US3730189A - Tobacco product - Google Patents

Tobacco product Download PDF

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Publication number
US3730189A
US3730189A US00215398A US3730189DA US3730189A US 3730189 A US3730189 A US 3730189A US 00215398 A US00215398 A US 00215398A US 3730189D A US3730189D A US 3730189DA US 3730189 A US3730189 A US 3730189A
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United States
Prior art keywords
tobacco
aroma
flavor
additive
product
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
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US00215398A
Inventor
W Rhode
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
RJ Reynolds Tobacco Co
Original Assignee
RJ Reynolds Tobacco Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by RJ Reynolds Tobacco Co filed Critical RJ Reynolds Tobacco Co
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Publication of US3730189A publication Critical patent/US3730189A/en
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Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/34Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a carbocyclic ring other than a six-membered aromatic ring

Definitions

  • Unitefl S1 ates Pafienfi 1191 Rhode May 11, 11973 TOBACCO PRODUCT 1,325,060 12/1919 Toms ..131 144 x 3,255,760 6/1966 Selke ...13l/143 X [75 1 Invent mmde Lake 3,316,919 5/1967 Green et al ..131/143 [73] Assignee: R. J. Reynolds Tobacco Company, 3,380,456 4/1968 Roberts et a1. ..l31/144X Winston-Salem, NC. Primary Examiner-Melvin D. Rein [22] Jan-4,1972 Azlorney-Albert H. Pendleton [21] Appl. No.: 215,398
  • ABSTRACT [52] U.S.C1. ..l3l/171R, 131/144 Addition of 2-hydroxy-3,5,5-trim-ethyl-2 cyclohexen- [51] Int. Cl. ..A24b 15/00 1,4-dione to tobacco in quanties of 0.0005 to 0.1 per- [58] Field of Search ..l3l/ 17.9, 144, 15 cent by weight for improving the flavor and aroma thereof.
  • a further object of this invention is the provision of a process for enhancing or otherwise improving the flavor, aroma and other qualities of certain domestic,
  • oriental, reconstituted or synthetic tobaccos which may be deficient in said flavor or aroma or other qualities.
  • An additional object of this invention is to provide a process of preparing a smoking tobacco or product which when smoked has an enhanced flavor or aroma.
  • a still further object of this invention is the provision of smoking products, such as cigarettes, cigars or pipe tobacco, and a process for forming same whereby the flavor and aroma before and during smoking are improved or enhanced.
  • the flavor and/or aroma of tobacco or tobacco products is improved by adding thereto a small amount of 2-hydro5ty-3,5,5- trimethyl-Z-cyclohexen-l,4-dione, which compound has been found in natural tobacco.
  • This compound can be represented by the formula the amount used will depend upon the amount of flavor and/or aroma desired.
  • the additive can be incorporated at any step in treatment of the tobacco but is preferably added after aging, curing and shredding and before the tobacco is formed into cigarettes or other products. Likewise, it will be apparent that only a portion of the tobacco need be treated and the thus treated tobacco can be blended with other tobaccos before the cigarettes or other tobacco products are formed. In such case the treated tobacco may have the additive in excess of the amounts aboveindicated so that when blended with other tobaccos the final product will contain a percentage of additive within the indicated range.
  • the tobacco additive of the invention when incorporated into tobacco products improves the flavor and/or aroma of the product. More particularly, the additive has been characterized as adding body to the flavor of tobacco smoke and contributing a chocolate, nutty side note to the aroma of packaged cigarettes to which it has been added.
  • the additive has been characterized as adding body to the flavor of tobacco smoke and contributing a chocolate, nutty side note to the aroma of packaged cigarettes to which it has been added.
  • definition or characterization of flavor or aroma in the tobacco art is almost purely subjective and different smokers may define the same flavor or effect quite differently.
  • an aged flue-cured andl shredded tobacco is sprayed with a 1 percent ethyl alcohol solution of 2- hydroxy-3,5,5-trimethyl-2-cyclohexen-l,4-dione in an amount to provide a tobacco containing 0.001 percent by weight of the additive on a dry basis. Thereafter the alcohol is removed by evaporation and the tobacco is manufactured into cigarettes by the usual techniques. It has been found that the cigarette when prepared as indicated has an improved character.
  • the additive employed in accordance with this invention may be applied to the tobacco by spraying, dipping or otherwise, utilizing suitable suspensions or solutions thereof.
  • water or volatile organic solvents such as alcohol, ether, acetone, volatile hydrocarbons and the like, may be used as the carrying medium for the additive while being applied to the tobacco.
  • other flavorand aroma-producing additives such as those disclosed in U.S. Pat. Nos. 2,766,145, 2,905,575, 2,905,576, 2,978,365 and 3,041,21 1 may be incorporated into the tobacco with the additive of this invention.
  • a tobacco product which includes the specified addi- 2.
  • a process for improving tobacco flavor and/or aroma which comprises adding thereto an amount of from about 0.00005 to 0.1 percent by weight and sufficient to alter the flavor or aroma of tobacco of 2- hydroxy-3,5 ,5-trimethyl-2-cyclohexen-l ,4-dione.
  • a process for producing a tobacco product which comprises adding thereto an amount of from about 0.00005 to 0.1 percent by weight and sufficient to alter the flavor or aroma of the tobacco product of 2- hydroxy-3 ,5,5-trimethyl-2-cyclohexen-1,4-dione.

Abstract

Addition of 2-hydroxy-3,5,5-trimethyl-2 cyclohexen-1,4-dione to tobacco in quanties of 0.0005 to 0.1 percent by weight for improving the flavor and aroma thereof.

Description

Unitefl S1ates Pafienfi 1191 Rhode May 11, 11973 TOBACCO PRODUCT 1,325,060 12/1919 Toms ..131 144 x 3,255,760 6/1966 Selke ...13l/143 X [75 1 Invent mmde Lake 3,316,919 5/1967 Green et al ..131/143 [73] Assignee: R. J. Reynolds Tobacco Company, 3,380,456 4/1968 Roberts et a1. ..l31/144X Winston-Salem, NC. Primary Examiner-Melvin D. Rein [22] Jan-4,1972 Azlorney-Albert H. Pendleton [21] Appl. No.: 215,398
[57] ABSTRACT [52] U.S.C1. ..l3l/171R, 131/144 Addition of 2-hydroxy-3,5,5-trim-ethyl-2 cyclohexen- [51] Int. Cl. ..A24b 15/00 1,4-dione to tobacco in quanties of 0.0005 to 0.1 per- [58] Field of Search ..l3l/ 17.9, 144, 15 cent by weight for improving the flavor and aroma thereof. [56] References Cited 3 Claims, No Drawings UNITED STATES PATENTS 858,289 6/1907 Hondius ..131/144 TOBACCO PRODUCT This invention relates to a tobacco product and has for an object the provision of a composition and process for improving the flavor and/or aroma of tobacco and tobacco smoke.
It is well known in the tobacco art that the flavor and aroma of the tobacco product and the smoke from the tobacco are very important considerations insofar as the ultimate consumer is concerned. Considerable efforts are exerted by the manufacturers of tobacco products to provide a product that will be acceptable to the consumer, particularly as regards flavor and aroma characteristics. It has been the common practice in the tobacco industry to prepare blends of domestic and oriental tobaccos in order to provide smoking tobacco which has a pleasing flavor and aroma before and during smoking. However, such a procedure is costly and may at times become prohibitive in the event that certain types of tobacco may be in short supply. Accordingly, it is a further object of this invention to 'provide an additive which when applied to the tobacco products improves and enhances the flavor and aroma of these products and the smoke emitted therefrom thereby increasing or enhancing the pleasure and other values that may be derived by the consumer from the use of these products.
A further object of this invention is the provision ofa process for enhancing or otherwise improving the flavor, aroma and other qualities of certain domestic,
oriental, reconstituted or synthetic tobaccos which may be deficient in said flavor or aroma or other qualities.
An additional object of this invention is to provide a process of preparing a smoking tobacco or product which when smoked has an enhanced flavor or aroma.
A still further object of this invention is the provision of smoking products, such as cigarettes, cigars or pipe tobacco, and a process for forming same whereby the flavor and aroma before and during smoking are improved or enhanced.
Further and additional objects will appear from the following description and the appended claims.
In accordance with this invention the flavor and/or aroma of tobacco or tobacco products is improved by adding thereto a small amount of 2-hydro5ty-3,5,5- trimethyl-Z-cyclohexen-l,4-dione, which compound has been found in natural tobacco. This compound can be represented by the formula the amount used will depend upon the amount of flavor and/or aroma desired. The additive can be incorporated at any step in treatment of the tobacco but is preferably added after aging, curing and shredding and before the tobacco is formed into cigarettes or other products. Likewise, it will be apparent that only a portion of the tobacco need be treated and the thus treated tobacco can be blended with other tobaccos before the cigarettes or other tobacco products are formed. In such case the treated tobacco may have the additive in excess of the amounts aboveindicated so that when blended with other tobaccos the final product will contain a percentage of additive within the indicated range.
The tobacco additive of the invention when incorporated into tobacco products improves the flavor and/or aroma of the product. More particularly, the additive has been characterized as adding body to the flavor of tobacco smoke and contributing a chocolate, nutty side note to the aroma of packaged cigarettes to which it has been added. However, it is to be apprecia'ted that definition or characterization of flavor or aroma in the tobacco art is almost purely subjective and different smokers may define the same flavor or effect quite differently.
In accordance with one specific embodiment of this invention, an aged flue-cured andl shredded tobacco is sprayed with a 1 percent ethyl alcohol solution of 2- hydroxy-3,5,5-trimethyl-2-cyclohexen-l,4-dione in an amount to provide a tobacco containing 0.001 percent by weight of the additive on a dry basis. Thereafter the alcohol is removed by evaporation and the tobacco is manufactured into cigarettes by the usual techniques. It has been found that the cigarette when prepared as indicated has an improved character.
The additive employed in accordance with this invention may be applied to the tobacco by spraying, dipping or otherwise, utilizing suitable suspensions or solutions thereof. Thus, water or volatile organic solvents, such as alcohol, ether, acetone, volatile hydrocarbons and the like, may be used as the carrying medium for the additive while being applied to the tobacco. Also, other flavorand aroma-producing additives, such as those disclosed in U.S. Pat. Nos. 2,766,145, 2,905,575, 2,905,576, 2,978,365 and 3,041,21 1 may be incorporated into the tobacco with the additive of this invention.
While this invention is principally useful in the manufacture of cigarette tobacco, it is also suitable for use in connection with the manufacture of pipe tobacco, cigars or other tobacco products. Furthermore, the additive can be added to certain tobacco substitutes of can be applied to the paper of the cigarette or to the wrapper of a cigar. Also, it can be incorporated into the filter tip, the packaging material or the seam paste employed for gluing the cigarette paper. Thus, a tobacco product is provided which includes the specified addi- 2. A process for improving tobacco flavor and/or aroma which comprises adding thereto an amount of from about 0.00005 to 0.1 percent by weight and sufficient to alter the flavor or aroma of tobacco of 2- hydroxy-3,5 ,5-trimethyl-2-cyclohexen-l ,4-dione.
3. A process for producing a tobacco product which comprises adding thereto an amount of from about 0.00005 to 0.1 percent by weight and sufficient to alter the flavor or aroma of the tobacco product of 2- hydroxy-3 ,5,5-trimethyl-2-cyclohexen-1,4-dione.

Claims (2)

  1. 2. A process for improving tobacco flavor and/or aroma which comprises adding thereto an amount of from about 0.00005 to 0.1 percent by weight and sufficient to alter the flavor or aroma of tobacco of 2-hydroxy-3,5,5-trimethyl-2-cyclohexen-1,4-dione.
  2. 3. A process for producing a tobacco product which comprises adding thereto an amount of from about 0.00005 to 0.1 percent by weight and sufficient to alter the flavor or aroma of the tobacco product of 2-hydroxy-3,5,5-trimethyl-2-cyclohexen-1,4-dione.
US00215398A 1972-01-04 1972-01-04 Tobacco product Expired - Lifetime US3730189A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US21539872A 1972-01-04 1972-01-04

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3903900A (en) * 1973-05-14 1975-09-09 Int Flavors & Fragrances Inc Tobacco articles and compositions containing 1,2-cyclohexanedione and methods for producing same

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US858289A (en) * 1905-08-31 1907-06-25 Pieter Hondius Process of impregnating tobacco by means of natural or artificial aromatic substances.
US1325060A (en) * 1919-12-16 Tobacco blend and process of making same
US3255760A (en) * 1962-08-03 1966-06-14 Kimberly Clark Co Tobacco product which produces less tars
US3316919A (en) * 1963-04-29 1967-05-02 Brown & Williamson Tobacco Processing of smoking tobacco
US3380456A (en) * 1965-08-02 1968-04-30 Reynolds Tobacco Co R Tobacco product

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1325060A (en) * 1919-12-16 Tobacco blend and process of making same
US858289A (en) * 1905-08-31 1907-06-25 Pieter Hondius Process of impregnating tobacco by means of natural or artificial aromatic substances.
US3255760A (en) * 1962-08-03 1966-06-14 Kimberly Clark Co Tobacco product which produces less tars
US3316919A (en) * 1963-04-29 1967-05-02 Brown & Williamson Tobacco Processing of smoking tobacco
US3380456A (en) * 1965-08-02 1968-04-30 Reynolds Tobacco Co R Tobacco product

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3903900A (en) * 1973-05-14 1975-09-09 Int Flavors & Fragrances Inc Tobacco articles and compositions containing 1,2-cyclohexanedione and methods for producing same

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CA956536A (en) 1974-10-22

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