US3540703A - Continuous lehr for the heat treatment of glass-based materials - Google Patents

Continuous lehr for the heat treatment of glass-based materials Download PDF

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Publication number
US3540703A
US3540703A US720816A US3540703DA US3540703A US 3540703 A US3540703 A US 3540703A US 720816 A US720816 A US 720816A US 3540703D A US3540703D A US 3540703DA US 3540703 A US3540703 A US 3540703A
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United States
Prior art keywords
heating chamber
lehr
glass
heat treatment
based materials
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Expired - Lifetime
Application number
US720816A
Inventor
Mikhail Ivanovich Kozmin
Ivan Fedotovich Mashir
Vasily Semenovich Bezbozhny
Veniamin Matveevich Olomsky
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ORDENA TRUDOVOGO KRASNOGO ZNAMENI ZAVOD AVTOSTEKLO
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ORDENA TRUDOVOGO KRASNOGO ZNAMENI ZAVOD AVTOSTEKLO
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Publication date
Priority claimed from SU1144460A external-priority patent/SU282621A1/en
Application filed by ORDENA TRUDOVOGO KRASNOGO ZNAMENI ZAVOD AVTOSTEKLO filed Critical ORDENA TRUDOVOGO KRASNOGO ZNAMENI ZAVOD AVTOSTEKLO
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B32/00Thermal after-treatment of glass products not provided for in groups C03B19/00, C03B25/00 - C03B31/00 or C03B37/00, e.g. crystallisation, eliminating gas inclusions or other impurities; Hot-pressing vitrified, non-porous, shaped glass products
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B25/00Annealing glass products
    • C03B25/04Annealing glass products in a continuous way
    • C03B25/06Annealing glass products in a continuous way with horizontal displacement of the glass products
    • C03B25/08Annealing glass products in a continuous way with horizontal displacement of the glass products of glass sheets
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B29/00Reheating glass products for softening or fusing their surfaces; Fire-polishing; Fusing of margins
    • C03B29/04Reheating glass products for softening or fusing their surfaces; Fire-polishing; Fusing of margins in a continuous way
    • C03B29/06Reheating glass products for softening or fusing their surfaces; Fire-polishing; Fusing of margins in a continuous way with horizontal displacement of the products
    • C03B29/08Glass sheets
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B32/00Thermal after-treatment of glass products not provided for in groups C03B19/00, C03B25/00 - C03B31/00 or C03B37/00, e.g. crystallisation, eliminating gas inclusions or other impurities; Hot-pressing vitrified, non-porous, shaped glass products
    • C03B32/02Thermal crystallisation, e.g. for crystallising glass bodies into glass-ceramic articles

Definitions

  • the present invention relates to lehrs for heat-treating and more particularly for' effecting crystallization of glass-based materials.
  • the lehrs are used for annealing glass, the process being employed to remove stresses, set up in glass, by slowly cooling it within the range of temperatures .from 610-590"C. to 420-370C. and by subsequent intenpart is direct-fired or heated by electric heaters situated under the roof, the products of combustion being removed from the chamber and underhearth ducts through flue ducts.
  • An the object of this invention is to provide a continuous lehr with an improved method of heating its heating chamber to insure the temperature conditions required for crystallization of glass-based materials.
  • Described in the present invention is a continuous lehr'for the heat treatment of glass-based materials with a conveying device which transports the material through the heating chamber of the lehr, this heating chamber being direct-fired in its upper and lower parts, and connected to flue ducts.
  • a hearth grating is provided below the conveying device to form combustion chambers under it, the combustion products entering from these combustion chambers into the heating chamber via the hearth grating.
  • cross partitions with apertures for the conveying device are provided in the, heating chamber of thelehr, the latter being thus subdivided by the partitions into several working chambers interconnected through the apertures.
  • the combustion chambers, under the hearth grating are longitudinally subdivided into several ducts, the preferred number of such ducts being two.
  • An advantageof the present invention is that it makes it possible to develop, by simple'means, the desired temperature conditions for the upper and lower parts of the heating chamber as well as to achieve a uniform heatingthroughout the material to be crystallized.
  • Another advantage of the invention is the possibility of maintaining and controlling the temperature conditions along the whole length of each working compartment as required for the crystallization process of the glass material.
  • FIG. 1 is a schematic representation of a continuous lehr according to the invention, shown in a longitudinal section;
  • FIG. 2 is the head portion of the lehr on enlarged'scale
  • FIG. 3 is an enlarged stepped section through line ABCD of the lehr, shown in FIG. 2.
  • the proposed continuous lehr for the heat treatment of glass-based materials has a direct-fired heating chamber I (FIGS. 1 and 3) defined by longitudinal sidewalls 2, roof 3 and hearth grating 4, enclosed in a metal framework 5 which carries and binds together the brickwork of the lehr.
  • I direct-fired heating chamber
  • the heating chamber 1 is direct-fired and ports and II are provided in the sidewalls 2 for this purpose.
  • the parts arearranged in a staggered pattern in their corresponding rows.
  • lnspirator-type gas burners 12 connected to manifold 13 of a combustible gas supply'are mounted at the entry of the ports 10 and 1].
  • the ports 11 discharge intocombustion chambers 14 formed under the hearth grating 4 through which the products of combustion are delivered into the heating chamber 1 via holes 15 of the grating.
  • the combustion chambers 14 are-separated by cross or transverse partitions 16 (FIGS. 1 and 2) while in the longitudinal direction these chambers are subdivided by partitions 17 into two parallel ducts 14a and 14b as shown in FIG. 3.
  • partitions 16 of two adjacent combustion chambers 14 vertical ducts 19 are provided, closed by slide dampers l8 and connecting the working space of the heating chamber 1 to a horizontal underhearth duct 20 whose middle portion enters flue duct 21 (FIG. 1). From the upper part of the heating chamber 1, the
  • the latter may be subdivided into several working compartments la, lb, lc(FIG. l) by means of cross partitions 2 8 with apertures 29 to let the material pass along the conveying device 9 and to connect the working compartments with each other.
  • thermocouples mounted in the heating chamber 1 and the combustion chambers 14.
  • the gas atmosphe're within the lehr is controlled by means of pressure indicators (not shown) and is adjusted by means of the slide dampers l8 and 22.
  • the rate of travel of the strip in the heating chamber '1 is adjusted by'changing the speed of the drive of the conveying device 9.
  • a continuous le'hr for the heat treatment of a glass-based material comprising: means providing a heating chamber having upper and lower parts, means for heating the heating chamber in its upper and lower parts respectively by direct-firing; a conveying device for transporting said material,
  • a lehr as claimed in claim 1 comprising a vault covering the heating chamber, means above the vault providing a horizontal duct extending along said heating chamber and connected by selected of said flue ducts to the latter, and slide dampers between the horizontal duct and heating chamber.
  • a lehr as claimed in claim 3 comprising cross partitions separating the combustion chambers. means providing vertical ducts between the latter said cross partitions coupling adjacent combustion chambers, and slide dampers in said vertical ducts.

Description

United States Patent [72] inventors Mikhail Ivanovich Kozrnin, Mashir App]. No. Filed Patented Assignee Priority I van Fedotovich Bezbozhny, Vasily Semenovich, Olomsky, and
Veniamin Matveevich, Konstantinovka Donetskoi Obluti, U.S.S.R. 720,816
April 12, 1968 Nov. 17, 1970 Ordena Trudovogo Krasnogo Znameni Zcvod Avtoltekltf,
Konstantinovlta Donetskoiobilsti, U.S.S.R. April 14, 1967 1,144,461 and 1,144,462
CONTINUOUS LEIIRFOR THE HEAT TREATMENT OF GLASS-BASED MATERIALS Primary Examiner-John J. Camby A rtorney- Waters, Roditi, Schwartz and Nissen ABSTRACT: A iehr having a heating-chamber below which are combination chambers on which is superposed a hearth grating. Direct heating devices are connected to the comcmmsJDnwin Figs bustion chambers and to the upper part of the heating US. Cl. 263/6; chamber through which extends a conveyor. The combustion 65/350 chambers are subdivided by a longitudinal partition.
I I L 1 i 3 2 2. 21 i2 2 1 1 2 2 2 2 6 j I l I \29 7 CONTINUOUS LEHR- ORTHE HEAT TREATMENT or GLASS-BASEDMATERIALS The present invention relates to lehrs for heat-treating and more particularly for' effecting crystallization of glass-based materials.
The lehrs, known in the prior art, are used for annealing glass, the process being employed to remove stresses, set up in glass, by slowly cooling it within the range of temperatures .from 610-590"C. to 420-370C. and by subsequent intenpart is direct-fired or heated by electric heaters situated under the roof, the products of combustion being removed from the chamber and underhearth ducts through flue ducts.
Owing to their temperature conditions, conventional lehrs are unsuitable for production of crystallized glass materials since it has been found that the process of crystallization requires the material, heated in the course of formation, to be slowly cooled down to 680720C. to insure the beginning of nucleation; soaked at this temperature for a period of time sufficient for complete nucleation; then heated to a temperature of 900980C. at which time a gradual precipitation and growth of crystals take place around the nuclei; subsequently annealed at 480C. and, finally, a cooled down to l-70C. Only in such a manner can structural transformations in the glass-based material be accomplished.
An the object of this invention is to provide a continuous lehr with an improved method of heating its heating chamber to insure the temperature conditions required for crystallization of glass-based materials.
Described in the present invention is a continuous lehr'for the heat treatment of glass-based materials with a conveying device which transports the material through the heating chamber of the lehr, this heating chamber being direct-fired in its upper and lower parts, and connected to flue ducts. According to a feature of the invention for heating the lower part of the heating chamber, a hearth grating is provided below the conveying device to form combustion chambers under it, the combustion products entering from these combustion chambers into the heating chamber via the hearth grating.
In the preferred embodiment of the present invention, cross partitions with apertures for the conveying device are provided in the, heating chamber of thelehr, the latter being thus subdivided by the partitions into several working chambers interconnected through the apertures.
For a more uniform heating of the lower part of the heating chamber, the combustion chambers, under the hearth grating are longitudinally subdivided into several ducts, the preferred number of such ducts being two.
An advantageof the present invention is that it makes it possible to develop, by simple'means, the desired temperature conditions for the upper and lower parts of the heating chamber as well as to achieve a uniform heatingthroughout the material to be crystallized.
Another advantage of the invention is the possibility of maintaining and controlling the temperature conditions along the whole length of each working compartment as required for the crystallization process of the glass material.
The invention will become more fully apparent from the following description of one embodiment which is given with reference to the accompanying drawings, in which:
FIG. 1 is a schematic representation of a continuous lehr according to the invention, shown in a longitudinal section;
FIG. 2 is the head portion of the lehr on enlarged'scale; and
FIG. 3 is an enlarged stepped section through line ABCD of the lehr, shown in FIG. 2.
- The description of theinvention and of the mode ofoperation will be madefor'the sheet material. t
The proposed continuous lehr for the heat treatment of glass-based materialshas a direct-fired heating chamber I (FIGS. 1 and 3) defined by longitudinal sidewalls 2, roof 3 and hearth grating 4, enclosed in a metal framework 5 which carries and binds together the brickwork of the lehr.
The heating chamber 1 is direct-fired and ports and II are provided in the sidewalls 2 for this purpose. The parts arearranged in a staggered pattern in their corresponding rows. lnspirator-type gas burners 12 connected to manifold 13 of a combustible gas supply'are mounted at the entry of the ports 10 and 1]. The ports 11 discharge intocombustion chambers 14 formed under the hearth grating 4 through which the products of combustion are delivered into the heating chamber 1 via holes 15 of the grating.
Along the length of the heating chamber 1, the combustion chambers 14 are-separated by cross or transverse partitions 16 (FIGS. 1 and 2) while in the longitudinal direction these chambers are subdivided by partitions 17 into two parallel ducts 14a and 14b as shown in FIG. 3. Between the partitions 16 of two adjacent combustion chambers 14 vertical ducts 19 are provided, closed by slide dampers l8 and connecting the working space of the heating chamber 1 to a horizontal underhearth duct 20 whose middle portion enters flue duct 21 (FIG. 1). From the upper part of the heating chamber 1, the
products of combustion areremoved through vertical ducts 23 provided in the roof 3 of the heating chamberand closed by slide dampers 22 (FIG. 3). These ducts are in communication. with a horizontal overroof duct 24 covered by a vault 25 which bears against the framework 5 of the lehr apart from the sidewalls 2. The overroof duct 24 is connected through two flue ducts 26 and '27, to smoke exhausters (not shown) arranged at the head and tail portions of the lehr.
In order to control and maintain the prescribed temperature conditions along the entire length of the heating chamber 1, the latter may be subdivided into several working compartments la, lb, lc(FIG. l) by means of cross partitions 2 8 with apertures 29 to let the material pass along the conveying device 9 and to connect the working compartments with each other.
Visual observations of the heat treatment of material can be accomplished through peepholes 30 (FIG. 2) disposed in the.
side walls 2 of the lehr along the entire length of the heating chamber 1.
The general principle of operation of the lehr is given below.
Glass materiaL-formed into a strip-31 (FIG. 3), enters the heating chamber 1 on the conveying device 9 through the aperture 8 in-t'he end wall 6, and is heat treated in accordance number of flames ente't'ing'the heating chamber 1 from the combustion chambers 14 via openings'ls in the hearth grating 4. The central portion of the strip, the width of which is equal to that of the partition 17, is heated less intensively than its. side portions, which results in an equalization of temperature in the lateral direction of the strip 31, warpage in the latter being thus avoided.
The temperature conditions in the lehr are controlled by means of thermocouples (not shown) mounted in the heating chamber 1 and the combustion chambers 14. The gas atmosphe're within the lehr is controlled by means of pressure indicators (not shown) and is adjusted by means of the slide dampers l8 and 22.
The rate of travel of the strip in the heating chamber '1 is adjusted by'changing the speed of the drive of the conveying device 9. When emerging from the lehr at its end wall 7, the
case of processing a crystalline glass strip of crystalline glass material is cut into sheets of desired size.
We claim: 1. A continuous le'hr for the heat treatment of a glass-based material comprising: means providing a heating chamber having upper and lower parts, means for heating the heating chamber in its upper and lower parts respectively by direct-firing; a conveying device for transporting said material,
disposed in said heating chamber; flue ducts connected to said heating chamber; a hearth grating disposed in said heating chamber below said conveying device; means providing combustion chambers to which said means for heating the lower part of the heating chamber is connected, said combustion chambers being covered from above by said hearth grating, the products of combustion being directed from said combustion chambers through said hearth grating, cross partitions, the heating chamber being subdivided into a plurality of working chambers by said cross partitions spaced longitudinally therein, said chambers being interconnected through apertures provided in said cross partitions through which extends the conveying device, and longitudinal partitions, the combustion chambers being subdivided below the hearth grating by said longitudinal partitions into at least two ducts.
2. A lehr as claimed in claim 1, wherein the second said means provides rows of ports opening into the upper part of the heating chamber and into the combustion chambers respectively, the ports in one row being staggered relative to the ports in the other row.
3. A lehr as claimed in claim 1, comprising a vault covering the heating chamber, means above the vault providing a horizontal duct extending along said heating chamber and connected by selected of said flue ducts to the latter, and slide dampers between the horizontal duct and heating chamber.
4. A lehr as claimed in claim 3 comprising cross partitions separating the combustion chambers. means providing vertical ducts between the latter said cross partitions coupling adjacent combustion chambers, and slide dampers in said vertical ducts.
US720816A 1967-04-14 1968-04-12 Continuous lehr for the heat treatment of glass-based materials Expired - Lifetime US3540703A (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
SU1144462 1967-04-14
SU1144460A SU282621A1 (en) 1967-04-14 INSTALLATION FOR CONTINUOUS MANUFACTURING OF SHEET GLASS CRYSTALLINE MATERIAL
SU1144461 1967-04-14

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US3540703A true US3540703A (en) 1970-11-17

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AT (1) AT290756B (en)
BE (1) BE713424A (en)
FR (1) FR1559535A (en)
GB (1) GB1198202A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4249895A (en) * 1977-10-07 1981-02-10 Welko Industriale S.P.A. Kiln
EP0504117A1 (en) * 1991-03-08 1992-09-16 POPPI S.p.A. A tempering furnace, in particular for sheets of glass and similar
US20120094079A1 (en) * 2009-03-31 2012-04-19 Falk Gabel Glass ceramic article and method and device for ceramizing glass

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4249895A (en) * 1977-10-07 1981-02-10 Welko Industriale S.P.A. Kiln
EP0504117A1 (en) * 1991-03-08 1992-09-16 POPPI S.p.A. A tempering furnace, in particular for sheets of glass and similar
US20120094079A1 (en) * 2009-03-31 2012-04-19 Falk Gabel Glass ceramic article and method and device for ceramizing glass
US9302931B2 (en) * 2009-03-31 2016-04-05 Schott Ag Glass ceramic article and method and device for ceramizing glass

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DE1758114B2 (en) 1972-11-02
DE1758114A1 (en) 1970-12-23
FR1559535A (en) 1969-03-07
BE713424A (en) 1968-10-09
AT290756B (en) 1971-06-25
GB1198202A (en) 1970-07-08

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