US428956A - Apparatus for the manufacture of gas - Google Patents
Apparatus for the manufacture of gas Download PDFInfo
- Publication number
- US428956A US428956A US428956DA US428956A US 428956 A US428956 A US 428956A US 428956D A US428956D A US 428956DA US 428956 A US428956 A US 428956A
- Authority
- US
- United States
- Prior art keywords
- cupola
- furnace
- pipe
- gas
- heating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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- 238000004519 manufacturing process Methods 0.000 title description 12
- 239000007789 gas Substances 0.000 description 114
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 20
- 150000002430 hydrocarbons Chemical group 0.000 description 20
- 238000010438 heat treatment Methods 0.000 description 18
- 229910052799 carbon Inorganic materials 0.000 description 16
- 239000000571 coke Substances 0.000 description 10
- 239000007788 liquid Substances 0.000 description 10
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 230000000630 rising Effects 0.000 description 8
- 239000004215 Carbon black (E152) Substances 0.000 description 6
- 239000003245 coal Substances 0.000 description 6
- 239000001257 hydrogen Substances 0.000 description 6
- 229910052739 hydrogen Inorganic materials 0.000 description 6
- UFHFLCQGNIYNRP-UHFFFAOYSA-N hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 6
- 240000004018 Rosa multiflora Species 0.000 description 4
- 238000002485 combustion reaction Methods 0.000 description 4
- 238000000354 decomposition reaction Methods 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 230000002441 reversible Effects 0.000 description 4
- BVKZGUZCCUSVTD-UHFFFAOYSA-N Carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 2
- 240000008881 Oenanthe javanica Species 0.000 description 2
- 235000000365 Oenanthe javanica Nutrition 0.000 description 2
- 239000003575 carbonaceous material Substances 0.000 description 2
- 239000003610 charcoal Substances 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 239000000446 fuel Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000000717 retained Effects 0.000 description 2
- 238000009751 slip forming Methods 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
- C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
- C01B3/04—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by decomposition of inorganic compounds, e.g. ammonia
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
- C10J1/00—Production of fuel gases by carburetting air or other gases without pyrolysis
- C10J1/213—Carburetting by pyrolysis of solid carbonaceous material in a carburettor
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/36—Hydrogen production from non-carbon containing sources, e.g. by water electrolysis
Definitions
- Figure l is a plan view of my invention.
- Fig. 2 is an end view thereof.
- Fig.3 is a longitudinal section on the line 0c at, Fig. l.
- the heating-iurnace is provided with a series of arches, as at P, these arches beingarranged in any suitable way so as to deflect the heat from one side to the other of the furnace, in order to provide for the proper heating of the retorts and cylinders therein, and being perforated on alternate sides, as at 2), to permit the passage of the gases, andthe spaces not occupied by the said retorts and pipes being filled with checker-work, as at (1, so that practically all the heat from the burning of the gas therein is stored within said cylinders, the walls ot the furnace, the arches, and the mass of checker-work serving to maintain a high heat within the retorts and chambers, so that the necessity for reversing at short intervals is overcome.
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Inorganic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
Description
(No Model.) 3 Sheets-Sheet 1,
R APPARATUS P0 E MA FACTURE OP GAS. l No. 428,956. Patented May 27, 1890.
V IWI 1,1 s N U I f l hl I Ik f w :1
(No Model.) `3 Sheets-Sheet 2.
' J. M. ROSE. APPARATUS PGR TH- E MANUFAGTURE OF GAS.
No. 428,956. Patented Mayz'l, 1890..
(No Model.) 3 Sheets-Sheet 3.
J. M. ROSE. vAPPAMTUS P01?. THB MANUPAGTURB 0F GAS. No. 428,956. Patented May 27, 1890.
UNITEn STATES PATENT OFFICE.
JAMES M. ROSE, OF ALLEGHENY, PENNSYLVANIA.
APPARATUS FOR THE MAN'UFACTURE OF GAS.
SPECIFICATION forming part of Letters Patent No. 428,956, dated May 27, 1890.
Application filed June l0, 1889. Serial No. 313,708. (No model.)
To a/ZZ whom t muy concern:
Be it known that I, JAMES M. ROSE, a resident of Allegheny, in the county of Allegheny and State of Pennsylvania, have invented a new and useful Improvement in Apparatus for the Manufacture of Gas; and I do hereby declare the following to be a full, clear, and exact description thereof.
My invention relates to the manufacture of gas, having special reference to apparatus for the manufacture of gas for fuel or heating purposes, though the apparatus may be employed, if desired, for making illuminatinggas and like purposes. Its object is to provide an apparatus in which avery large body of gases may be rapidly and continuously formed, and in which parts of the apparatus may be retained at the high heat necessary for such gas-making purposes, both for the superheating and decomposition of steam, the decomposition of hydrocarbons, and the lixing of the resultant gases. Y
My apparatus comprises two sets of gasgenerating apparatus, which are preferably located and operated together, each'such sethaving at the base thereof two cupola-generators, and above said generators a casing containing a heating-furnace or regenerator with which one of said generators communicates, and through which a series of horizontal retorts extend, said rctorts being connected at the ends, and said heating-furnace having also a vertical cylinder passing through the same and communicating at the base thereof with the other cupola-generator, whereby the gases formed in one such generator may be burned Within the heating-furnace to maintain the said retorts and vertical cylinder at a high heat, the retorts being employed for heating coal, coke, or other carbon contained in the same, through which steam is passed for the manufacture of .water-gas, While hydrocarbons are introduced into said vertical cylinder, and, as will hereinafter be described, the gases formed, together with the further portions of steam, can be-united and subsequently be iixed by a passage through the heating-furnace and through the body of incandescent carbon in one of the cupola-generators, all of which will be hereinafter more particularly described.
My improvements in connection with the said apparatus will be specifically set forth in the claims.
To enable others skilled in the art to make and use my invention, I will describe the same more fully, referring to the accompanying drawings, in whichl Figure l is a plan view of my invention. Fig. 2 is an end view thereof. Fig.3 is a longitudinal section on the line 0c at, Fig. l.
Like letters of reference indicate like parts in each.
As above stated, I prefer to employ my invention with two sets of apparatus, one set being marked A and the other set B. Each set of apparatus has the same parts thereto, and I will first describe the set of apparatus marked A, the set of apparatus marked B being the same, and lettered the same, except that the letters are marked to distinguish them from those of the other set of apparatus in the description of the operation thereof. At the base of the apparatus are the cupola-generatorsO D, the cupola-generator O communieating through a port in the top thereof with the heating-furnace or generator E, which is built WithinV a suitable plate-metal casing e, this casing and the furnace being preferably rectangular in shape, as shown.
The cupola-generator O has the air-entrance c, and has also suitable grate-bars and feeding and discharge doors, as is usual in the construction of such generators. It has also the eduction-pipe f leading therefrom near the base of the cupola and controlled by the valve F. The cupola D has the air-port d, and has like grate-bars and feeding and discharge doors. This cupola D communicates with the vertical cylinder G,Which extends entirely through the heating-furnace and opens into a pipe 7L' at the top thereof. Extending through the heating-furnace E are also one or more steam-superheating pipes M, each of which communicates at the base thereof With the cupola-generator D, and has at the upper end thereof suitable steam-entrance m, as shown, Extending through the heating-furnace E are a series of horizontal retorts or cylinders K, there being four such cylinders shown in the drawings, and these cylinders extending through the walls of the heating-furnace aud communicating with each other at the ends-that is, the two upper cylinders having ICO their communicating pipe 7U shown at the let't of the drawings, the middle cylinders having a like communicating pipe 7c. at the right of the drawings, and the end elyinders having t-heir communicating pipe 7i; atthe left of the dawings, these pipes therefore forming a continuous course from the top to the bottom of the series through which the steam maybe passed, and the lower cylinder opening by suitable valve-controlled ports into the two cupola-generators C D, the opening 'L' into the cupolagenerator C being controlled by a valve L, and the opening j into the cupolagenerator D being controlled by a valve J. The upper cylinder communicates through a pipe Zwith the pipe 71 said pipe being controlled by the valve L, and the pipe 7L communieates with the upper end of the furnace E through the valve ll. Extending between the two sets of apparatus is the pipe N, through which the gases flow, as hereinafter described, in the making of the The heating-iurnace is provided with a series of arches, as at P, these arches beingarranged in any suitable way so as to deflect the heat from one side to the other of the furnace, in order to provide for the proper heating of the retorts and cylinders therein, and being perforated on alternate sides, as at 2), to permit the passage of the gases, andthe spaces not occupied by the said retorts and pipes being filled with checker-work, as at (1, so that practically all the heat from the burning of the gas therein is stored within said cylinders, the walls ot the furnace, the arches, and the mass of checker-work serving to maintain a high heat within the retorts and chambers, so that the necessity for reversing at short intervals is overcome. Suitable air-ports are provided in the upper part of the cupola-generator C and at intervals intheheating-furnace E to provide for the complete combustion of the producergas employed in heating the same.l The furnace has also the relief-valve Q, which can be opened while the gas is bein g burned within said surface 'for heating purposes, as above referred to. The eduction-pipe f communicates through the valve F with a pipe R, leading to the hydraulic main or storage-tank, this pipe R leading into both sets of apparatus, and also communicating with the eduction-pipe f' ot' the other set of apparatus through the valve F. Suitable steam-pipes conununieate with the series of retorts K-one steam-pipe s communicating with the lower retort and a like steam-pipe f communicating with the upper retort-so that steam can be fed in either course through said series of retorts. 'lhe said retorts are closed at their ends by any suitable removable caps, as at vu, which may be clamped by any suitable means upon the ends ot the retorts.
As above referred to, the parts in the set ot apparatus marked 13 are the same as in the set marked A, and without referring particularly to each part it will be found that they are lettered the same, except that each letter is marked with the cupola-generators being ("D, the furnace E', vertical cylinder G', the.
The operation of the apparatus is as follows: The several cupola-generators are iilled with coal or coke, and the several retorts are filled with coa-l, coke, or charcoal, as Vmay be desired. 3y means of the air-blast gas is generated in the several cupolas, the gases from the cupolas C C' being burned in the furnaces E E' and the gases formed in the cupolas D D' being burned in the vertical chambers G i'. lVhentheapparatusisbrought to the proper heat, the relief-valve Q ot' the heating-furnace E is closed, and the valve in the air-supply pipe c to the generator() is closed, while air is continued to the chamber D. Air is also shut oit from the chamber D', but continued within the chamber C of the other set of apparatus. The eduction-valve F, the valve ll, the valve Ti iu the Iirst set of apparatus and the valve J in the second set ot" apparatus are opened. All th e other valves remain closed; and it may be here incidentally stated that the valves I and l are not opened during gas-making, being only opened when the cylinders are being emptied ot their carbonaceous materials. Steam is then admitted through the steam-inlet t', which passes down through each successive retort K', passing through the furnace E', the steam bei ngdecomposed by the incandescent carbon within said retorts or cylinders, and then passing through the valve J and passage/j' into the eupola-generator D'. At the same time steam is admitted through the steam-entrance m' at the upper end of the vertical superheating-cylinder M', and in passing down through said cylinder the steam is highly superheated, and it also enters the cupola-generator D', being forced by its expansion down into the mass of incandescent coke contained therein, and being to some extent decomposed by said incandescent coke. At the same time oil is sprayed into the cylinder (r through the oilentrance g' at the top thereof, and the water, gas and steam formed in the horizontal cylinders K and passing from the superheatcr M pass upwardly through this cylinder G', meeting the current of liquid hydrocarbons, which, as they descend through said cylinder against the current of gases are spread, the oil separating into drops, which are again divided into smaller globules or spray, and iinally so intermingled with the gases rising through the cylinder that they are vaporized and unite with said gases, the gases then passing from the cylinder i' through the pipe N to the valve Il', which is open, as above set forth, so that the gases can pass down into the heating-fu rnace or regenerator E. At the same time the air-blast in the cupolagenerator l) is continued, and the producergas passing upwardly through the cylinder G is intermingled with the superheated steam, which entered said generator from the superheatiugcylinder M, the intermingled pro- IOO ducer-gas andsteam rising through the cylinder G and against the current of liquid hydrocarbons introduced through the oil-entrance g, which descend against the current of gases, being intermingled therewith and finally united therewith, as described in an application for patent iiled by me on the 14th day of March, 1889, Serial No. 308,313, and these gases also pass into the pipe 7i, intermingling with the other gases entering through the pipe N and passing downwardly through the regenerator E. At the same time steam is admitted through the pipe s at the lower end of the series of horizontal cylinders K, and this steam passes through the mass of incandescent carbon in the several cylinders and is decomposed, thereby forming water-gas, which passes through the pipe Z and Valve Ii into the pipe 7L, and thence through the valve H with the other gases into the regenerator E. All these gases are ntermingled in this regenerator E, and they pass through the masses'ot checker-work between the several arches therein, and are properly heated and fixed in said regenerator or fixing-chamber, the gases then passing downwardly' through the massof incandescent carbon in the cupola-generator C, where they are rendered still more stable by the heat thereof, and any carbonic acid contained therein is converted into carbonio oxide, the gases then passing through the eduction-pipe f and Valve F into the pipe R, and thence to the hydraulic main and tank.
I am thus enabled to obtain a large quantity of gas of high heating powers, the gas formed containing a large proportion of hydrogen and carbonio oxide, as well as a large proportion of marsh-gas or like hydrocarbon ,gases formed by the union of the hydrogen with thel hydrocarbon, and the gas having little or no nitrogen, as but little of the producer-gas is employed, and the nitrogen introduced with the air is combined with the hydrogen in the presence of the steam andk body of hydrocarbons, as described in an application filed by me October 4, 1888, Serial No. 287,148, and is consequently absorbed in the hydraulic main and eliminated from the During this operation the producer-gas from the cupola-generator C' is passing into and burning in the heating-furnace or regenerator E', and a suitable quantity of air being fed thereto, so that a high heat is generated therein, and the several cylinders passing through the regenerator, together with the checker-work therein, are raised to ahigh heat and the said regenerator highly heated for the fixing ot' the gases on the reversal of the apparatus. The gases passing through this chamber are permitted to escape through the relief-valve Q', or, if desired, may be carried to the steam-generator and completely consumed.
On the reversal of the apparatus the gases pass in exactly the opposite direction, and the Valves are reversed', as required, for the purpose, the relief-valve Q' being closed and the relief-Valve Q opened, the Valves RII, L, and J being closed and the valves F', H', L', and J being opened, the air-blast being cut off from the cupola-generators D and C' and opened to the cupola-generatorsD' and O, the producer-gas from the cupola C being employed to again heat up the regenerator or furnace E. Steam is then admitted atthe upper end of the series of horizontal retorts or cylinders K, and passing down through the incandescent carbon therein enters the cupolagenerator D, steam being also admitted to the superheating-cylinder M, and passing down into said cupola-generator D, and the combined gases and steam rising through the.
cylinder G against the current of liquid hydrocarbons introduced therein. Steam is also continued to the superheater M', and passes down into the cupola-generator D', mingling with the producer-gas therefrom, and rising against the current of liquid hydrocarbon introduced into the cylinder G'. Steamis also introduced at the lower end of the series of re-v torts K', and passing upwardly through said retorts passes through the pipe Z' and Valve" L', the gases all intermingling in the pipe 7L',
and passing through the Valve H', through the heating-furnace E', and through the cupola-z generator C to the eduction-pipe f', and through the valve F' to the pipe R. In this way it is seen that a high heat maybe maintained in the entire apparatus proper for the generation of gases and the fixing of the same, and that a large body of water-gas may be formed and the gases properly intermingled with the liquid hydrocarbons, whiler the apparatus is compact in form and adapted to generate a very large body of gases. I am also enabled to utilize the heat obtained in the Iixingchambers for heating a series of retorts and decomposing steam and forming water-gas in said retorts and to maintain the heat in said series ot' retorts by the means ot' heated checker-work around the same, together with the direct combustion formed in one ot' such heating-furnaces around the retorts during the making of gas therein. In case of the distillation of tar or any such substances from the coal within such retorts means are provided for introducing the same into the cupola-generator below, Where it can be broken up 'and formed into gases, direct communication being formed with such generators through the valves I I' and J J', though the mass of such materials would be taken up with the steam in passing through said body of carbon in the retorts.
If desired, one set of apparatus may be employed instead of the two sets, and the course of the gases formed in the cupola-generator C, and then the blast being turned off from the saine and the gases passing from the series of retorts into the cupola-generator D,
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thence through the vertical cylinder G, and thence down through the heating-furnace E and cupola-generator C to the eduction-pipe. In the use of the double apparatus in this way a continuous manufacture of gas can be carried on.
That I claim as my invention, and desire to secure by Letters Patent, is
l. A gas-making apparatus having two cupola-generators and a heating-furnace or regenerator above the same, with which 011e of said cupolagenerators communicates, a vertical cylinder communicating with the other generator and extending through the heatingfurnace, a series of horizontal retorts or cylinders extending through the heating-furnace, and a pipe connecting said vertical cylinder and said series of horizontal cylinders, substantially as and for the purposes set forth.
2. A gas-making apparatus having two cupola-generators, a heating-furnace above the same, with which one of said cupola-generators communicates, a vertical cylinder communicating with the other cupola-generator and extending through the heating-furnace, a series of horizontal retorts communicating with each other and at the lower end with the second cupola-generator and having a steam-entrance at the upper end thereof, and a pipe connecting said vertical cylinder and said series of horizontal cylinders, substantially as and for the purposes set forth.
3. A gas-making apparatus having two cupola-generators, a heating-furnace above the same, with which one of said cupola-generators communicates, a vertical cylinder communicating with the other cupola-generator and extending through the heating-furnace, a series of horizontal retorts or cylinders extending through the heating-furnace, and a steam-suporheating pipe extending through the heating-f urn ace, having a steam-entrance at its upper end and communicating at its lower end with a cupola-generator, substantially as and for the purpose set forth.
4. A gas-makin g apparatus havin ga cupolagenerator, a heating-furnace above the same, with which said generator communicates, and a series of horizontal retorts passing through said heating furnace and communicating with each other at their alternate ends, and also communicating at the lower end with said cupola-generator, substantially as and for the purposes set forth.
5. A gas-making apparatus having two cupola-generators, a heating-furnace above the same, with which one of said generators communicates, said furnace havin g a seri es of horizontal retorts extending through the same and communicating with each other, and communicating through a valve-controlled pipe with a pipe above said furnace, and having a vertical cylinder extending through said heating-furnace and communicating at the base with the other cupola-generator and at the top with said pipe above the heating-furnace, substantially as and for the purposes set forth.
G. A gas-making apparatus having two cupola-generators, a heating-furnace above the same, with which one of said generators communicates, said furnace havinga series of horizontal retorts extending through the same and communicating with each other, and communicating through a valve-controlled pipe with a pipe above said furnace, and having a vertical cylinderl extending through said heating-furnace and communicating at the base with the other cupola-generator and at the top with said pipe above the heating-sun face, and a valve-controlled entrance from said pipe into the upper end of said heatingfurnace, substantially as and for the purposes set forth.
7. In a gas-making apparatus the combination of two seis of apparatus each having two cupolagenerators, a heating -furnace above the same, with which one of said cupola -generators communicates, a series of horizontal retorts or cylinders extending through the same and communicating with each other and with a pipe above the gas apparatus, a vertical cylinder passing through the furnace and communicating at its lower end with the other cupola-generator and at its upper end with the pipe ahove the gas apparatus, and a connecting-pipe between said two 'sets of apparatus, whereby the gases formed in one setmay be carried into the other set for treating and a continuous gas operation obtained, substantially as and for the purposes set forth.
In testimony whereof I, the said 'JAMES M. ROSE, have hereunto set my hand.
JAMES M. ROSE.
Iitnessesz WM. P. MERCER, B. W. HAINEs.
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US428956A true US428956A (en) | 1890-05-27 |
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