US421935A - John holliday - Google Patents
John holliday Download PDFInfo
- Publication number
- US421935A US421935A US421935DA US421935A US 421935 A US421935 A US 421935A US 421935D A US421935D A US 421935DA US 421935 A US421935 A US 421935A
- Authority
- US
- United States
- Prior art keywords
- holliday
- john
- alkaline
- nitrate
- soda
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- 229910052787 antimony Inorganic materials 0.000 description 4
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical class [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 229910002651 NO3 Inorganic materials 0.000 description 3
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 3
- IOVCWXUNBOPUCH-UHFFFAOYSA-M Nitrite anion Chemical compound [O-]N=O IOVCWXUNBOPUCH-UHFFFAOYSA-M 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 239000003518 caustics Substances 0.000 description 2
- 229940072033 potash Drugs 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 235000015320 potassium carbonate Nutrition 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 1
- 159000000011 group IA salts Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 235000011121 sodium hydroxide Nutrition 0.000 description 1
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G30/00—Compounds of antimony
- C01G30/02—Antimonates; Antimonites
- C01G30/023—Antimonates; Antimonites of ammonium, alkali or alkaline-earth metals or magnesium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
Definitions
- Metallic antimony by preference pulverized, is treated in a boiling solution of nitrate or nitrite of soda or potash and canstic soda or potash, or in any mixture of either alkaline nitrate or nitrite with either caustic alkali.
- the operation is ended and the solution isan alkaline antimonite.
- the propertions may be considerably varied and other non'active ingredients-such as saltmay be added without detriment to the process. It is then allowed to stand as it is or diluted with water and allowed to settle. The clear solution of antimonoso antimonate is then run off and used as it is or evaporated to dryness.
- alkaline antimonites generally considered antimonosoantimonates
- metallic antimony in a hot aqueous solution of an alkaline nitrate or nitrite and caustic alkali, substantially as described.
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Dental Preparations (AREA)
Description
UNITED STATES PATENT OEEIcE.
N. DIOKERSON, OF
NEW YORK, N. Y.
PROCESS OF MAKING ALKALINE SALTS OF ANTIMONY.
SPECIFICATION forming part of Letters Patent No. 421,935, dated February 25, 1890.
Application filed September 11, 1886.
To all whom it may concern.-
Be it known that I, JOHN HOLLIDAY, of the city of Brooklyn, in the State of New York, have invented a new process for the manufacture of soluble antimonites, generally considered antimonoso-antimonates, of which the following is a specification.
Metallic antimony, by preference pulverized, is treated in a boiling solution of nitrate or nitrite of soda or potash and canstic soda or potash, or in any mixture of either alkaline nitrate or nitrite with either caustic alkali.
In executing my invention I prefer toproeeed as follows: Into a covered tank or retort connected with a condenser and heated by fire or steam I put one thousand pounds of caustic soda, one thousand pounds of nitrate of soda, and run in about four hundred (400) gallons of water. The contents are heated and solution takes place When boiling, I add gradually from one thousand (1,000) to fifteen hundred (1,500) pounds of finely-pulverized antimony, maintaining the liquid at a steady boil. Much ammonia is evolved during the reaction Which ensues, which condenses in the worm. \Vhen ammonia ceases Serial No. 213,328, (No specimens.)
to distill,the operation is ended and the solution isan alkaline antimonite. The propertions may be considerably varied and other non'active ingredients-such as saltmay be added without detriment to the process. It is then allowed to stand as it is or diluted with water and allowed to settle. The clear solution of antimonoso antimonate is then run off and used as it is or evaporated to dryness.
I do not in this specification claim the ordinary fire process for the manufacture of salt.
I claim as my invention- The process of manufacturing alkaline antimonites, generally considered antimonosoantimonates, by treating metallic antimony in a hot aqueous solution of an alkaline nitrate or nitrite and caustic alkali, substantially as described.
In testimony whereof I have signed my name to this specification in the presence of two subscribing witnesses.
JOHN HOLLIDAY.
Witnesses:
ANTHONY GREE, WILLIAM A. POLLOCK.
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US421935A true US421935A (en) | 1890-02-25 |
Family
ID=2490853
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US421935D Expired - Lifetime US421935A (en) | John holliday |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US421935A (en) |
-
0
- US US421935D patent/US421935A/en not_active Expired - Lifetime
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