US5658A - Improvement in the manufacture of bromine - Google Patents
Improvement in the manufacture of bromine Download PDFInfo
- Publication number
- US5658A US5658A US5658DA US5658A US 5658 A US5658 A US 5658A US 5658D A US5658D A US 5658DA US 5658 A US5658 A US 5658A
- Authority
- US
- United States
- Prior art keywords
- bromine
- bittern
- retort
- manufacture
- retorts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 title description 10
- WKBOTKDWSSQWDR-UHFFFAOYSA-N bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 title description 10
- 238000004519 manufacturing process Methods 0.000 title description 6
- 241001131796 Botaurus stellaris Species 0.000 description 20
- 239000004927 clay Substances 0.000 description 8
- 229910052570 clay Inorganic materials 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 239000002253 acid Substances 0.000 description 6
- 238000009835 boiling Methods 0.000 description 6
- 239000011521 glass Substances 0.000 description 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000000571 coke Substances 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 229910052571 earthenware Inorganic materials 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000003780 insertion Methods 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- PWHULOQIROXLJO-UHFFFAOYSA-N manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 2
- 229910052748 manganese Inorganic materials 0.000 description 2
- 239000011572 manganese Substances 0.000 description 2
- NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Inorganic materials O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000001105 regulatory Effects 0.000 description 2
- 235000011149 sulphuric acid Nutrition 0.000 description 2
- 239000001117 sulphuric acid Substances 0.000 description 2
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/09—Bromine; Hydrogen bromide
- C01B7/096—Bromine
Definitions
- the nature of our invention consists in the use of earthen retorts made with an admixture of pulverized coke-boiling bittern for heating the retorts and a mixture of clay and bittern for luting.
- the retorts of cylindrical form have two holes in the topone for the insertion of glass connecting-tube, the other for inserting materials.
- the connecting-tube is bent to a little more than a right angle three or four inches from end, of sufficient length to reach from hole in the retort as it stands in the pan to the condensing-tube.
- condensing-tube is of glass or lead, its bore large enough to admit the end of the connecting-tubes. It is bent near the middle, passed through a wooden vessel containing cold water, enters perpendicularly a receiver made of glass, containing a few inches of water, the
- the pan is nearly filled with bittern of saltwater, made to boil, the retort-s nearly filled with three parts boiling and one part cold bittern.
- Sulphuric acid diluted with about twelve times its bulkof water,is added and well mixed with the bittern in the retort.
- the retort is then placed in the pan.
- the bent end of the connecting-tube is luted into one of the holes in the retort.
- the other end enters the COIlv densing tube and the junction also luted.
- Black oxide of manganese is then added to the contents of the retort at the other aperture and it luted.
- the quantity of acid used is regulated by the 'quanity of bromine contained in the bit tern, eight or nine fluid ounces of acid being required to make five or six ounces, by weight, of bromine; the quantity of manganese about two-thirds the weight of acid.
- the luting is made of pipe-clay mixed to the proper consistence with bittern.
- the bittern in the pan is kept boiling until the brominein the retort is all run off, the retort then lifted out of the pan, and its contents emptied, refilled, 85c.
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Cookers (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Description
UNITED STATES PATENT QFFICEG DAVID ALTER AND EDWARD GILLESPIE, OF FREEPORT, PENNSYLVANIA.
IMPROVEMENT IN THE MANUFACTURE OF BROMINE.
Specification forming part of Letters Patent No. 5,658, dated July 5, 1848.
To all whom it may concern:
Be it known that we, DAVID ALTER and En- WARD GILLESPIE, of Freeport, in the county tion.
The nature of our invention consists in the use of earthen retorts made with an admixture of pulverized coke-boiling bittern for heating the retorts and a mixture of clay and bittern for luting.
To enable others skilled in the art to make and use our invention, we will proceed to describe its construction and operation.
We construct a fire-place and flue, on which is placed a metallic boiler or pan wide enough to admit two rows of retorts, and of sufficient length to receive all the retorts intended to be used, its depth to correspond with the height of retorts. Theretorts are madeof good earthenware clay, with the addition of pulverized coke, and are in the form of ajug or cylinder,
having handles or ears on each side (if ears,
iron hooks are required to handle the retort) and knobs on bottom. The retorts of cylindrical form have two holes in the topone for the insertion of glass connecting-tube, the other for inserting materials. The connecting-tube is bent to a little more than a right angle three or four inches from end, of sufficient length to reach from hole in the retort as it stands in the pan to the condensing-tube. The
condensing-tube is of glass or lead, its bore large enough to admit the end of the connecting-tubes. It is bent near the middle, passed through a wooden vessel containing cold water, enters perpendicularly a receiver made of glass, containing a few inches of water, the
lower end of condensing-tube being under the surface of the water in the receiver.
The pan is nearly filled with bittern of saltwater, made to boil, the retort-s nearly filled with three parts boiling and one part cold bittern. Sulphuric acid, diluted with about twelve times its bulkof water,is added and well mixed with the bittern in the retort. The retort is then placed in the pan. The bent end of the connecting-tube is luted into one of the holes in the retort. The other end enters the COIlv densing tube and the junction also luted. Black oxide of manganese is then added to the contents of the retort at the other aperture and it luted.
The quantity of acid used is regulated by the 'quanity of bromine contained in the bit tern, eight or nine fluid ounces of acid being required to make five or six ounces, by weight, of bromine; the quantity of manganese about two-thirds the weight of acid.
The luting is made of pipe-clay mixed to the proper consistence with bittern. The bittern in the pan is kept boiling until the brominein the retort is all run off, the retort then lifted out of the pan, and its contents emptied, refilled, 85c.
What we claim as our invention, and desire to secure byLetters Patent, is-- I The application of the kind of retorts specified, the use of the bittern as a means of applying a proper heat to the retorts, and the clay and bittern luting in the manufacture of bromine.
DAVID ALTER. ED. GILLESPIE.
Witnesses:
J. A. GILLESPIE, J. D. Tonnn'r'r.
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US5658A true US5658A (en) | 1848-07-05 |
Family
ID=2065959
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US5658D Expired - Lifetime US5658A (en) | Improvement in the manufacture of bromine |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US5658A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2006047738A2 (en) | 2004-10-27 | 2006-05-04 | Mcneil-Ppc, Inc. | Dosage forms having a microreliefed surface and methods and apparatus for their production |
-
0
- US US5658D patent/US5658A/en not_active Expired - Lifetime
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2006047738A2 (en) | 2004-10-27 | 2006-05-04 | Mcneil-Ppc, Inc. | Dosage forms having a microreliefed surface and methods and apparatus for their production |
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