US6054672A - Laser welding superalloy articles - Google Patents

Laser welding superalloy articles Download PDF

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Publication number
US6054672A
US6054672A US09/153,477 US15347798A US6054672A US 6054672 A US6054672 A US 6054672A US 15347798 A US15347798 A US 15347798A US 6054672 A US6054672 A US 6054672A
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US
United States
Prior art keywords
article
welding
laser
weld
superalloy
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US09/153,477
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English (en)
Inventor
Michael F. Foster
Kevin J. Updegrove
Christopher A. Thurston
Dan L. Lovelace
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chromalloy Gas Turbine Corp
Original Assignee
Chromalloy Gas Turbine Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chromalloy Gas Turbine Corp filed Critical Chromalloy Gas Turbine Corp
Assigned to CHROMALLOY GAS TRUBINE CORPORATION reassignment CHROMALLOY GAS TRUBINE CORPORATION ASSIGNMENT OF ASSIGNORS INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: FOSTER, MICHAEL F., LOVELACE, DAN L., THURSTON, CHRISTOPHER A., UPDEGROVE, KEVIN J.
Priority to US09/153,477 priority Critical patent/US6054672A/en
Priority to PCT/US1999/016271 priority patent/WO2000015382A1/en
Priority to JP2000569958A priority patent/JP4889858B2/ja
Priority to ES99969056T priority patent/ES2306538T3/es
Priority to BR9913669-4A priority patent/BR9913669A/pt
Priority to CA002343639A priority patent/CA2343639C/en
Priority to DE69938563T priority patent/DE69938563T2/de
Priority to MXPA01002651A priority patent/MXPA01002651A/es
Priority to PT99969056T priority patent/PT1148967E/pt
Priority to KR1020017003302A priority patent/KR100593053B1/ko
Priority to AT99969056T priority patent/ATE392290T1/de
Priority to AU14395/00A priority patent/AU1439500A/en
Priority to EP99969056A priority patent/EP1148967B1/de
Publication of US6054672A publication Critical patent/US6054672A/en
Application granted granted Critical
Assigned to LEHMAN COMMERCIAL PAPER, INC. reassignment LEHMAN COMMERCIAL PAPER, INC. GUARANTEE AND COLLATERAL AGREEMENT Assignors: CHROMALLOY GAS TURBINE LLC
Assigned to BARCLAYS BANK PLC reassignment BARCLAYS BANK PLC ASSIGNMENT OF SECURITY INTEREST Assignors: LEHMAN COMMERCIAL PAPER INC.
Assigned to CHROMALLOY GAS TURBINE CORPORATION reassignment CHROMALLOY GAS TURBINE CORPORATION RELEASE BY SECURED PARTY (SEE DOCUMENT FOR DETAILS). Assignors: BARCLAYS BANK PLC
Assigned to BARCLAYS BANK PLC reassignment BARCLAYS BANK PLC NOTICE AND CONFIRMATION OF GRANT OF SECURITY INTEREST IN PATENTS Assignors: CHROMALLOY GAS TURBINE LLC
Assigned to BARCLAYS BANK PLC reassignment BARCLAYS BANK PLC NOTICE AND CONFIRMATION OF GRANT OF SECURITY INTEREST IN PATENTS Assignors: ATLANTIC RESEARCH CORPORATION, BLUE JAY ACQUISITION CORPORATION, CASCO INVESTORS CORPORATION, CHROMALLOY AMERICAN LLC, CHROMALLOY COMPONENT SERVICES, INC., CHROMALLOY COOPERATIVE HOLDINGS LLC, CHROMALLOY MATERIAL SOLUTIONS LLC, CHROMALLOY SAN DIEGO CORPORATION, JET SERVICES (DELAWARE), INC., MIDWEST METAL COATINGS, LLC, PACIFIC GAS TURBINE CENTER, LLC, PRECOAT METALS ACQUISITION CORP., PRECOAT METALS CORP., PRECOAT METALS HOLDINGS CORP., SEQUA CAPITAL CORPORATION, SEQUA COATINGS LLC, SEQUA CORPORATION, SEQUA FINANCIAL CORPORATION, SEQUA HOLDINGS, INC., SEQUA INVESTMENTS CORPORATION I, CHROMALLOY CASTINGS TAMPA CORPORATION, CHROMALLOY GAS TURBINE LLC
Assigned to CHROMALLOY GAS TURBINE LLC reassignment CHROMALLOY GAS TURBINE LLC CHANGE OF NAME (SEE DOCUMENT FOR DETAILS). Assignors: CHROMALLOY GAS TURBINE CORPORATION
Assigned to BARCLAYS BANK PLC reassignment BARCLAYS BANK PLC SECOND LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Assignors: CHROMALLOY GAS TURBINE LLC, SEQUA CORPORATION
Assigned to BARCLAYS BANK PLC reassignment BARCLAYS BANK PLC FIRST LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Assignors: CHROMALLOY GAS TURBINE LLC, SEQUA CORPORATION
Anticipated expiration legal-status Critical
Assigned to BELAC LLC, CHROMALLY GAS TURBINE LLC, SEQUA CORPORATION reassignment BELAC LLC RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY COLLATERAL (RELEASE OF REEL 042374 FRAME 0448 Assignors: BARCLAYS BANK PLC
Assigned to CHROMALLOY GAS TURBINE LLC, BELAC LLC, SEQUA CORPORATION reassignment CHROMALLOY GAS TURBINE LLC RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY COLLATERAL Assignors: BARCLAYS BANK PLC, AS COLLATERAL AGENT
Expired - Lifetime legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23KSOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K26/00Working by laser beam, e.g. welding, cutting or boring
    • B23K26/60Preliminary treatment
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23KSOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K26/00Working by laser beam, e.g. welding, cutting or boring
    • B23K26/14Working by laser beam, e.g. welding, cutting or boring using a fluid stream, e.g. a jet of gas, in conjunction with the laser beam; Nozzles therefor
    • B23K26/144Working by laser beam, e.g. welding, cutting or boring using a fluid stream, e.g. a jet of gas, in conjunction with the laser beam; Nozzles therefor the fluid stream containing particles, e.g. powder
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23KSOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K26/00Working by laser beam, e.g. welding, cutting or boring
    • B23K26/20Bonding
    • B23K26/32Bonding taking account of the properties of the material involved
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23KSOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K2101/00Articles made by soldering, welding or cutting
    • B23K2101/001Turbines
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23KSOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K2103/00Materials to be soldered, welded or cut
    • B23K2103/18Dissimilar materials
    • B23K2103/26Alloys of Nickel and Cobalt and Chromium
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F05INDEXING SCHEMES RELATING TO ENGINES OR PUMPS IN VARIOUS SUBCLASSES OF CLASSES F01-F04
    • F05BINDEXING SCHEME RELATING TO WIND, SPRING, WEIGHT, INERTIA OR LIKE MOTORS, TO MACHINES OR ENGINES FOR LIQUIDS COVERED BY SUBCLASSES F03B, F03D AND F03G
    • F05B2220/00Application
    • F05B2220/30Application in turbines
    • F05B2220/302Application in turbines in gas turbines

Definitions

  • the present invention relates to a process for welding superalloy articles which are difficult to weld, and more particularly to a process for laser welding such articles.
  • jet engine components are developed there is a continuing demand for improved capability to withstand increasingly higher temperatures due to the high temperature demands placed upon these components in the engine.
  • Today's high pressure turbine blades and vanes are subjected to extremely adverse high temperature conditions (e.g. greater than 2000° F.).
  • These jet engine parts may require welding processes during the manufacture of the components, or after seeing engine operations and require repair as a result of wear and cracking.
  • this invention provides a process for laser welding a nickel and/or cobalt based superalloy article having a gamma prime phase comprising preheating the entire weld area and region adjacent to the weld area of the article to a ductile temperature within the range of 1400° F. to 2100° F. and maintaining such temperature during welding and solidification of the weld; and welding the preheated article utilizing a laser with a powder alloy feed, with the speed of the laser controlled to less than 10 inches per minute, preferably less than about 5 inches per minute, to minimize cracking at grain boundaries.
  • This invention provides a process for welding superalloy articles, particularly gas turbine engine components including blades, vanes and rotors.
  • the superalloys are nickel and/or cobalt based superalloys which are difficult to weld by state-of-the-art processes. These superalloys have a gamma-prime phase and include directionally solidified and single crystal alloys of gamma-prime nickel base precipitation hardened alloys. Generally, the gamma-prime precipitation-strengthened superalloys contain titanium and aluminum in a combined amount of at least about 5%.
  • Suitable superalloys include R'80, DSR'80h, R'108, IN 738, R'125, DSR'142, R'N4, R'N5 Mar-M-247DS, In 792Hf, and CMSX-4.
  • the nominal composition of some of these superalloys is described in U.S. Pat. No. 5,554,837, the disclosure of this patent being incorporated by reference.
  • grain boundary strengtheners In the directionally solidified (DS) alloys there are trace elements added as grain boundary strengtheners.
  • the grain boundary strengtheners typically consist of carbides and borides, often tungsten and tantalum. When laser welding these alloys using typical procedures there is a consistent problem with micro-crack formation at the grain boundaries.
  • the metallurgical composition of the grain boundaries is such that they melt at a lower temperature than the remainder of the base material. If the grain boundaries then cool too rapidly they fracture.
  • Metallurgical evaluation of weld samples has shown that parts welded using typical CO2 laser parameters suffer micro-cracks at the grain boundaries. In some cases the micro-cracks remain small. In others, they tear open and can progress completely through the new weld. Larger cracks can often be individually repaired.
  • a critical parameter in controlling the generation of micro-cracks when welding the DS alloys is the rate of resolidification of the base alloy.
  • that rate is controlled by the traverse speed of the laser beam.
  • the traverse speeds most commonly used are in the range of 10 to 30 inches per minute, with 18 ipm being typical. Speeds in this range have been thought necessary to take advantage of the low overall heat input allowed by the laser weld system.
  • Conventional practice held that the best way to minimize cracks on all superalloys was to closely control the size of the weld puddle and minimize the depth of the weld penetration along with the associated heat affected zone.
  • micro-cracks are caused when the grain boundaries solidify so quickly that residual tensile stresses exceed the yield strength of the alloy in those locations. Increasing the preheat temperature helps reduce large tears, but micro-cracks can still be generated.
  • FIG. 1 illustrates a laser welding system useful for carrying out the invention in which the components are not engaged, the apparatus is comprised of a laser 11 with a powder feed 12, an induction heater 13 with its induction heating coil 14 and a motion system 15 on which the article 20 is fixtured.
  • the article (a turbine blade is shown) is fixtured by mounting on a stage 16 in a very precise manner utilizing a clamp, as is conventional.
  • a pyrometer 17 and an inert gas shroud (shield) 18 with an inert gas feed line 19 and gas diffuser 21 are also shown.
  • the superalloy article e.g.
  • a vane or blade is preheated by an induction heating coil.
  • the entire weld area of the superalloy article and region adjacent to the weld area is heated by the induction heating coil to a ductile temperature within the range of 1400° F. to 2100° F., preferably 1725° F. to 1975° F.
  • the ductile temperature to which the weld area of the article is heated is above the aging or precipitation hardening temperature, but below the incipient melting temperature of the particular superalloy article substrate.
  • Critical to this process is to maintain thermal equilibrium before, during and after the welding/cladding process, leading to less severe thermal gradients across the weld/adjacent base metal thus reducing residual stresses and subsequent cracking.
  • the reduction of thermal gradients lessens the impact of the heat from welding on the heat affected zone, i.e. the process "relocates" the heat affected zone away from the fusion line. Since the entire weld area and adjacent region is preheated above the precipitation hardening temperature, this results in a uniform thermal distribution that precludes the contraction and resultant residual stresses that are normally focused at the weaker heat affected zone. The entire weld area and adjacent region undergoes thermal contraction as a result of the aging reaction with the residual stresses that result from this reaction being distributed over a much larger area, not only concentrated in the spot being welded.
  • the entire weld area and region adjacent to the weld are heated, by induction heating, to the ductile temperature.
  • the region adjacent to the weld area being heated is at least sufficiently large to be able to encompass the heat affected zone, preferably larger.
  • the heat affected zone is defined as that portion of the base metal which has not been melted, but whose mechanical properties or microstructure have been altered by the heat of welding (see Metals Handbook Ninth Edition, Volume 6, ASM, 1983). Generally this adjacent region being heated is at least 0.25 inches preferably 0.5 to 1 inch from the weld.
  • the laser and powder feed are engaged for welding.
  • the radiation from the laser forms a small molten pool of the substrate as the powder from the powder feed is dispersed over the molten pool and welded (clad) to the part by the laser beam.
  • the solidification process is precisely controlled by the radiation of the beam and the heating energy imparted by the induction coil and relative movement of the beam and the article to control the thermal and resulting strains and stresses to form a crack-free weld during and after the solidification process.
  • the article weld area is shrouded in an inert gas (e.g. argon or helium) in order to minimize the oxidation and oxide contamination of the base superalloy and filler metal alloy powder during the heating and welding process.
  • an inert gas e.g. argon or helium
  • the temperature of the weld area is controlled throughout the process in spite of added heat from the laser beam by using an optical pyrometer with feedback voltage loop (inferometer) controlling the induction heater.
  • the part is preheated in the 1400° F. to 2100° F. range and remains in this range during welding and solidification despite localized laser heat input.
  • the inferometer feedback loop
  • This preheating process reduces stresses and cracking from welding and allows the base superalloy article to be laser welded (clad) with a powder alloy feed which also comprises a superalloy, i.e.
  • a powder alloy can be utilized which is substantially the same as the alloy of the superalloy article. The reduction of stresses and cracking therefrom is especially needed when welding a directionally solidified superalloy with a gamma prime strengthened powder alloy due to the susceptibility for cracking along grain boundaries.
  • the laser welding of the article is controlled through use of a computer numerical control (CNC) means which controls the laser, powder feed and motion system on which the article is fixtured. Extensive programming and parameter development corroborated by metallurgical analysis is required for a metallurgically sound fusion bond without cracks.
  • the control means includes a vision system which digitizes the article configuration in order to drive the motion system holding the article beneath the focused laser beam and converged powder feed.
  • the control system permits efficient and economical operation of the process allowing a variety of complex configuration to be welded.
  • the vision system which is employed sets a precise path for the laser welding system which is individualized for the weld area of the particular article being welded. This is accomplished with a computer numerical control utilizing a program for the article, but with the precise path set by the vision system. After the article is secured in its fixture, the height is checked to ascertain the build-up needed during welding (cladding). Then after setting the contrast of the weld area, the camera of the vision system views (i.e.
  • the motion system whose path is set by the control system is at least a 3-axis, preferably a 4 or 5-axis motion system to provide the detailed motion required for various complex welding area surfaces.
  • the 3-axis motion would be along the X, Y and Z directions, the 4-axis motion for more complex flat surfaces would combine X, Y and Z directions with rotation (see FIG. 1), while a 5-axis motion for contoured surfaces would combine X, Y and Z directions with rotation and tilt.
  • Suitable lasers include those known to those skilled in the art including a CO 2 laser.
  • the power density of the laser may be between 10 5 watts/in 2 and 10 7 watts/in 2 with a beam spot size in the range of 0.040 to 0.150 inches.
  • the powder alloy feed is operated to deliver a stream of alloy particles generally -120 to +400 mesh at a rate of 5 to 15 grams/min. With the reduced laser weld speeds of this invention preferably the laser power utilized is from 10 4 to 10 6 watts/in 2 , and the powder alloy feed rate is from 2 to 6 grams per minute.
  • Test coupons made of directionally solidified Rene 142 material were cut to an approximate size of 1.0 inch long ⁇ 0.750 inch wide ⁇ 0.040 inch thick.
  • the nominal composition by weight of Rene 142 is AL 6.15%, Cr 6.80%, Co 7.50%, Mo 1.45%, W 4.90%, Ta 6.35%, Hf 1.45%, Re 2.80%, C 0.12%, Zr 0.022%, B 0.015%, and balance Ni.
  • the grain structure was oriented perpendicular to the long axis of the coupon, so that welding on a long side would be representative of welding around the tip rail of a turbine blade.
  • the blades were cycled through a high temperature vacuum stress relief cycle. They were then acid etched and processed through a high sensitivity fluorescent penetrant inspection (FPI), followed by a cleaning cycle.
  • FPI fluorescent penetrant inspection
  • CF6-80C2 Stage 1 HPT blades made of a directionally solidified Rene 142 material were welded. As part of the normal repair process the blades were sent through the initial high temperature vacuum stress relief cycle. Following that, all initial cracks were manually repaired by TIG welding. The blades were then sent through high sensitivity FPI and x-ray inspection to ensure that they were crack free prior to CO2 laser weld. At the CO 2 laser the blades were welded using the following parameters: weld speed 2 ipm, powder feed 3.5 grams per minute, 1550° F. preheat temperature, laser power 575 watts at the part. After weld the blades were ground to final length, belt/sanded to restore the external contour, and electro discharge machined to clean the tip pocket.
  • the blades were sent through final high temperature vacuum heat treatment, followed by etch, high sensitivity FPI, and x-ray inspection. No cracks were detected by the various inspections. Finally, the blades were subjected to destructive metallurgical evaluation. Again, no cracks or micro-cracks were detected.

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  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Optics & Photonics (AREA)
  • Plasma & Fusion (AREA)
  • Mechanical Engineering (AREA)
  • Laser Beam Processing (AREA)
  • Turbine Rotor Nozzle Sealing (AREA)
US09/153,477 1998-09-15 1998-09-15 Laser welding superalloy articles Expired - Lifetime US6054672A (en)

Priority Applications (13)

Application Number Priority Date Filing Date Title
US09/153,477 US6054672A (en) 1998-09-15 1998-09-15 Laser welding superalloy articles
EP99969056A EP1148967B1 (de) 1998-09-15 1999-07-26 Laserschweissen von artikeln aus superlegierungen
AT99969056T ATE392290T1 (de) 1998-09-15 1999-07-26 Laserschweissen von artikeln aus superlegierungen
ES99969056T ES2306538T3 (es) 1998-09-15 1999-07-26 Soldadura por laser de articulos de superaleacion.
BR9913669-4A BR9913669A (pt) 1998-09-15 1999-07-26 Processo para soldagem a laser de um artigo de superliga à base de nìquel e/ ou cobalto
CA002343639A CA2343639C (en) 1998-09-15 1999-07-26 Laser welding superalloy articles
DE69938563T DE69938563T2 (de) 1998-09-15 1999-07-26 Laserschweissen von artikeln aus superlegierungen
MXPA01002651A MXPA01002651A (es) 1998-09-15 1999-07-26 Soldadura con laser de articulos de superaleacion.
PT99969056T PT1148967E (pt) 1998-09-15 1999-07-26 Soldadura a laser de artigos em superliga
KR1020017003302A KR100593053B1 (ko) 1998-09-15 1999-07-26 초내열합금 제품의 레이저 용접 방법
JP2000569958A JP4889858B2 (ja) 1998-09-15 1999-07-26 超合金製品のレーザー溶接
AU14395/00A AU1439500A (en) 1998-09-15 1999-07-26 Laser welding superalloy articles
PCT/US1999/016271 WO2000015382A1 (en) 1998-09-15 1999-07-26 Laser welding superalloy articles

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Application Number Priority Date Filing Date Title
US09/153,477 US6054672A (en) 1998-09-15 1998-09-15 Laser welding superalloy articles

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US6054672A true US6054672A (en) 2000-04-25

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US (1) US6054672A (de)
EP (1) EP1148967B1 (de)
JP (1) JP4889858B2 (de)
KR (1) KR100593053B1 (de)
AT (1) ATE392290T1 (de)
AU (1) AU1439500A (de)
BR (1) BR9913669A (de)
CA (1) CA2343639C (de)
DE (1) DE69938563T2 (de)
ES (1) ES2306538T3 (de)
MX (1) MXPA01002651A (de)
PT (1) PT1148967E (de)
WO (1) WO2000015382A1 (de)

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US20150108097A1 (en) * 2012-01-10 2015-04-23 Siemens Aktiengesellschaft Laser welding of nickel-based superalloys
US9987708B2 (en) 2015-03-02 2018-06-05 United Technologies Corporation Automated weld repair of combustor liners
US10702961B2 (en) 2017-04-11 2020-07-07 General Electric Company Multiframe blade tip welding fixture
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WO2000015382A1 (en) 2000-03-23
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ATE392290T1 (de) 2008-05-15
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AU1439500A (en) 2000-04-03
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DE69938563D1 (de) 2008-05-29
KR100593053B1 (ko) 2006-06-26

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