US4983298A - Process for the disinfection and aerobic stabilization of sewage sludge - Google Patents

Process for the disinfection and aerobic stabilization of sewage sludge Download PDF

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Publication number
US4983298A
US4983298A US07/483,045 US48304590A US4983298A US 4983298 A US4983298 A US 4983298A US 48304590 A US48304590 A US 48304590A US 4983298 A US4983298 A US 4983298A
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sludge
stage
days
process according
entering
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US07/483,045
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English (en)
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Leonhard Fuchs
Martin Fuchs
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Priority claimed from DE19893905228 external-priority patent/DE3905228C1/de
Priority claimed from DE19893928846 external-priority patent/DE3928846C1/de
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage
    • C02F3/02Aerobic processes
    • C02F3/12Activated sludge processes
    • C02F3/1205Particular type of activated sludge processes
    • C02F3/121Multistep treatment
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage
    • C02F3/02Aerobic processes
    • C02F3/12Activated sludge processes
    • C02F3/1205Particular type of activated sludge processes
    • C02F3/1221Particular type of activated sludge processes comprising treatment of the recirculated sludge
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage
    • C02F3/02Aerobic processes
    • C02F3/12Activated sludge processes
    • C02F3/1236Particular type of activated sludge installations
    • C02F3/1263Sequencing batch reactors [SBR]
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W10/00Technologies for wastewater treatment
    • Y02W10/10Biological treatment of water, waste water, or sewage

Definitions

  • the present invention relates to a process for the disinfection and aerobic stabilization of concentrated sewage sludge in several steps, employing one or more heat-insulated containers, preferably with stirring, with the addition of oxygen-containing gas.
  • the quality of the issuing sludge liquor is often unsatisfactory; this sludge liquor, in general is recycled into the biological waste water purification.
  • the sewage sludge, aerobically stabilized and disinfected in accordance with the known process has been used in the past as a fertilizer. However, this use has been restricted by recent laws and regulations so that in the future the sewage sludge obtained will often have to be disposed of or combusted. Thus, it is of particular importance that the treated sewage sludge can be readily thickened and dehydrated and that a sludge liquor water is obtained which has a low residual contamination.
  • the object of the invention to develop a process for the disinfection and aerobic stabilization of concentrated sewage sludge in several steps, using one or more heat-insulated containers, preferably with stirring, with the addition of oxygen-containing gas.
  • the process works safely and reliably, disinfects and stabilizes perfectly, even under conditions of varying crude sewage sludge input, varying temperatures of the crude sewage sludge, and/or the environment.
  • the process avoids unacceptable odor problems, is comparable to current processes in cost aspects and provides a well-settling sludge with a water effluent of low contamination.
  • the sludge is disinfected by further aerobic degradation without supplying external heat at about 50° C. to 55° C. for at least 20 hours or at >55° C. for at least 10 hours, and
  • the sludge is stabilized at mesophilic temperature by active cooling to from 25° C. to 45° C. and further aerobic degradation within from 2 to 8 days, and preferably within from 3 to 5 days.
  • the steps (a), (b) and (c) are carried out in the same container.
  • That container is furnished with a heat exchanger, for example one using pipe coils or flushable plate-coolers, in order to optionally pre-heat the concentrated crude sludge, but mostly to carry away the heat at the end of step (b) and during the step (c) and thereby to effect the active cooling.
  • a heat exchanger for example one using pipe coils or flushable plate-coolers
  • That one container-process in order to effectively utilize the heat to be removed at the end of step (b) and, in addition, to increase the flexibility of the process, may be extended in that two or more batches are run in two or more containers at different times so that the amount of heat recovered at the beginning of step (c) of a preceding batch is employed for pre-heating the concentrated crude sludge of step (a) of a subsequent batch.
  • three or more containers can be provided and another embodiment of the process can be used, which is particularly simple and economical, in which embodiment the steps (a), (b) and (c) are allowed to take place in three separate stages A, B and C connected in series, wherein the containers of the stages B and C have capacities several times the capacity of the container of stage A.
  • the heating of the crude sludge in stage A is generally effected by way of heat exchange with the sludge in stage C. However, it is also possible to effect the heating of the crude sludge in stage A by way of a heat exchange with the sludge of stage B. If desired, heat may be extracted also from the effluent from stage C.
  • stage C it has been found that in the regular operation of stage C, more heat is released and has to be removed than is required for warming the concentrated crude sludge in stage A. Thus, amounts of heat from stage C exceeding the amount of heat needed in stage A are removed by heat exchange and can be utilized otherwise, if desired.
  • stage A it is of course possible to satisfy the heat requirements of stage A also in part by means of a heat exchange with the sludge in stage B.
  • heat may be transferred to stage A from stage B in order to further increase the temperature in the former stage.
  • the temperature in stage A must be at least 25° C. prior to transferring a batch to stage B. Temperatures in excess of 45° C. occur rarely in stage A, because even with stronger aeration in stage A, the temperature rise due to aerobic degradation is not so fast that the maximum temperatures of stage C will be essentially exceeded.
  • the supply to stage A may be batch or continuous. Stage A is preferably agitated and aerated, but this is not absolutely required.
  • the aerobic degradation in stage B is so vigorous that temperatures in excess of 50° C. will be generated. At temperatures between 50° C. and 70° C., with appropriate residence times, the disinfection is safely assured.
  • the time between two feeding cycles can be made to depend on the temperature in stage B. At 50° C., a time between two feeding cycles of one day will be sufficient. With temperatures in excess of 65° C., even a time between two feeding cycles of three hours will be sufficient to obtain a perfect disinfection. However, as a safety measure, disinfection should be carried out for at least ten hours.
  • the temperature in stage B can be controlled by the amount of the oxygen supply. In addition, it may also be made to depend on the time available between two feeding cycles.
  • the variation in the amounts of concentrated crude sludge to be processed can be compensated by an appropriate adaption of the filling height in the containers and, if necessary, by turning on or off additional containers connected in parallel or in series and operating for the respective stage.
  • stage C the temperature is reduced to from 25° C. to 45° C., and preferably to about 35° C. At these temperatures there is formed a sludge which has an especially good settling behavior and an effluent with low contamination.
  • the average residence times in general are:
  • a concentrated sewage sludge as that from mechanical and/or biological purification of sewage or industrial waste waters, wherein a solids content of from 2 to 8% has been attained by static and/or machine concentration.
  • Such concentrated sewage sludges in general, have a sufficient content of degradable matter required for the exothermal aerobic degradation in stage B, while, on the other hand, they still have rheological properties so that they are easy to handle.
  • the supply of the oxygen-containing gas is generally effected by aeration. In special cases, more or less pure oxygen may be added as well. Oxygen-containing gases having an oxygen-content of less than 15% are only used as an exception, because then the oxygen supply becomes increasingly uneconomical. Furthermore, with such low-oxygen gases care is needed to ensure that anaerobic degradation is avoided, since this results in an odor problem.
  • the oxygen supply may be controlled by the intensity of aeration and/or the oxygen content of the gas supplied.
  • Agitation and aeration in the stages B and C and, optionally, in stage A can be effected by any means known in waste water technology and process technology.
  • Aerating stirrers such as those manufactured, for example, by the company Fuchs Gas- und Wasser-technik, Mayen, have proven to be particularly useful in the process of the invention.
  • the containers may be any of the reactors equipped with a stirrer and gas-introducing means as conventionally used in waste water technology, which reactors preferably may also be provided with additional foam cutters and foam controllers. Heat supply and removal is effected by means of conventional heat exchangers. Undesirable heat losses are eliminated by providing the containers with a sufficient heat insulation.
  • the process of the invention can be employed not only for the disinfection and aerobic stabilization of sewage sludge, but also for the treatment of liquid manure and other organic concentrates such as yeast wastes, etc.. It has been shown that the process of the invention reliably and flexibly results in disinfection and good stabilization, whereby a well-settling sewage sludge and a sludge liquor of good quality and low residual contamination are formed. In contrast to only thermophilic or anaerobic degradation processes, no odor nuisance is produced. Due to the mesophilic residue stabilization, ammonium is also largely subjected to nitrification, whereby the pH value decreases from a value in excess of 8 to the neutral range or somewhat lower.

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  • Life Sciences & Earth Sciences (AREA)
  • Biodiversity & Conservation Biology (AREA)
  • Microbiology (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Treatment Of Sludge (AREA)
  • Immobilizing And Processing Of Enzymes And Microorganisms (AREA)
  • Aeration Devices For Treatment Of Activated Polluted Sludge (AREA)
  • Physical Water Treatments (AREA)
  • Measuring Volume Flow (AREA)
  • Apparatus For Radiation Diagnosis (AREA)
  • External Artificial Organs (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)
  • Activated Sludge Processes (AREA)
US07/483,045 1989-02-21 1990-02-21 Process for the disinfection and aerobic stabilization of sewage sludge Expired - Lifetime US4983298A (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DE19893905228 DE3905228C1 (en) 1989-02-21 1989-02-21 Process for disinfection and aerobic stabilisation of sewage sludge
DE3905228 1989-02-21
DE3928846 1989-08-31
DE19893928846 DE3928846C1 (da) 1989-08-31 1989-08-31

Publications (1)

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US4983298A true US4983298A (en) 1991-01-08

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US07/483,045 Expired - Lifetime US4983298A (en) 1989-02-21 1990-02-21 Process for the disinfection and aerobic stabilization of sewage sludge

Country Status (8)

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US (1) US4983298A (da)
EP (1) EP0384162B1 (da)
AT (1) ATE88166T1 (da)
CA (1) CA2010156C (da)
DE (1) DE59001181D1 (da)
DK (1) DK0384162T3 (da)
ES (1) ES2039968T3 (da)
TR (1) TR26660A (da)

Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5540847A (en) * 1993-04-29 1996-07-30 Stultz; Jeffrey H. Sludge digestion
US5948261A (en) * 1998-02-05 1999-09-07 Pressley; Richard L. Process for treating biosolids from wastewater treatment
US6168717B1 (en) 1998-02-05 2001-01-02 Thermal Process Systems, Llc Process for controlling foam in a treatment reactor
US6203701B1 (en) 1998-02-05 2001-03-20 Thermal Process Systems, Llc Process and apparatus for treating biosolids from wastewater treatment
US6685834B1 (en) * 1999-12-20 2004-02-03 Kruger, Inc. Method for conditioning and dewatering thermophilic aerobically digested biosolids
US6719903B1 (en) 1998-02-05 2004-04-13 Thermal Process Systems, Llc Process and apparatus for treating biosolids from wastewater treatment
US20050077236A1 (en) * 2001-11-09 2005-04-14 Son Le Incubation treatment of sludge for pathogen reduction prior to digestion
US20050145566A1 (en) * 2001-08-28 2005-07-07 Clearvalue Technologies Methods, processes and apparatus for bio-solids recycling and the product of bio-solids from such methods, processes and apparatus
US6966983B1 (en) 2004-10-01 2005-11-22 Mixing And Mass Transfer Technologies, Llc Continuous multistage thermophilic aerobic sludge digestion system
US20080210627A1 (en) * 2005-04-22 2008-09-04 Leonhard Fuchs Process for the Aerobic-Thermophilic Stabilization and Disinfection of Sludge
WO2010145810A1 (de) * 2009-06-16 2010-12-23 Holger Blum Verfahren und vorrichtung zum reinigen von abwasser
GB2496723A (en) * 2011-10-07 2013-05-22 Anglian Water Services Ltd Sludge treatment process using hydrolysis and pasteurisation
US20140158940A1 (en) * 2012-07-24 2014-06-12 Shahram Navaee-Ardeh Production of Synthesis Gas From Biosolid-Containing Sludges Having a High Moisture Content
ES2528337A1 (es) * 2014-10-31 2015-02-06 Abengoa Water, S.L. Sistema de digestión aerobia termófila autosostenida y procedimiento asociado
CN112566884A (zh) * 2018-08-01 2021-03-26 恩维罗库尔股份有限公司 植物和土壤用营养组合物的制造方法

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2844785B1 (fr) * 2002-09-25 2005-07-08 Ondeo Degremont Procede et dispositif de reduction de la production de boues des stations de traitement d'eaux residuaires par cultures biologiques fixees
FR2844786B1 (fr) * 2002-09-25 2005-06-03 Ondeo Degremont Procede et dispositif de reduction de la production de boues des stations de traitement d'eaux residuaires par cultures biologiques fixees
CZ303001B6 (cs) * 2004-12-20 2012-02-15 Fortex - Ags, A.S. Zpusob a zarízení pro komplexní úpravu cistírenských kalu
DE102005018893B4 (de) 2005-04-22 2007-06-14 Martin Fuchs GbR (vertretungsberechtigte Gesellschafter: Dipl.-Ing. Leonhard Fuchs, Martin Fuchs, 56727 Mayen) Verfahren und Vorrichtung zur aerob-thermophilen Stabilisierung und Entseuchung von Schlamm

Citations (8)

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Publication number Priority date Publication date Assignee Title
US3864247A (en) * 1971-03-25 1975-02-04 Laval Separator Co De Biological decomposition of organic material by thermophilic microorganisms
US3892660A (en) * 1973-04-04 1975-07-01 Dag Romell Method of rendering decay processes more effective
US4026793A (en) * 1975-08-21 1977-05-31 Rein David A Aerobic sewerage digestion process (42 C. process)
US4246099A (en) * 1979-04-06 1981-01-20 Union Carbide Corporation Aerobic/anaerobic sludge digestion process
US4276174A (en) * 1980-03-26 1981-06-30 Union Carbide Corporation Control of sludge temperature in autothermal sludge digestion
GB2105318A (en) * 1981-07-15 1983-03-23 British Oxygen Co Ltd Treatment of aqueous waste material
DE3240009A1 (de) * 1982-10-28 1984-05-03 Linde Ag, 6200 Wiesbaden Verfahren und vorrichtung zur biologischen behandlung von schlamm
EP0157317A2 (de) * 1984-04-04 1985-10-09 Fried. Krupp Gesellschaft mit beschränkter Haftung Verfahren und Vorrichtung zur biologischen aeroben Reinigung von Abwasser

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3864247A (en) * 1971-03-25 1975-02-04 Laval Separator Co De Biological decomposition of organic material by thermophilic microorganisms
US3892660A (en) * 1973-04-04 1975-07-01 Dag Romell Method of rendering decay processes more effective
US4026793A (en) * 1975-08-21 1977-05-31 Rein David A Aerobic sewerage digestion process (42 C. process)
US4246099A (en) * 1979-04-06 1981-01-20 Union Carbide Corporation Aerobic/anaerobic sludge digestion process
US4276174A (en) * 1980-03-26 1981-06-30 Union Carbide Corporation Control of sludge temperature in autothermal sludge digestion
GB2105318A (en) * 1981-07-15 1983-03-23 British Oxygen Co Ltd Treatment of aqueous waste material
DE3240009A1 (de) * 1982-10-28 1984-05-03 Linde Ag, 6200 Wiesbaden Verfahren und vorrichtung zur biologischen behandlung von schlamm
EP0157317A2 (de) * 1984-04-04 1985-10-09 Fried. Krupp Gesellschaft mit beschränkter Haftung Verfahren und Vorrichtung zur biologischen aeroben Reinigung von Abwasser

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
G. W. F. Wasser/Abwasser, Sep. 1986, No. 9, Neue Einsatzbereiche f r aerob thermophile Prozesse zur Stabilisierung und Entseuchung von Abwasserschl mmen mit Bioenergienutzung , K. Breitenb cher. *
G. W. F.-Wasser/Abwasser, Sep. 1986, No. 9, "Neue Einsatzbereiche fur aerob-thermophile Prozesse zur Stabilisierung und Entseuchung von Abwasserschlammen mit Bioenergienutzung", K. Breitenbucher.

Cited By (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5540847A (en) * 1993-04-29 1996-07-30 Stultz; Jeffrey H. Sludge digestion
US20060011540A1 (en) * 1998-02-05 2006-01-19 Pressley Richard L Process and apparatus for treating biosolids from wastewater treatment
US5948261A (en) * 1998-02-05 1999-09-07 Pressley; Richard L. Process for treating biosolids from wastewater treatment
US6168717B1 (en) 1998-02-05 2001-01-02 Thermal Process Systems, Llc Process for controlling foam in a treatment reactor
US6203701B1 (en) 1998-02-05 2001-03-20 Thermal Process Systems, Llc Process and apparatus for treating biosolids from wastewater treatment
US6514411B2 (en) 1998-02-05 2003-02-04 Thermal Process Systems, Llc Process for controlling foam in a treatment reactor
US6719903B1 (en) 1998-02-05 2004-04-13 Thermal Process Systems, Llc Process and apparatus for treating biosolids from wastewater treatment
US6685834B1 (en) * 1999-12-20 2004-02-03 Kruger, Inc. Method for conditioning and dewatering thermophilic aerobically digested biosolids
US8123944B2 (en) * 2001-08-28 2012-02-28 Clearvalue Technologies, Inc. Processes of aqueous solids treatment
US20050145566A1 (en) * 2001-08-28 2005-07-07 Clearvalue Technologies Methods, processes and apparatus for bio-solids recycling and the product of bio-solids from such methods, processes and apparatus
US7452465B2 (en) 2001-11-09 2008-11-18 United Utilities Plc Incubation treatment of sludge for pathogen reduction prior to digestion
US20050077236A1 (en) * 2001-11-09 2005-04-14 Son Le Incubation treatment of sludge for pathogen reduction prior to digestion
US7329340B2 (en) 2004-10-01 2008-02-12 Mixing And Mass Transfer Technologies, Llc Continuous multistage thermophilic aerobic and aerobic-anaerobic sludge treatment systems
US6966983B1 (en) 2004-10-01 2005-11-22 Mixing And Mass Transfer Technologies, Llc Continuous multistage thermophilic aerobic sludge digestion system
US7563374B2 (en) 2004-10-01 2009-07-21 Mixing & Mass Transfer Technologies, Llc Continuous multistage thermophilic aerobic and aerobic-anaerobic sludge treatment process
US20060070938A1 (en) * 2004-10-01 2006-04-06 Mixing And Mass Transfer Technologies, Llc Continuous multistage thermophilic aerobic and aerobic-anaerobic sludge digestion systems
US20080210627A1 (en) * 2005-04-22 2008-09-04 Leonhard Fuchs Process for the Aerobic-Thermophilic Stabilization and Disinfection of Sludge
US7531093B2 (en) * 2005-04-22 2009-05-12 Leonhard Fuchs Process for the aerobic-thermophilic stabilization and disinfection of sludge
CN102482127A (zh) * 2009-06-16 2012-05-30 H·布卢姆 净化污水的方法和设备
WO2010145810A1 (de) * 2009-06-16 2010-12-23 Holger Blum Verfahren und vorrichtung zum reinigen von abwasser
US8945378B2 (en) 2009-06-16 2015-02-03 Holger Blum Apparatus for cleaning wastewater
GB2496723A (en) * 2011-10-07 2013-05-22 Anglian Water Services Ltd Sludge treatment process using hydrolysis and pasteurisation
GB2496723B (en) * 2011-10-07 2016-07-13 Anglian Water Services Ltd Sludge treatment process
US20140158940A1 (en) * 2012-07-24 2014-06-12 Shahram Navaee-Ardeh Production of Synthesis Gas From Biosolid-Containing Sludges Having a High Moisture Content
ES2528337A1 (es) * 2014-10-31 2015-02-06 Abengoa Water, S.L. Sistema de digestión aerobia termófila autosostenida y procedimiento asociado
WO2016066880A1 (es) * 2014-10-31 2016-05-06 Abengoa Water, S. L. Sistema de digestión aerobia termófila autosostenida y procedimiento asociado
CN112566884A (zh) * 2018-08-01 2021-03-26 恩维罗库尔股份有限公司 植物和土壤用营养组合物的制造方法
CN112566884B (zh) * 2018-08-01 2022-12-06 恩维罗库尔股份有限公司 植物和土壤用营养组合物的制造方法

Also Published As

Publication number Publication date
DE59001181D1 (de) 1993-05-19
CA2010156A1 (en) 1990-08-21
TR26660A (tr) 1995-03-15
CA2010156C (en) 1996-03-19
EP0384162A1 (de) 1990-08-29
EP0384162B1 (de) 1993-04-14
ES2039968T3 (es) 1993-10-01
ATE88166T1 (de) 1993-04-15
DK0384162T3 (da) 1993-05-17

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