US9501A - Cal nicolas - Google Patents

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US9501A
US9501A US9501DA US9501A US 9501 A US9501 A US 9501A US 9501D A US9501D A US 9501DA US 9501 A US9501 A US 9501A
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gas
nicolas
retort
cal
oil
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10BDESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B53/00Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form

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  • the cylinder C receives an average charge of one hundred kilograms, (equal to two hundred and twenty-four pounds) of half-seasoned wood. It is introduced into the retort A, heated to a lively cherry-red. As soon as the head of this :retort is put on, the distillation commences. The hydrogen gas, the vegetable tar, and pyroligneous acid escape through the tubes D and E into the reservoir l. rIhe liquids ⁇ settle therein, and the gas in passing through the tubes from II to H undergoes a cooling, which causes it to precipitate still more tar and acid.
  • the hydrogen gas scarcely or not at all carbureted according to the nature of the wood intended for carbonization, reaches thc retort B B', which is lled with scrap-iron, or spirally-twisted sheet-iron, through the tube 11.
  • the hydrogen gas meets in I a stream of resin, oil, grease, or fatty substance, or melted resin which falls into the retort B B.
  • rIlhis retort like the retort A, is heated to a rather lively cherry-red.
  • the oils or fatty substances produce a percarbureted gas, which, traversing the double retort with the hydrogen gas from the retort A, combines with it by the aid of the heat and the ⁇ 'two gases united, and, thus combined, reach the small barrel Q through the tubes Ii and the plunger L', in the condition of sufficiently carbureted gas.
  • the gas of the small barrel or hydraulic main Q cools and deposits a black oil in passing from the tubes from M to MW to the purifiers, registers, and gasholder of the manufactory. rllhe gas, when it enters the small barrel Q, will be carbureted in proportion to the stream of oil, melted grease, or resin which shall have been introduced by the siphon J.
  • the operator should regulate the stream according to the poverty or richness in carbon of the gas proceeding from the distillation of the wood, and, consequently, according to the nature of the wood.
  • the tars and acids of the reservoir P and the black oil of the small barrel Q overflow through the sluice -pipe N andthe siphon G.
  • the wood according to its nature, leaves in the cylinder O from twenty to thirty per cent. of a perfectly pure charcoal of a very superior quality, and which, when ignited, emits no smoke, owing to its preparation apart from fatty substances.
  • a vegetable tar of equally superior quality, and a pyroligneous acid the use of which is well known.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

` 2 Sheets-Sheet l. DANRE, NICOLAS & LOPEZ.
Gas Retort.
No. 9,501. Patented Dec. 28. 1852.
lllll TH e Annulla 2 I DANRE, NICOLAS L LOPEZ. Sheets Sheet 2 vGas Heim.
Patented Dec. 28, 1852.'
Inventor:
fym, 6%/
Witnesses:
AM. FHDTO'LITHQCDANX. (DSBORNE'S PROCESS) NITRO STATES nrErrr @Erica DANRF, NICOLAS & LOPEZ, OF BIARSEILLFS, FRANCE.
ilViPROl/EIVIENT IN THE PROCESS OF MAKING lLLUhfliNATlNG-GAS.
Specification forming part of Letters Patent NofL-ell. dated December '38, 151.0
To LZZ whom 15 may concern.-
Be it known that we, GEORGE Danni), PascAL NICOLA s, and FELIX LOPEZ, of Marseilles,
in France, have invented a new, cheap, and
improved mode of combining, by mechanical and chemical processes, the hydrogen gas of different kinds of wood with the percarbureted gas of resin, oil, grease, or other fatty substa-nce by which a carbureted gas of any required density can be obtained at the pleasure ofthe operator, inferior on] y to that of oil-gas, 1
drawings, lineal and perspective, in duplicate,
with the letters of reference and explanations thereon, in which- Figure 1 is a longitudinal elevation of the machinery; Figs. 3, 4, and 5, end elevations ofthe same; and Figs. 2 and 6, perspective views of parts thereof.
The cylinder C receives an average charge of one hundred kilograms, (equal to two hundred and twenty-four pounds) of half-seasoned wood. It is introduced into the retort A, heated to a lively cherry-red. As soon as the head of this :retort is put on, the distillation commences. The hydrogen gas, the vegetable tar, and pyroligneous acid escape through the tubes D and E into the reservoir l. rIhe liquids `settle therein, and the gas in passing through the tubes from II to H undergoes a cooling, which causes it to precipitate still more tar and acid. Finally, the hydrogen gas, scarcely or not at all carbureted according to the nature of the wood intended for carbonization, reaches thc retort B B', which is lled with scrap-iron, or spirally-twisted sheet-iron, through the tube 11. The hydrogen gas meets in I a stream of resin, oil, grease, or fatty substance, or melted resin which falls into the retort B B. rIlhis retort, like the retort A, is heated to a rather lively cherry-red. The oils or fatty substances produce a percarbureted gas, which, traversing the double retort with the hydrogen gas from the retort A, combines with it by the aid of the heat and the` 'two gases united, and, thus combined, reach the small barrel Q through the tubes Ii and the plunger L', in the condition of sufficiently carbureted gas. The gas of the small barrel or hydraulic main Q cools and deposits a black oil in passing from the tubes from M to MW to the purifiers, registers, and gasholder of the manufactory. rllhe gas, when it enters the small barrel Q, will be carbureted in proportion to the stream of oil, melted grease, or resin which shall have been introduced by the siphon J. The operator should regulate the stream according to the poverty or richness in carbon of the gas proceeding from the distillation of the wood, and, consequently, according to the nature of the wood. lThe tars and acids of the reservoir P and the black oil of the small barrel Q overflow through the sluice -pipe N andthe siphon G. The wood, according to its nature, leaves in the cylinder O from twenty to thirty per cent. of a perfectly pure charcoal of a very superior quality, and which, when ignited, emits no smoke, owing to its preparation apart from fatty substances. There Hows from the reservoir l? a vegetable tar of equally superior quality, and a pyroligneous acid, the use of which is well known.
It will be seen at once that the ready sale for charcoal, vegetable tar, pyroligneous acid, and black oil (the basis of lubricating-grease) reduces almost to nothing the price of producinga gas, richer in carbon than the average qualities of coal-gas, and completely free from sulphur-ous substan ccs. In view ofthe purity, the richness, and the whiteness ofthe gas, as well as upon the ground of economy in its manufacture, the discoveries, inventions, and improvements effected by our long labors give us an incontestible right to the title of invent-l ors. It is on account of the results obtained in the different products which we have just pointed out, and ofthe principles upon which our entire combination is based that we claim the right of inventors, whatever modification government of France for ifteen years to us, GEORGE DANEE, PAscAL NIOOLAs, and FELIX LOPEZ, dated September 27th, 1851, which Letters' Patent were for an apparatus and mechanical and chemical processes, Which introduce important improvements and great economy in the combination of hydrogen gas with carbonized matter, by which processes hydrogen gas scarcely, or not at all, carbureted, eX- tractcd from diierent kinds of Wood employed in the preparation or production of the carbon is combined with the percarbureted gas of resin, oil, grease, or any other fatty body, and there is obtained, at the will of the operator, a carbureted gas of any required density inferior to that of Oil-gas, but superior to the average density of coal-gas, and having also the no small advantage of being exempt from all sulphurous fumes.
That We claim as our invention, and desire to secure by Letters Patent from the United States of America, is-
Tlie combination of Woody and fatty substances in gas-generators, as described, so that the excess of hydrogen in the former may combincwith the excess of carbon in the latter, and produce a rich carbureted gas of any required density and free from sulphurous fumes.
c. DANKE. rAscAL NICOLAS. FELIX LOPEZ.
Titnessesz L. NOILLY, JOHN P. HOLGE.
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