US3637980A - Electrical and mechanical connections and support for evaporating boats - Google Patents
Electrical and mechanical connections and support for evaporating boats Download PDFInfo
- Publication number
- US3637980A US3637980A US54135A US3637980DA US3637980A US 3637980 A US3637980 A US 3637980A US 54135 A US54135 A US 54135A US 3637980D A US3637980D A US 3637980DA US 3637980 A US3637980 A US 3637980A
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- United States
- Prior art keywords
- boat
- electrical
- support
- plates
- clamp
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/24—Vacuum evaporation
- C23C14/26—Vacuum evaporation by resistance or inductive heating of the source
Definitions
- Nonarcing means are provided to connect the electrical supply to the boat and at the same time to permit the boat to expand and contract as it is heated and cooled without so confining the boat or so bending the boat as to cause breakage thereof.
- the nonarcing means includes tight electrical connections to the ends of the boat and the support means for the electrical connections permit linear motion thereof.
- the clamps must be tightly fixed to the ends of the boat to prevent electrical arcing between the clamps and the boat because the arcing causes the material of the boat or of the clamps to be vaporized whereby the workpiece will be coated with contaminated material.
- the boat must be allowed to expand and contract without great enough confinement thereof or without sufficient twisting or bending thereof to cause the boat to break.
- the electrical clamps to the boat have been tightly fixed thereto but the clamps have comprised parts in electrical contact with each other through which the heating current flows, these parts being allowed to slide with respect to each other to permit expansion and contraction of the boat.
- Such prior art support and heating means for the boat has been unacceptable since it is impossible to eliminate all arcing between the sliding contacts.
- Other prior art supports and heating means have included rigid electrical clamps to the boat mounted on a flexible support. However, the expansion and contraction of the boat has caused the flexible support to bend, causing a bending motion to be applied to the brittle boat, causing breakage thereof, making this type of support also unacceptable.
- clamping means are provided that may be tightly clamped to the ends of a boat to make electrical connections to the ends of the boat, said clamping means being linearly slideably supported, whereby said boat may be heated by electrical currents passing therethrough and no, or very little, confining or twisting or bending force is applied to the boat.
- FIG. 1 shows a boat, including the clamping means of this invention, arranged to evaporate a material which is to be plated ,on a workpiece,
- FIG. 2 is an elevational view of the boat and boat guards which are applied to said boat and which are shown in FIG. 1,
- FIG. 3 is an end view of the boat and boat guards of FIG. 2,
- FIG. 4 is a section of FIG. 1 on line 4-4 thereof showing a feature of the clamping means of this invention.
- FIG. 5 is an end elevational view of the guide block of FIG. I comprising a portion of the clamping means thereof.
- a chamber 10 is arranged to be evacuated.
- the chamber 10 comprises a cylindrical portion 12 and end portions 14 which can be removed to allow access to the cylindrical portion 12.
- a boat 16 is supported in a manner to be described.
- the boat 16 is made of high-resistance, highly refractive material such as Union Carbide Aluminide Boride Intermetallic boat material.
- the boat is of rectangular parallelepiped shape and it is dished out to provide a trough 18 to receive material to be evaporated.
- Boat guards 20 arefitted on the boat beyond the ends of the trough 18 from the middle thereof.
- These boat guards 20 may be of any refractory material such as graphite, may have rectangular outer outline and have a central hole through which the boat fits. I y
- the boat 16 is raisedto the evacuation temperature of the material to be evaporated. This is done by passing electrical currents through the boat,16.
- An electrical conductive clamp 22 is provided for each end of the boat 16.
- the clamp 22 comprises an upper plate 24 and a lower plate 26, each of which is conductive.
- a bolt 28 passes through one, the upper plate 24, and is threaded into the other, the lower plate 26.
- a spacer comprising a bolt 30 is threaded into the upper plate 24 and bears against the lower plate 26. By adjustment of the bolt 30, the plates 24 and 26 may be made parallel to the boat 16.
- the plates 24 and 26 may be so tightly clamped to the boat 16 asto prevent any chance of arcing between the plates 24 and 26 and the boat 16.
- Two clamps 22 are provided, one for each end of the boat 16.
- a flexible electrical cable 32 is connected to each plate 24 and 26 and current is caused to flow through the boat 16 by connecting a supply of current to the cables 32 in a known manner.
- the support 34 may be U-shaped having parallel top and bottom arms and a vertical arm.-
- the top arm 36 is slotted at 38, see FIG. 4.
- a bolt 40 extends through the top and bottom plates 24 and 26 and through-a guide block 42.
- the guide block 42 as shown in FIG. 5, hasa lower restricted portion 44 which slideably fits into the slot 38 in the top arm 36 and an upper enlarged portion which bears on the arm 36 on each side of the slot 38.
- the bolt 40 also extends through the block 42 and through the slot 38 and into a nut 46. Therefore, the clamps 22 can move towards and away from each other as the boat 16 contracts and expands but they cannot twist or turn or move other than in a straight line.
- the boat 16 is so supported on the U-shaped members 34 that there can be no are between the boat and the electrical connections thereto and also there is little or no confining or bending force applied to the boat by the clamps 22 or by the means for support of the clamps 22 including the U-shaped members 34. Therefore, no arcing takes place between any electrical connections and the boat and, at the same time, the boat is allowed to contract and expand as required in the use thereof.
- the system of FIG. 1 is used for evaporative plating of a workpiece.
- the workpiece 46 may be one or more semiconductive bodies and the workpiece 46 may be supported on a mask 48 having holes provided therethrough to provide a pattern through which evaporative material may flow to be deposited on the workpiece 46 in accordance with the pattern of the mask 48.
- said support means having a U-shaped slot therein, and a guide block on said clamp means, said guide block having a portion which fits into said slot in a slideable manner, and means for holding said guide block slideably in said slot.
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physical Vapour Deposition (AREA)
Abstract
Evaporating boats which are heated by passing electrical current therethrough are made of material which exhibits high resistance and is refractory. Such material is very brittle. Nonarcing means are provided to connect the electrical supply to the boat and at the same time to permit the boat to expand and contract as it is heated and cooled without so confining the boat or so bending the boat as to cause breakage thereof. The nonarcing means includes tight electrical connections to the ends of the boat and the support means for the electrical connections permit linear motion thereof.
Description
United States Patent Fox et a1.
[54] ELECTRICAL ANDMECHANICAL CONNECTIONS AND SUPPORT FOR EVAPORATING BOATS [72] lnventors: Philip J. Fox; John W. Wright, both of Scottsdale, Ariz.
[73] Assignee: Motorola, Inc., Franklin Park, 111.
[22] Filed: July 13, 1970 [21] App1.No.: 54,135
[56] References Cited UNITED STATES PATENTS 2,793,140 5/1957 Ostrofsky et a1 ..118/49 X 51 Jan. 25, 1972 FOREIGN PATENTS OR APPLlCATlONS 1,169,517 11/1969 Great Britain ..219/271 PrimaryExaminer-C. L. Albritton Attorney-Mueller and Aichele [57] ABSTRACT Evaporating boats which are heated by passing electrical current therethrough are made of material which exhibits high resistance and is refractory. Such material is very brittle. Nonarcing means are provided to connect the electrical supply to the boat and at the same time to permit the boat to expand and contract as it is heated and cooled without so confining the boat or so bending the boat as to cause breakage thereof. The nonarcing means includes tight electrical connections to the ends of the boat and the support means for the electrical connections permit linear motion thereof.
2 Claims, 5 Drawing Figures IZIQ III/I1 IllIIIIIIIIIIIIIII/Ill]Ill/1111111111111] 1/1961 Alexander ..219/271 BACKGROUND In evaporating material to be vapor deposited on a workpiece, either directly or through holes in a pattern, the materialto be evaporated may be deposited in the dished out portion of an evaporation boat. The boat may be made of refractory, high-resistance material which is very brittle. The boat is heated to material evaporation temperature by passing a currenttherethrough, clamps being provided to connect an electrical source to the ends of the boat. The clamps must be tightly fixed to the ends of the boat to prevent electrical arcing between the clamps and the boat because the arcing causes the material of the boat or of the clamps to be vaporized whereby the workpiece will be coated with contaminated material. The boat must be allowed to expand and contract without great enough confinement thereof or without sufficient twisting or bending thereof to cause the boat to break.
I Otherwise, the brittle boat will be destroyed. As will be understood, these two requirements that the electrical leads to the boat be tightly connected thereto and that the boat be allowed to expand and contract freely and without restriction are inconsistent requirements.
In accordance with the prior art, the electrical clamps to the boat have been tightly fixed thereto but the clamps have comprised parts in electrical contact with each other through which the heating current flows, these parts being allowed to slide with respect to each other to permit expansion and contraction of the boat. Such prior art support and heating means for the boat has been unacceptable since it is impossible to eliminate all arcing between the sliding contacts. Other prior art supports and heating means have included rigid electrical clamps to the boat mounted on a flexible support. However, the expansion and contraction of the boat has caused the flexible support to bend, causing a bending motion to be applied to the brittle boat, causing breakage thereof, making this type of support also unacceptable.
It is an object of this invention to provide means for clamping electrical connections to a boat in a nonarcing manner and to support'the boat in a manner to permit its expansion and contraction and yet not to break or damage the boat due to motion caused by the expansion and contraction thereof.
SUMMARY In accordance with this invention, clamping means are provided that may be tightly clamped to the ends of a boat to make electrical connections to the ends of the boat, said clamping means being linearly slideably supported, whereby said boat may be heated by electrical currents passing therethrough and no, or very little, confining or twisting or bending force is applied to the boat.
DESCRIPTION The invention will be better understood upon reading the following description in connection with the accompanying drawing in which FIG. 1 shows a boat, including the clamping means of this invention, arranged to evaporate a material which is to be plated ,on a workpiece,
FIG. 2 is an elevational view of the boat and boat guards which are applied to said boat and which are shown in FIG. 1,
FIG. 3 is an end view of the boat and boat guards of FIG. 2,
FIG. 4 is a section of FIG. 1 on line 4-4 thereof showing a feature of the clamping means of this invention, and
FIG. 5 is an end elevational view of the guide block of FIG. I comprising a portion of the clamping means thereof.
Turning first to FIG. 1, a chamber 10 is arranged to be evacuated. The chamber 10 comprises a cylindrical portion 12 and end portions 14 which can be removed to allow access to the cylindrical portion 12. In the cylindrical portion 12, a boat 16 is supported in a manner to be described. The boat 16 is made of high-resistance, highly refractive material such as Union Carbide Aluminide Boride Intermetallic boat material. The boat is of rectangular parallelepiped shape and it is dished out to provide a trough 18 to receive material to be evaporated. Boat guards 20 arefitted on the boat beyond the ends of the trough 18 from the middle thereof. These boat guards 20 may be of any refractory material such as graphite, may have rectangular outer outline and have a central hole through which the boat fits. I y
In the operation of the equipment of FIG. I, after the material to be evaporated is placed in the trough l8 and the chamber 10 is either evacuated or is filled with a neutral atmosphere, the boat 16 is raisedto the evacuation temperature of the material to be evaporated. This is done by passing electrical currents through the boat,16. An electrical conductive clamp 22 is provided for each end of the boat 16. The clamp 22 comprises an upper plate 24 and a lower plate 26, each of which is conductive. A bolt 28 passes through one, the upper plate 24, and is threaded into the other, the lower plate 26. A spacer comprising a bolt 30 is threaded into the upper plate 24 and bears against the lower plate 26. By adjustment of the bolt 30, the plates 24 and 26 may be made parallel to the boat 16. By adjustment of the bolt 28, the plates 24 and 26 may be so tightly clamped to the boat 16 asto prevent any chance of arcing between the plates 24 and 26 and the boat 16. Two clamps 22 are provided, one for each end of the boat 16. In a known manner, a flexible electrical cable 32 is connected to each plate 24 and 26 and current is caused to flow through the boat 16 by connecting a supply of current to the cables 32 in a known manner. 1
As the boat 16 heats up, it expands. Since the clamps 22 tightly fit the boat 16, they must move as the boat expands and contracts as it is heated and cooled. The contraction and expansion of the boat must not be so confined or opposed as to break or damage the brittle boat. Supports 34 and their connections to the clamps 22 are provided to permit expansion and contraction of the boat without causing breakage thereof.
The support 34 may be U-shaped having parallel top and bottom arms and a vertical arm.- The top arm 36 is slotted at 38, see FIG. 4. A bolt 40 extends through the top and bottom plates 24 and 26 and through-a guide block 42. The guide block 42, as shown in FIG. 5, hasa lower restricted portion 44 which slideably fits into the slot 38 in the top arm 36 and an upper enlarged portion which bears on the arm 36 on each side of the slot 38. The bolt 40 also extends through the block 42 and through the slot 38 and into a nut 46. Therefore, the clamps 22 can move towards and away from each other as the boat 16 contracts and expands but they cannot twist or turn or move other than in a straight line. Therefore, the boat 16 is so supported on the U-shaped members 34 that there can be no are between the boat and the electrical connections thereto and also there is little or no confining or bending force applied to the boat by the clamps 22 or by the means for support of the clamps 22 including the U-shaped members 34. Therefore, no arcing takes place between any electrical connections and the boat and, at the same time, the boat is allowed to contract and expand as required in the use thereof.
As is noted above, the system of FIG. 1 is used for evaporative plating of a workpiece. The workpiece 46 may be one or more semiconductive bodies and the workpiece 46 may be supported on a mask 48 having holes provided therethrough to provide a pattern through which evaporative material may flow to be deposited on the workpiece 46 in accordance with the pattern of the mask 48.
The boat guards 20, which are here described for completion of the disclosure, are described and claimed in an application filed in the name of the inventor Philip J. Fox and assigned to the assignee of this application.
What is claimed is: T
I. In combination:
an evaporation boat and supports and electrical connections thereto comprising;
clamp means tightly fixed to an end of said boat;
means for linearly slideably affixing said clamp means to said support means.
2. The combination according to claim 1 including:
said support means having a U-shaped slot therein, and a guide block on said clamp means, said guide block having a portion which fits into said slot in a slideable manner, and means for holding said guide block slideably in said slot.
Claims (2)
1. In combination: an evaporation boat and supports and electrical connections thereto comprising; clamp means tightly fixed to an end of said boat; said clamp means including an upper and a lower plate for receiving a portion of said boat therebetween, means to space said plates and means to draw said plates together whereby said plates may be fixed to an end of said boat and be positioned parallelly thereto sufficiently tightly so as to avoid any arcing between said plates and said boat; means for making an electrical connection to said clamp means; support means for said clamp means; and means for linearly slideably affixing said clamp means to said support means.
2. The combination according to claim 1 including: said support means having a U-shaped slot therein, and a guide block on said clamp means, said guide block having a portion which fits into said slot in a slideable manner, and means for holding said guide block slideably in said slot.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US5413570A | 1970-07-13 | 1970-07-13 |
Publications (1)
Publication Number | Publication Date |
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US3637980A true US3637980A (en) | 1972-01-25 |
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ID=21988994
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Application Number | Title | Priority Date | Filing Date |
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US54135A Expired - Lifetime US3637980A (en) | 1970-07-13 | 1970-07-13 | Electrical and mechanical connections and support for evaporating boats |
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3919525A (en) * | 1973-02-24 | 1975-11-11 | Bosch Gmbh Robert | Vaporizer apparatus for vapor deposition equipment |
US5167984A (en) * | 1990-12-06 | 1992-12-01 | Xerox Corporation | Vacuum deposition process |
US5179622A (en) * | 1990-05-19 | 1993-01-12 | Leybold Aktiengesellschaft | Series evaporator for vacuum vapor-deposition apparatus |
US5261964A (en) * | 1991-12-03 | 1993-11-16 | Leybold Aktiengesellschaft | Evaporator boat for an apparatus for coating substrates |
US5343022A (en) * | 1992-09-29 | 1994-08-30 | Advanced Ceramics Corporation | Pyrolytic boron nitride heating unit |
US5410631A (en) * | 1993-09-10 | 1995-04-25 | Advanced Ceramics Corporation | Clamp assembly for a vaporization boat |
US5481086A (en) * | 1994-08-09 | 1996-01-02 | Dynamic Systems Inc. | High temperature deformable crucible for use with self-resistively heated specimens |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2793140A (en) * | 1953-10-20 | 1957-05-21 | Ohio Commw Eng Co | Method of gas plating with a chromium compound and products of the method |
US2969448A (en) * | 1959-03-03 | 1961-01-24 | Continental Can Co | Heater vaporizer element support |
GB1169517A (en) * | 1966-09-30 | 1969-11-05 | Edwards High Vacuum Int Ltd | Apparatus for the Vaporisation of Metals or Metalloids. |
-
1970
- 1970-07-13 US US54135A patent/US3637980A/en not_active Expired - Lifetime
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2793140A (en) * | 1953-10-20 | 1957-05-21 | Ohio Commw Eng Co | Method of gas plating with a chromium compound and products of the method |
US2969448A (en) * | 1959-03-03 | 1961-01-24 | Continental Can Co | Heater vaporizer element support |
GB1169517A (en) * | 1966-09-30 | 1969-11-05 | Edwards High Vacuum Int Ltd | Apparatus for the Vaporisation of Metals or Metalloids. |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3919525A (en) * | 1973-02-24 | 1975-11-11 | Bosch Gmbh Robert | Vaporizer apparatus for vapor deposition equipment |
US5179622A (en) * | 1990-05-19 | 1993-01-12 | Leybold Aktiengesellschaft | Series evaporator for vacuum vapor-deposition apparatus |
US5167984A (en) * | 1990-12-06 | 1992-12-01 | Xerox Corporation | Vacuum deposition process |
US5261964A (en) * | 1991-12-03 | 1993-11-16 | Leybold Aktiengesellschaft | Evaporator boat for an apparatus for coating substrates |
US5343022A (en) * | 1992-09-29 | 1994-08-30 | Advanced Ceramics Corporation | Pyrolytic boron nitride heating unit |
US5410631A (en) * | 1993-09-10 | 1995-04-25 | Advanced Ceramics Corporation | Clamp assembly for a vaporization boat |
US5481086A (en) * | 1994-08-09 | 1996-01-02 | Dynamic Systems Inc. | High temperature deformable crucible for use with self-resistively heated specimens |
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