US3869632A - Glow cathode - Google Patents

Glow cathode Download PDF

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US3869632A
US3869632A US391056A US39105673A US3869632A US 3869632 A US3869632 A US 3869632A US 391056 A US391056 A US 391056A US 39105673 A US39105673 A US 39105673A US 3869632 A US3869632 A US 3869632A
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mounting
electron emitter
glow cathode
electron
glow
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Friedhelm Schulz
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Gesellschaft fuer Kernforschung mbH
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J27/00Ion beam tubes
    • H01J27/02Ion sources; Ion guns
    • H01J27/022Details

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  • This device can be operated at a gas pressure of approximately 0.2 to 0.5 Torr and a heating voltage of 100 to 200 volts to provide deute- References cued rium orhydrogen ions for a cyclotron UNITED STATES PATENTS 1972.078 2/1961 Levi .1 313/346 R 1 .Clalms, 2 Drawmg Flgures GLOW CATHODE
  • the present invention relates to a glow cathode with g a current input and output and to the use of such a glow cathode.
  • a tungsten wire bar heated with 100 to 300 amperes direct current serves as the glow cath ode.
  • a low pressure gas discharge burns at a low gas pressure (e.g. Torr deuterium gas) between the glow cathode and the burn chamber which is formed of graphite.
  • the discharge plasma is constricted by a strong magnetic field which is disposed in theplane of the tungsten wire bar or in a plane parallel thereto to form a more or less precisely defined column between the glow cathode and a reflector for electrons which is insulated from the burn chamber.
  • the reflector is negatively charged during operation.
  • the ions are extracted transversely to the magnetic field through a slit in the burn chamber by a high frequency voltage at an acceleration sector.
  • An increase in the ion yield through an increase in the heating of the glow cathode of the ion source, or of the gas pressure in the burn chamber or of the discharge voltages is secured only at the expense of an even shorter life for the ion source.
  • the relatively large area of the tungsten wire bar as the emission surface for the electrons and the area ofthe reflector prevent an increase in the electron density in the discharge plasma, make a perfect congruence in the centering more difficult and permit no further approximation of the reflector and the glow cathode due to the mechanical constriction in the burn chamber of'the ion source in the area of the slit for taking off the ions.
  • the tungsten wire bars are hot resistant against ion bombardment and are not stable enough against transverse magnetic forces.
  • FIG. 1 is a sectional view of a preferred embodiment I of the present invention.
  • FIG. 2 is a sectional view of a detail.
  • any of the metals or metal carbides which are used in known electron sources may be used, but tungsten is preferred.
  • graphite is preferred as the mounting material in electricalcontact with the electron emitter of this invention. but other materials having the indicated physical and electrical properties may be used.
  • FIG. l is a vertical view. partly in section. of an electron source embodying this invention.
  • FIG. 2 isanother vertical view, also partly in section,
  • tion emits electrons andin which the direct vicinity, at 7 electron-emitting means composed of a highly refractory, substantially infusible material having a high elec tron work function.
  • the mounting for the emitter means is more-or-less in the form of an inverted U with the upper, arcuate connecting portion having a cross section of lesser area than that of the lower depending arms.
  • FIG. I shows the lower portion of an ion source for an isochron cyclotron (not shown) in which, by a low pressure gas discharge of ap proximately 0.2 to 0.5 Torr, deuterium or hydrogen ions are produced in the throat 2 of a burn chamber 1.
  • the discharge burns between emitter means 3 and a reflector (not shown) in the throat 2 at a heating voltage between and 200 volts.
  • the magnetic field is disposed in or parallel to the sectional plane of the illustrated device.
  • the ions produced in the discharge plasma are extracted by a high frequency voltage (approximately 40 kV and 33 MHz) (1 MHz lMC/s) in an acceleration sector (not shown) in a direction transversely to the magnetic field through a slit (also not shown) in the wall of the burn chamber throat 2.
  • a high frequency voltage approximately 40 kV and 33 MHz
  • the glow cathode 3 can be designed as a pill or button, which may be rectangular or cylindrical with straight or tapering sides, and is heated by a direct current of lOO to 300 amperes. This strong direct current heats the emitter 3 in such a Way that with an arc voltage of approximately 200 V an arc current of 1.5 ampere can flow for the discharge plasma. resulting in an arc output of 300 watt.
  • the electron emitter 3 which may be made of a metal or a metal carbide such as, for example, tungston hafnium carbide, zirconium carbide, molybdenum carbide, or an alloy of 1 these carbides, is mounted in conductive elements 5 and 6 which consist of a highly refractory, substantially infusible material with a high electron workfunction. This is preferably graphite.
  • the current conductors 5 and 6 form the arms of a U-shaped device, and each has a cross section larger than that of the arcuate connecting portion 7, so that in this region the resistance to the heating current for the emittermeans 3 isincreased.
  • Portion 7 is provided with a bore 8 which .is conically tapered, flaring outwardly at its upper region and terminating at its lower region in a recess 9 of reduced cross section with such dimensions as to at least partially enclose the pill 3 and retain it snugly.
  • bo're 8 can be so designed that the tip 4 of the emitter means will extend beyond the surface of portion 7.
  • the material of portion 7 which contacts the pill 3 must be such that the two do not react chemically.
  • the arms 5 and 6 of the retaining means each of which may be made of a single piece of graphite in the same manner as the curved portion 7 are provided, respectively, with leads l and 11 which serve as connections to the source of current for operating the device.
  • these leads l0 and 11 are designed in the form of rods which are inserted into recesses 12 and 13 in the arms and 6, and are retained therein threadedly, frictionally, or in any other conventional manner out of contact with the electron emitter button 3, as it-may be observed in FIG. 1. a
  • FIG. 2 is a vertical view of the glow cathode transversely of the are 7 of the mounting means.
  • the cross section of the arcuate retainer 7 is less, at least in the region 9 containing the pill or button 3 therein, than the cross section of the arms 5 or 6.
  • a bore 14 is preferably the mounting means, through which a pin may be inse'rted to eject the spent pill out of recess 9.
  • Glow cathode comprising: a. an electron emitter of button shape, made of a metal or metal carbide having a high melting point; b. an electrically conductive mounting made of a highly refractory, substantially infusible material having a high electron work function, said electron emitter being held bysaid mounting; and
  • lead wire means in contact with said mounting and out of contact with said electron emitter for passing an electric current through said electron emitter for heating the same.
  • Glow cathode as defined in claim 3, including means defining a bore in said connecting portion of said mounting, said electron emitter being disposed in.
  • electron emitter is in the form of a cylinder made of, hafnium carbide, zirconium carbide", molybdenum carbide or alloy of these carbides.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Electron Sources, Ion Sources (AREA)

Abstract

An improved glow cathode for use as an ion source for cyclotrons is provided wherein the electron-emitting means is formed as a pill or button of a high melting point metal or metal carbide which is supported in a mounting of a highly refractory, substantially infusible material having a high electron work function. Preferably, the electron-emitting button is formed as a cylinder of tungsten and the mounting is formed of graphite. This device can be operated at a gas pressure of approximately 0.2 to 0.5 Torr and a heating voltage of 100 to 200 volts to provide deuterium or hydrogen ions for a cyclotron.

Description

U I i United States Patent 1191 1111 3,869,632 Schulz Mar. 4, 1975 I GLOW CATHODE 32/11/239 8/1966 Lozicr ct al 313/346 R 173L454 5 i973 Okz kl 313 346 R [75] inventor: Friedhelm Schulz, Liedolshelm, lgd let a ern .3 1 mny Primary I;.\'c1n11nerM1chael J. Lynch Asslgnee? Ges'ellschaft Fur Kemforschung Assistant Etanziner--Saxfield Chatmon, Jr.
" Katl$whe- Germany Attorney, Agent, or FirmSpencer & Kaye [22] Filed: Aug. 24, 1973 211 App]. No.1 391,056 [57] ABSTRACT An improved glow cathode for use as an ion source 30] Foreign Appncafion priority Data for cyclotrons is provided wherein the electron- 1 (H I I M41986 emitting means is formed as 21 3111 or button of a high SLPI' 1mm) melting point metal or metal carbide which is sups ported in a mounting of a highly refractory, substan- [52] u 313/346 tially infusible material having a high electron work 7 function. Preferably, the electron-emitting button is [2;]
gl 3 /J3 l 6 gglg 2 1 0 formed as :1 Cylinder of tungsten and the mounting is l 0 can 2 6 formed of graphite. This device can be operated at a gas pressure of approximately 0.2 to 0.5 Torr and a heating voltage of 100 to 200 volts to provide deute- References cued rium orhydrogen ions for a cyclotron UNITED STATES PATENTS 1972.078 2/1961 Levi .1 313/346 R 1 .Clalms, 2 Drawmg Flgures GLOW CATHODE The present invention relates to a glow cathode with g a current input and output and to the use of such a glow cathode.
BACKGROUND OF THE INVENTION t Jones (The Review of Scientific Instruments, Volume 25. Number 6, June 1954, pages 252-557). In one of these ion sources, a tungsten wire bar heated with 100 to 300 amperes direct current serves as the glow cath ode. At a predetermined voltage, a low pressure gas discharge burns at a low gas pressure (e.g. Torr deuterium gas) between the glow cathode and the burn chamber which is formed of graphite. The discharge plasma is constricted by a strong magnetic field which is disposed in theplane of the tungsten wire bar or in a plane parallel thereto to form a more or less precisely defined column between the glow cathode and a reflector for electrons which is insulated from the burn chamber. The reflector is negatively charged during operation. The ions are extracted transversely to the magnetic field through a slit in the burn chamber by a high frequency voltage at an acceleration sector.
Such ion sources furnish beam currents up to lOO pA (luA 1 micro amps) deuterons when deuterium gas is used for the low pressure gas discharge and have a maximum life of 0.5 to 1.0 mAh (l mAh =1 X 10 Ampere hours). An increase in the ion yield through an increase in the heating of the glow cathode of the ion source, or of the gas pressure in the burn chamber or of the discharge voltages is secured only at the expense of an even shorter life for the ion source. Moreover, the relatively large area of the tungsten wire bar as the emission surface for the electrons and the area ofthe reflector prevent an increase in the electron density in the discharge plasma, make a perfect congruence in the centering more difficult and permit no further approximation of the reflector and the glow cathode due to the mechanical constriction in the burn chamber of'the ion source in the area of the slit for taking off the ions. Also. the tungsten wire bars are hot resistant against ion bombardment and are not stable enough against transverse magnetic forces.
SUMMARY-OF THE INVENTION It is an object of the present invention to provide a glow cathode in which only a predetermined fixed por- BRIEF DESCRIPTION OF THE DRAWING FIG. 1 is a sectional view of a preferred embodiment I of the present invention.
.FIG. 2 is a sectional view of a detail.
DESCRIPTION OF THE PREFERRED EMBODIMENTS Improvement in ion yield, electron density in the discharge plasma, ion emitter life'and stability against transverse magnetic forces and other objects of this invention are achieved by providing the electronemitting portion of the glow cathode in the form of a pill or button of a high melting point metal or metal carbide and a mounting therefor of a highly refractive, substantially infusible material with a high electron work function.
For the emitter, any of the metals or metal carbides which are used in known electron sources may be used, but tungsten is preferred. Similarly, graphite is preferred as the mounting material in electricalcontact with the electron emitter of this invention. but other materials having the indicated physical and electrical properties may be used.
The present invention is disclosed in further detail in the following description and the'accompanying drawing, wherein FIG. l is a vertical view. partly in section. of an electron source embodying this invention. and
' FIG. 2 isanother vertical view, also partly in section,
tion emits electrons andin which the direct vicinity, at 7 electron-emitting means composed of a highly refractory, substantially infusible material having a high elec tron work function. i
These and other objects will be apparent to workers in this art from the following detailed description and the accompanying drawing.
of the emitter and mounting means of this invention.
In a preferred embodiment of the invention, the mounting for the emitter means is more-or-less in the form of an inverted U with the upper, arcuate connecting portion having a cross section of lesser area than that of the lower depending arms.
Referring now to the drawing, FIG. I shows the lower portion of an ion source for an isochron cyclotron (not shown) in which, by a low pressure gas discharge of ap proximately 0.2 to 0.5 Torr, deuterium or hydrogen ions are produced in the throat 2 of a burn chamber 1. The discharge burns between emitter means 3 and a reflector (not shown) in the throat 2 at a heating voltage between and 200 volts. Between the glow cathode 3 and the throat 2, the discharge plasma is disposed which is constricted to a precisely defined column by a strong magnetic field of approximately 10 kG l kG= l0 gaussy The magnetic field is disposed in or parallel to the sectional plane of the illustrated device. The ions produced in the discharge plasma are extracted by a high frequency voltage (approximately 40 kV and 33 MHz) (1 MHz lMC/s) in an acceleration sector (not shown) in a direction transversely to the magnetic field through a slit (also not shown) in the wall of the burn chamber throat 2. In order to obtain a particularly high yield of electrons from the emitter 3, it must be brought as closely as possible to the throat portion 2 of the burn chamber. To meet this requirement, the glow cathode 3 can be designed as a pill or button, which may be rectangular or cylindrical with straight or tapering sides, and is heated by a direct current of lOO to 300 amperes. This strong direct current heats the emitter 3 in such a Way that with an arc voltage of approximately 200 V an arc current of 1.5 ampere can flow for the discharge plasma. resulting in an arc output of 300 watt.
In order to keep the discharge stable. the electron sourcemust be locally stable. when the electrical conductors in contact with the glow cathode are of metal In order to prevent this almost completely, the electron emitter 3, which may be made of a metal or a metal carbide such as, for example, tungston hafnium carbide, zirconium carbide, molybdenum carbide, or an alloy of 1 these carbides, is mounted in conductive elements 5 and 6 which consist of a highly refractory, substantially infusible material with a high electron workfunction. This is preferably graphite.
The current conductors 5 and 6 form the arms of a U-shaped device, and each has a cross section larger than that of the arcuate connecting portion 7, so that in this region the resistance to the heating current for the emittermeans 3 isincreased. Portion 7 is provided with a bore 8 which .is conically tapered, flaring outwardly at its upper region and terminating at its lower region in a recess 9 of reduced cross section with such dimensions as to at least partially enclose the pill 3 and retain it snugly. If desired, bo're 8 can be so designed that the tip 4 of the emitter means will extend beyond the surface of portion 7. The material of portion 7 which contacts the pill 3 must be such that the two do not react chemically.
The arms 5 and 6 of the retaining means, each of which may be made of a single piece of graphite in the same manner as the curved portion 7 are provided, respectively, with leads l and 11 which serve as connections to the source of current for operating the device.
In a preferred embodiment, these leads l0 and 11 are designed in the form of rods which are inserted into recesses 12 and 13 in the arms and 6, and are retained therein threadedly, frictionally, or in any other conventional manner out of contact with the electron emitter button 3, as it-may be observed in FIG. 1. a
FIG. 2 is a vertical view of the glow cathode transversely of the are 7 of the mounting means. The cross section of the arcuate retainer 7 is less, at least in the region 9 containing the pill or button 3 therein, than the cross section of the arms 5 or 6. In order to' readily remove emitter 3 from recess 9 when unserviceable for replacement with a new unit,.a bore 14 is preferably the mounting means, through which a pin may be inse'rted to eject the spent pill out of recess 9.
. 4 not be bent by strong extraneousmagnetic fields.
It will' be understood that the above description of the present invention is susceptible to various modificaworked in the underside 15 of the arcuate portion 7 of The leads l0 and 11 for arms 5 and6 of the bar may I worked so as to provide retaining means, suchas a screw'thread, for example. Bythus placing the leads l0 and 11 within the arms Sand 6 the leads also provide reinforcement for their respective arms so that they will tions, changes and adaptations, and the same are intended tobe comprehended within the meaning and range of equivalents of the appended claims.
I claim: l. Glow cathode comprising: a. an electron emitter of button shape, made of a metal or metal carbide having a high melting point; b. an electrically conductive mounting made of a highly refractory, substantially infusible material having a high electron work function, said electron emitter being held bysaid mounting; and
0. lead wire means in contact with said mounting and out of contact with said electron emitter for passing an electric current through said electron emitter for heating the same. 2. Glow cathod as defined in claim 1 wherein the material of said mounting is g aphite.
3. Glow cathode as defined in claim 1 wherein the mounting has a substantially U-shaped configuration including a connecting portion and arms, the connecting portion has a' smaller crosssectional area than that of the arms. J
4. Glow cathode as defined in claim 3, said connecting portion of said mounting including means for hold ing said electron emitter.
5. Glow cathode as defined in claim 3, including means defining a bore in said connecting portion of said mounting, said electron emitter being disposed in.
and held by said bore for at least partially embedding 9. Glow cathode as defined in claim 1 wherein the, I
electron emitter is in the form of a cylinder made of, hafnium carbide, zirconium carbide", molybdenum carbide or alloy of these carbides. J
10. Use of the glow cathode as defined in claim 1 as the electron source for the ion source of a cyclotron. l1. Glow cathode as defined in claim 1 wherein the electron emitter is in the form of a tungsten cylinder. 12. Glow cathode as defined in claim 1 wherein said lead wire means have end portions embedded in said mounting.

Claims (12)

1. Glow cathode comprising: a. an electron emitter of button shape, made of a metal or metal carbide having a high melting point; b. an electrically conductive mounting made of a highly refractory, substantially infusible material having a high electron work function, said electron emitter being held by said mounting; and c. lead wire means in contact with said mounting and out of contact with said electron emitter for passing an electric current through said electron emitter for heating the same.
2. Glow cathod as defined in claim 1 wherein the material of said mounting is graphite.
3. Glow cathode as defined in claim 1 wherein the mounting has a substantially U-shaped configuration including a connecting portion and arms, the connecting Portion has a smaller cross-sectional area than that of the arms.
4. Glow cathode as defined in claim 3, said connecting portion of said mounting including means for holding said electron emitter.
5. Glow cathode as defined in claim 3, including means defining a bore in said connecting portion of said mounting, said electron emitter being disposed in, and held by said bore for at least partially embedding said electron emitter.
6. Glow cathode as defined in claim 3, wherein the arms of the U-shaped mounting receive said lead wire means.
7. Glow cathode as defined in claim 5 wherein the bore is conically tapered outwardly with the inner portion forming a recess substantially conforming to the shape and size of the electron emitter for holding the same.
8. Glow cathode as defined in claim 7 wherein the depth of the recess is less than the height of the electron emitter.
9. Glow cathode as defined in claim 1 wherein the electron emitter is in the form of a cylinder made of, hafnium carbide, zirconium carbide, molybdenum carbide or alloy of these carbides.
10. Use of the glow cathode as defined in claim 1 as the electron source for the ion source of a cyclotron.
11. Glow cathode as defined in claim 1 wherein the electron emitter is in the form of a tungsten cylinder.
12. Glow cathode as defined in claim 1 wherein said lead wire means have end portions embedded in said mounting.
US391056A 1972-09-01 1973-08-24 Glow cathode Expired - Lifetime US3869632A (en)

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DE (1) DE2242986C3 (en)
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GB (1) GB1433238A (en)
IT (1) IT991864B (en)
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003075305A2 (en) * 2002-03-06 2003-09-12 Applied Materials, Inc. Indirectly heated button cathode for an ion source
US20040061068A1 (en) * 2002-09-30 2004-04-01 Applied Materials, Inc. Indirectly heated button cathode for an ion source
CN111816532A (en) * 2020-07-17 2020-10-23 核工业西南物理研究院 Replaceable filament assembly for hot cathode arc discharge ion source

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2192751B (en) * 1986-07-14 1991-02-13 Denki Kagaku Kogyo Kk Method of making a thermionic cathode structure.

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2972078A (en) * 1959-01-23 1961-02-14 Philips Corp Carburization of dispenser cathodes
US3270239A (en) * 1963-09-20 1966-08-30 Union Carbide Corp Solar simulation apparatus
US3732454A (en) * 1971-11-24 1973-05-08 Hitachi Ltd Glow discharge tube for atomic light-absorption analysis

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1046639A (en) * 1964-08-17 1966-10-26 Gen Electric Improvements in dispenser cathode
DE2029571C3 (en) * 1970-06-16 1980-09-11 Kernforschungszentrum Karlsruhe Gmbh, 7500 Karlsruhe Ion source for a cyclotron

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2972078A (en) * 1959-01-23 1961-02-14 Philips Corp Carburization of dispenser cathodes
US3270239A (en) * 1963-09-20 1966-08-30 Union Carbide Corp Solar simulation apparatus
US3732454A (en) * 1971-11-24 1973-05-08 Hitachi Ltd Glow discharge tube for atomic light-absorption analysis

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003075305A2 (en) * 2002-03-06 2003-09-12 Applied Materials, Inc. Indirectly heated button cathode for an ion source
WO2003075305A3 (en) * 2002-03-06 2003-11-27 Applied Materials Inc Indirectly heated button cathode for an ion source
US20040061068A1 (en) * 2002-09-30 2004-04-01 Applied Materials, Inc. Indirectly heated button cathode for an ion source
US6878946B2 (en) 2002-09-30 2005-04-12 Applied Materials, Inc. Indirectly heated button cathode for an ion source
CN111816532A (en) * 2020-07-17 2020-10-23 核工业西南物理研究院 Replaceable filament assembly for hot cathode arc discharge ion source

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IT991864B (en) 1975-08-30
CH557597A (en) 1974-12-31
CA1030589A (en) 1978-05-02
FR2198249B1 (en) 1976-05-14
NL7311915A (en) 1974-03-05
SE389255B (en) 1976-10-25
DE2242986B2 (en) 1980-09-04
DE2242986C3 (en) 1981-05-07
GB1433238A (en) 1976-04-22
DE2242986A1 (en) 1974-03-07

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