US55253A - Improved process for pulping wood - Google Patents

Improved process for pulping wood Download PDF

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US55253A
US55253A US55253DA US55253A US 55253 A US55253 A US 55253A US 55253D A US55253D A US 55253DA US 55253 A US55253 A US 55253A
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water
digester
lime
magnesia
heated
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    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00Pulping cellulose-containing materials
    • D21C3/02Pulping cellulose-containing materials with inorganic bases or alkaline reacting compounds, e.g. sulfate processes

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  • Myimprovement consists in circulating water containing common lime or magnesia, or a mixture of lime and magnesia in solution, highly heated and under pressure, continually through the mass of Wood or woody matter to be pulped.
  • the solution of lime or magnesia in the digester is heated by contact with a steam or hot-water coil, introduced at I and passing out at K.
  • I is a pump, which continually forces a circulation of the highly-heated lime or magnesia water, in a liquid state under pressure, from the bottom tothe top of the digester A.
  • Giifard injector or fresh-water pump, placed, which forces fresh water into the digester whenever desired.
  • Q is the exit-pipe for the refuse water filled with gummy and resinous matter. Itis covered with a weighted or safety-valve, so adjusted as to open whenever fresh water is forced in.
  • an apparatus shown iu Fig. 2 which consists of a digester, A, similar to that shown in Fig. 1, with its upper and lower diaphragm and heating-coil, Ste., the same as in Fig. 1.
  • P is a boiler placed over the fire, or heated otherwise, as may be most convenient.' This boiler is connected to the digester by two tubestube a, which passes from the boiler up on to the top of the digester, and tube b, which passes across from the bottom of the digester to boiler' P.
  • the effect of this apparatus is to cause a circulation of the heated lime or magnesia water up the tube a, and across through b, from the bottom of the digester, into the heating-boiler P continually.
  • FIG. 3 Another manner for applying my invent-ionA is shown in Fig. 3, and consists in employing a digester under pressure, such as digester A, Fig. 3, fitted up exactly as in Fig. l.
  • fresh water may be introduced, either by an injector or pump, S, S', or S", to the upper part of the digesters, either at intervals or continuously, before or after the lime or magnesia water treatment.
  • the cock Q, Q', or Q" is so loaded in each case as to 4open at intervals, or whenever fresh water is forced into the digester at. S, S', or S".
  • a sufficient quantity of highly-heated water under pressure must be passed through it and drained of, so as to leave no gummy matter in it when the Woody matter is discharged from the digester by openin g the slide-valves F, F', or F".

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Description

PATENT OFFICE.
JOHN W. DIXON, OF PHILADELPHIA, PENNSYLVANIA.
IIVIPROVED PROCESS FOVR PULPING WOOD.
Specification forming part of Letters Patent No. 55,253, dated June 5, 1866.
To all 'whom it may concern;
ABe it known that I, JOHN W. DIXON, of the city of Philadelphia and State of Pennsylvania, have invented a new and useful Improvement in the Process of Pulping Wood and Woody Matter, applicable also to straw, cane, and other similar vegetable ibrous material and I do hereby declare the following to be a full and exact description of the same, reference being had to the annexed drawings, which represent three forms of apparatus convenient for applying1 my improved process.
Myimprovement consists in circulating water containing common lime or magnesia, or a mixture of lime and magnesia in solution, highly heated and under pressure, continually through the mass of Wood or woody matter to be pulped.
It is also important to force into the woody mass, either before'or after the treatment with lime or magnesia water, either at intervals or continuously. a supply offresh water to replace the gummy or resiuous water simultaneously forced out by the fresh water forced in.
In applying my process, I prefer the apparatus heretofore described by me, which consists of a strong iron digester, H, capable of sustaining a pressure of about two hundred pounds to four hundred pounds per square inch. It has a man-hole on top and closefittin g cover, an upper perforated diaphragm, C, with a central openin g, D, and a lower perforated diaphragm E, and central opening, F, and sliding valve covering the cen trai passage, Gr, for leading off the digested mass of pulp when produced. The solution of lime or magnesia in the digester is heated by contact with a steam or hot-water coil, introduced at I and passing out at K.
I is a pump, which continually forces a circulation of the highly-heated lime or magnesia water, in a liquid state under pressure, from the bottom tothe top of the digester A. At F is a Giifard injector, or fresh-water pump, placed, which forces fresh water into the digester whenever desired. v
Q is the exit-pipe for the refuse water filled with gummy and resinous matter. Itis covered with a weighted or safety-valve, so adjusted as to open whenever fresh water is forced in.
Instead of the foregoin g, an apparatus shown iu Fig. 2 may be adopted, which consists of a digester, A, similar to that shown in Fig. 1, with its upper and lower diaphragm and heating-coil, Ste., the same as in Fig. 1. P is a boiler placed over the fire, or heated otherwise, as may be most convenient.' This boiler is connected to the digester by two tubestube a, which passes from the boiler up on to the top of the digester, and tube b, which passes across from the bottom of the digester to boiler' P.
The effect of this apparatus, the principle of which is well known, is to cause a circulation of the heated lime or magnesia water up the tube a, and across through b, from the bottom of the digester, into the heating-boiler P continually.
Another manner for applying my invent-ionA is shown in Fig. 3, and consists in employing a digester under pressure, such as digester A, Fig. 3, fitted up exactly as in Fig. l.
From the lower part of the digester a tube, g, passes up above the diaphragm C. A jet of steam is introduced from another boiler at L, below the mouth of this pipe, to force up the water, and thus establish a circulation of highly-heated lime or magnesia water Linder pressure. These plans are mere illustrations of alternative modes of applying my invention.
The wood or woody matter, straw, Ste., having been fed into either of the digesters A or A or A" through the man-hole at the top, and the aperture D D D in the diaphragms C C C" closed up, the pump F, Fig. l, is started, to cause a circulation from bottom to top. In Fig. 2 the heating apparatus itself' causes the circulation, and in Fig. 3 the jet of steam introduced at L causes the circulation. In either a circulation of highly-heated lime or magnesia water under pressure is caused from the top down through the mass of woody matter, through diaphragm E E' E, where the water is strained fromthe woody matter, whence the water so strained is again forced up to the top. This rapid circulation of the highly-heated lime or magnesia water Linder pressure through the woody matter enables the highly-heated lime or magnesia water un der pressure to dissolve and carry from the woody matter its gummy, gelatinous, and silicious matter.
In connection with the foregoing operation fresh water may be introduced, either by an injector or pump, S, S', or S", to the upper part of the digesters, either at intervals or continuously, before or after the lime or magnesia water treatment. The cock Q, Q', or Q" is so loaded in each case as to 4open at intervals, or whenever fresh water is forced into the digester at. S, S', or S". Before the woody matter is to be Withdrawn, a sufficient quantity of highly-heated water under pressure must be passed through it and drained of, so as to leave no gummy matter in it when the Woody matter is discharged from the digester by openin g the slide-valves F, F', or F".
I prefer, in operating on Wood, to maintain the lime or magnesia water at a pressure of one hundred and fty pounds and upward, and the temperature due thereto, although fair result-s may be obtained with increased length of time at a somewhat lower pressure-say one hundred and twenty-live pounds.
l do not desire herein to claim any of the forms of apparatus shown above, as these are merely illustrations of apparatus ,suitable for applying my invention.
Having thus described my invention, what I claim as new therein isl. The circulation of a highly-heated soluv l JOHN W. DIXON. Witnesses:
GEO. BUGKLEY,
BENJ. MGMAKIN, Jr.
US55253D Improved process for pulping wood Expired - Lifetime US55253A (en)

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