 of the heating chamber 6 and into said heating chamber, lwhere they are suitably connected with thelpipes which form the heating coil. Provision is made for admitting water into the pipes i of the heating coil as shown b v 'the pipes leading from the reservoir 9, and

in which and with suitable space apart are the valves 10 and 11, though any other well known and suitable device could be used. I have assumed that oil he used as a fuel for suppiying heat and in the drawings I have f means of supplyingr steam to the oil burner h'v the pipe 13 and the cock 1l. lthough it will be apparent that any other fuel adapted to any other well known furnace method could be used. suitable tlue/ 15 is provided leading from the combustion chantber. 13 is `an opening through which the. air for supporting combustion passes.

i 'ituin the casing l, and near its top. is a V-shaped Atrough ICL/with perforation.`- 1T l shown the ftt'el oil supply pipe 1'3 and a l l l along its bottoni, or the tingle of the said trough where its two sides meet. Leading into the trough 1G is the pipe 1S that is connected with the reservoir 19 provided to snppl)` the fluid to be distilled to the still. A suitable valve '21 is provided in this pipe 1S. i \Vitliin the casing 1 and at. or near, its hottoni is another trough QQ provided to receive Q3 that is provided with a suitable tra p il. At the uppei' part of the casing l is the otitlet pipe 25 provided to carry the distillatcs l to ain suitable condenser 2G.

For fractional distillate# I provide horifazontal partitions 'which art` adapted to be inserted in the c: sing l at suitable points as desired. One of these partitions QG I have shown in place in Fig. 1. and more in detail in Fig. 3. The partition 2li is provided with i a L l-shaped notch at QG' into which the bend i -t tits so as to permit the withdrawal of the partition. vIn detail the partition 2G has a 'i V-shapcd troughE 2.7 inserted at or near its 1 center willi pcrft'ipations 1T along the angle of the said trough where its two sides meet. These partitionsare designed to be inserted horizontally within the casing 1 between any series of the tnbe's 3 as may be desired with its trough part directly beneath the tube g above it. In the upper part ot' the chamber so formed within the casing 1 b'v the part outlet :29 for the distillatcs produced in that g chamber and leading to the condenser 31.

l For the purposes of illust rating the operaltion of in v invention. I will suppose that 'l petroleum is to be distilled, though it. will l be appartenu .tlliii'ti it can be adapted for use l in nio-st, if not all, processes where-distillal tion is carried jon.

K the residuuni and corr)v it to the outlet pipe y For a better tuioerstant'hng of my inven- -tioii reference is made to the accompanying 2 tition 26. as shown in Fig. 1, I provide an .a extend through the casing 1 at suitable the hydro-carbones of the. petroleum. The

has been admitted into the pipes of the petroleum passes from one chamber to the heating coil arid'fires in the furnace have other through the pertoratiousinthetroughbeen lighted, it will be seen that. the Steam or shaped portions of the partitions. The

vapor procluced will pass to the pipes inr the products of the distiil'ations ort than car casing l. Now oil is admitted from the resried to eonrlensers by outlets prov-ined from erroir 19 by ieansof the pipe 18. The oil each of the chambers made in the easing l will flow into the trough ltaml pass through by the insertion of the partitions. K the perforations in its bottom in a thin tilm I (lo not limit myself to the f'.-

over the heated pipes and longitudinally struction and arrangement herein desi-ruimt with the pipes. It. will be seen that the oil and shown in the drawings. I1 desire t.. coming in Contact with the pipes will absorb avail myself of such mi cation .intl a portion of the heat units produeecl-in said equivalents as fall properly within the pipes by the heated vapor within. This will spirit of my invent-ion. y

"i reduce the temperature of the vapor Within Having thus described my invention. what the pipes over which the oil flows and cause I claim as new and cle-sire to .ferme "n: Le?n a flow of the vapor from theheatingp coil ters Patent isiinto the pipes Within the easing 1. Thus will A still comprising a casing, a plurality ot b1 created a continuous passage of the vapor pipes arranged horizontaily one aber@ the 20 turough the series of pipes Within the tlisother Within said Casing anti continuously nung, hamber and the heating coil. The connected together. means for supplying oil as it flows through the apertures ofthe heated vapors to said pi s, a V-sliapefl V shaped trough comes into Contact with the trough having ieri'oraiions in bottoni loupper pipe of the series an' gis-'es ofi' some cateil above the uppermost pipe. nu;A

L@ vapor ir. its passage over it. Then the oil supplying the fluid to he tlisiiiletl o drops to the next pipe and isvfurthel retrough. a removable horizontal partition in duced. This repetition over the series of the casing, below one of the horizontal pipas, pipesV makes a complete distillation of all a V shaped trough forming part of sairl the hydro-earbons that will be given of? at a partition, saii trough in 'ing perforation-s temperature that is desired to be produced in its bottom, antl'tho lower e h of srtifl and maintained in the. apparatus. The protltrough being:r located immediately ahw-:e the uets of. distillation are carried by means of horizontal pipe which is lofxilezl inmoralithe outletpipes pro itletl to conclelisers. ately bolo said partition while is upper while. the resiluum escapes by means of the edges extend on each sitle of lieho oatni f outlet pipe arranged above soul parution.

Should fractional distillations be required In testimony whereof l have aift'ti mj. other partitions are inserted at suitable signature in the presence or" tiro Witwe points between the pipes of the .series thus JOHN T. lfYi, o forming :iseries of chaml'iers in which are lVitnesses: mamtameu temperatures suitable to the FIL-xxi; L. Can? .'aporizing points of the various gravities of A. Duma'.

Assuming: that. a desired quantity of Water

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