US659842A - Composition for blasting-powder. - Google Patents
Composition for blasting-powder. Download PDFInfo
- Publication number
- US659842A US659842A US70401599A US1899704015A US659842A US 659842 A US659842 A US 659842A US 70401599 A US70401599 A US 70401599A US 1899704015 A US1899704015 A US 1899704015A US 659842 A US659842 A US 659842A
- Authority
- US
- United States
- Prior art keywords
- powder
- carbon
- nitrate
- blasting
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000843 powder Substances 0.000 title description 8
- 239000000203 mixture Substances 0.000 title description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 20
- 229910052799 carbon Inorganic materials 0.000 description 20
- 239000007800 oxidant agent Substances 0.000 description 8
- 239000002360 explosive Substances 0.000 description 6
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 6
- 239000004615 ingredient Substances 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 239000011347 resin Substances 0.000 description 5
- 229920005989 resin Polymers 0.000 description 5
- 238000009877 rendering Methods 0.000 description 4
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 3
- 239000003610 charcoal Substances 0.000 description 3
- 235000010333 potassium nitrate Nutrition 0.000 description 3
- 229910052717 sulfur Inorganic materials 0.000 description 3
- 229960005349 sulfur Drugs 0.000 description 3
- 235000001508 sulfur Nutrition 0.000 description 3
- 239000011593 sulfur Substances 0.000 description 3
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 2
- 229910002651 NO3 Inorganic materials 0.000 description 2
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 2
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 2
- MWPLVEDNUUSJAV-UHFFFAOYSA-N anthracene Chemical compound C1=CC=CC2=CC3=CC=CC=C3C=C21 MWPLVEDNUUSJAV-UHFFFAOYSA-N 0.000 description 2
- 238000005422 blasting Methods 0.000 description 2
- 229910052804 chromium Inorganic materials 0.000 description 2
- 239000011651 chromium Substances 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 150000002823 nitrates Chemical class 0.000 description 2
- 238000003825 pressing Methods 0.000 description 2
- NDVAMUMVOJRAJV-UHFFFAOYSA-N 10h-phenanthren-9-one Chemical compound C1=CC=C2C(=O)CC3=CC=CC=C3C2=C1 NDVAMUMVOJRAJV-UHFFFAOYSA-N 0.000 description 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 239000010426 asphalt Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000005474 detonation Methods 0.000 description 1
- SOCTUWSJJQCPFX-UHFFFAOYSA-N dichromate(2-) Chemical compound [O-][Cr](=O)(=O)O[Cr]([O-])(=O)=O SOCTUWSJJQCPFX-UHFFFAOYSA-N 0.000 description 1
- 230000003467 diminishing effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- -1 lac Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 238000009527 percussion Methods 0.000 description 1
- 239000011295 pitch Substances 0.000 description 1
- 229940072033 potash Drugs 0.000 description 1
- 235000015320 potassium carbonate Nutrition 0.000 description 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000002966 varnish Substances 0.000 description 1
- 238000004078 waterproofing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K17/00—Soil-conditioning materials or soil-stabilising materials
- C09K17/14—Soil-conditioning materials or soil-stabilising materials containing organic compounds only
- C09K17/18—Prepolymers; Macromolecular compounds
- C09K17/32—Prepolymers; Macromolecular compounds of natural origin, e.g. cellulosic materials
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/34—Filling pastes
Definitions
- powders are nitrate of soda or othbr nitrates, with or without nitrate of potash and sulfur, together with. a specially-prepared carbon carrier, as hereinafter described.
- the main part'of this invention consists in the special treatment of the carbon carrier,
- the special treatment of the carbon carrier has the additional advantage of diminishing the dangerous sensibility and frequent unstableness. of the oxidizing agents, and my invention renders them comparatively safe against friction and percussion, while at the sane time this treatment largely prevents crystallizingout and consequent danger of explosion from a variety of causes. This aotion of rendering the oxidizing agent more stable is independent of the, added carbon.
- the mixture is constantly stirred until the ingredients have been thoroughly mixed.
- the mixture is then cooled or dried and ground to an extremely-fine powder, or the. mixture maybe used in a fluid or viscous state, as-may be found most convenient.
- Hie carbon carrier composed of iento sixteen. parts resin, one to two'and one-half parts chromium oxidizing agent and five parts carbon all incorporated coherently together, as and for the purposes set forth.
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Wood Science & Technology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Soil Sciences (AREA)
- Carbon And Carbon Compounds (AREA)
Description
PATENT i ntros.
GEORGE BENEKE, OF SOUTHPORT, ENGLAND.
COMPOSITION FOR BLA STlNG-POWDER.-
SPEGIFICATION forming part of Letters Patent No. 659,842, dated October 16, 1900.
Application filed January 31, 1899 n'erial No. 704,015. (No, specimens.)
specially-prepared carbon carrier, as hereinafter described, whereby greatly-improved" efiects are obtained. The substances chiefly used in the manufacture of the said blasting. powders are nitrate of soda or othbr nitrates, with or without nitrate of potash and sulfur, together with. a specially-prepared carbon carrier, as hereinafter described.
The main part'of this invention consists in the special treatment of the carbon carrier,
which can be made from one or more of the following: asphaltum, pitch, resin, lac, varnish, oils, naphthalene, anthracene, 'phenanthrone, all kinds of wax, and the like. In carrying out my preliminary treatment of the carbon carrierl make use of an oxidizing agent withor without additional carbon, such as charcoal, coke, or the like.
The special treatment of the carbon carrier has the additional advantage of diminishing the dangerous sensibility and frequent unstableness. of the oxidizing agents, and my invention renders them comparatively safe against friction and percussion, while at the sane time this treatment largely prevents crystallizingout and consequent danger of explosion from a variety of causes. This aotion of rendering the oxidizing agent more stable is independent of the, added carbon.
In my experiments on flame-reducing substances and nitrate-of-ammonium compounds I have used melted resin'for the purpose of waterproofing the flame-reducing salts; but I have now discovered that I can use the melted resin (and other substances above indicated) for the purpose of rendering the oxidizing agent more stable, and I am enabled v by my discovery to make safe and reliable explosives from nitrate of soda and nitrate of potash and other nitrates.
Variousexplosives have been invented from time to time, consisting principally of saltthen be proceeded with.
peter or nitrate of soda, sulfur, and other ingredients simultaneously admixed with a plastic substance, which will bind the powder together into a hard mass under pressure. These explosives, however, have this very scrious defect that their temperature of ignithis serious defect is remedied under the following process of manufacture:
Example: Inorder to carryout my invention, I first'proceed" to make a specially-prepared carrier of carbon. By way of example I melt (by heating) or dissolve (by means of a suitable solvent) from ten to sixteen parts ofpitch or resin or other suitable carbon carrier until it isin a fluid state and stir into it one to two and ione-half parts of finely-powdered bichromate of potash and about five parts of finely-powdered charcoal or other finely-powdered carbon. The mixture is constantly stirred until the ingredients have been thoroughly mixed. The mixture is then cooled or dried and ground to an extremely-fine powder, or the. mixture maybe used in a fluid or viscous state, as-may be found most convenient. The incorporation of the oxidizing agent and charcoal or other finel'y powdered carbon into the carbon carrier is of very great importance and renders the mixture more easily combustible and not so inert;, but, as before explained, the added carbon has little or no effect in rendering the oxidizing agent stable. To about eighteen to twenty-three parts of this powder or liquid mass I add sixty-five to seventy parts of dry and finely powdered nitrate of soda and mix them well together and then add five to ten parts of nitrate of potash and ten to twelve parts of sul-- fur previously ground together into a fine powder. The mixing of the ingredients and subsequent pressing of the powder should Before pressing the powder should be heated to a temperature which will slightly soften the carbon carrier,
or it may be pressed cold, a.ccording to the carbon carrier selected. It is then-gran ulated.
in lieu of nitrate-0f soda and -sulfu'r,'es above described in order to form explosive niixtu res capable of being employed in blasting operations.
The specially-prepared carbon carrier in addition to rendering theoxidizing agent more stable" also insures the better ignition and detonation of the -explosive compounds herein referred to, of which it forms aninv gredient. v
What I claim, and desire to secure byLetters'Patent, is- 1. As a, new article of manufacture for use as an ingredient in the subsequent manufacture-of nit-rate, explosives thc carbon carrier composed ofresin, a chromium oxidizing agent and carbon, all incorporated coherently together as and for the purposes set forth.
' 2. As a new article'oi' manufacture for use as ah ingredient in the subsequent manufacture of nitrate explosives, Hie carbon carrier composed of iento sixteen. parts resin, one to two'and one-half parts chromium oxidizing agent and five parts carbon all incorporated coherently together, as and for the purposes set forth. i
In witness ivhereofl have hereunto signed my name-in the presence of two subscribing witnesses. i
y e oReE ENEnE.
Witnesses: I v 1 l I WM. G. MURRAY, S. MOCREADY.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US70401599A US659842A (en) | 1899-01-31 | 1899-01-31 | Composition for blasting-powder. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US70401599A US659842A (en) | 1899-01-31 | 1899-01-31 | Composition for blasting-powder. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US659842A true US659842A (en) | 1900-10-16 |
Family
ID=2728407
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US70401599A Expired - Lifetime US659842A (en) | 1899-01-31 | 1899-01-31 | Composition for blasting-powder. |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US659842A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2563265A (en) * | 1943-09-21 | 1951-08-07 | Aerojet Engineering Corp | Rocket motor with solid propellant and propellant charge therefor |
-
1899
- 1899-01-31 US US70401599A patent/US659842A/en not_active Expired - Lifetime
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2563265A (en) * | 1943-09-21 | 1951-08-07 | Aerojet Engineering Corp | Rocket motor with solid propellant and propellant charge therefor |
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